Document 4JvZJN8Q3j9V2DQmmrobwJ1bj

Internal Correspondence To: From: Subject: Date: COMMERCIAL CHEMICALS ANALYTICAL REPORT #346 E. G. GORTNER - RIKER SAFETY EVALUATION - 218-3S-03 R. M. PAYFER - COMMERCIAL CHEMICALS - 236-28 FINAL EVALUATION OF FM-3924 (T-2999CoC) FOR RIKER STUDY NO. 0681TR0362 June 22, 1982 References: Commercial Chemicals A n a ly tic a l Requests #16474, 18319, A n a ly t ic a l R eport #318 A l i g h t , s tra w - c o lo re d wax y s o lid la b e le d FM-3924, Lo t 547 was re c e iv e d f o r a n a ly s is f o r R ik e r te ra to lo g y stu d y #0681TR0362. The m a te ria l has been analyzed w ith th e fo llo w in g r e s u lts : Gas Chromatography o f Sample As Received In e rts Amide c3 C4 c5 Ce C7,Cg High B o ile rs QC(14310 12/3/80 0.5 10.6 fo r a l l low b o ile rs 88.9 - 0.4 0.6 1.2 1.8 1.5 4.8 88.9 0.6 A ll in Area % 3/31/81 3/5/82 0.7 0.6 1.3 1.7 1.6 4.3 88.9 0.8 0.4 0.6 1.2 1.8 1.5 4.8 88.9 0.6 5/27/82 0.7 0.2 1.3 2.2 1.9 4.9 88.9 0.2 A l l va lu es a re w it h in exp erim e nta l and in te g ra tio n param eters. meet QC s p e c if ic a t io n s . . 004331 - 2- Elem ental A n a lys is % Theor. % Found 3/5/82 % Found c H N S F 0 by d iffe re n c e 25.2 1.75 2.45 5.6 56.66 8.4 24.6 1.5 2.6 5.3 57.0 9.0 ; 25.0 1.8 2.7 6.1 55.3 9.1 MW - 571 M e ltin g P o in t: I n i t i a l 38-48C Recheck 38-48C 5/28/82 38-48C S p e c tro s c o p ic : In f r a r e d s p e c tra 16474-2,3,4 and 18318-1 a re id e n t ic a l t o each o th e r and match re fe re n c e s p e c tra . 16474-2 was 16474-3 was 16474-4 was 18318-1 was obtained obtained obtained obtained 11/14/80 3/31/81 3/5/82 5/28/82. NMR sp e c tra H8385, H8387, F8390, F8391 were o b ta in e d on 12/1/80 and 12 /2 /8 0 . These were to c o n firm s t r u c t u r e and not re p e a te d . S tru c tu re was c o n firm e d . The isom er d is t r ib u t io n was found to be 69.6% s t r a ig h t c h a in , 10.9% (CF3 ) 2 CF branched, and 19.5% backbone b ra n c h in g . C o n c lu s io n s : FM-3924, Lot 547 has an a n a ly s is w it h in s p e c if ic a t io n s , is s ta b le and is re p re s e n ta tiv e o f commercial m a te ria l. dc: M. T. Case - 218-2 E. 6. Lamprecht - 218-3 W. C. McCormick - 220-2E-02 W. H. P e a rl son - 223-6SE-04 L. D. W in te r - 236-2B 004332