Document 3eaVDBdZbGGZXMB94XN9rkg43
Inspection Entry Date/Time
Inspection Exit Date/Time Regulatory Program Type of Inspection
EPA REGION 6 Enforcement Division
INSPECTION REPORT
11/06/2024 14:00 (CT) 11/06/2024 15:30 (CT)
Announced: No (tenants and related facilities) Access: Granted
RCRA Focused Compliance Inspection (FCI)
Facility or Site Name Facility/Site Identifier Facility/Site Physical Address City, State, Zip Code County/Borough Generator Status NAICS Type of Operation
Geographic Coordinates
Martin Operating Partnership LP TXR000060909 10 Sulfur Plant Rd. Beaumont, TX 77701 Jefferson County Very Small Quantity Generator (VSQG) 42471 Martin Operating Partnerships LP is a storage terminal facility for chemical products including molten sulfur, crude oil, sulfuric acid, and asphalt. 30.0294, -94.0566
Additional Persons Participating in Inspection:
Name
Title
Organization
Angela Hays
Inspector
EPA REGION 6
Sandesh Thapa
Inspector
EPA REGION 6
Jon Herbay
Contractor
Eastern Research Group (ERG)
Email Hays.Angela@epa.gov Thapa.Sandesh@epa.gov Jon.Herbay@erg.com
Lead Inspector: Vince Damiano
Chemical Engineer ERG
Vincent Damiano
Digitally signed by Vincent Damiano Date: 2025.02.06 11:28:13 -05'00'
Vince.Damiano@erg.com
Phone (214) 665-2285 (214) 665-2265 (412) 780-9931
02/06/2025 (703) 633-1732
Page 1 of 5
Martin Operating Partnership LP
Inspection Date: 11/06/2024
SECTION I - INTRODUCTION
Site Entry and Purpose of the Inspection
The Port Beaumont and surrounding facilities were selected for inspection based on an Environmental Justice and Regional initiative to evaluate facilities at ports receiving or transporting Resource Conservation and Recovery Act (RCRA)-regulated hazardous wastes, and/or have an International Convention for the Prevention of Pollution from Ships (MARPOL) Annex V Certificate of Adequacy (COA) issued by the U.S. Coast Guard (USCG).
This report is based on information supplied by the facility representatives, inspector observations, port related facilities, and records including photographs taken (see Appendix 1), verbal or written statements made during or after the on-site inspection, and/or materials shown, demonstrated, or submitted to the Environmental Protection Agency (EPA) during or after the on-site inspection. In addition, information gathered prior to or after the inspection from a review of EPA, State, and public records may be included in this report.
Attendees
Title/Organization
Name
Phone
Lead Inspector/ Contractor/ERG
Vince Damiano
(703) 633-1732
Inspector/Enforcement Officer/EPA Region 6
Angela Hays
(214) 665-2285
Inspector/Enforcement Officer/EPA Region 6
Sandesh Thapa
(469) 616-8578
RCRA Inspector/ Contractor/ERG
Jon Herbay (412) 780-9931
Martin Operating Partnership, Josh Tallina (409) 790-3424 LP
Martin Operating Partnership, James
LP
Alford
(409) 673-9423
Email Vince.Damiano@erg.com
Openi ng Closing
Conf. Conf.
Yes Yes
Hays.Angela@epa.gov
Yes Yes
Thapa.Sandesh@epa.gov
Yes Yes
Jon.Herbay@erg.com
Yes Yes
Joshua.Tallina@MartinCP.com Yes Yes
James.Alford@MartinCP.com Yes Yes
Page 2 of 5
Martin Operating Partnership LP Facility General Description
Inspection Date: 11/06/2024
Tenant/Area Martin Operating Partnership LP
Inspection Date
11/06/24
Process Description Martin Operating Partnership LP (MOP) is a storage terminal facility for chemical products including molten sulfur, crude oil, sulfuric acid, and asphalt. MOP moves products via trucks, barges, ships, and rail cars. The facility maintains a MARPOL COA for annexes I, II, and V.
Area of Concern
Yes
SECTION II - OBSERVATIONS
Tenant: Martin Operating Partnership LP
Section: 2.1
Date: 11/06/24, 2:00 PM Contains AOC: Yes Contains CBI: No
Lead Inspector: Vince Damiano Attendees: Josh Tallina (Operations Superintendent), James Alford (Terminal Manager)
MOP is located in Beaumont, TX, and operates as a storage terminal facility for chemical products including molten sulfur, crude oil, sulfuric acid, and asphalt. Mr. Alford explained how each product is transported in and out of the facility. Molten sulfur is shipped in by truck and rail while being shipped out by ship and barge. Crude oil is shipped in by truck and shipped out by barge. Sulfuric acid is shipped in and out by truck, rail, and barge. Asphalt is shipped in and out by truck, rail, and barge. The facility stores products in 10 tanks ranging in storage capacity from 25,000 to 85,000 barrels. The facility maintains a MARPOL COA through the U.S. Coast Guard but said it does not allow transfers of waste over its dock spaces. The company does allow thirdparty launch services to remove waste from vessels over the water. However, they are not involved in this process as it relies on the ship and the ship's agent. MOP is registered with the EPA and operates as a VSQG of hazardous waste (TXR000060909).
Upon finishing the opening conference, the inspection team observed MOP's dock space and chemical storage area. The inspection team first arrived at Dock 1 and found one half-full 55-gallon drum and one three-quarter-full 55-gallon drum at the base of the dock entrance (see Appendix 1--Photos 1 to 2). MOP representatives were unsure what was in the drums but stated they believed it was left from contractors on site. The drums were unlabeled at the time of the inspection. The inspection team requested a waste determination on the drums [AOC #1 - MOP did not make a hazardous waste determination - 40 CFR 262.11]. No other areas of concern (AOCs) were found at MOP's dock space.
The inspection team moved to the chemical storage area where MOP informed the inspection team they are storing several totes of acid waste. Upon entering the chemical storage area, the inspection team observed nine 300-gallon totes ranging in capacity from one-quarter full to completely full (see Appendix 1 - Photos 3 to 13). Four of the totes were sodium hydroxide products used in MOPs neutralization process. The other five totes were sulfuric acid and water waste generated from a valve leak and clean up activity (Appendix 1 - Photos 3 to 7). MOP representatives stated the acid waste in these drums will be neutralized using soil and hydrated lime before they are shipped off as non-hazardous waste, but the representatives stated they are waiting until they have enough acid waste to do one batch neutralization. The inspection team requested a hazardous waste determination because MOP representatives did not definitively state if they were managing the acid wastewater as hazardous waste or not (see AOC#1). On 11/21/24 following the inspection, MOP followed up with determination stating the acid waste was hazardous generated from an episodic event
Page 3 of 5
Martin Operating Partnership LP that began on 11/05/2024. The notification form is included in Appendix 4.
Inspection Date: 11/06/2024
The inspection team did not observe other AOCs at the time of the inspection. However, further EPA review may change or add to their potential AOCs. A closing conference was conducted at approximately 3:20 PM with MOP personnel. The AOCs were communicated during the closing.
On 11/21/24, Mr. Scott Ranalli (MOP Environmental personnel), sent a response letter to the inspection team addressing the AOCs observed during the inspection (see Appendix 2):
The two 55-gallon drums observed by Dock 1 were determined to be oily water drums originated from Martin Marine, whose vessel LaForce and barge Margaret Sue transported them to Martin Energy's Port Arthur Dock for used oil storage, with plans for Holcomb Company to recycle the fluids once the tank nears capacity. Non-hazardous material manifest and the Used Oil Registration information for the Port Arthur Dock are presented in Appendix 3.
The used sulfuric acid tote fluids resulted from a leaking tank valve, with the acid mixing with rainwater within the containment area. The fluids were temporarily stored in totes, then neutralized with clean soil and hydrated lime to a non-hazardous pH. The resulting solids will be solidified and disposed of at the Republic Services Golden Triangle Facility. Photos of the affixed hazardous waste labels on totes of acid waiting to be naturalized and copies of the Waste Determination Form, sulfuric acid SDS, STEERs state waste code entry, and Episodic Notification for Regulated Generators form are in Appendix 4. The Neutralized Sulfuric Acid profile, analytical, and hydrated lime SDS are provided in Appendix 5.
The MARPOL COA and vapor combustion unit approval are included in Appendix 6.
A copy of the registration information for the Acid Neutralization Waste Treatment Unit is in Appendix 7.
SECTION III - RECORDS REVIEW
No RCRA-regulated records were reviewed during this focused onsite inspection.
SECTION IV - AREAS OF CONCERN
The presentation of Area(s) of Concern does not constitute a formal compliance determination or violation. Tenant: Martin Operating Partners LP
AOC #1 - MOP did not make a hazardous waste determination.
Citation: 40 CFR 262.11
Section: 2.1
SECTION V - FOLLOW UP
Follow-Up Any facility follow-up items are as discussed in the observations in Section II. Documents or files provided by the facility were transmitted via email and included responses to AOCs or provision of documents requested.
Page 4 of 5
Martin Operating Partnership LP Communication Log
Inspection Date: 11/06/2024
During and after the inspection, additional information was emailed to EPA including:
1. 11/21/24 MOP email - Scott Ranalli sent follow up photos and documents responding to the AOCs observed during the inspection.
SECTION VI - LIST OF APPENDICES Appendix 1. Photograph Log Appendix 2. MOP 11/21/24 Response Appendix 3. Non-Hazardous Material Manifest Appendix 4. Spent Sulfuric Acid Waste Determination and Episodic Event Form Appendix 5. Neutralized Sulfuric Acid Profile Appendix 6. MARPOL COA and Vapor Combustion Unit Approval Appendix 7. Acid Neutralization Waste Treatment Unit Registration
Page 5 of 5
APPENDIX 1. PHOTOGRAPH LOG
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 1
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7665 Date of Photo: 11/06/2024 Time of Photo: 14:57 hrs. Photographer: Vince Damiano Description: View of a half-full 55-gallon drum found on the shore at Dock 1 which was storing unidentified liquid at the time of the inspection.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 2
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7666 Date of Photo: 11/06/2024 Time of Photo: 14:57 hrs. Photographer: Vince Damiano Description: View of a 3/4 full 55-gallon drum found on the shore at Dock 1 which was storing unidentified liquid at the time of the inspection.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 3
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7667 Date of Photo: 11/06/2024 Time of Photo: 15:09 hrs. Photographer: Vince Damiano Description: View of a full 300-gallon tote found in the chemical storage area that was storing diluted sulfuric acid corrosive waste.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 4
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7668 Date of Photo: 11/06/2024 Time of Photo: 15:10 hrs. Photographer: Vince Damiano Description: View of a full 300-gallon tote found in the chemical storage area that was storing diluted sulfuric acid corrosive waste.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 5
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7669 Date of Photo: 11/06/2024 Time of Photo: 15:10 hrs. Photographer: Vince Damiano Description: View of a full 300-gallon tote found in the chemical storage area that was storing diluted sulfuric acid corrosive waste.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 6
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7670 Date of Photo: 11/06/2024 Time of Photo: 15:11 hrs. Photographer: Vince Damiano Description: View of a full 300-gallon tote found in the chemical storage area that was storing diluted sulfuric acid corrosive waste.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 7
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7671 Date of Photo: 11/06/2024 Time of Photo: 15:11 hrs. Photographer: Vince Damiano Description: View of a full 300-gallon tote found in the chemical storage area that was storing diluted sulfuric acid corrosive waste.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 8
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7672 Date of Photo: 11/06/2024 Time of Photo: 15:12 hrs. Photographer: Vince Damiano Description: View of a product label on a tote of sodium hydroxide solution found in the chemical storage area. This material is a product.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 9
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7673 Date of Photo: 11/06/2024 Time of Photo: 15:12 hrs. Photographer: Vince Damiano Description: View of a product tote of sodium hydroxide solution found in the chemical storage area.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 10
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7674 Date of Photo: 11/06/2024 Time of Photo: 15:12 hrs. Photographer: Vince Damiano Description: View of a product label on a tote of sodium hydroxide solution found in the chemical storage area. This material is a product.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 11
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7675 Date of Photo: 11/06/2024 Time of Photo: 15:12 hrs. Photographer: Vince Damiano Description: View of a product tote of sodium hydroxide solution found in the chemical storage area.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 12
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7676 Date of Photo: 11/06/2024 Time of Photo: 15:14 hrs. Photographer: Vince Damiano Description: Overview of the nine 300-gallon totes found inside the chemical storage area.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Photograph Log
Photo No. 13
Location: Martin Operating Partnership LP
City: Beaumont
County/Parish: Jefferson
State: Texas
Photo File Name: DSCN7677 Date of Photo: 11/06/2024 Time of Photo: 15:14 hrs. Photographer: Vince Damiano Description: Overview of the nine 300-gallon totes found inside the chemical storage area.
APPENDIX 2. MOP 11/21/24 RESPONSE
Environmental Department Three Riverway, Suite 400
Houston, Texas 77056
November 21, 2024
Mr. Vince Damiano ERG - Chantilly Office 703-835-6281
RE: Stanolind Cut Terminal Email: `Follow-Up from EPA Visit on 11/6' SWR: 87582
Dear Mr. Damiano:
This letter serves as a response to questions raised by EPA proxy representatives on Tuesday 11/05/2024, at the Martin Operating - Stanolind Cut Terminal. The indicated representatives (from the ERG company), arrived on a "spot visit" and raised questions regarding waste storage, and related items, at the Martin facility. A follow-up e-mail on 11/07/2024, from ERG's Vince Damiano to Martin's James Alford listed the questionable items. A copy of the e-mail is provided as Attachment A.
These items are summarized and addressed below:
Stanolind Cut - Items of Concern
Waste determinations on two 55-gallon drums found by Dock 1. The oily water drums were determined to originate from Martin Marine, another subsidiary of the Martin Companies. Martin Marine vessel `LaForce' (and its accompanying barge, `Margaret Sue') picked-up the drums and transported them to the Martin Energy - Port Arthur Dock for storage in their used oil tank. When the tank approaches capacity, the Holcomb company shall transport the fluids to their facility for recycling to one of their customers.
Copies of the non-hazardous material manifest and the Used Oil Registration information for the Port Arthur Dock are presented as Attachment B. Labeling issues on seven totes of acid or base found in drum storage area. Please provide a waste determination on these drums and a written statement on how this waste is generated, rate of generation, any SDS sheets or analytical data you have for these totes, how they are currently being managed, how they are disposed of, and/or other information you deem necessary.
The Used Sulfuric Acid tote fluids were the result of a leaking tank valve. When operators went to repair or replace the valve seal, it was noted that the acid had leaked into standing rainwater within the containment. The spent acid fluids were pumped into the totes for temporary storage. The fluids shall be mixed with clean soil and hydrated lime to neutralize the material to non-hazardous pH. The resulting solids and sludge shall be transported for solidification and landfill disposal at the Republic Services Golden Triangle Facility.
Photos of the affixed hazardous waste labels and copies of the Waste Determination Form, sulfuric acid SDS, STEERs state waste code entry, and Episodic Notification for Regulated Generators form are presented in Attachment C. Copies of the Neutralized Sulfuric Acid profile, analytical, and hydrated lime SDS are provided in Attachment D. The base materials noted at the Facility are in active use and not a waste material. And they are properly labeled, as provided by the manufacturer.
EPA ID TXR000060909
MARPOL COA A copy of the professional engineer approval letter for operation of the VCU unit is presented as Attachment E.
Any permits you may have related to neutralization of your acid waste A copy of the registration information for the Acid Neutralization Waste Treatment Unit, is presented as Attachment F.
Please review the attached paperwork and contact me at (713) 350-6827, if you have any questions or comments.
Sincerely,
Scott Ranalli
Scott Ranalli Sr. Environmental Specialist, Corporate EH&S
cc: Mr. James Alford - Beaumont Terminals Manager Martin Files
Enclosure
APPENDIX 3. NON-HAZARDOUS MATERIAL MANIFEST
From: To: Cc: Subject: Date: Attachments:
Carl DiMario Scott Ranalli Robert Cast; Greg Peabody; MESPortArthur Re: La Force Paperwork.pdf Friday, November 8, 2024 12:42:51 PM image001.png
See below.
Facility Name
Facility Address
EPA I.D. Number
Used Oil
Martin Resource Management Corporation Waste Program Manager Senior Environmental Specialist.
Port Arthur Dock 2400 S. Gulf Way, Port Arthur, TX 77640
TXD067940957
TXD067940957, A85980
Carl DiMario
On Nov 8, 2024, at 11:44, Scott Ranalli <Scott.Ranalli@martinmlp.com> wrote:
Guys
Please send me any Registration/Licensing paperwork for MES Port Arthur.
Thanks,
Scott Ranalli
Sr. Environmental Specialist Corporate Environmental, Health & Safety <image001.png> Martin Resource Management Corporation
Three Riverway, Suite 400 Houston, Texas 77056 (713) 350-6827 (Ofc) (409) 504-1489 (Cell) Mail to: Scott.Ranalli@martinmlp.com
-----Original Message----From: Robert Cast <Robert.Cast@martinmlp.com> Sent: Friday, November 8, 2024 10:05 AM To: Carl DiMario <Carl.DiMario@martinmlp.com>; Scott Ranalli <Scott.Ranalli@martinmlp.com> Cc: Greg Peabody <Greg.Peabody@martinmlp.com>; MESPortArthur <MESPortArthur@martinmlp.com>
APPENDIX 4. SPENT SULFURIC ACID WASTE DETERMINATION AND EPISODIC EVENT FORM
ATTACHMENT C1 PHOTOS: LABELED HAZARDOUS WASTE TOTES
Martin Operating Stanolind Terminal
Hazardous Waste Sticker Affixed to Tote
Re-Labeled Totes
GENERATOR WASTE PROFILE SHEET
Is this a renewal? Is this a one-time waste stream?
YES or NO YES or NO
Waste Profile #
I. Generator Information
Date Submitted: 11/20/2024
Generator Name:
MARTIN OPERATING PARTNERSHIP LP - BEAUMONT STANOLIND TERMINAL
Generator Site Address: #10 SULFUR PLANT RD
City: BEAUMONT
County: JEFFERSON
State: TX
Zip: 77701
State ID/Reg No:
SWR 87582
State Approval/Waste Code: 0030-102-H
SIC Code: 5169
Generator Mailing Address (if different):
City:
County:
State:
Generator Contact Name: SCOTT RANALLI, MARTIN RESOURCE MGMT
Phone Number:
713-350-6827
Fax Number:
Zip: 713-350-2827
II. Waste Stream Information Name of Waste: USED SULFURIC ACID AND WATER
Process Generating Waste:
MAINTENANCE ACTIVITIES
When operators went to perform maintenance and repairs on a valve seal on the Sulfuric Acid Storage Tanks, it was determined
that leaking acid and already merged with standing rainwater in that containment. The mixture was pumped into totes for temp-
prary storage, pending neutralization treatment and disposal.
Type of Waste Physical State:
INDUSTRIAL PROCESS WASTE or
SOLID
SEMI-SOLID
POWDER
POLLUTION CONTROL WASTE
LIQUID
OTHER:
:
III. Representative Sample Certification
NO SAMPLE TAKEN
Is the representative sample collected to prepare this profile and laboratory analysis, collected in accordance with U.S. EPA 40 CFR 261.20(c) guidelines or equivalent rules?
YES or NO
Sample Date:
Type of Sample: COMPOSITE
GRAB
Laboratory:
Sample ID Numbers:
Samplers Employer:
Samplers Name (printed):
Signature:
Supporting documentation attached: SDS
YES or NO (for process knowledge please provide data)
IV. DOT Shipment Information
DOT Shipping Name:
Not Applicable
Method of Shipment:
Bulk
Tanker
Other (Specify):
Frequency of Shipment:
Daily Monthly Other (Specify):
Estimated Annual Volume:
CUBIC YARDS:
Special Handling Instructions:
ERG Guide#:
RQ: NA
LDR Required with Shipment:
YES or NO
Drum Weekly TONS:
One-Time GALLONS
OTHER:
Martin Resource Management Corporation REV 4
July 2014
GENERATOR WASTE PROFILE SHEET (continued)
Waste Profile #
V. Physical Characteristics of Waste
Characteristic Components
% by Weight (range)
1. WATER
40-70%
2. SULFURIC ACID
30-60%
3. SEDIMENT
0-2%
4.
5.
Color
Odor (describe)
Free Liquids
Orange
Mild Sulfur
YES or NO
Content 100 %
% Solids
pH:
Flash Point
0 0-2 <2.0 >200 F
% Halogens
NA
Attach Laboratory Analytical Report (and/or Material Safety Data Sheet) Including Required Parameters Provided for this Profile
Does this waste or generating process contain regulated concentrations of the following Pesticides and/or Herbicides: Chlordane, Endrin, Heptachlor (and its epoxides), Lindane, Methoxychlor, Toxaphene, 2,4-D, or 2,4,5-TP Silvex as defined in 40 CFR 261.33?
Yes or No
Does this waste or generating process cause it to exceed OSHA exposure limits from high levels of Hydrogen Sulfide or Hydrogen Cyanide as defined in 40 CFR 261.23?
Yes or No
Does this waste contain regulated concentrations of Polychlorinated Biphenyls (PCBs) as defined in 40 CFR Part 761?
Yes or No
Does this waste contain regulated concentrations of listed hazardous wastes defined in 40 CFR 261.31, 261.32, 261.33, including RCRA F-Listed Solvents?
Yes or No
Does this waste contain regulated concentrations of 2,3,7,8-Tetrachlorodibenzodioxin (2,3,7,8-TCCD), or any other dioxin as defined in 40 CFR 261.31?
Yes or No
Is this a regulated Toxic Material as defined by Federal and/or State regulations?
Yes or No
Is this a regulated Radioactive Waste as defined by Federal and/or State regulations?
Yes or No
Is this a regulated Medical or Infectious Waste as defined by Federal and/or State regulations?
Yes or No
Is this waste generated at a Federal Superfund Clean Up Site?
Yes or No
VI. Waste Codes
Hazardous Waste TSCA Waste
YES or NO Non Hazardous Waste YES or NO
YES or NO Municipal Waste YES or NO
LIST WASTE CODES BELOW
0030-102-H
Martin Resource Management Corporation REV 4
July 2014
GENERATOR WASTE PROFILE SHEET (continued)
VII. Transporter & TSDF Information Transporter Name: NA Address: City: EPA ID#:
County:
State:
Zip:
Transporter Name: Address: City: EPA ID#:
County:
State:
Zip:
Transporter Name: Address: City: EPA ID#:
County:
State:
Zip:
TSDF or Disposal Facility Name #1: Address: City: EPA ID#:
TSDF or Disposal Facility Name #2: Address: City: EPA ID#:
County: 39098
County:
State:
Zip:
State:
Zip:
TSDF or Disposal Facility Name #3: Address: City: EPA ID#:
County:
State:
Zip:
Form R Information:
8.1c: 0 % 8.1d: 0 %
8.7 100 %
Martin Resource Management Corporation REV 4
July 2014
GENERATOR WASTE PROFILE SHEET (continued)
VIII. EPA Reporting Codes / Waste Reduction & Effort Codes
EPA Reporting Codes:
Management Method Code:
H121
Source Code:
G32
Form Code:
W103
Waste Minimization Code:
A
This Year Ratio
HW Reduction
Goal Year Ratio
Goal Year
Change in Toxicity
Reformulation/redesign of product
Waste Toxicity Reduction Effort Codes Training of Technical Assistance
In process recycling/process Modification
Technical Feasibility
Equipment/Technology Modification
Economic Practicality
Substituting Raw Materials
Measurement/Accounting
Improved Operations
State Hazardous Waste Regulations
Reduction/Research Planning
Implementation Previous Efforts
No Effort
Other Reduce Toxicity of Waste
Explain reported data (If applicable)
High Cost of HW Management
X
Accidental Generation
Other
If No numeric goal, explain why: CONTINUED INITIATIVES TO RECYCLE OFF-SITE
Martin Resource Management Corporation REV 4
July 2014
GENERATOR WASTE PROFILE SHEET (continued)
IX. Generator Certification
I hereby certify that to the best of my knowledge and belief, the information contained herein is a true, complete, and accurate description of the waste material being offered for disposal and all known or suspected hazards have been disclosed. All Analytical Results/Material Safety Data Sheets submitted are truthful and complete and are representative of the waste. I further certify that by utilizing this profile, neither I nor any other employee of the company will deliver for disposal or attempt to deliver for disposal any waste which is classified as toxic waste, hazardous waste or infectious waste, or any other waste material this facility is prohibited from accepting by law. I shall immediately give written notice of any change or condition pertaining to the waste not provided herein. I agree that if there is a discrepancy between the waste received and any information supplied on this form, that either Martin Operating Partnership or the generator may initiate further testing and evaluation in accordance with the terms and conditions of the contract between Martin Operating Partnership and the generator; that this profile certification may be amended accordingly; and that additional expenses incurred by Martin Operating Partnership in order to manage the waste in accordance with Federal, State, and Local regulatory requirements will be the sole responsibility of the generator, including return of the material to the generator at generators expense.
SCOTT RANALLI, SR. ENVIRONMENTAL SPECIALIST
Scott
Authorized Representative Name And Title (Printed)
Ranalli
Digitally signed by Scott Ranalli DN: cn=Scott Ranalli, o, ou=Martin Corporate EH&S, email=scott.ranalli@martinmlp.com, c=US Date: 2014.07.25 15:24:20 -05'00'
Authorized Representative Signature
MARTIN RESOURCE MANAGEMENT
Company Name
11/20/2024
Date
X. Martin Waste Decision
Approved
Rejected
Expiration: _________________
Conditions:
Name, Title
Signature
Date
Martin Resource Management Corporation REV 4
July 2014
Sulfuric acid
Chemical Name SULFURIC ACID
OSHA TWA (ppm)
OSHA TWA (mg/m3)
1
OSHA STEL (ppm)
OSHA STEL (mg/m3)
OSHA Tables (Z1,
Z2, Z3)
1
OSHA Carcinogen
OSHA Skin designation
NIOSH TWA (ppm)
NIOSH TWA (mg/m3)
1
NIOSH STEL (ppm)
NIOSH STEL (mg/m3)
NIOSH Carcinogen
Chemical Name SULFURIC ACID
ACGIH TWA (ppm)
ACGIH TWA (mg/m3)
0.2 (T)
ACGIH STEL (ppm)
ACGIH STEL (mg/m3)
ACGIH Carcinogen
A2
ACGIH Notations
A2 (M)
ACGIH TLV Basis
Pulm func
CAS 0007664-93-9 0007732-18-5
Chemical Name SULFURIC ACID WATER
% By Weight
Regulation List
72% - 98% DSL,CERCLA,SARA312,SARA313,IARCCarcinogen,TSCA,TX_ESL,CA_Prop65 - California Proposition 65,CA_Prop65_Type_Toxicity_Cancer - CA_Proposition65_Type_Toxicity_Cancer,OSHA
8% - 18% DSL,TSCA
SCOTT RANALLI SR. ENVIRONMENTAL SPECIALIST
MARTIN RESOURCE MGMT (on behalf of Martin Operating Ptnrshp) 409-504-1489 scott.ranalli@MartinMLP.com
From: To: Subject: Date: Attachments:
Microsoft Outlook Wasteval@tceq.texas.gov Relayed: MARTIN OPERATING - STANOLIND: Unplanned Haz Waste Thursday, November 21, 2024 8:55:30 AM MARTIN OPERATING - STANOLIND Unplanned Haz Waste.msg
Delivery to these recipients or groups is complete, but no delivery notification was sent by the destination server: Wasteval@tceq.texas.gov (Wasteval@tceq.texas.gov) <mailto:Wasteval@tceq.texas.gov> Subject: MARTIN OPERATING - STANOLIND: Unplanned Haz Waste
APPENDIX 5.NEUTRALIZED SULFURIC ACID PROFILE
51202319306
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Page 7 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
December 21, 2023
Scott Boudreaux Earth Analytical Sciences, Inc. 4825 Ward Dr Beaumont, TX 77705 TEL: (409) 842-0658 FAX: (409) 842-9793
RE: 3L15038 Dear Scott Boudreaux:
Order No.: 23121399
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/19/2023 for the analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Holly Florea
Project Manager
3310 Win St. Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 11
Page 8 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
CLIENT: Earth Analytical Sciences, Inc. Project: 3L15038
Case Narrative
WO#:
23121399
Date:
12/21/2023
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below.
Page 2 of 11
Original Page 9 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
Workorder Sample Summary
WO#: 23121399 21-Dec-23
CLIENT: Project:
Earth Analytical Sciences, Inc. 3L15038
Lab SampleID Client Sample ID
23121399-001 3L15038-01
Tag No
Date Collected
12/15/2023 11:30:00 AM
Date Received
12/19/2023 10:30:00 AM
Matrix
Solid
Page 3 of 11
Page 10 of 18
Lab ID: 23121399-001 Client Sample ID 3L15038-01
Analysis
Result
METALS ANALYSIS (6010D)
Sulfur(S)
868
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
Analytical Report
(consolidated)
WO#:
23121399
Date Reported: 12/21/2023
MDL
4.81
Collection Date: 12/15/2023 11:30:00 AM Matrix: SOLID
PQL Qual Units Dilution Batch
Date Analyzed
EPA 6010 D
EPA 3050 Analyst: RJE
48.1
mg/Kg
1 71465 12/21/2023 8:38:00 AM
Qualifiers:
B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected RL Reporting Detection Limit
Page 4 of 11
E Value above quantitation range M Manual Integration used to determine area response PL Permit Limit W Sample container temperature is out of limit as specified at testcode
Page 11 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
QC SUMMARY REPORT
WO#:
23121399 21-Dec-23
Client: Project:
Earth Analytical Sciences, Inc. 3L15038
Sample ID: MB-71465 Client ID: PBS
Analyte Sulfur(S)
SampType: MBLK Batch ID: 71465
Result ND
BatchID: 71465
TestCode: Mtl-ICP_S(60 Units: mg/Kg
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL 48.5
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
RunNo: 176723 SeqNo: 4786694
%RPD RPDLimit Qual
Sample ID: LCS-71465 Client ID: LCSS
Analyte Sulfur(S)
SampType: LCS Batch ID: 71465
Result 88.2
TestCode: Mtl-ICP_S(60 Units: mg/Kg
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL 467
SPK value SPK Ref Val
93.46
0
%REC 94.4
LowLimit HighLimit RPD Ref Val
80
120
RunNo: 176723 SeqNo: 4786696
%RPD RPDLimit
Qual J
Sample ID: LCS-71465 Client ID: LCSS
Analyte Sulfur(S)
SampType: LCS Batch ID: 71465
Result 393
TestCode: Mtl-ICP_S(60 Units: mg/Kg
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL 46.7
SPK value SPK Ref Val
467.3
0
%REC 84.2
LowLimit HighLimit RPD Ref Val
80
120
RunNo: 176723 SeqNo: 4786697
%RPD RPDLimit Qual
Sample ID: 23121275-001AMS Client ID: BatchQC
Analyte Sulfur(S)
SampType: MS Batch ID: 71465
Result 1310
TestCode: Mtl-ICP_S(60 Units: mg/Kg-dry
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL 45.2
SPK value SPK Ref Val
90.44
1313
%REC -4.85
LowLimit HighLimit RPD Ref Val
75
125
RunNo: 176723 SeqNo: 4786699
%RPD RPDLimit
Qual S
Qualifiers:
B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits PL Permit Limit W Sample container temperature is out of limit as specified at testcode
E Value above quantitation range M Manual Integration used to determine area response RL Reporting Detection Limit
Page 5 of 11
H Holding times for preparation or analysis exceeded ND Not Detected S Spike Recovery outside accepted recovery limits
Original
Page 12 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
QC SUMMARY REPORT
WO#:
23121399 21-Dec-23
Client: Project:
Earth Analytical Sciences, Inc. 3L15038
Sample ID: 23121275-001AMS Client ID: BatchQC
Analyte
SampType: MS Batch ID: 71465
Result
BatchID: 71465
TestCode: Mtl-ICP_S(60 Units: mg/Kg-dry
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
RunNo: 176723 SeqNo: 4786699
%RPD RPDLimit Qual
Sample ID: 23121275-001AMSD SampType: MSD
Client ID: BatchQC
Batch ID: 71465
Analyte Sulfur(S)
Result 1340
TestCode: Mtl-ICP_S(60 Units: mg/Kg-dry
TestNo: SW6010
SW3050B
Prep Date: 12/19/2023 Analysis Date: 12/20/2023
PQL 44.0
SPK value SPK Ref Val
88.08
1313
%REC 25.7
LowLimit HighLimit RPD Ref Val
75
125
1308
RunNo: 176723 SeqNo: 4786700
%RPD 2.04
RPDLimit 20
Qual S
Qualifiers:
B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits PL Permit Limit W Sample container temperature is out of limit as specified at testcode
E Value above quantitation range M Manual Integration used to determine area response RL Reporting Detection Limit
Page 6 of 11
H Holding times for preparation or analysis exceeded ND Not Detected S Spike Recovery outside accepted recovery limits
Original Page 13 of 18
Summit Environmental Technologies, In 3310 Win S
Cuyahoga Falls, Ohio 4422 TEL: (330) 253-8211 FAX: (330) 253-448
Website: http://www.settek.co
Qualifiers and Acronyms
WO#: Date:
23121399 12/21/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U J H D E MC * m d N P C X B MB+ G QC-/+ R/QDR QL-/+ QLR QM-/+ QMR QV-/+ S W Z
The compound was analyzed for but was not detected above the MDL. The reported value is greater than the Method Detection Limit but less than the Reporting Limit. The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant. The result is reported from a dilution. The result exceeded the linear range of the calibration or is estimated due to interference. The result is below the Minimum Compound Limit. The result exceeds the Regulatory Limit or Maximum Contamination Limit. Manual integration was used to determine the area response. Manual integration in which peak was deleted The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. The second column confirmation exceeded 25% difference. The result has been confirmed by GC/MS. The result was not confirmed when GC/MS Analysis was performed. The analyte was detected in the Method Blank at a concentration greater than the RL. The analyte was detected in the Method Blank at a concentration greater than the MDL. The ICB or CCB contained reportable amounts of analyte. The CCV recovery failed low (-) or high (+). The RPD was outside of accepted recovery limits. The LCS or LCSD recovery failed low (-) or high (+). The LCS/LCSD RPD was outside of accepted recovery limits. The MS or MSD recovery failed low (-) or high (+). The MS/MSD RPD was outside of accepted recovery limits. The ICV recovery failed low (-) or high (+). The spike result was outside of accepted recovery limits. Samples were received outside temperature limits (0 6 C). Not Clean Water Act compliant. Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl Regulatory Limit
MSD Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB Continuing Calibration Blank
RT
Retention Time
RLC Reporting Limit Check
CF
Calibration Factor
il i
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Page 7 of 11
Original Page 14 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
Client: Project:
Sample ID 23121399-001A
Earth Analytical Sciences, Inc. 3L15038
Client Sample ID
Collection Date
3L15038-01
12/15/2023 11:30:00 AM
Matrix Solid
Test Name Metals Analysis (6010D)
DATES REPORT
WO#:
23121399 21-Dec-23
Leachate Date
Prep Date
Analysis Date
12/20/2023 8:10:00 AM 12/21/2023 8:38:00 AM
Page 8 of 11
Original Page 15 of 18
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
Accreditation Program Analytes Report
WO#:
23121399 21-Dec-23
Client: Earth Analytical Sciences, Inc. Project: 3L15038
Test Name Metals Analysis (6010D)
Matrix Solid
State: TX Program Name: TX_DW_NPW_S
Analyte
Status
Sulfur
N
AL N CA-NELAP N
CT N HI-DW N IL-NELAP N
Not Accredited Not Accredited Not Accredited Not Accredited Not Accredited
AR A Accredited
CO U Unavailable
FL-NELAP A Accredited
ID IN_DW
U PUagnaeva9iloabfle11
U Unavailable
AR N CT A FL-NELAP N IL-NELAP A KS - NELA A
Not Accredited Accredited Not Accredited
Original #1
Accredited Accredited
Page 16 of 18
Page 10 of 11
Page 17 of 18
Client Name: EAR-TX-77705
Summit Environmental Technologies, Inc. 3310 Win St.
Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://www.settek.com
Sample Log-In Check List
Work Order Number: 23121399
RcptNo: 1
Logged by:
Christina N. Gemma
Completed By: Christina N. Gemma
Reviewed By: Salwa A. Najjar
Chain of Custody 1. Is Chain of Custody complete? 2. How was the sample delivered?
Log In 3. Coolers are present?
12/19/2023 10:30:00 AM 12/19/2023 11:53:04 AM 12/19/2023 4:48:32 PM
Yes FedEx
Yes
No
Not Present
No
NA
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No.
Seal Date:
5. Was an attempt made to cool the samples?
Yes
No
Yes
No
Signed By:
Yes
No
Not Present NA
6. Were all samples received at a temperature of >0 C to 6.0C
Yes
No
NA
7. Sample(s) in proper container(s)?
Yes
No
8. Sufficient sample volume for indicated test(s)?
Yes
No
9. Are samples (except VOA and ONG) properly preserved?
Yes
No
10. Was preservative added to bottles?
Yes
No
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
12. Were any sample containers received broken?
Yes
13. Does paperwork match bottle labels?
Yes
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
15. Is it clear what analyses were requested?
Yes
16. Were all holding times able to be met?
Yes
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
No
No VOA Vials
No
No
No No No
No
NA
Person Notified: By Whom: Regarding: Client Instructions:
Date: Via:
eMail
Phone Fax
In Person
18. Additional remarks:
Cooler Information
Cooler No Temp C
Condition Seal Intact *RRG 1RW3UHVHQW
Seal No
Seal Date Signed By
Page 11 of 11
Page 18 of 18
Hydrated Lime - January 27, 2020 SAFETY DATA SHEET
SECTION 1 Product
IDENTIFICATION
Name: Hydrated Lime
Other Names: Hydrate; High-Calcium Hydrated Lime
Recommended Uses: Water Treatment; pH adjustment; FGT; Construction
Company Identification:
US Operations:
Canadian Operations:
Lhoist North America, Inc. 5600 Clearfork Main St, Ste. 300 Fort Worth, TX 76109 817-732-8164
Lhoist North America of Canada, Inc. 20303-102B Ave. Langley, BC V1M 3H1 604-888-4333
Emergency Phone Number: Chemtrec 1-800-424-9300
SECTION 2 Classification
HAZARDS(S) IDENTIFICATION Eye Damage - Category 1
Carcinogen - Category 1
Skin Irritation - Category 2
Specific Target Organ Toxicity Single Exposure - Category 3 (Respiratory System)
Specific Target Organ Toxicity Repeat Exposure - Category 1 (Respiratory System)
Labeling:
Pictograms:
Signal Word(s): Danger
Hydrated Lime - January 27, 2020
Hazard Statements: Causes serious eye damage.
Causes skin irritation.
May cause respiratory irritation.
Causes damage to lungs through prolonged or repeated exposure when inhaled.
May cause cancer through inhalation.
Precautionary Statements:
Wear protective gloves and eye protection. Wash exposed skin thoroughly after handling. Do not breathe dust. Use only outdoors or in a well-ventilated area. Obtain special instructions before use. Do not handle until all safety precautions have been read and understood. Do not eat, drink or smoke when using this product.
If on skin: wash exposed skin with plenty of water. If skin irritation occurs: Get medical attention. Take off contaminated clothing and wash it before reuse.
If in eyes: Rinse cautiously with water for several minutes. Remove contact lenses if present and easy to do. Continue rinsing. Seek medical attention immediately. If inhaled: Remove person to fresh air and keep comfortable for breathing. Seek medical attention if you feel unwell.
If exposed or concerned: Get medical advice
Dispose of contents or containers in accordance with applicable regulations.
Other Hazards:
None.
SECTION 3 Chemical Name: Calcium hydroxide
COMPOSITION/ INFORMATION ON INGREDIENTS
Common names and synonyms: Hydrate; High-Calcium Hydrated Lime
Chemical Identity Calcium Hydroxide Magnesium Oxide Crystalline Silica
CAS # 1305-62-0 1309-48-4 14808-60-7
Concentration, % Wt. > 90% < 3% < 2%
Hydrated Lime - January 27, 2020
SECTION 4 Eye Contact:
FIRST AID MEASURES Contact can cause severe irritation or burning of eyes, including permanent damage. Immediately flush eyes with generous amounts of water for as long as needed. This may take several minutes. Pull back the eyelid to ensure that all lime dust has been washed out. Seek medical attention immediately. Do not rub eyes.
Inhalation:
This product can cause severe irritation of the respiratory system. Move victim to fresh air. Seek medical attention if necessary. If breathing has stopped, give artificial respiration.
Skin Contact: Contact can cause severe irritation or burning of skin, especially in the presence of moisture. Wash exposed area with large amounts of water. Seek medical attention immediately.
Ingestion:
This product can cause severe irritation or burning of gastrointestinal tract if swallowed. Do not induce vomiting. Seek medical attention immediately. Never give anything by mouth unless instructed to do so by medical personnel.
Most important symptoms and effects, both acute and delayed: Irritation of skin, eyes, gastrointestinal tract or respiratory tract. Long-term exposure by inhalation may cause permanent damage. This product contains crystalline silica, which has been classified by IARC as (Group I) carcinogenic to humans when inhaled. Inhalation of silica can also cause a chronic lung disorder, silicosis.
Note to Physician: Provide general supportive measures and treat symptomatically.
SECTION 5 Extinguishing Media
FIREFIGHTING MEASURES
Appropriate Extinguishing Media: Use dry chemical fire extinguisher
Inappropriate Extinguishing Media: Do not use halogenated compounds.
Firefighting
Fire Hazards: Hydrated Lime is not combustible or flammable. Hydrated Lime is not considered to be an explosive hazard, although reaction with incompatible materials may rupture containers.
Hazardous Combustion Products: None
Hydrated Lime - January 27, 2020
Special Protective Equipment and Fire Fighting Instructions: Keep personnel away from and upwind of fire. Wear full fire-fighting turn-out gear (full Bunker gear), and respiratory protection (SCBA).
SECTION 6
ACCIDENTAL RELEASE MEASURES
Personal Precautions: Use proper protective equipment.
Environmental Precautions: For large spills, as much as possible, avoid the generation of dusts. Prevent release to sewers or waterways.
Methods and Materials for Containment and Cleaning Up:
Small Spills: Use dry methods to collect spilled materials. Avoid generating dust. Do not clean up with compressed air. Store collected materials in dry, sealed plastic or metal containers. Residue on surfaces may be washed with water or dilute vinegar.
Large Spills: Use dry methods to collect spilled materials. Evacuate area downwind of clean-up operations to minimize dust exposure. Store spilled materials in dry, sealed plastic or metal containers.
SECTION 7
HANDLING AND STORAGE
Precautions for Safe Handling: Keep in tightly closed containers. Protect containers
from physical damage. Avoid direct skin contact with the material.
Conditions for Safe Storage, Including any Incompatibilities: Store in a cool, dry, and well-ventilated location. Do not store near incompatible materials (see Section 10 below). Keep away from moisture. Do not store or ship in aluminum containers.
SECTION 8 Control Parameters:
EXPOSURE CONTROLS/ PERSONAL PROTECTION
Component Calcium Hydroxide Magnesium Oxide Crystalline Silica
CAS # 1305-62-0
1309-48-4
14808-60-7
Exposure Limits OSHA PEL: 15 mg/m3 (total) 5 mg/m3 (respirable) ACGIH TLV: 5 mg/m3 OSHA PEL: 15 mg/m3 ACGIH TLV: 10 mg/m3 OSHA PEL: 0.050 mg/m3 as an 8 hr. TWA (respirable) ACGIH TLV: 0.025 mg/m3 (respirable)
Hydrated Lime - January 27, 2020 Appropriate Engineering Controls: Provide ventilation adequate to maintain PELs.
Personal Protection
Respiratory Protection: Use NIOSH approved respirators if airborne concentration exceeds PEL.
Eye Protection: Use safety glasses with side shields or safety goggles. Contact lenses should not be worn when working with lime products.
Skin Protection: If there is a risk of skin contact, wear appropriate clothing and gloves to prevent contact.
Other: Eye wash fountain and emergency showers are recommended.
SECTION 9 Appearance
PHYSICAL AND CHEMICAL PROPERTIES
Physical State:
Solid
Color:
White
Odor:
Odorless
Odor Threshold: N/ A
pH:
12.44 @ 25o C when made into a saturated solution
Melting Point:
N/ AF
Initial Boiling Point: N/ A
Freezing Point:
N/ A
Flash Point:
N/ A
Evaporation Rate: N/ A
Flammability (solid, gas): Non-flammable
Explosion Limits: N/ A
Vapor Pressure:
N/ A
Vapor Density: Relative Density:
N/ A 0.4 - 0.7 g/ cm3 (apparent)
Solubility(ies):
Solubility is 1.6 g/L at 25o C
Partition coefficient: Relatively insoluble
Hydrated Lime - January 27, 2020
Auto-ignition Temperature: N/ A Decomposition Temperature: 580o C / 1076o F
Viscosity: N/A
SECTION 10 Reactivity:
STABILITY AND REACTIVITY
Chemical Stability: Hydrated Lime is chemically stable.
Possibility of Hazardous Reactions: See reactivity above
Conditions to Avoid: Do not allow Hydrated Lime to come into contact with incompatible materials.
Incompatible Materials: Hydrated Lime should not be mixed or stored with the following materials, due to the potential for violent reaction and release of heat:
Acids (unless in a controlled process) Reactive Fluoridated Compounds Reactive Brominated Compounds Reactive Powdered Metals Organic Acid Anhydrides Nitro-Organic Compounds Reactive Phosphorous Compounds Interhalogenated Compounds
Hazardous Decomposition Products: None
SECTION 11
TOXICOLOGICAL INFORMATION
Health Effects: see First Aid discussion in Section 4
Routes of Exposure: see First Aid discussion in Section 4
Symptoms Related to Exposure: see First Aid discussion in Section 4
Carcinogen Listing: Hydrated Lime is not listed by MSHA, OSHA, or IARC as a carcinogen, but this product contains crystalline silica, which has been classified by IARC as (Group I) carcinogenic to humans when inhaled.
SECTION 12
ECOLOGICAL INFORMATION
Ecotoxicity: Because of the high pH of this product, it would be expected to produce
significant ecotoxicity upon exposure to aquatic organisms and aquatic systems in
high concentrations.
Hydrated Lime - January 27, 2020 Persistence and Degradability: Reacts with atmospheric CO2 over time to form calcium
carbonate
Bioaccumulation Potential: This material shows no bioaccumulation effect or food chain concentration toxicity.
Mobility in Soil: Minimal mobility in soil. Reacts with clay portion of soil to form calcium silicates and calcium aluminates
Other Adverse Effects: This material is alkaline and if released into water or moist soil will cause an increase in pH
SECTION 13
DISPOSAL CONSIDERATIONS
Disposal Recommendations: Dispose of in accordance with all applicable federal, state, and
local environmental regulations.
Regulatory Disposal Information: If this product as supplied, and unmixed, becomes a waste, it will not meet the criteria of a hazardous waste as defined under the Resource Conservation and Recovery Act.
SECTION 14 UN Number: Not Regulated
TRANSPORT INFORMATION
UN Proper Shipping Name: Not Regulated
Transport Hazard Class(es): Not Regulated
Packing Group: Not Regulated
Marine Pollutant (y/n): This material is alkaline and if released into water or moist soil will cause an increase in pH.
Special Precautions: None SECTION 15 National Chemical Inventory Listings:
REGULATORY INFORMATION
All chemical ingredients are listed on the USEPA TSCA Inventory List.
US Regulations: RCRA Hazardous Waste Number: not listed (40 CFR 261.33) RCRA Hazardous Waste Classification (40 CFR 261): not classified CERCLA Hazardous Substance (40 CFR 302.4) unlisted specific per RCRA, Sec. 3001; CWA, Sec. 311 (b) (4); CWA, Sec. 307(a), CAA, Sec. 112 CERCLA Reportable Quantity (RQ) not listed. SARA 311/312 Codes: not listed. SARA Toxic Chemical (40 CFR 372.65): not listed. SARA EHS (Extremely Hazardous Substance) (40 CFR 355): Not listed, Threshold Planning Quantity (TPQ): not listed
Hydrated Lime - January 27, 2020 Specific State Regulations: WARNING: This product can expose you to chemicals, including crystalline silica, which is known to the State of California to cause cancer. For more information, go to www.P65Warnings.ca.gov These naturally occurring impurities may also be regulated by other States.
Canadian DSL: Listed
Canadian NPRI: None of the components are listed
CEPA Toxic Substances: None of the components are listed
SECTION 16
OTHER INFORMATION
Prepared By: Lhoist North America Technical Services
Date Prepared: January 27, 2020
Revision: 2020-1
Abbreviations:
N/A
Not Available or Not Applicable
IARC
International Agency for Research on Cancer
IATA
International Air Transport Association
ACGIH American Conference of Governmental
ACGIH Industrial Hygienists
TWA
Time Weighted Average
PEL
Permissible Exposure Limit
TLV
Threshold Limit Value
REL
Recommended Exposure Limit
Lhoist North America provides the information contained herein in good faith but makes no
representation as to its comprehensiveness or accuracy. This document is intended only as a
guide to the appropriate precautionary handling of the material by a properly trained person.
Individuals receiving this information must consult their own technical and legal advisors and/
or exercise their own judgment in determining its appropriateness for a particular purpose.
Lhoist North America makes no representations or warranties, either express or implied,
including without limitation and warranties of merchantability or fitness for a particular
purpose with respect to the Information set forth herein or the product(s) to which the
information refers. Accordingly, Lhoist North America will not be responsible or liable for any
claims, losses or damages resulting from the use of or reliance upon or failure to use this
information.
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PROPRIETARY INFORMATION
THIS DRAWING INCLUDES VALUABLE PRODUCT INFORMATION, A SUBSTANTIAL PORTION OF WHICH IS PROPRIETARY TO JORDAN TECHNOLOGIES, AS SUCH, THIS DRAWING IS SUBMITTED IN CONFIDENCE TO THE PARTY TO WHICH IT IS ADDRESSED. ANY EFFORT TO COPY OR SHARE THIS INFORMATION WITH ANOTHER PARTY WILL BE CONSIDERED A VIOLATION OF JORDAN TECHNOLOGIES PROPRIETARY PROPERTY RIGHTS AND A BASIS FOR LEGAL ACTION. FURTHER, THIS ENTIRE DOCUMENT IS THE SUBJECT OF COPYRIGHT PROTECTION UNDER TITLE 17 UNITED STATES CODE AND THE PARIS CONVENTION. 2014 JORDAN TECHNOLOGIES ALL RIGHTS RESERVED.
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Enclosure 5
Commandant United States Coast Guard
2703 Martin Luther King Jr. Ave SE Stop 7509
Staff Symbol: CG-ENG-5
Phone: (202) 372-1412 Fax: (202) 372-8380
16703/2020-01-06T174800 February 12, 2020
Warner Nicholson Consultants, PLLC Attn: Jon Young Principal Engineer PO Box 24 Wellborn, TX 77881
Subj: ACCEPTANCE - CERTIFYING ENTITY FOR 33 CFR 154, MARINE VAPOR CONTROL SYSTEMS
Dear Mr. Young:
This is in response to your e-mail of December 31, 2019, which requested an update to your company's name for facility marine vapor control system (VCS) certifications. Your company is currently approved under the name Warner Nicholson Engineering Consultants, PC (WNEC). You stated that the name will change to Warner Nicholson Consultants, PLLC (WNC). You are the sole owner and employee of Warner Nicholson Consultants, PLLC and will be the point of contact for marine VCS certifications.
Because you will have the same personnel for marine VCS certifications, Warner Nicholson Consultants, PLLC (WNC) is found acceptable to continue to certify marine VCSs as meeting the requirements of Title 33 Code of Federal Regulations (CFR) part 154, subpart P. You will be listed as WNC's point of contact. All the terms of CDR R. F. Corbin's letter of October 26, 1998, initially establishing WNEC as a facility marine VCS certifying entity, and CDR L. M. Roldan's letter of November 15, 2010, updating the company information, still apply. We understand that WNEC still has contracts to finish, so you will keep WNEC open until those contracts are finished. You will notify our office once all current WNEC contracts are completed at which time we will remove WNEC from our list of approved Certifying Entities. All new contracts will be with WNC.
If you have any questions, please contact my staff at hazmatstandards@uscg.mil.
Sincerely,
M. J. MONTEMERLO Commander, U. S. Coast Guard Chief, Hazardous Materials Division By direction
Warner Nicholson Consultants, PLLC
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PROPRIETARY INFORMATION
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PROPRIETARY INFORMATION
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PROPRIETARY INFORMATION
THIS DRAWING INCLUDES VALUABLE PRODUCT INFORMATION, A SUBSTANTIAL PORTION OF WHICH IS PROPRIETARY TO JORDAN TECHNOLOGIES, AS SUCH, THIS DRAWING IS SUBMITTED IN CONFIDENCE TO THE PARTY TO WHICH IT IS ADDRESSED. ANY EFFORT TO COPY OR SHARE THIS INFORMATION WITH ANOTHER PARTY WILL BE CONSIDERED A VIOLATION OF JORDAN TECHNOLOGIES PROPRIETARY PROPERTY RIGHTS AND A BASIS FOR LEGAL ACTION. FURTHER, THIS ENTIRE DOCUMENT IS THE SUBJECT OF COPYRIGHT PROTECTION UNDER TITLE 17 UNITED STATES CODE AND THE PARIS CONVENTION. 2014 JORDAN TECHNOLOGIES ALL RIGHTS RESERVED.
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