Document 445wwoeedawmkp0vVEN2gQxmG
..........
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-4cfr'ifeft*.* .CORF YC-it-A r-'KG
JUL 2 4 m
G2J75
/"d St I")"'" ~(LOT NUMBER)
. ES7* WT*. 2126* LBS*
; PREPARATION NOTES :
'
DATE PRINTED'- 1 2/22/B1/t^ D.V. \30d, Bi5\ 317, 322,
PROCESSES (C)YC-1 1 -A < )
APPROVED BY JJG' 6/1G/81 EUK 10/21/81
TYPED BY: JMH STANDARD HRS * _________
f____ ________________l M~
TINE
EQUIP WENT
'""~I___
NAME: DALAMAR YELLOW
uBTAIN 5-NITRO-2-AHINOANISOLE FOR $6
'
OBTAIN ACETO ACET ORTHO ANISIDIDE FOR S22
CLEAN, DRESS, CLOSE 24" CLARIF PRESS -
\ 15 FRAMES
...
! USE i LBS
| ! I I
BLEEDING
! N-CODE j ACCT ]|
i 557-C i t 43~C J
RUN~17" <595"G>-WAflR~iNT0
j WEIGH IN HYDROCHLORIC ACID FROM V-324
I M__L_______ 5* fL2L_%
{ DUMP & RINSE IN .5-NITRQ-2-AMIN0~ANISGLE
1 DRUMS FROM SI
LOT.
* 100%
%
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___I
2S-D 557-C
458 974
-i
...I I
121982
STIR 10 MIN OR LONGER TO WET
ADJ TO-33" <1155 G> AT 28-32 DEG F. (ICE)
SIPHON IN SODIUM NITRITE IN 12-15 nMi%sc . * .
STIR 30 MIN AT 2S-32 DEG F MAINTAINING
|
+ CR, + KT FOR S 12 . /?
i
RECORD: TIME, START
CR__i ( + ) ,
I
KI___(-H
I
NOTE:(i> IF CR-, KI-, ADD 205: "AS 'IS"
I
INCREMENTS HYDROCHLORIC ACID
i
ASSUME 32% I
RECORD: CR< + >, KI(+)
I
(2) IF CR+,KI-, ADD 20$ "AS IS" 5NCREHENTSI
' SODIUM NITRITE
ASSUME 33% I
RECORD: CR_________ < + >, KI______ < + )
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j <330
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1
57-A !
725-A
28-D
DUPO 50463722
"r. ISTRUCTIO NS:BATCH UNIT
EQUIP 1 MENT I ' | PAGE 2 OF 3
CG 46 CODE YC-li-A
T ~u5i~"7 "n -c o d g m ~ACCT
(C) ! LBS f
i LBS
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SLURRY IN 40 GAL WAFER IN DRUM & PRECOAT i
i
1
i CLARIF PRESS WITH DICALITE FILTER AID
I 5 1 777-A 1
5
1 1 u / '1
DV
iW*]~ WHEN SIS STIR COMPLETE, DUMP IN ACTIVATED .!
15
_____ i 113-B i
15
4' \^er CARBON DUMP IN DICALITE FILTER AID
1 .1 1 10 1 777--A J
10
s m -STIR 30 MIN AT 28-32 DEG ^MAINTAINING
\ i
i + CR, + KI FOR S 20 i. RECORD: TIME START/L^SJf^,
CR. -t .( + >
1 '1 1- -1 57-A | *
Kliafr.___(+>
l NOTE: (1) IF CR~, KI~, ADD 2$ "AS IS *
INCREMENTS HYDROCHLORIC ACID.
1
ASSUME 32% I________ I
2S-D i______
- RECORD: CR< + KI( + >
I1
1i f. I II
(2) IF R+,KI~, ADD 205= "AS, IS" INCREMENTS I
i
SODIUM NITRITE
' ASSUME 33% I________ 1
RECORD: CR_______< + ), KI_______( + > I 1
725--A i______
? RUN"7o~~(970~G)'"wATiR~lNTO'"vZI2iICI"*!"'-
5 | ^ INSTALL TEMP CHART
.
POUR IN SODIUM HYDROXIDE . M_/o_L__ ,
`>1^1 ADJ T0 40 43904 G) AT 66-70 DEG F
X'&TX CLOSE STACK DAMPER
lj/1 STIR FOR S 22
I I.
ii i t>s ! i ,,J_TJ2\ I 3X330 i I1 1!
II
^`wHlN^rTriiiR cpMPLiTE7~TisT mT&i RECORD
fc. I CR'Z|1.,,_( + ) , KI_4r_,,<+)LTEMP:JSJ--J(28-32 F) NOTE': (i) IF CR-, KI-, ADD 20$ "AS IS"'
l
INCREMENTS HYDROCHLORIC ACID
ASSUME 32% l._______'I
RECORD: CR< + ) , KI< + )
II
(2) IF CR+,KI-, ADD- 20$ "AS IS" INCREMENTS I
I
SODIUM NITRITE
"ASSUME 33%
RECORD: CR< + ), KI( + >
TURN ON
AGITATOR, CHOP & ADD ICE. 1^X3301
THEN SHUT OFF AGITATOR.
PUMP DV THRU CLARIF PRESS INTO DV
II
MAINTAINING TEMP AT .28-33 DEG F
RECORD: TIME START ,.^05M TOTAL MIN.
i
1 DUMP INTO CV FROM S2 ACETO ACET ORTHO
ANISIDIDE
. -.NOTE,:, ft', BREAK UP
LOT
$100%
%
| LUMPS
i TO MXN TO DISSOLVE
STACK DAMPER
Lsrir r u n in u n d e r s u r f a c e in 20-9
r
M&Pe/z.
m..
5 MIN 4 RECORD: PH
I2STI IF NECESSARY, ADJ TO PH 2>.8--6.3
i* f ' I1
SODIUM HYDROXIDE
. ASSUME 50%
ACETIC ACIDCVAP^J!?J ASSUME 70%
I ' 5 RECORD: PH_______ '<5.8-6^3) - ';
7-D 5 7-A
28-D 1_,,. 1
725-A
57-A i2fc
46-C 1 1265 I
30--D
713
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DUP050463723
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h-A's*.-
1- l , , \ PAG 3
OF
CG 46 CODE YC-11-A
I USE (C) I LBS
i
WHEN S 21 CLARIF COMPLETE, WASH DV (S 4)
LINES, PUMP & PRESS FOR 20 MTf! OR TO A ~CR
TEST' ON A SAMPLE TO TOTAL PRESS EFFLUENT, 1
WHICHEVER COMES FIRST. COLLECT WASHINGS
TKl tV
CORD:" "TIME STARt 3-5S__CR_--L<- OR +)
P
ACCT LBS
i
STIR 5 MIN 6 RECORD: TEMP^gl.(28-32 DEG F) 6 IF NECESSARY, ADJ TO 28-32 DEG F RECORD: ___J3EG F
>7-A
5'MIN & RECORD: KI,,_ ECESSARY. ADJ TO-fKI & RECORD:
MISC a
CV Iff
l
r-J O-
ODIUM HYDROXIDE IN DRUMS FOR S41__ .. m__<i _____,j*Er%
DISSOLVE IGEPAL C0630IN 2 GAL WATER IN i DRUMS FDR S43
\3J.\
| '62 ! II I1
7-D 979-D
W | WHENS 3 COMPLETE, ADJ CV TO 48" (4685 G)
ii
\wr\ cChHECK ACCURACY: HT_LJjfe^-DEG F 6
|
i
r e c o r d e r _'_Jk >__. d e g f IMMEDIATELY RUN IN DV THRU UNDERSURFACE DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV
'i l i
I AT 80-84 DEG F I^BECORD:. TIME START
TOTAL MIN`_^r
WHEN S 38 COMPLETE, STIR 10 MIN IMMEDIATELY AFTER COUPLING DISCONNECT!
TRANSFER LINE AT CV
I
RECORD: NOTE:
DIAZO_j s --= __<->, BASE,,_JrL_< + >,
PH 14.3-4.7) ' ..
f
| |
1
(1) IF DIAZO +, BASE
AND PH BELOW 4.3:
(A) ADJ ,T0 PH 4.3-4.?. SODIUM HYDROXIDE
(B> RECORD;' PH '
'ASSUME.50%
7-D
(2) IF DIAZO +, BASE -, 6 PH 4.3 OR ABOVE:
(A) ADD 8# 100% N-7-D .SODIUM HYDROXIDE TO A 55G DRUM
1B> ADJ WITH WATER TO 25G (C> ADD 20# 100% N-46-C ACETO ACET ORTHO
ANISIDIDE (D) STIR TO DISSOLVE (E> POUR INTO CV
7-D
____ I 46-C l__ _ 1i
(F) STIR 10 MIN
(3) REPEAT (1)6 (2) ABOVE AS NECESSARY TO - DIAZO, + BASE
IN N-7-D SODIUM HYDROXIDE FROM S34 & 5 MIN. RECORD: PH_fcSX8.0-8.5) & IF NECESSARY ADJ i
I
TO PH 8.0-11.5.' SODIUM HYDROXIDE. ASSUME 50%!
|
RECORD PHjSrJW1 HYDROCHLORIC ACID.ASSUME 32%I ___ _|
7-D
DUP050463724
DUP050463725
N32597.01
DUP050463726