Document 4JxvpEmDj9vOr43oMBLNqd8rR

AR 226 _ 0882 BIODEGRADATION (BODICOD) IesTsuestance 0 Identity: MreifxetrurreedctoontaasinPiFnOgSp,erFfCl-u9o5r,ooocrtaansesauclfoomnpaotneewnhticohf mFCa-y30a0l3so. b(e1Octanesulfonic acid) (CAS # 2795-39-3). iRseFmCa-r3k0s0:3, idTehnteif3ied pbryotdhuectliaobnorlaottonruymabserR1w3a1s.notCugrirveennt. iTnfhoermtaetsitosnample i7n9d.i3ca9t%eswaittesr,a 2mi%xtSuurietoonfe1f%oaPmFerO,S,1.155%%sdoideituhmyloecnteylglsyuclofaltbe,ut1yl%etshoedr,ium decyl sulfate, 0.06% sodium lauryl sulfate, and 0.05% benzotiiazole. cThhaerafcotlelroiwiznegd scounmcmenatrryataipopnlsioesftiompaurmiitxiteusr.eDwaittha imnacyomnpoltetaeclcyurately reflect degradationof the fluorochemical component of the test sample. ME0 THOD: 0000 Method: OECD Guideline. TGyLpPe:: NAoerobic Year completed: 1997 CInoonctualcutmt:imeP:oly2s8edeadyNsX, Lot D257, Polybac Corporation, Bethelem, PA m0 esw0rs00000000000 Chemical Oxygen Demand (COD): 377,000 mg/kg Biochemical Oxygen 5Day: Demand (CBOD): 132,000 mglkg 2100.DDaayy:: 229467,.000000 mmggkkgg 28.Day: 368,000 mgkg tSRhueebmsfatlraukonsrc:oecTRheeesimtciaanrlgkwsprafosipeolcdro.tniTdonuhceatlveoadnleo.unesthreepmoirxtteudraepapslydetosctrhiatbemdixitn utrhee aTnedstnot c0 onclusio0 ns 0000 No conclusions given. SPuabumli,tMtienrn:esot3a, C5o1m3p3any, Environmental Laboratory, P.O. Box 33331, St. 002687 pa0 raQuaury0000 Reliability: Kiimisch ranking = 2. This study meets the criteria for quality tsetsutdiyngl.acHkoswaenvaelryt,ictahlecsoanmfiprlmeatpiuorniotyfwtahes anomtouprnotpeorflfylucohraorcahcetmeriiczaeldparonpdortthieon in solution. R0 EFEREN0 CES 000000 "DTihviissitoens,t wDualsutcho,nMduNcattedthbeyrAeSqculesCtoorfpotrhaeti3oMn,CDoumlputahnyE,nvLiarbonRmeeqntuaelstTensutminbger R1331, 1997. o0 rWer0000000000 Last changed: 6/26/00 002688 SuEbAnmSivctilecdoCon0rmpao3srMaatCTioeonsm/ipAnaSgenlyD-Di-u8lou5tn7h ASCLDETD Sudy 1D 15010 06 R1331 BOD REPORT FOR 3M COMPANY A Submitted to 3M Environmental Technology and Safety Services 935 Bush Avenue Building 2-3E-09 i' PO Box 33331 St. Paul, MN 55133-3331 Prepared by k EAnSvcilroCnomrepnotraaltiToens/tAiSncgl-DDiuvilsuitohn : 4444 Airpark Boulevard Duluth, Minnesota 55811 SSppoonnssoorr:Su3dMy CToDmFpRanyI AUGUST 1997 002689 m rt mm mso aon COD = 377,000 mg O, / kg chemical. Dates of BOD test: 7/18/97 - 8/15/97. `Water bath temperature range during the test: 19.8 - 20.6C. Lot number of Polyseed NX: D257. TABLE 1. BOD Dilution Information for R1331 Sample. o o o wwweeeeeT [ T T T eT w e Tw a ] ] ID (mg/L) Stock Solution Concentration (mg/L) Sample Volume (uml) `Sample Concentration ---- (mg/L) _ TABLE 2. BOD Blank Calculations for R1331 [C=o=sT| | =T[ on[m m[sorreweuo nmo.[e|oso owmTo|[ on s[|co oorwemwnee.u|oo msoonm]]| oCoeeTToo oewnT [oeeT[ooos[[oene [[eao[|ee eno ] Com ToT en ToToo on Tos ee] `Sponsor: IM Company `Sponsor Study IDA R1331 -1- 2 002650 SuEbAnmvSiirtoCnoinspao3irasiTCoonim/pnAeSrcDDiuiloannh ASELBETD Sup 15 roo TABLE 3. BOD Seed Correction Factor Calculations for R1331 i 3 = ElEE EN dl |wreors | ecowmmen 4 Devp. | Drop | oo TsTewT [5w 0Too[ow | sor |ow |oo | ea] [0Tolow [om[0[wo [ow[c | a |s -| *SCF = (9.0.drop * mlseedintest) /mi seedinseed blank. 5 TABLE 4. BOD Reference and Tox Blanks Calculations for R1331 = = erTwTonToa TawTo [as[ome 2| ] |mewwem | common L 1 -_| Drop | Drop m/L A _DO. | Drop. Drop | mi [ooTsToolon[a[o em [s ouJus]ow[aomm[w] i| di*aReifoenr.ence = 150 m glucose and 150 m glutamic acd in 1 ltr BOD dilution wter, tested 212% 5 * BOD mg/L = (corrected D.O. drop) * 300 ml BOD volume / 6 ml reference. `Sponsor: 3M Company `Sponsor Study IDF R1331 -2- Ll 002691 TABLE 5. BOD Calculations for R1331 SuESbnvmliirtoCnompeno3tr4siTnCoiomAnpSagenkyDDi- 8uo9an3 ASSLETD Suds 15 FSoio00n =|][5 Tow[onTome onTem[ae [on] om| Fe][AboooJ| epno Pw | oaTo we| Tow [oo Dor| Dor| mo | ow[on |v] [| {=|< LomTow Loaf on[se om [im|=Jon[on om| ao | moms|[on[en [an[ow oan| us |] [| [so TsToa vor[amo[ons| sor | mom|[aos [cos [om| cor | nom| rr em] 1 : ae] (Foo]ol][{oeoo[[ooaon[DsoenT[ooonr T[oamnosr[a[oorw[[oorm[|s0ur||aemeo[|somoomno|| [2[0[ios]Cen[on on[ou [oom [= ToTowle [eos[au | vio [vom [on [rn[a| [ms[cos[ves | cor [sen| rae [ovo] ema] eal [io Too Lust oon TsoTow|aw | ava [LoLooTonosJi om[on[om |a [am[ss |5 | oom| [an[ae a| ato |smm | [oo [oofon [om[ow| ca |somo [elolol elTT [am|ane[war| Tolwl- cor | mo| | [L FooTe e [For nTom[om s owTom wn Jom[a on[om|e] o'e | [L=e [LoaT[voa]d[eonfTeooasLeonT [suT Toon [am [vo[2a | so [man | HenFa 7] felonDeloTaos ToT Tans =| | eww] an] *BOD = corrected drop x 1,000,000 / test concentration. Omidt atatpoe intds: FDi.naOl. Ddr.o0p. c<or0r.e5ctemdglfLo.r SCF too low (<2.0). _--= SSppoonnssoorr:St3udMy C[oDm4pRanyI 3. -: 002692