Document 45ogNJd4QpQ30QDbpJVMzNwN

M & U 6 - 07LO MICROBIAL INHIBITION (DEHYDROGENASE ACTIVITY TEST) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was not noted. The test sample is FC-203. Current information indicates it is a mixture of 1.34% PFOS, 35% diethylene glycol butyl ether, 37.85% water, 20% ethylene glycol, 2.66 % Sultone foamer, 3% sodium octyl sulfate, 0.1% sodium lauryl sulfate, and 0.05% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data may not accurately reflect inhibition by the fluorochemical component of the test sample. METHOD:________________________________________________________ Method: Not noted. GLP: No Year completed: 1973-1974 Analytical monitoring: % Transmittance Statistical methods: Results were determined by calculation of the % transmittance and comparison with the blank. Test organism source: Not given Contact time: Not given. RESULTS ________ ;________________________________________ Nominal concentrations: Blank control, 0.01, 0.1,0.5,1, 5, and 10% cone. Element values: Not given. CONCLUSIONS___________________________________________________ No conclusions given. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY___________________________________________________ Reliability: Klimisch ranking = 3. Study lacks description and records of the method followed. Sample purity was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. 000566 REFERENCES The studies were conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request Numbers 2034, 2036, 2093, 1973-1974. OTHER__________________ ___________ :____________________________ Last changed: 6/27/00 000567 F O R M t 06 2 0-PWO cc: LAB REQUEST BOOK - 42-5W File: Water and Wastewater REQUEST FOR LABORATORY WORK Lab Rec<uest No' <2036 TO: ENVIRONMENTAL ENGINEERING LABORATORY - BUILDING 53-6N Requestor Lab Personnel Name: Request D ate. Project No. U6 Prob. No. 0 6 j^orie^ Description: P C -2 0 '3 -t- L - 3 2 4 3 Sample D a te :_________ . Date Needed: Hold Sample F o r. .Days Est. Tim e:. neo Hrs. MDate Rec'd. Sample:___ Analyst:_____ Z Y r" ` Date Completed:. Hrs. Spent: ____ B / W /77 'K 'K . Sample Description fC -263 L- 3243 Total Hardness, mg/l as CaC03 Calcium Hardness, mg/l as CaC03 "P" Alkalinity, mg/l as CaC03 "M " Alkalinity, mg/l as CaC03 pH Sulfate, mg/l as SO4 Nitrate, mg/l as NO3 Chloride, mg/l as Cl Silica, mg/l as Si02 Fluoride, mg/l as F Ortho Phosphate, mg/l as P Total Phosphate, mg/l as P Total Chromium, mg/l as Cr Hex. Chromium, mg/l as Cr Total Cyanide, mg/l as CN Ferrocyanide, mg/l as CN Iron, mg/l as Fe Manganese, mg/l as Mn Surfactant, mg/l as LAS Phenol, mg/l BOD, mg/l COD, mg/l (Short, Long, Dilute) Total Suspended Solids, mg/l "Volatile Suspended Solids, mg/l Turbidity, mg/l Silica Total Solids, mg/l Total Volatile Solids, mg/l Conductivity, mhos Total Bacteria, No./100 ml Total Coliform, No./100 ml Fecal Coliform, No./100 ml Fecal Streptococcus, No./100 ml Ammonia Nitrogen, mg/l as N Kjedldahl Nitrogen, mg/l as N Oil and Grease, mg/l /' / C. Comments: ** L.tAUM '- y 5,640 r BT7n3 mr % Tra pa1fa*\ee 71 106 Tra* !ft 70 AL f' IM A A l IL AM lo4.5 * (pia 00056SflcrtioB iM i White -- Environmental Engrg. Lab Canary -- Environmental Engrg. Lab Pink -- Environmental Engrg. Lab Gotdenrod -- Requesters Copy cc: LAB. RE BEST T.BOi 2-5W Water and Wastewater File: REQUEST FOR LABORATORY WORK Lab Re^uest No- TO: ENVIRONMENTAL ENGINEERING LABORATORY - BUILDING 53-6N Requestor Name 'rojttut T5>; Description: _ Sample Date: Hold Sample For C O <yJ Request D ate. ' h . Prob. No. 0 V'- Code . Date Needed: .Days Est. T im e:. ih i '0 0 . Hrs. Sample Description Total Hardness, mg/l as CaCC>3 /w u Calcium Hardness, mg/l as CaCCh "P" Alkalinity, mg/l as CaCC>3 "M " Alkalinity, mg/l as CaC03 ___ C o a . >.o j y r Sulfate, mg/l as SO4 Nitrate, mg/l as NO3 A .l 0, ^ Chloride, mg/l as Cl | Silica, mg/l as Si02 Fluoride, mg/l as F S' 7a 1Q 7 a Ortho Phosphate, mg/l as P C ,O ^ W a t' M L + U j pfl' H T E Total Phosphate, mg/l as P Total Chromium, mg/l as Cr Hex. Chromium, mg/l as Cr Total Cyanide, mg/l as CN Ferrocyanide, mg/l as CN Iron, mg/l as Fe Manganese, mg/l as Mn Surfactant, mg/l as LAS Phenol, mg/l BOD, mg/l COD, mg/l (Short, Long, Dilute) Total Suspended Solids, mg/l Volatile Suspended Solids, mg/l Turbidity, mg/l Silica 4 74 Total Solids, mg/l Total Volatile Solids, mg/l Conductivity, mhos Total Bacteria, No./100 ml Total Coliform, No./100 ml Fecal Coliform, No./100 ml Fecal Streptococcus, No./100 ml Ammonia Nitrogen, mg/l as N Kjedldahl Nitrogen, mg/l as N Oil and Grease, mg/l Lab Personnel Date Rec'd. Sample:_ ' / S O Analyst: > H Date Completed:. z w 24 Hrs. Spent: ____ j8 _ - F c t o i Z 3 2 ff'Z . ^ / V ^ C 'IO b 1 - ftT 26 n /2 .5 -- 4 /.S " *>S.S zu * trr /e 1 3 .S /q 34 5 *S' ... q s ZL -- T 14 i3 3 4 S"8 2U -- Comments: f/s . .^ sh. Q./< ~{^ - -y Z Tre.- r uA yfUjdli*ii-';t- *--C _/ r t / ' L(.t- U --. g {* , i y . j .. / 5 ^ . . . f l ,, r < / , 000569 30 I m Whito -- Environmental Engrg. Lab Canary -- Environmental Engrg. Lab Pink -- Environmental Engrg. Lab GoldenroO -- Requesters Copy ioio. PRODUCT ECOLOGICAL ASSESS>NT REQUEST FOR LABORATORY WORK K -. _ 5 Q 3 j? A l..'; L- ( flU t Q A /*-VtV .* f? w 2 a -c / fC ^ L O 3 -- ' ' REQUESTOR NAME : -1 i . REQUEST DATE: PROJECT NO .: CODE NO .: SAMPLE DATE: DATE NEEDED: PROB. NO.: LABORATORY L 37.4-3 DATE RECEIVED SAMPLE: ANALYST: v/rA**ir DATE COMPLETED: if??/74HOURS SPENT: 15kr Y a _ ?-- DESCUfTION: TURPOSE OF TESTS: BIOASSAY . V ; . ;* H& - ; Freshwater Fish" Marine Fish . Microorganisms Aquatic Plants Land Plants Birds Mammals . LEACHABILITY Parent M aterial pH COD ag/g BOD mg/g BOD, u ltim a te T5c GC Bioassay Other V'?'; i&J ' v>;:' Leachate . T. . - N\- pH COD mg/g BftD" mg/g BOD7 u ltim a te TOC cc Bioassav Other . ' - *' * . > r-' . c v *.-..V r - "it ' /S ` `f . '/ //t : : . a; V r^. > . # \ B E S T C O P Y A V A IL A B L E 0 0 0 5' ro B E S T C O P Y A V A IL A B L E r P P H S I O A L f, C H f c M i r u ' . p k o p e r t i l s h e a t i.f i . o m b u s n o n h e n s i:y Asii C o rro s ive n e ss c a l/g (B T U /lb .) r WAT!K PO LLUTIO N pH r.ou BOi T Oxygen U ptake 'l l e a t a b i 1 i t y - S t u d y o riiD t ' .. .1 <y ;; J iv "mSStSSc* * l * ---* , V ' /> --V J M U V ; M e - J ]\ t i u * Q b i u a c c u n u l a t i jr. r c a . -, s L uv ri ^ -* P e rs is te n c e P e g rid a tro n P ro d ucts R e c y c la b l1 i ty B u rn a b ility - -- (. t t c . r _ ,K X x. X ,< ^ ' , i y j x y, y AX X K -^ ' i ' ' \ *- - i V-..L <r *- * . * > , . .V,- - ; 9 r. /G ! : V ;; ;. A 4- \ . - ,`V ' <d 5 ( .-1 4 -7 * 1 000571 File : Page No. EN\TPONMENTA L F.NGR. LAD - WORK SHEET SAMPLE DESCRUTI 0:'' v. T . 7 X G1' e< w\ A-vr IV/ - e .v/ B E S T C O P Y A V A IL A B L E / v-iiV' r Date : ^2oM 3 Analyst ; * J Hrs.: F C -Z O '*/ - .......... -V 1V ___ f 1j 1d o .. A- < / /f. . 7 -I//.0 _ /O m i/ / oo " _ U <//_o_ 2 . C w ?i C -f 6 .5 . A1 . Ad. m .-s < f./ l.S " 1,0 r .0 0 . ///a /// JtkL 67 il 86 67 i " " ' ' ' " ~ n C(*S 77 File: Page No. ENVIRONlKNTAL ENGR. LAB - WORK SHEET SAMPLE DKSCRIPT] (N r T TC B E S T C O P Y A V A IL A B L E D st * Analyst Hrs. :