Document 3egbDEg8EaQeJaVDn3oRqGQnJ
BettyBoros Russo-FW L2604996- Cyof SalemPFOAPPFOS (41h roundofSamping)
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DEPZ.SDWB-000277
To Cres
008 GS
L206 04 29L-1
Ti esti Amera ica
ANALYTICAL REPORT
PFOAPFOS Analysis Lot: DsDOdsze
Nic smith S1o2au0Ct5hLIanamdbpuosirtosrtnio,arliPeHAsi,g1ih6nw9ca.6y6 TostAmerica aboratoris, inc.
Fo: fk A. Johnston Project Manager
/ April 17, 2008
958 aro See Ani,CORR ASE e307 soemsesametclnccom DEP2-SOWB.000278
Table Of Contents Standard Deliverables
Report Contents
pTSrhtesaoonvfdehaiLsrSedetDnredalaiDvhoeevRreeagrebrlCeosnaecpaagThriescroenpsoirdtesrecdonimgrpaal issallegesnicatdnhsToteof Contes re ies
+ TaofbColnteents
+ CaseNarrative
Executive
Summary ~Detection Highlights
Methods Summary
+ Method/Analyst Summary
+ LotSampleSummary
+ Analytical Reslts
QCDataAssociation Summary
+ Chain-of-Custody
Total Number
of Pages
TestAmerica
1
DEPZ.SDWB-000279
CasDeeDN0a40rzr6a1tive
dTipnareatescastcseAohnmertaedertadinciicaoneatDwsheisisnirhsvetephrionerutttmhwieeeztnrohlseoeUdarsSnparEilenPytczAaiecoadanplfpodofr.othvDaoeidrpsemasoerunalltmhsaeotcdetsrosisnsaatlnledadn1aool0yt1eincoatlemsweaotrrhkoo.dpsTrshoevuesadmmopenlepSsaacghe
huts lle coy somes n te port ad oot al imentsof NELAC, AL
datahavebeen revfiore comwple iandce withthe laboratoryQA/QC plan `compliant with laboratory protocols with any exceplions noted below.
and
havefound
tobe
Pleaso nol that Non-Deloct (ND) results have been evalualed down the Method Detection
LSiamiitd(hMaDvLe)baenednsdhroyulWdebigehctocnosmidoecreedd NDat the MOL. Unless otherwisenoted,resultsfor
"This report shall not be reproduced except in full, without the wisn approval of he laboratory. "`GTSohacemfupomllaoorwiAierndgvsaraelpanonretdcRoSonctaoailnpast tSho Bradanlytic enresuTlhsofcoroenpesae mplee received4ea/a4s0n8,aacording cd0 femperaturo of 23C. No anomalies wers encouniored during somplo recip.
`S(AnPtaFalOnyAdt)iac.radPlssFtOaSndiasrdascwoomrmeeprrceipaalrperdeupsairnegd haendacciodrfoeudnosfotluhbeocn.ompoundperuoroocianaicadd iaPnneitrnrofomadlluaostctrtaehnoodda-erxdntfr{oarc1dqioou,cnatn2saiin.focap,ataon4ncd-dowfwaPasCFsuOsAne.dalPs oaen dianrttteuhmae1fel.cxs2ttlr.aaa3ncd4tua"dirCod.nsJofotocrotprqaanunaalodnewsiuai-lslauoin-oastnfeewadsas PFS.
`Sample Extraction and Analysis TDheensvearm'pslSeOprPeDsEenNt-eLdCi-n00t1hi2sAr.eportwas analyzed forthetargetanalyteby TestAmerica
Faonrdwtatserexstarmapctleedsuas2in5g0somlLdapihqausoet eofxeraacchosnamepclheniisquaocwkiilhedmevtihtahn1olmc.oonfdi6tNioHnCedIsGo1u8ion
`cartridges. Each sample is spiked with the intemal standard, prior to extraction. After ee `sample ispassed through thecartridge, theanalytes are eluted with 4 mL of methanol. final volumeis broughtto 5mL using methanol and the extractis analyzedby LC/MS/MS.
MatQChSamopldes TheMethodBlankisprocessedreagentwaterspikedwithsuogateandpreparedwitheach mi `batchof20samplesofthesamemalrix. Themethodblankwasnon-detectatthereporting
Ea`ocnhcebniartacthioinplreoveplasroofdwLiabtohraatLoarbyorGaotonroyCoSnatmrpolleSsawmeprloe(wiLlCiSn)coTnhtreolrmoacs.overofiwoso
Teathnerica
2
DEPZ.SDWB-000280
Analytical Comments
p`rTehpeaSntadndLaCrcdonOdpietriaotnisn.gPTrhoeceadulret(eSOraPr)aewlatissa.tiletdoebreneldosswl.ightlyfor thesesamplesinthesample
TShesaampPlmreespDwpietrrolapnrcooepsp:edfolowingthenormalprocedurofor SOP DEN-LC-0012, Revisio4n uapsuuntsiel dseicntiioana1d0o.f1.a3.P10.hTheesnesoamSpmtlaeesswXenrceoclnuoxmtna.ciTdhiefiseadmapnldeaswWearteersnOeaesdis2 Waexscwoilnumn
mLofformicacid solution insteadofHPLC gradewater, which differs from section 10.1.3.19.
`vTahleofro.rmSieccaticoinds1olu0tio1n i.spars3eapfp.eede2bdyb0dyilaudtdiingng2.422m5Lmoif.o1f%88a%mfmoernmiucmachidytod1r00oimnLxmewitihtdahneol
toeachcartridgeinsteadof 4mLof methanol.
Noother anomwaeraiobiseervesd.
TestAmerica
3
DEPZ.SDWB-000281
EXECUTIVE SUMMARY - Detection Highlights DaDot0261
onenTER. 12604596-1 04/02/08 09:00 001
ron
Resor RELRoOaRrTING ours 0.0083 0.010 uae
AMeAsLoTnICAL omy 10-0012
Testamerica
DEP2.SDWB-000282
METHODSSUMMARY Dabosozer
ParvETER
ARMLemYoTnICNL
we/ws/vs, Bron
Dew -1c-0012
References:
EY
Severn Trent Laboratores, Operating Procedure:
Denver,
Facility
Standard
wPERTEHPOADRATION
Testmerica
5 DEP2.SDWB-000283
METHOD / ANALYST SUMMARY `Danoss261
MReTmoI
move
aN -1c-0012
Jaqueline Bonnett
References:
om OSepveerrantiTnrgenPtrocLeadbuorrea.tores, Denver, Facility Standard
RTMOAST a03601
TestAnerica
6 DEP2.SDWB-000284
SAMPLESUMMARY DaDosoz6i.
Ho # smerer cura snes KKQVE 001 12604996-1 wTohras(s)t:nah 5 og od oe rd ep 0cn epeeerrede iefrcld iPetpseretebippd,sreee,preidotn4he l 4p ,of cr brery,de, bi,se, oo,
pyr,cnc, el pen ec, lO,me,Hen,
SpLED Sap os oe 04/02/08 09:00
TestAmerica
7 DEP2.SDWB-000285
0 Laboratories
Client Sample 10: 12604996-1
nec
LDoatt-eSSamapmlpele..d.:.: D04O/D0O2M/002861-0090:100 WDoartke ROredceeriv.e.d...:: X04K/Q0V4I/Z0A0A
PrPreeppDBaattche......:: 08140/00132/108 Dilution Factor: 1
AAnnaallyyssitss TDaitmee....+ 0004:/2191/08
Method.........: DEN -1C-0012
Matrix... WATER .
rpoannes ros
R0e.s0u0L5T8. 3 w
RweaporRTING murs 0o.0o10 wga/rtn
s1u3m0R4oaparToEA 1304 pros
REpCeORVcEaRTY 1n08
RLeacosvery (50 - 260) (50 - 200)
BoTR(S+)
TestAnerica
8 DEP2.SDWB-000286
sneer 001
QC DATA ASSOCIATION SUMMARY DaD0so261
Sample Preparation and Analysis Control Kumbers
wmIK npowmToIen, WER DEN -Lc-o012
BaAnTcCH
BeAsTeHE s10021
Ms ow 820006
Testamerica
s DEP2-SDWB-000287
METHOD BLANK REPORT
MCl5ieLnott-Lsoakmpl.e..#:: ADnialluytsitosn DFaatcet.o.r::
rPohunaTER eros
`3su0R4RoGpArToE.n 1304 pros oCrao(sn) epoch
RDOGDDO3K00020601-121 WorkOrder ...:KIXMTINA 04/10/08 PPrreepp BDaattec.h........:: 80140/00132/108 1
Rwesour ww
RiEaPOrRTING wars 00.001100 uwga/sut
~REmRcocvRsTRY fEym
`LRaecrovsERY ((5500 -- 220000))
og i kore hdri
Matrix.......WA.T.E:R oalysis Time..: 23:50
saeme-n1G-0012 BN -Lc-0012
Testamerica
10 DEP2.SDWB-000288
'LABORKTORY CONTROL, SAHPLE EVALUATION REPORT
me
C1l0iSenLtotL-oStam9p.l.e.d:DSRD3OD0G9O0206010-121WorkOrder ...:KIWTIAC PPrreoppBDaattceh...#......:: 0841/00091/2010 A`Annaallyyssiiss DTaitme.e..:: 0004:/0131/08 Dilution Factor: 1
Matrix..TE.R
eEneynarsR. Pros
vREECROCVEENRTY 0%
RLEmCMOIVTESRY 0(33--1123000)
eDeow n-1c-o01z Daw -1c-002
s13u0R4RooParTosn. 1301 pros
ReeecrocavNeTry 1"0
RLemcaotvsery ((500 -- 220000)
CHhoriR(nS)ep vort fe --
tfre hth.
~
EE
Testamerica
1 DEP2.SDWB-000289
LABORATORY CONTROL SAMVL DATA REPORT
CliLoetn..t.: DIDOA0261 Work Order F...:KKWTIAC LPCrSepLoDta-tSoa.m.p.l.e.d.:: R084D/00390/00080-121 Amalysis Date..: 04/11/08 DPirleuptBiaontcFhact.o.r.:: 81100121 `Boalyais Time..: 00:03
Matrix..MAT.ER
pnroEnTER Pros
msoewxesr MwEAoSUnRED ums 00..220000 00..119876 waarltte
gaeRcCoRvNeTy Memon %Ey Dbmrx 1160--00001122
`Tsiucmemospartosn. 13c4 PROS
eRaerccaorn 10"8
ReLpcaorvresry ((5500 -- 220000)
ocToRne(sSw)epnt or in ro esod
Testamerica
12 DEP2-SDWB-000250
LABORATORY CONTROL SAMPLE EVALUATION REPORT
wc
IClCienTtoLt-oStam8p.l.e.d:: RDIIDDO0A300206010-121WorkOrder ...: KKXHTLAD PPrreepp BDaatcthei...... 8041/00031/2018 MAaaxallyyssiios TDaitne.e... 0004:/1161/08 Dilution Factor: 1
Matrix... WATER
ramonnsTER. eos
BPEEcRoCvEeNRTe %0
LREoCwOVsERY 3[9E-1E20T)
sErii= on r Dew -nc-ooxz
-- ace pr-- on 13c4 pros Colrisn)i: et io ok pmots emes
mca mTios ver 5
REcovERY Smoar-s2_0_0 (50 - 200
Testhnerica
3 DEP2-SDWB-000281
LABORXTORY CONTROL SABLE DATA REPORT
were
C10SlLoitL-oSetamnp.l.et.f:: DRI8DDO0A300206010-121WorkOrder F...: XKWFIAD Prreepp DBaattec.h..#......:: 08140/00132/108 A`hnoaallyyssiiss DTaitmee....:: 0040/:1116/08 Dilution Factor: 1
Matrix.......WA.T.E:R
ProEnTER wos
mseorweT MmaRosuuRED outs oo.l0o220000 60..010596 wnga/tL
sPeEcRoCvEeNRTy Mgmiob
5
DDaewx 1-16c--00001122
`Ts3ucmeRopuraoTn 134 prOS
remroocvasNsTr "1s
RLEiCaOrVsERY ((5500 -- 2200007)
CorRn(s) ptevl nig oo cr a pe dr coers.
Testamerica
1 DEP2.SDWB-000252
MATRIX SPIKE SAMPLE EVALUATION REPORT
wee
C5lieLontt-SLoatmp#l.e..#:: DDAIDD00A4O02366)2-001 WorkOrder J...: KKKGQUVLVIAADC--MM5SD DParteep SDaamtpel.e.d.......:: 0044//0029//0088 08:30 ADoaatleyRseicseiDvaetde....:: 0044//0141//0008 PDrielputBiaotnchFact.o.r.:: 81100121 Analysis Time:. 00:55.
Mabrix.........: WATER
EeDae: vrs
RPEEcRoCvEeNRTy| iREmCaOmVsERY
o5s5
0(0--13B0o)y
o BY
((3399--112200))
RED LomnMTS 0.44 (0-200 1.3 (0200
DMaemH1OD6-0012 DpmEsX _-cC--00001122 pms -1c-0012
`1su3RksooPnRtOeN. 1301 PROS
RE`ECROcVRENRTY mm22 a0
a Lusd s ((5500 -- 220000)7 ((5500 -- 2200000)
CHooroE(nS)vepotdr mi dot cre cid
Testanerica
15 DEP2.SDWB-000283
MATRIX SPIXE SAMPLE
ec
CMlSicLoatt-sLoakmpl#.e..:: DDS8DDO0A0O226621-001 WorkOrder ...: PDraetpeDSaamtpele.d....:. 0044//0029//0080 0:30 MDoaatleysRiesceiDvaetd.e..: DPirleuptBiaotnchFa#c.t.o.r:: 81100121 Analysis Tice:.
EprDamaTER ros
SMWOPNLTE SMerxe vAMEORDSNRTD 00.00330 00.221300 00..222390 000.008022 00..22100 00..115925
`TsamcRsooPaRTosA. 1304 ROS
RpecRocvazRTy 1122 aa
Csolmoens)v:eprot oi ptds otpron
nd 8hn
DATA REPORT
KRKQUQVWLIAADC--MHSSD. 0044//1014//0088 00:55
Mabrix.........: WATER
ITs ReEmCRVaRNYT ROD METHOD uuge/sL 595 o.e4 Dpeww 11c6--00001122 uugo//Ln 8o Lo RDwm o10z-c0o0m1z2
Roeacrovsery ((5500 -- 220000)) ((5500 -- 220000))
TestAmerica
16 DEP2.SDWB-000284
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