Document 4JmrKyBL5d2zGn7n7DDDMdjqR
S'.V-.'*
C,\
D,V. 303, 315, 2M, fz22,)z{z
* CG 4
CODE RT-539--D PKG ____
J^lLisai ___GSH28,,
( DATE )
(LOT HUMBER)
ESIV NW T
L.BS.
PROCESSES C > ET--539--D (N)
APPROVED BY
JaG 3/18/81 EWK 12/2/81
TYPED BY:JHH JOB* 40RT539DMN STANDARD HRS. ___________ TIME _______ H
EQUIP MENT i
NAME: NAPHTHANIL RED DARK
MISC 1
NOTE: N24C (4NITE0--2 AMINOANISOL.E HYDRO
CHLORIDE) IS AN EXPERIMENTAL CARCINOGEN. I ALTHOUGH MONITORING VERIFIES WE ARE WELL
BELOW THE RECOMMENDED EXPOSURE LEVEL, IT IS ESSENTIAL THAT YOU ADHERE STRICTLY TO THE
SAFETY RULES WHEN HANDLING N24C, THIS IN i CLUDES RUBBER.GLOVES, LONG SLEEVES, SAFETY
GLASSES, RESPIRATOR AND WASH UP AFTERWARDS, SEE YOUR SUPERVISOR IF YOU"HAVE QUESTIONS. [ / f ..OBTAIN 4-NITR0-2-AMIN0ANIS0LE HYDROCHLORIDE 1 X( FOR STEP 6 I 4 i OBTAIN 'METANITROANILIDE OF B-HYDROXY ! ^NAPHTHOIC ACID FOR STEP 31 . ! gr I CLEAN, DRESS, CLOSE 24" CLARIF1"PRESS =r
I i 15 FRAMES
DV i XjslZUN
<398 G) WATER INTO V-'
2 ! 71 PUN IN HYDROCHLORIC ACID FROM V-324,, ^
m___/.________
DUMP IN FROM Si LOT
#i0%
'%
J 4-NITRO--2-
________
[ AHINQANISOLE 'DROCHLORIBE
aj.. A&---
24-w.D 151-C
28-D
60
24-C,
763
mis ; OR i
STIR 15 MIN TO WET
________
TO U... " ( 71 0 G) AT 28-32 DEG F
IF HON IN SODIUM NITRITE IN 4-6 MIN.
____ ,
STIR 5 MIN & RECORD: CE< + )KI< + >
NOTE: (1) IF CR-,KI- ADD 204 "AS IS1 IN
CREMENTS, HYDROCHLORIC ACID ASSUME 32%
RECORD: CE..... _,,_< + ) KI<+).
(2) J.F CR+.KI-, ADD m "AS IS" INCREMENTS
SODIUM NITRITE ASSUME 33%
RECORD:
___ ( + ) KI>
STIR 30 MIN AT 28-32 DEG F MAINTAINING +CR
+KI FOR Si 7 RECORD TIME START
6X330
JUL
i SLURRY IN 4G GAL WATER IN DRUM t, -PRECOAT LARIF PRESS WITH
UN 5" <60G) WATER INTO V-....Jit.....
OUR IN SODIUM HYDROXIDE ASSUME 50% OOP IN ACETIC ACID fc Si IF: 3 MIN ASSUME
/fM. 69
28-D
1882
72S-A
7-D 50-D
DUP050463611
HHiUPilr ifH^ i r;uu 1 J. U f'l .i : i H i U r! UHl 1
ECU IF' I MENT 1
1 1 RAGE 2 OF 3 CG 40 CODE RT-539-D (N)
1 USE '1 N-CODE ! ACCT
1 LBS 1
1 LBS
4 CONT*
\U, 1TM
11 1|
RECORD: PH_.Z2r,,<6.5-7*5> & IF NECESSARY
ACETIC ACID ~
ASSUME 70%
ADJ TO PH 6*5-7*5 RECORD PH
*/ SODIUM HYDROXIDE ASSUME 50%
1 |
1 1---------
1 1
! ]
30-D 7-D
I i
1 1 _____
DV \\Y\ WHEN S11 STIR COMPLETE, TEST DV & RECORD: I
5 1 I CR ___C+> KI__f__< + ) TEMP __^4r__28-32*F I.
57-A |
I i NOTE: (IV IF CR-,KI-,ADD 20* "AS IS* INCRE-!
i
i I MENTS
HYDROCHLORIC ACID
ASSUME 32% 1.
28-D |
1 | RECORD: CR( + > KI( + )
I
I
I I <2> IF CR+, KI-, ADD 1 OS "AS IS" INCREMENTS I
iv
SODIUM NITRITE
ASSUME 33%
I 725-A I.
1/RECORD-: CR( + ) KI( + )
1
IGB SULFAMIC ACID IN RUBBER BUCKET AND
WASH INTO DV ,R..5 MIN L RECORD: KI___ jfc____<-) NECESSARY, ADJ TO -KI & RECORD:__--___ <->
IMP IN ACTIVATED CARBON
--
25
395-D '
395-D 1i3-B
! | j
! _jl | 25
DUMP DICALITE FILTER AID IN & STIR 15 MIN.
1 777-A | 10
TURN ON
AGITATOR ADD ICE, THEN
1
I L>SHUT OFF AGITATOR
2X330
57-A j .itJLSL
\2JA\ PUMP DV THRU CLARIF PRESS INTO DV USED IN
1 | S23 MAINTAINING TEMP AT 28-32*F* RECORD:
I I TIME START___ TOTAL MIN
______
I WHEN S23 CLAR-IM9MRL&TE, WASH DV <S4) .
LINES, ?UMFX'PRSS FOR 20.MIN OR TO A
-CR TEST ON A SMPL OF TOTAL PRESS EFFLUENT,
UHICHEVER-CO'ITES^IRST 'XOLLECT WASHINGS IN
(S23)
R 5 MIN & RECORD: TEMP,,J;__<23-32 F)
IF NECESSARY ADJ TO 28-32 DEG F AND
I_______ i
57-A
RECORD ______ 3jk._____DEG F
II
RECORD: VAT_iL,," AND HOLD'TOR S45
/&/ 6
STALL V-/8 TEMP CHART & SET AGITATOR AT i
RPM
RUN IN 20s (1988G) WATER
i
RUN W C457 G) WATER INTO V-3^T Jf/J
1
SCURRY IN 20G WATER AND POUR IN TRISULF'HOILl
DAP D
I
DUMP'IN META NITROANILIDE OF B-HYDROXY
NAPHTHOIC ACID FROM S2
LOT _ ,,
AND STIR 10 MIN * TO WET
FOR S38,
13
39-A 151 -C
13 308
i.
MISC
BUGGIE & HOLD
8 ^ | ^T'FOR S35
ASSUME 50%
1 56" I
133 i WEIGH ACETIC ACID IN RUBBERLINEHX DRUM AND
I 1 HOLD FOR S39
M__ ____,
__Mr!
;Ii|WBIP"C5
i | NOTE: <1)DO NOT PROCEED WITH BATCH <S'S 35
I . If THRU 50)UNTIL S26 CLARIFICATION COMPLETE
! * | (2) WHEN S26 COMPLETE PROCEED WITH BALANCE
I j OF BATCH WITH NO DELAYS TO PREVENT N-151-C
I I SOL1N HYDROLYSIS RESULTING IN BLUE TINE*
I I (3) SUPV'R WILL PROVIDE RELIEF IF NECESSARY
7-D 30-D
78 58
DUP050463612
t
EQUIP MENT
PAGE 3 OF 3 CG 40 CODE RT-539-D (N>
USE LBS
26/82
I N-CODE I ACCT I | LBS
.WHEN S26 COMPLETE, POUR IN N-7-D FROM S32 HEAT TO 155-162*F AFAP RECORD: MIN_yjL,,_ STIR 5 MIN TO DISSOUTC FOR S38. RECORD: SOLUTION COLOR_____PV/__(DARK BROWN) CLARITY4S^1__(MUST BE CLEAR) NOTE: IF SOLUTION NOT DARK BROWN & CLEAR, HEAT TO 185-192#F AFAP AND RECORD: COLOR<DARK BROUN)'
LARITY(MUST BE CLEAR)
I
EN S3? COMPLETE WITH
AGITATOR OFF, f
i
IMMEDIATELY RUN N-330 INTO V-260 AFAP
|
MNEDIATELY TURN ON V-^S&> AGITATOR & SIPHON!
IN N-30-D FROM S33 IN 5-8 MIN*
I
STIR 5 MIN ONLY & RECORD PH_jSjL(11 .0-12.0) I
IF NECESSARY, ADJ TO PH 11.0-12.0
I
SODIUM HYDROXIDE ASSUME 50% 1
RECORD PH _____ ACETIC ACID ASSUME 70% !
RUN IN V-302 OR V-314. FROM SI A'
I
7-D 30-D
AT TO 148-152#F IN 15-20 MIN AND RECORD: I
fiT__J0__*F AND RECy*&___*F
WHEN S44 COMPLETE, IMMEDIATELY COUPLE DV
UNDERSURFACE IN 65-70 MIN. MAINTAIN CV AT, -1 52*F.. RECORD START,jCfg2?T0TAL MIN_*<|_.
^,_R 5 .MIN & RECORD: DIAZQ,,^r__,,<~ OR )
BASEif^kjMUST BE + PH_,,f*i_ (4.5-5.0)
R 15 MIN 6 DISCONNECT TRANS-FER LIN&rAT-
CV RECORD: START_fj>jflJ!?__
i WHEN S47 STIR COMPLETE, TEST CV AND --------
! RECORD!/DIAZO___ n__ MUST BE
'
I BASEJ^f_<MUST BE 4-) FOR BOTH HEALTH AND
! SAFETY REASONS, IF RT-539-D FINISHES WITH AI I + DIAZO, WHEN IT DRIED, IT CAN PRESENT A
I THREAT OF FIRE OR EXPLOSION ON GRINDING IN i FINISHING AREA. SEE YOUR SUPERVISOR IF
! THERE ARE ANY QUESTIONS.
49 ! IF S48 DIAZO IS + AND BASE IS ALSO + SIFT I IN 20-5 N-3-A, SODIUM CARBONATE, t> STIR TO
I - DIAZO. WATCH FOAM,
I RECORD: DIAZO;________________ MUST BE -
I BASEMUST .BE +
j PH<4.8-3.2)
OTAL MIN SINCE S43'___ jtJdZ_____
FLOOD TO 82" <8126 G) AND STOP AGITATOR
I f VAT -
V--303 V-315 V-317 ,V-322 V-323|
1S4 (39SG) 16* 12* 12" 12* 12' I fSB (71OG) 29* 2?" 21 * 21 ` 21 '
1
1 1 START | _____
! __________
FIN ,, JAl L. ,.
OPTR ____
i
1
1 *
*
! 3-A |
DUP05046361 3
N32566.01
DUP050463614