Document 3rD0ga1D7QGDLed2Z94ojrvO

32) Differential Scanning Calorimetry (DSC), Melting point (273 C) Filename: Data Collected: Operalor ID: Sample ID: Sample Weight: Comment: C:\PE\Pyris\Da. ..\111269-48KOT10001DSCR.dsd 11/13/01 1:55:00 PM TAK GID #26596 SB "LOT 10001(NB#I 11269-48)" 7.894 mg 75 70 65 I 60 I 55 - E a 3 3 50 C W z - lL 5 45 I 40 Peak = 24.337 " C Area = 259.{59 rnJ - t Delta H = 32.906 Jlg 717 "C I Area = 2421134 rnJ Delta H = 30.673 Jlg 35 ~______. Ii - 30 - ._ 25 ..... __ 23 70 80 100 120 140 Sample ID:T-7485 SB "LOT 10001(NB#111269-48)": 111269-48KOT10001DSCR.dsd Heat Flpw Endo Up (rnw) : Slep: 1 Contains NOCBI SB "LOT 10001(NB#ll1269-48)": 111269-48KOT10001DSCR.d~d Heal Flow Endo Up (rnw):Step: 5 -. .~___ PerkinElmer Thermal Analysis ! - Area/= 112.999 m4 Delta H = 14.315 J!g 1 Peak = 455.670 "C __ 1 - t 1 - - I I I -I 1 Area = 10.781 rnJ Delta H = 1.q66 Jig i Peak = 23(0.6:& /I I ' Inset = 225.374 "C ,/,ji I Onset = 25 I I i 1 I Peak = 255.733 "C Prea = 113.645 rnJ i ---___ I Della H = 14.395 Jlg I 1 I I * - -L- _ - L.- I i I 3 = 8.663 rnJ i I L-L Peak = 233.066,"C iI 1 __ I/ / iI DEIC 0 9 2003 ! Peak 273.337 "C ' I Area = 146.345 I I Delia H = 18.53E I 1 I I 1 j II i! I 55 "G !- lj 1I I Onset = 270.s 9 "C i ! i J IDelia H = 18.18: 1 Jki ! ~~~ :1---- I ! I Ill ! II laa oc I & k e t = 270.s I 7 "C 160 180 200 220 240 260 280 300 310 Temperalure ("C) 1) Heal from -2O.OO"C lo 300.00"C al20.00"Clmin 2) Hold for 1.0 min a! 300.00"C 3) Cool from 300.00"C lo -2O.OO"C at 40.00"Clmin ~~ ~~ 4) Hold for 2.0 rnin al -2O.OO"C 5) Heat from -2O.OO"C l Q 300.00"C a l 20.00"C/min 11/13/01 2:19:32 PM ___-__