Document 4QYbg6qk7RYBE5ZQzZkMV16KV
N38101
PRODUCT NAME = WATCHUNG RED B
CG 32 CODE RT-880-D
l o t F2K37 Ch
EST. WT. 2026* LBS.
PKG_____
4UH /4> 1982
NUN-BLEEDING
-1
Pr o c e s s e s
appr o ved by
RT-8S0-D (F) EWK 12-28-81
ALTERNATE
TYPED BY JMH MAKING NOTES_____
'
'
JOB NAME: 32RT880DPF
wtf
VAT DATE
INSTRUCTIONS
1HH00\| Ii
I
|C3iXS V
PRESSING
tI
PRESSLOAD
STARTED
TIME
CAKES USED
RELEASED,BY
WATER ON
PRESS
HRS. WASHED
NO.OF CAKE
I M MHOS
PRESS WITHOUri^GTTATION
HRS. WASHED
WASH TO 333 M' MHOS - 35-75 F WATER M MHOS .
TEST AFTER 6 HOURS
HRS. WASHED
LOAD ON 6 CARS
M MHOS
PRESS IMMEDIATLEY CODE
CAKE CONDITION 1
INSTURCT MAKING AREA TO ADD 10*
NO CARS LOADED
N-588-A HALF-WAY THRU PRESSING.
EXPLAIN LOSSES
CLEAN MAGNETIC SEPARATOR AFTER '
PRESSING. CLEANED BY:
.1,
TIME CLEANED:___ _;___ ___|
MEMBRANCE PRESS-SLURRY TEMP MUST NOT! SAMPLED BY
EXCEED 160*F OR 15PSI BACK PRESS* ATI RELEASED BY
THE INLET FEED GAUGE. WATER TEST, J SAMPLED BY
FILL, WASH 6 COMPRESS PER OP iP.^0^81 ) RELEASED BY
Si#PLES
JAR
SAMPLED BY
DELIVER TO
RELEASED BY
4THI 5TH I
V.Y - DRYING =
DRY 20 HOURS AT 22 F
1 LUMP:. OK - WET - SALTS. - CONTAMlNATD
HOLD ON TRACK 30 MIN BEFORE DUMPING J _____________
PANS._______._______ ____________ I_______________ ________ i.
___________ :____________ ____ i___________________
[
. ~,r r *
ZZ~Z~~-~Z-Z~2ZZZ2ZZZ~-Z~ZZ~Lt.ZZZZZZZ I ~ADDlf IONAL"DRYINGrtlOURS_REQUiRED'"'" ~~"
. ____________________ ___________ ___ I_____________ ______ ____ ^
SAMPLES
i
----
- ~ ^ 5r 0ms "~~7o
I NO CARS PULLED
LUMP WGT t fiL
DELIVER- TO .
.. I SAMPLED BY
I RELEASED BY
* GRINDING =
MILL 2 LSP 1/8'RP SCREEN 1800 RPM ! SCREEN
RPM.
MAX. TEMP. '140 F
1 MAX. TEMP.
F
INERT WITH C02 WHEN GRINDING PER
I___ _______ ___________
O.P. #0.F. 0043.
' "
: !________ ______________________
_
___ _____ _________________ _1 EXPLAIN LOSSES .
SAMPLE
WITHOUT MIXING
SAMPLES 2 ENV & 1 PT CAN
DELIVER TO CTL
! DATE MIXED
i "s a mp l e d ~b y 3^3^:: "" I RELEASED BY
DUP050047251
*
37 51 17
0.00 *
2.06 + o.n -
2.11 +
o.H 2.11 + O.H - i 2.12 + ! 0.14 - i 2.21 * i o.H - ;
2.21 + i
O.H 2.15 + O.H 2.17 + O.H 2.04 0.14 1.68 + O.H 19.46 *
*
J>|:
i
...
DUP050047252
? .. <r * vy *
C*v^90
CG 32
CODE RT-880-D PKG
JUIU6 1982 _ _FJ2K37__
TBa t FT " "Tl o t n u h Se r >
` EST. WT. 2026* UBS. PREPARATION NOTES:___
DATE PRINTED; 6/02/82
D.V. 902/904
PROCESSES ( )RT-8S0-D <F)
APPROVED BY . EWK 12-28-81
TYPED BY: JMH STANDARD HRS. 9.3
TIME ______ M
>"
EQUIP 1 MENT |
I
I I
| i | I
NON-BLEEDING
NAME: WATCHUNG RED B
I USE . | N-CODE I LBS I
NOTE: BATCH MUST BE PRESSED PROMPTLY TO I
CONTROL COLOR. DO NOT START IF PRESS WILL |
NOT BE AVAILABLE WITHIN 3 HRS AFTER MAKING.|
RECORD:
I
PRESS WILL BE READY_____ M____ ,_____PR SUPV I
START - MAKING_______ M_____ /___-_____ MAKING SUPV |
I
NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF |
AREA UNDER V-922.
I
|-NOTE:vRUN 15* WATER INTO V-904. PUMP WATER I
LJi&f| FRQN^V-904 THRU DISTRIBUTOR.. IF WATER DOES I COME OUT OF ALL DISTRIBUTOR HOLES WITH |
| FULL FORCE, NOTIFY SUPERVISOR
I
ACCT . LBS
PREP 1
922 3
| L^T RECORD:__BATCHES SINCE SPARKLER LAST
r ! CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
i | SPARKLER & PRE-COAT WITH 15* DICALITE,
1 1 FILTER AID
I
[ J2-'T OBTAIN FOR Si 1 2-CHLDR0-4-AMIN0T0LUENE-5- I
| USULFONIC ACID
I
l^^TpBTAlN FOR S27 3-HYDR0XY-2-NAPHTH0IC ACID I
I INSTALL DV & CV RECORDER CONTROLLER CHART|
777-A | 740-C I
82-C I
RUN 9* (90G) WATER INTO
ADJ TO
I
, 80-100 DEG F
-I
\JT\ ADD IN 2-3 MIN DRESINATE XX
I SB
STIR 5 MIN & RECORD PH_jLSL.._C9.5-1.5) I
\^r STIR 20 MIN OR LONGER TO DISSOLVE FOR S36 j
1
99-A* '
88
jW 23.19p2
|^PLr UN31' (639G) WATER-INTO V-922
I
\\#T\
WEIGH
\&k2IN SODIUM HYDROXIDE IN V-926 & RUN INI ' m__Z:____ r_z
I TURN ON AGITATOR & STEAM & DUMP IN FROM S2 |
LOT,
*100%
% I_
| 2-CHLORD
___
I I 4-AMINO j&SJL___
___
I S.M.
TOLUENE ___________ *_________ __________ I______
5-SULFONIC___________
________ _ _______
ACID
___________ ,____ _______
.____ I_______
7-D I 740-C I
N38101.02
DUP050047253
DATE PRINTED: 6/02/82
EQUIP WENT
1. USE PAGE 2 * OF 4 CG 32 CODE RT-880-D CF> I LRS
N-CODE
ACCT LBS'
922 3 CONT*
IN ACTIVATED CARBON
U^T DUMP IN FILTER'AID'
J }
TO 212-214 DEG F WATCH FOAM! !
)
^ SRECORD: BY_*t__ MUST BE +, ADJ IF NECESSARY|
SODIUM HYDROXIDE
ASSUME 50%
I.
STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF}
STEAM WATCH FOAM! NOTE: RECORD SPARKLER I
PRESSURE _J2--._PSI* IF NOT ZERO NOTIFY
^--SUPERVISOR *
*
yC\ CIRCULATE 15 MIN OR LONGER THRU SPARKLER
I |
I
'iMMjMI UNTIL SOL'N IS CLEAR* MAINTAIN AT 1,90-195 ' I
l DEG F FOR S24* RECORD: STARTJ?
I
AL MIN___/J5ul__CLARITY,,Cr^C. .
I
RECORD: HT__t3fX_ F & PEC
F .'
I
25 | 10 i
113-B ! 25 777-A ! 10
1 1 7-D I___ _
I
MI SC 4
\12.2<\ -T.f: I
WEIGH SODIUM NITRITE IN PT^P FOR S45
M___
WEIGH SODIUM NITRITE IN DRUM FOR,,, S51
M 9- --
WEIGH SODUM NITRITE IN DRUM, FOR.-$52;
fX./ ' M..
MEASURE 91
UNITS IN V-928 FOR S42
HYDROCHLORIC ACID
3904/ .1 ^RUN 1" C______G) WATER INTO
I
CV T L-NQTE USE CV IF MTY, IF CV NOT MTYrUSE V-904`1
5 l>WKT WHEN SI8 IS COMPLETE, PUMP IN V-922
THRU I
I } SPARKLER, MAINTAIN V-922 AT 190-195 DEG F* |
I f RECORD: START_2l #z1* TOTAL MIN.J&_____ . f
725-A I 301.:
} 725-A | '. 355
1 '^A
725-A t :>'35f -*r0&n`
* ,v. *
28-D I 447ii
902 RUN 53V (1383G) WATER INTO V-902
I
6 WEIGH SODUM HYDROXIDE IN V-926` & RUN IN , ,
1 DUMP IN FROM S3
M^JA___ 1, mSo s ij l .1-7-4Z-1
: 'LtmTfc/^
'~
7-D | ,380 82-C j 848
3-HYDROXY
. .;;..74.4.y
) } 2-NAPHTHOIC ACID
______
Ig^f^ADJ TO 70-90 DEG F &"sf IR~T0~DISSQLVE
/Ir < '-*->* I
r1
' .- THbrn-.. . ^
j
922 }39nWHEN S24- COMPLETE, SHUT OFF' PUMP INSERT l'i
I
7 I lit-922 FOOT-PLUG
/
}|
I30AT RUN IN 10* (209G) WATER & HEAT TO i90-195 Fi
I
K 1 CIRCULATE. 15 MIN THRU SPARKLER* . V
|44> J
} I CIRCULATE 15 MIN THRU SPARKLER* -w
r1
/
; IV ' : : I
^:r' i
i
,V?:7>V
904/CVI30BTPUMP V-922 THRU SPARKLER.INTO V-904/CV
a1
;
I! i- i
RUN IN 5* (104.G) WATER & HEAT TO 190-195 F |
CIRCULATE 15 MIN THRU SPARKLER* .
I
1
' V.
1
904/CV '10 * .
} PUMP V-922 THRU SPARKLER INTO V-904/CV WHEN MTY BLOW OUT SPARKLER INTO V-904/CV
DUP050047254
PATE PRINTED: 6/02/82
EQUIP 11
\ I USE I N-CODE
HENT I | >PAGE 3 OF 4 CG 32 CODE RT-88-D .(F) I LBS ' J
\J& \--*--- j
-- ------ '---- --
''
---! --- -- I --*---- | --r~
904/CV g DISSOLVE ALKANOL XC IN 2G WATER'AT 135-1451
|
1 I IE WATERFROM HOT WATER MIXER IN DRUM 6 POURI 26 I 133-B
CONT I ]/IN
' >4
HEAT V-904/CV TO 165-170 F nE(JR S41
ACCT LBS
26
WHEN S28 COMPLETE, MEASURE TRISULPHOIL SOAP D IN CALIBRATED CONTAINER, SLURRY,WITH 46G WATER IN DRUM 6 POUR INTO V-902 STEAM EJECT IN V-921/931 FROM S8 '
RUN SODIUM HYDROXIDE INTO FT MJ.Q.
-ADJ TO 17' <59G) STIR 5 MIN OR LONGER FOR S57
84
39-A
84
7-D 106
I NOTE: IF N-740-C SOLUTION WAS PUMPED | DIRECTLY FROM SPARKLER TO CV AT
I S'S 23 6 24, OMIT S'S 40 6 41
CV RUN 1 * C95G) WATER INTO V-_JLQL-
13 4J IF V-904 IS USED, PUMP V-94 .AT 165-17 F THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAR
|
<12-15 RECORD:
MSINTA) RMTJAJILN'dTUAJINtJL1K6. 5-T1O7TALDEMGINF__/
NTT RUN IN N-28-D HYDROCHLORIC ACID FROM S22
' | >IN 12-15 MIN.
|4^> STIR 5 MIN 144^1 ADJ TO 37* (3496G) AT 32-38 DEG _F
4X330
57-A I J.
\4SrtT . 'I RECORD: TEMPOS*. F, STICK RUN IN N-725-A SODIUM NITRITE FROM SI 9 AFAR
| >5-1 MIN) 6 RINSE IN STIR 2 MIN AT 32-38 F MAINTAINING +CR,
I 57-A
1 +KI FOR S54 RECORD: TIME
*
I CR__^T___< + ) KI__jt_;^< + ) NOTE': .
I 1) IF CR-, KI-, ADD 20# *AS IS" INCREMENTS
| RECORD: CR____ < +) KI_> + )
| HYDROCHLORIC ACID
ASSUME 32%
28-D
J 2) IF CR+, KI-, ADD 20$ *AS IS" INCREMENTS
i RECORD: CR____ < + ) KI_____< + )
SODIUM NITRITE
ASSUME 33%
725-A |__
i in in
DUMP IN CALCIUM CHLORIDE
935 20-A i 93
DUMP IN STRONTIUM NITRATE KrT DUMP IN BARIUM SULFATE j>@n ADD FOR MAINTAINING AT 32-38 DEG F DURING
205 246-B,E| 2
44
65-A. .57-a
i I
mi4P4
f |-COUPLING I^TPOUR IN N-725-A SODIUM NITRITE FROM S2
I
POUR N-725-A SODIUM NITRITE FROM S21 INTO ,V-92 DUMP IN AMMONIUM CHLORIDE 6 STIR 2-3 MIN
\5jn IMMEDIATELY COUPLE 902 THRU UNDERSUFACE
I
JkxAslSmDISTRIBUTOR INTO CV IN 18-22 MIN. MAINTAIN I
AT 32-38 DEG F , RECORD ; START
*I
t d a t l min .
__ I
5T | INSTALL 5/16* ORIFICE IN UNDERSURFACE ~~ I
-'5 I J^ADDITION LINE
-I
WHEN 5T54 COMPLETE. STIR 3 MIN .6 RECORD: I
I 172 | 165-A | 172
DUP050047255
EQUIP WENT
cv
15 , CONT
4 OF 4
DATE PRINTED: 6/02/82"
*
CG 32 CODE RT-880-D <F)
n -c o d e
ACCT LBS
N N-7-D FROM S39 THRU 5/16* ORIFICE
Ihi'SE IN RECORD: _feO__MIN^< 40-50 MIN)
t,20 MIN RECORD: PH_jot&;_<7.0-8.5>
BELOW 7*0 ADJ TO PH 7*0-8.5 WITH
ONLY. RECORD PH__slJL_ ASSUME 50%
SODIUM HYDROXIDE 'IN V-926 & RUN IN
ASSUME 50% '
15,MIN & RECORD: BASE__rT__ < + >
IAZO_jk__(-) PH,,_Se^>--~ < 9.0-9.8 > -
BELOW 9.0 ADJ TO PH 9.0-9*8 WITH
-D ONLY* RECORD PH
'SODIUM HYDROXIDE
' ASSUME 50%
MEASURE I O.CTANOL IN CALIBRATED CONTAINER
UR IN
--. - "
T0L/iS3-(L95 DEG F. IN 75-80 MIN. RECORD
}
ECORD: HT_rr2_,,DEG F & RECjnsL-DEG F 60 MIN AT W3-195 DEG F. RECORD:
20 MIN S66 STIR
RECORD:
` PH_JL4l _C8.8-9.3)
BELOW 8.8, ADJ TO PH ,8'.8-9.3 WITH
o n l y . Re c o r d PtLfkVL..-
UM HYDROXIDE
*
ASSUME 50%
S66 COMPLETE, FLOOD TO 180-190*
3,OOOG)
STOP AGITATOR
>-
J |_
WHEN INSTRUCTED BY PROCESSING AREA HALFWAY-
1 I THRU PRESSING
LI
(1 > DUMP IN I OCTANQL `
(2) STIR 5 MIN,
(3) ADVISE PROCESSING TO RESUME PRESSING'
]
Ai
I )
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