Document 3eGyeKE79Kw8GO88oQ9epGDDn
Data Package
Contract Lab Program Data Package for
DERS/DuPont Env Remed Services
TYPE IV INORGANICS DATA PACKAGE
DuPont Fort Madison GW Monitoring-1996 Annual Water Samples
Collected on 09/19/96 - 09/20/96 sample No. 2585287-2585295
d at e r ec eiv ed
OCT 2 11996 SAM -----BY -------
PA Cert. # 36-037 NY Cert. # 10670 NJ Cert. # 77011
A CED-------BY,------
Prepared by_ Quality Assurance Revie1 Date / o![1 hi* Delivery Date_-/Q&))%
Lancaster Laboratories
A Thermo Analytical Laboratory
N36818
Lancaster Laboratories 2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681
DUP050306981
Lancaster Laboratories A division of Thermo Analytical Inc. IA/here quality ts a science
Sample Reference List for 806 # FMD04 with a Package Type of XV-I
Lab sample Humber
2585287 2585288 2585289 2585290 2585291 2585292 2585293 2585294 2585295
Sample Code
XSDXS XDDXS DXS2D DXS2S DXS4S DXS3S DXS3D 3DDUP FBK2D
Client Sample Description
FMN-MRA-1S-DIS Filtered Hater sample FMN-MRA-1D-DXS Filtered Hater sample FMN-MRA-2D-DIS Filtered Hater sample FMN-MRA-2S-DXS Dnspiked Filtered Hater Sample FMN-MRA-4S-DI8 Filtered Hater Sample FMN-MRA-3S-DXS Filtered Hater Sample FMN-MRA-3D-DIS Filtered Hater Sample FMN-MRA-3D-DUP-DIS Filtered Hater Sample FMN-MRA-FBLK-2-DIS Filtered Hater Sample
Lancaster laboratories 2425 New Holland Bov. 12425 Lancaster PA 17C05-2425 717-556-2300 Fa* ?7-656-26S'
Shipping Address: Lancaster Laboratory* 2425 New Holland Pikvlancaster. PA 17GC* /?7-656-2.300 f-c/ 7'7-656-26`
Environmental `Foods `Pharmaceuticals A subsidiary of Thermo lerra'iech Inc.. a Thermo Electron ccrnoarty
DU P050306982
TABLE OF CONTENTS
A. Case Narrative-Conformance/Nonconformance Summary.................................1
B. Sample Data.......................................................... ................................................................ .. C. Quality Control Data................................................................................
4 14
D. Verification of Instrument Parameters.................
.....38
E. Preparation and Run Logs....................................................................................................54
F. Raw Data................................................................................................................................................82
1. ICP Data........................................................................................................................83
2. Furnace Data............................................................................................................152
4. Mercury Data...................................
237
5. Extraction/Distillation/Digestion Logs..................................244
G. Chain-of-Custody Record..................................................
248
DU P050306983
Case Narrative Conformance/Nonconformance Summary
l DUP050306984
#Lancaster Laboratories A Thermo Analytical Laboratory Where quality is a science.
CASE NARRATIVE FOR INORGANICS
Laboratory Name: Lancaster Laboratories SDG Number: FMD04 Date Received: 09/21/96
Analysis: The following run logs are included to demonstrate the
need for dilution into calibration range:
Method GFAA
Analvte Pb
Date 09/25/96
Calibration Standards: Instrument calibration standards are prepared monthly from stock
solutions purchased from Spex Industries Inc., JT Baker, Aldrich Chemical, VWR Scientific, EM Science, or VHG Laboratories.
Case Narrative reviewed and approved by: _______Date_ `hohf,
Betty L/ Umble, Administrator III Inorganic Data Packages
Lancaster Laboratories 2425 New Holland Pike, P0 Box 12425, Lancaster, PA 17605-2425 717-656-2300 Fax: 717-656-2681 A subsidiary of Thermo Process Systems Inc., a Thermo Electron company
2
DU P050306985
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: LANCASTERJLABORATORIES
Lab Code: _________
Case No.:
SOW No.: ILM04.0
EPA SAMPLE No.
3DDUP _DIS2D______ _DIS2S______ _DIS3D______ _DIS3S______
DIS4S______ _FBK2D______
IDDIS______ ISDIS______
Contract:
SAS No.: _________ SDG No.: FMD04
Lab Sample ID. _2585294___ _2585289___ _2585290___ 2585293___ _2585292___ _2585291___ _2585295___ _2585288 2585287
Were ICP interelement corrections applied ?
Were ICP background corrections applied ? If yes - were raw data generated before application of background corrections ?
Comments:
Yes/No Yes/No Yes/No
YES YES NO_
I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for other
than the conditions detailed above. Release of the data contained in this
hardcopy data package and in the computer-readable data submitted on
diskette has been authorized by the Laboratory Manager or the Manager's
aesigi--
r foiiKing si9"-
Signature:,
Name: _Betty L. Umble_____
Date:
Title: COVER PAGE - IN
Administrator III Inorganic Data Packages
ILM04.0
3
DUP050306986
Sample Data
4
DUP050306987
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_:LABORATORIES____ Contract:
3DDUP
T.ab Code: _________
Case No.: ____
Matrix (soil/water): WATER
SAS NO.!
SDG No.: FMD04
Lab Sample ID: 2585294
Level (low/med):
LOW
Date Received: 09/21/96
% Solids
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 Aluminum 7440-36-0 Antimony_ 7440-38-2 Arsenic 7440-39-3 Barium 7440-41-7 Beryllium
7440-43-9 Cadmium "7440-70-2 Calcium
7440-47-3" Chromium 7440-48-4 Cobalt
7440-50-8.. Copper 7439-89-6 Iron
7439-92-1" Lead 7439-95-4 Magnesium 7439-96-5 Manganese 7439-97-6 Mercury___ 7440-02-0 Nickel 7440-09-7 Potassium 7782-49-2 Selenium 7440-22-4 Silver
7440-23-5 Sodium 7440-28-0 Thallium 7440-62-2 Vanadium 7440-66-6 Zinc
28.1 U 11.5 U
6.3 B 140 B
0.83 U 0.38 U 90400
2.9 U 2.7 B 9.4 U 150 0.84 B 28000 527 0.059 B 2.6 U 3260 B 0.70 U 2.2 U 51200
1.1 u 2.0 u
9.6 B
W
WN w*
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color After: COLORLESS Comments:
Clarity Before: CLEAR clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
5
DUP0503 06988
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIS____ Contract: ____________
DIS2D
T,aYi code: _________
Case No.: _____________ SAS No.: ______SDG No.: FMD04
Matrix (soil/water): WATER
Lab Sample ID: 2585289
Level (low/med):
LOW
Date Received: 09/21/96
% Solids:
0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L____
CAS No.
Analyte Concentration C Q
7429-90-5 Aluminum 7440-36-0 Antimony 7440-38-2 Arsenic 7440-39-3 Barium 7440-41-7 Beryllium
7440-43-9 Cadmium "7440-70-2 Calcium
7440-47-3 Chromium 7440-48-4 Cobalt 7440-50-8 Copper 7439-89-6 Iron 7439-92-1 Lead 7439-95-4 Magnesium 7439-96-5 Manganese
7439-97-6 Mercury 7440-02-0 Nickel
7440-09-7 Potassium 7782-49-2.. Selenium 7440-22-4 Silver
7440-23-5"" Sodium 7440-28-0 Thallium 7440-62-2 Vanadium 7440-66-6 Zinc
28.1 U
11.5 u 1.3 u
98.4 B
0.83 U 0.38 U 80000
2.9 U 2.3 U
9.4 u 15.5 u 0.84 u
27900 102
0.062 B 2.6 U
3730 B 0.70 U
2.2 U 64000
1.1 u 2.0 u 9.6 u
WN *
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLEAR, Clarity After: CLEAR
Texture: Artifacts:
FORM I - IN
ILM04.0
6
DUP050306989
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Lab Code: ______
Case No.: _
Matrix (soil/water}: WATER
Level (low/med):
LOW
contract:
DIS2S
SAS No.:
SDG No.: FMD04
Lab Sample ID: 2585290
Date Received: 09/21/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 Aluminum 7440-36-0 Antimony 7440-38-2'" Arsenic 7440-39-3 Barium 7440-41-7 Beryllium 7440-43-9 Cadmium 7440-70-2 Calcium 7440-47-3 Chromium 7440-48-4 Cobalt
7440-50-8 cooner 7439-89-6 Iron
7439-92-1 Lead 7439-95-4 Magnesium 7439-96-5 Manganese
7439-97-6 Mercury 7440-02-0 Nickel 7440-09-7 Potassium 7782-49-2 Selenium
7440-22-4 silver
7440-23-5 Sodium 7440-28-0 Thallium 7440-62-2 Vanadium-1 7440-66-6 Zinc
34.5 B 11.5 U
1.3 U 68.6 B 0.83 U 0.38 U 149000
2.9 U 2.3 U 9.4 U 15.5 U
0.92 B 50100
14.3 B 0.061 B
2.6 U 1540 B 97.0
2.2 U
53400 1.1 U 2.0 U
9.6 U
WN *
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLEAR_______ Clarity After: CLEAR_______
Texture: Artifacts:
A
FORM I - IN
ILM04.0
7
DUPO50306990
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Lab Code: _______
Case No.:
Matrix (soil/water): WATER
Level (low/med):
LOW
Contract:
DIS3D
SAS No.:
SDG No. FMD04
Lab Sample ID: 2585293
Date Received: 09/21/96
% Solids:
0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L.
CAS No.
7429-90-5 7440-36-0 7440-38-2 7440-39-3 "7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 "7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Analyte Concentration C
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt
Conner Iron Lead Magnesium Manganese
Mercury Nickel Potassium Selenium
Silver
Sodium Thallium
Vanadium Zinc
3o. ' B
11.5 U 1.5 B 142 B
0.83 U 0.38 U 91600
2.9 U 5.3 B 9.4 U 158 0.84 U 28400 532 0.060 B 2.6 U 3340 B 0.70 U
2.2 U
52100 1.1 U
2.0 U 10.3 B
Q w
WN *
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color After: COLORLESS. Comments:
Clarity Before: CLEAR. Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
8
DUP050306991
U.S. EPA - CLP
1 INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES____ Contract: ____________
DIS3S
Lab Code: Matrix (soil/water)
Case No WATER
SAS No.: _________ SDG No.: FMD04 Lab Sample ID: 2585292
Level (low/med):
LOW
Date Received: 09/21/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2
7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4
7440-23-5 7440-28-0 7440-62-2 7440-66-6
Aluminum Antimony
Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Conner Iron Lead Magnesium Manganese Mercury
Nickel Potassium
Selenium Silver
Sodium Thallium Vanadium Zinc
28.1 U 11.5 U
1.3 U 230 0.83 U 0.38 U 140000
2.9 U 2.3 U
9.4 u 15.5 u 0.84 u
43000 5.1 B
0.057 B 2.6 U
1780 B
163 2.2 U
26800 1.1 U 2.0 U
13.7 B
WN
s*
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS. Comments:
Clarity Before: CLEAR. Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
9
DUPO 50306992
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Contract:
DIS4S
Lab Code: _________
Case No.: _
SAS No.
SDG No.: FMD04
Matrix (soil/water): WATER
Lab Sample ID: 2585291
Level (low/med):
LOW
Date Received: 09/21/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS NO.
7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Analyte Concentrat ion C
Aluminum Antimony Arsenic Barium Beryl lTuim Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium selenium Silver Sodium Thallium Vanadium Zinc
28.6 B 11.5 U
1.3 U 18.2 B 0.83 U 0.38 U 431000
2.9 U 2.3 U
9.4 U 15.5 U
8.6 B 134000
392 0.058 B
15.4 B 4880 B 21.1
2.2 U 92700
1.1 U 2.0 U 9.6 U
Q W
WN *
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color After: COLORLESS. Comments:
Clarity Before: CLEAR Clarity After: CLEAR
Texture: Artifacts:
FORM I - IN
ILM04.0
10
DUP050306993
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER_LABORATORIES_
Lab Code:
Case No.: _
Matrix (soil/water): WATER
Level (low/med):
LOW
Contract: SAS No.:
FBK2D SDG No.: FMD04
Lab Sample ID: 2585295
Date Received: 09/21/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
Analyte Concentration C Q
7429-90-5 Aluminum 7440-36-0 Antimony_ 7440-38-2 Arsenic 7440-39-3 Barium 7440-41-7 Beryllium 7440-43-9 Cadmium 7440-70-2 Calcium 7440-47-3 Chromium 7440-48-4 Cobalt 7440-50-8'"' Conner 7439-89-6 Iron
7439-92-1 Lead 7439-95-4 Magnesium 7439-96-5 Manganese
7439-97-6 Mercury___ 7440-02-0... Nickel 7440-09-7" Potassium 7782-49-2 Selenium 7440-22-4 Silver 7440-23-5 Sodium 7440-28-0 Thallium 7440-62-2 Vanadium 7440-66-6 Zinc
28.1 U
11.5 u
1.5 B 1.6 B
0.83 U
0.38 u
104 B 2.9 U 2.3 U 9.4 U 15.5 U 1.1 B 29.1 U 1.9 U 0.055 B 2.6 U 233 U 0.70 U 2.2 U 237 B 1.1 U 2.0 U 9.6 U
N
W* W
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS Comments:
Clarity Before: CLEAR Clarity After: CLEAR.
Texture: Artifacts:
FORM I - IN
ILM04.0
11 A
DUP0503 06994
U.S. EPA - CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO,
Lab Name: LANCASTER. LABORATORIES,
Contract:
IDDIS
Lab Code: ________
Case No.: _
SAS No.:
SDG No.: FMD04
Matrix (soil/water): WATER
Lab Sample ID: 2585288
Level (low/med):
LOW
Date Received: 09/21/96
% Solids:
0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS NO.
Analyte Concentration C Q
7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-89-6 7439-92-1 7439-95-4 7439-96-5 7439-97-6 7440-02-0 7440-09-7 7782-49-2 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Conner Iron Lead Magnesium Manganese
Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
28.1 U
11.5 u 1.3 u
60.7 B
0.83 U 0.38 U
155000
2.9 U
5.8 B 9.4 U 138
0.84 U 38200
1800
0.061 B 7.7 B
4620 B 0.70 U
2.2 U
78700
1.1 u 2.0 u 9.6 u
s
WN *
M
P P F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS. Color After: COLORLESS Comments:
Clarity Before: CLEAR. Clarity After: CLEAR
Texture: Artifacts:
FORM I - IN
ILM04.0
12
DUP050306995
U.S. EPA CLP
INORGANIC ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: LANCASTER,LABORATORIES.
Lab Code: _______
Case No.: _
Matrix (soil/water): WATER
Level (low/med):
LOW
Contract:
ISDIS
SAS No.:
SDG No.: FMD04
Lab Sample ID: 2585287
Date Received: 09/21/96
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS NO.
Analyte Concentration C
7429-90-5 Aluminum 7440-36-0 Antimony 7440-38-2 Arsenic 7440-39-3 Barium 7440-41-7 Beryllium 7440-43-9 Cadmium 7440-70-2 Calcium 7440-47-3 Chromium 7440-48-4... Cobalt 7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead 7439-95-4 Magnesium 7439-96-5 Manganese 7439-97-6 Mercurv 7440-02-0 Nickel 7440-09-7 Potassium 7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium 7440-28-0 Thallium 7440-62-2 Vanadium 7440-66-6 Zinc
28.1 u 11.5 u
1.3 u
84.5 B
0.83 u 0.38 u
103000
2.9 u 2.3 u 9.4 u 15.5 u 0.84 u
37600
5.2 B
0.057 B 2.6 U
672 B
0.89 B
2.2 U
29400
1.1 u 2.0 u
32.4
Q
WN *
M
P P
F P P P P P P P P F P P CV P P F P P F P P
Color Before: COLORLESS Color After: COLORLESS, Comments:
Clarity Before: CLEAR________ Clarity After: CLEAR________
Texture: Artifacts:
FORM I - IN
ILM04.0
13
DUPO 50306996
Quality Control Data
14
DUP050306997
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES_____
code: __________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Initial Calibration
True
Found %R(1)
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper_____ Iron Lead Magnesium Manganese
Mercury___ Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
30000.0 6000.0 50.0 6000.0 600.0 600.0
60000.0 6000.0 1200.0 6000.0 6000.0 20.0
30000.0 6000.0
2.0 12000.0 60000.0
20.0 600.0 60000.0
50.0 2400.0 6000.0
30684.78 5891.79 50.52 5836.84 585.94 594.13
62586.42 5867.06 1139.68 5909.62 5894.70 19.90
30948.50 5842.69 2.06
11605.25 61524.47
19.58 570.14 61937.01
46.77 2365.81 5870.96
102.3 98.2
101.0 97.3 97.7 99.0
104.3 97.8 95.0 98.5 98.2 99.5
103.2 97.4
103.0 96.7
102.5 97.9 95.0
103.2 93.5 98.6 97.8
True
Continuing Calibration
Found %R(1)
Found %R(1)
25000.0 5000.0 40.0 5000.0 500.0 500.0
50000.0 5000.0 1000.0 5000.0 5000.0 25.0
25000.0 5000.0 1.0
10000.0 50000.0
25.0 500.0 50000.0
40.0 2000.0 5000.0
25990.57 5070.27 42.60 4888.21 497.59 502.33
53267.01 5081.98 989.86 5061.77 5074.60 26.11
26070.51 4977.46 1.03 9862.19
50084.95 24.85
483.17
51831.14 40.16
1985.81 5023.85
104.0 101.4 106.5
97.8 99.5 100.5 106.5 101.6 99.0 101.2 101.5 104.4 104.3 99.5 103.0 98.6 100.2 99.4 96.6 103.7 100.4 99.3 100.5
25824.41 5004.59 42.16 4915.69 487.74 500.89
51937.91 4956.49 968.62 5036.41 4935.31 26.29
25685.48 4883.00
0.98 9640.30 50598.64
24.76 480.76
51796.00 38.49
1958.59 4927.94
103.3 100.1 105.4
98.3 97.5 100.2 103.9 99.1 96.9 100.7 98.7 105.2 102.7 97.7 98.0 96.4 101.2 99.0 96.2 103.6 96.2 97.9 98.6
M
P P F P P P P P P P P F P P CV P P F P P F P P
(1) Control Limits: Mercury 80-120? Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
15
DUP050306998
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES____
T.aVi code: __________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury > Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial calibration
True
Found %R(1)
True
Continuing Calibration
Found %R(1)
Found %R(1)
M
25000.0 25407.36 101.6
5000.0 4901.69 98.0
40.0
41.65 104.1
5000.0 4706.17 t 94.1
500.0 476.24 95.2
500.0 497.42 99.5
50000.0 51021.68 102.0
5000.0 4861.62 97.2
1000.0 950.31 95.0
5000.0 4898.29 98.0
5000.0 4879.64 97.6
25.0
26.22 104.9
25000.0 25173.38 100.7
5000.0 4779.55 95.6
1.0
1.07 107.0
10000.0 9459.83 94.6
50000.0 48741.45 97.5
25.0
24.18 96.7
500.0 469.03 93.8
50000.0 50645.45 101.3
40.0
43.11 107.8
2000.0 1906.56 95.3
5000.0 4851.26 97.0
39.39 _98.5
26.64 106.6 24.67 98.7 42.07 105.2
P P F P P P P P P P P F P P CV P
P F P P F P P
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
16
DUP050306999
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES_____
Lab Code: _________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: __________________
SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
True
Continuing Calibration
Found %R(1)
Found %R(1)
M
40.0
25.0 25.0
37.39 93.5
26.24 105.0 23.45 93.8
24.66
98.6
NR NR F NR NR NR NR NR NR NR NR F NR NR NR NR NR F NR
NR NR NR NR
(1) Control Limits: Mercury 80-120; other Metals 90-110? Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
17
DUP050307000
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_IABORATORIES_____
Code: __________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI__________.
Contract: SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper____ Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
50.6
49.15 98.3
True
Continuing Calibration Found %R(1) Found %R(1)
M
40.0 25.0
41.04 102.6 24.24 97.0
40.10 100.2
NR NR F NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR
NR NR
NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
18
DUP050307001
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER_LABORATORIES_____
Lab Code: __________
Case No.:
___________
Initial Calibration Source:
LLI
Continuing Calibration Source: LLI
Contract: __________________
SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Initial Calibration
True
Found %R(1)
Aluminum Antimony_ Arsenic Barium
Beryllium
Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese
Mercury___ Nickel Potassium Selenium Silver Sodium Thallium
Vanadium Zinc
50.0 20.0
48.75 97.5 19.08 95.4
True
Continuing Calibration
Found %R(1)
Found %R(1)
M
40.0 25.0
41.75 104.4 24.26 97.0
43.58 109.0 23.80 95.2
NR NR F NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR
NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
19
DUP050307002
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTERJLABORATORIES____
T^b Code: __________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing calibration source: LLI
Contract: ________________
SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
50.0
46.49 93.0
20.0
19.01 95.0
True
Continuing Calibration
Found %R(1)
Found %R(1)
M
40.0 25.0
41.42 103.6 24.62 98.5
42.67 106.7 24.55 98.2
NR NR F NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
20
DU P050307003
U.S. EPA - CLP
2A INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTERJLABORATORIES____
Lab Code: __________
Case No.: ______________
Initial Calibration Source:
LLI
Continuing calibration source: LLI
Contract: SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese
Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Initial Calibration
True
Found %R(1)
True
Continuing Calibration
Found %R(1)
Found %R(1)
M
25.0
24.01 96.0
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR
NR NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM04.0
21
DUP050307004
U.S. EPA CLP
2B CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTERJLABORATORIES_____
r.ah code: __________
Case No.:
-_________
AA CRDL Standard Source: LLX
ICP CRDL Standard Source: LLI_______
Contract: __________________
SAS No.: __________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum" Antimony_ Arsenic___ Barium Beryllium Cadmium Calcium Chromium_ Cobalt_____ Copper_____ Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium_ Vanadium_ Zinc
CRDL Standard for AA
True
Found
%R
True
CRDL Standard for ICP
Initial
Final
Found %R Found
%R
10. t)
3.0 0.2 5.0 10.0
_____120.0 _____129.12 107.6 _____123.59 103.0 10.82 108.2
10.0 10.0
10.03 100.3 9.78 _97.8
10.03 100.3 9.99 _99.9
20.0 100.0
50.0
18.28 91.4 103.37 103.4
55.82 111.6
20.43 102.2 100.28 100.3
51.96 103.9
3.29 109.7
0.23 115.0
30.0 80.0
31.31 104.4 82.59 103.2
31.31 104.4 77.78 _97.2
4.05 _81.0
20.0
21.43 107.2
19.10 _95.5
8.73 __87.3
100.0 40.0
101.29 101.3 41.32 103.3
97.67 97.7 40.37 100.9
FORM II (PART 2) - IN
ILM04.0
22
DUP050307005
U.S. EPA - CLP
223 CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER_LABORATORIES
Lab Code: __________
Case No.:
AA CRDL Standard Source: LLI____
ICP CRDL Standard Source: LLI____
Contract: SAS No.: _________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
CRDL Standard for AA
True
Found
%R
10.6
9.61 96.1
5.0
3.63 72.6
True
CRDL Standard for ICP
Initial
Final
Found %jR Found
%R
FORM II (PART 2) - IN
ILM04.0
23
DUP050307006
U.S. EPA - CLP
2B CRDL STANDARD FOR AA AND I CP
Lab Name: LANCASTER_LABORATORIES____
j.a'h code: j_________
Case No.: ______________
AA CRDL Standard source: LLI_________'
TCP CRDL Standard Source: LLI
Contract: __________________
SAS No.: _________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
CRDL Standard for AA
True
Found
%R
True
CRDL Standard for ICP
Initial
Final
Found %R Found
%R
Aluminum
Antimony
Arsenic
10.0
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
5.0
Silver
A Sodium
Thallium
Vanadium
Zinc
8.03 180.3 4.54 90*8
FORM II (PART 2) - IN
ILM04.0
24
DUP050307007
U.S. EPA - CLP
26 CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER_LABORATORIES_____
Contract:
Lab Code: __________
Case No.:
___________ SAS No.: __________
AA CRDL Standard Source: LLI
ICP CRDL Standard Source: LLI_________
SDG No.: FMD04
Concentration Units: ug/L
Analyte
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
CRDL Standard for AA
True
Found
%R
10.0
11.01 110.1
True
CRDL Standard for ICP
Initial
Final
Found %R Found
%R
FORM II (PART 2) - IN
ILM04.0
25
DUPO 503 07008
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER_LABORATORIES_____
Contract:
Tah Code: __________
Case No.: ______________ SAS No.: __________
Preparation Blank Matrix (soil/water): WATER_
Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_
SDG No.: FMD04
Analyte
Initial Calib. Blank (ug/L)
C
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
28.1 Tf 11.5 U
1.3 u 1.8 B 0.83 U 0.38 U 41.1 U 2.9 U
3.5 B 9.4 U 15.5 U 0.84 U
29.1 U 2.6 B
0.055 B 2.6 U 233 U
-0.98 B 2.2 U
84.4 U 1.1 U 2.0 U
9.6 U
Continuing Calibration Blank (ug/L)
1C2 C3
C
58.6 B 11.5 U
1.3 U
1.4 B 0.83 U 0.38 U 68.0 B
2.9 U 2.3 U 9.4 U 22.1 B 0.84 U
38.0 B
1.9 U
0.050 B 2.6 U 233 U
-1.2 B 2.2 U
84.4 U 1.1 U 2.0 U 9.6 U
28.1 U 11.5 U
1.3 U 1.6 B 0.83 U 0.38 U 41.1 U 2.9 U 2.3 U 9.4 U 15.5 U 0.84 U 29.1 u 2.1 B
0.050 B 2.6 U
233 U
-1.5 B 2.2 U
84.4 U -1.7 B
2.0 U
9.6 U
56.4 B 11.5 U
1.3 U
1.4 B 0.83 U 0.38 U
63.9 B 2.9 U 2.3 U 9.4 U
23.1 B 0.85 B 48.5 B
1.9 U 0.054 B
2.6 U 233 U 0.70 U 2.2 U 84.4 U 1.1 U 2.0 U 9.6 U
Prepa ration
Blank
C
M
28.100 U 11.500 U
1.300 U 0.840 O 0.830 U 0.380 U 41.100 U 2.900 U 2.300 U 9.400 U 15.500 U 0.840 U
29.100 U 1.900 U 0.065 B 2.600 U
233.000 U -1.390 B 2.200 U 84.400 U 1.100 U 2.000 U 9.970 B
P P F P P P P P P P P F P P CV P P F P P F P P
FORM III - IN
ILM04.0
26
DUP050307009
U.S. EPA CLP
3 BLANKS
Lab Name: LANCASTER_]LABORATORIES____
Contract: ____________
Lab Code: __________
Case No.: ______________ SAS No.: __________
SDG No.: FMD04
Preparation Blank Matrix (soil/water): ________________
Preparation Blank Concentration Units (ug/L or mg/kg): ________________
Analyte
Initial Calib. Blank (ug/L)
C
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
"
Continuing Calibration Blank (ug/L)
1C2 C 3
1.3 U
1.3 U
C
0.85 B
0.84 U
-1.2 B 1.1 U
0.70 U
0.70 U
Prepa ration
Blank
C
M
NR NR F NR NR NR NR NR
NR NR NR F NR NR NR NR NR F NR NR F NR NR
FORM III - IN
ILM04.0
27
DUP05030701 0
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER_LABORATORIES____
Contract: __________________
Lab Code: _________
Case No.: ______________ SAS No.: __________
SDG No.: FMD04
Preparation Blank Matrix (soil/water): ________________
Preparation Blank Concentration Units (ug/L or mg/kg): ________________
Analyte
Initial Calib. Blank (ug/L)
c
Aluminum Antimony_ Arsenic Barium Beryllium Cadmium
Calcium Chromium Cobalt Cooper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thai livim Vanadium Zinc
l. B
_
Continuing Calibration Blank (ug/L)
1C2 C 3
1.4 B
1.9 B
-1.5 B
_
Prepa ration C Blank c M
NR NR F NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR
FORM III - IN
ILM04.0
28
.ww ..
DUP050307011
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER_LABORATORIES_
Contract:
Lab Code: __________
Case No.:
SAS No.:
Preparation Blank Matrix (soil/water): ________________
Preparation Blank Concentration Units (ug/L or mg/kg):
SDG No. FMD04
Analyte
Initial Calib. Blank (ug/L)
C
Aluminum
Antimony_ Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium
Silver Sodium Thallium Vanadium Zinc
1.3 U
-1.4 1
_
Continuing Calibration Blank (ug/L)
1C2 C 3
2.3 B
1.3 u
1
H
-1.8 B
_
B
Prepa ration C Blank C M
NR NR F NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR
FORM III - IN
ILM04.0
A
29
DUP050307012
U.S. EPA - CLP
3 BLANKS
Lab Name: LANCASTER,LABORATORIES____
Contract:
Lab Code: __________
Case No.: ______________ SAS No.: __________
SDG No.: FMD04
Preparation Blank Matrix (soil/water): _______________ Preparation Blank Concentration Units (ug/L or mg/kg):
________________
Analyte
Initial Calib. Blank (ug/L)
C
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium
Silver Sodium Thallium Vanadium Zinc
2.4 1 -0.75 B
Continuing Calibration Blank (ug/L)
1C2C3
1.8 B
1.3 U
C
0.70 U
0.70 u
0.70 u
Prepa ration
Blank C . M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR F NR NR NR NR NR
FORM III - IN
ILM04.0
30
DUP050307013
U.S. EPA CLP
4 ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER_LABORATORlES____
contract: ___:
Lab Code: __________
Case No.: ___________ SAS No.: __________ SDG No.: FMD04
ICP ID Number: 03144___________
ICS Source: LLI
Concentration Units: ug/L
Analyte
True
Sol.
Sol.
A AB
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
500000 0
0 0
500000 0 0 0
200000
500000 0
0 0
0 0
0 0
500000 600
500 500
500000 500 500 500
200000
500000 500
1000 0
200 0
500 1000
Initial Found
Sol.
Sol.
A AB %R
506161 503979.5 100.8
-14
579.4 96.6
7 488.0 97.6 -2 477.6 95.5
491001 2
-1 5
184810
490843.4 472.7 454.3 482.7
184464.2
98.2 94.5 90.9 96.5 92.2
518589 516667.5 103.3 -4 464.2 92.8
-11 20
898.6 89.9 -59.3
-9 186.2 93.1 80 52.9
-1 475.1 95.0 17 965.3 96.5
Final Found
Sol.
Sol.
A AB
%R
495144 502156.3 100.4 0 596.7 99.4
7 481.4 96.3 -1 473.5 94.7
480247 4 4
-3 181360
485273.2 465.7 449.9 480.9
183197.2
97.1 93.1 90.0 96.2 91.6
506703 513273.8 102.7 -6 457.0 91.4
-11 99
885.1 88.5 -59.3
-8 184.9 92.4 92 47.7
-2 471.3 94.3 17 961.5 96.2
FORM IV - IN
ILM04.0
31
DUP050307014
U.S. EPA - CLP
4 ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: __________
Case No. : ______________ SAS No. : __________
ICP ID Number: 05478___________
ICS Source: LLI
SDG No. : FMD04
Concentration Units: ug/L
Analyte
True
Sol.
Sol.
A AB
Initial Found
Sol.
Sol.
A AB %R
Final Found
Sol.
Sol.
A AB
%R
Aluminum 500000 ___500000
Antimony
Arsenic
Barium
Beryllium
Cadmium
0 1000
Calcium
500000 ___500000
Chromium
Cobalt
Coooer
Iron
200000 200000
Lead
Magnesium 500000 ___500000
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
___539361 531407.5 106.3 ___539718 537995.5 107.6
1 903.9 90.4
1 914.8 91.5
___515934 502391.0 100.5 ___518171 510622.3 102.1
211680 207040.0 103.5
212670 209969.7 105.0
___557856 537459.5 107.5 ___558446 543949.3 108.8
FORM IV - IN
ILM04.0
82
DUP050307015
U.S. EPA - CLP
5A SPIKE SAMPLE RECOVERY
EPA SAMPLE NO.
Lab Name: LANCASTER_]LABORATORIES____ Contract:
DIS2SS
Lab Code: __________
Case No.: ______________ SAS No.: _________ SDG No.: FMD04
Matrix (soil/water) : WATER_________
Level (low/med):
LOW
% Solids for Sample: 0.0
Concentration Units (ug/L or mg/kg dry weight) : UG/L
Analyte
Control Limit %R
Spiked Sample Result (SSR) C
Aluminum 75-125
Antimony 75-125
Arsenic 75-125
Barium
75-125
Beryllium 75-125
Cadmium 75-125
Calcium
Chromium 75-125
Cobalt
75-125
Copper
75-125
Iron
75-125
Lead
75-125
Magnesium
Manganese 75-125
Mercury___ 75-125
Nickel
75-125
Potassium
Selenium
Silver
75-125
Sodium
Thallium 75-125
Vanadium 75-125
Zinc
75-125
i
2053.6500 520.2400 33.9100
2013.5900 48.1500 49.2300
194.5900 474.9900 246.2800 976.4100
14.5100
496.2000 1.0700
478.5900
102.6500 46.9400
40.2400 484.7800 493.0000
Sample
Spike
Result (SR) C Added (SA)
34.4700 B 11.5000 U
1.3000 U 68.6000 B
0.8300 U 0.3800 U
2000.00 500.00 40.00
2000.00 50.00 50.00
2.9000 U 2.3000 U 9.4000 U 15.5000 U 0.9200 B
200.00 500.00 250.00 1000.00
20.00
14.2900 B 0.0610 B 2.6000 U
500.00 1.00
500.00
97.0000 2.2000 U
10.00 50.00
1.1000 U 2.0000 U 9.6000 U
50.00 500.00 500.00
%R Q
101.0 104.0
84.8 97.2 96.3 98.5
97.3 95.0 98.5 97.6 68.0
N
96.4 100.9
95.7
56.5 93.9
80.5 97.0 98.6
iVi',avawawa ^
Comments:
FORM V (PART 1) - IN
ILM04.0
33
DUP050307016
U.S. EPA - CLP
6 DUPLICATES
EPA SAMPLE NO.
Lab Name: LANCASTERJLABORATORIES
Contract
DIS2SD
Lab Code: _________
Case No. : _____________ SAS No.: _________ SDG No.: FMD04
Matrix (soil/water): WATER
Level (low/med):
LOW
% Solids for Sample: 0.0
% Solids for Duplicate : o.o
Concentration Units (ug/L or mg/kg dry weight): UG/L____
Control Analyte Limit
Aluminum Antimony Arsenic
Barium Beryllium
Cadmium Calcium Chromium Cobalt Copper iron Lead
Magnesium Manganese Mercury Nickel Potassium Selenium
Silver Sodium Thallium Vanadium Zinc
25.0
Sample (S)
C
34.4700 B
11.5000 U
1.3000 U 68.6000 B
0.8300 U 0.3800 U
148528.1500 2.9000 U 2.3000 U 9.4000 U
15.5000 U 0.9200 B
50105.7000 14.2900 B 0.0610 B 2.6000 U
1541.0700 B 97.0000 2.2000 U
53400.0700 1.1000 U 2.0000 U 9.6000 U
Duplicate (D) C
28.1000 U 12.1900 B
1.3000 U 66.7400 B
0.8300 U 0.3800 U 146363.2600 2.9000 U 2.3000 u 9.4000 u 15.5000 u 0.8400 u 49536.8700 13.7800 B 0.0540 B 2.6000 U 1323.7400 B 123.2323 2.2000 U 52766.2800 1.1000 U 2.0000 U 15.8700 B
RPD 200.0 200.0
2.7
1.5
200.0 1.1 3.6
12.2 15.2 23.8
1.2
200.0
QM
P P
F P P P P P P P P F P P CV P P *F P P F P P
FORM VI - IN
ILM04.0
34
DUP050307017
U.S. EPA - CLP
7 LABORATORY CONTROL SAMPLE
Lab Name: LANCASTER_LABORATORIES_
Lab Code: _________
Case No.:
Solid LCS Source: __________________
Aqueous LCS Source: LLI_
Contract SAS No.:
SDG No.: FMD04
Analyte
Aqueous (ug/L)
True
Found %R
Aluminum_ Antimony_ Arsenic___
Barivun Beryllium Cadmium Calcium Chromium_
Cobalt Copper____ Iron Lead Magnesium Manganese Mercury Nickel^___ Potassium Selenium_ Silver____ Sodium
Thallium_
Vanadium_
Zinc
2000.0 500.0 40.0
2000.0 50.0 50.0
4000.0 200.0 500.0 250.0
1000.0 20.0
2000.0 500.0 1.0 500.0
4000.0 10.0 50.0
4000.0 50.0
500.0 500.0
2094.52 557.26 37.32
"2005.53 50.16 51.34
"4311.85 " 202.14
505.02 260.14 "1041.79
21.96 2078.75
506.93 0.99
510.17 "4010.74
8.27 49.83 4156.02
48.38 502.19 514.79
104.7 111.5
93.3 100.3 100.3 102.7 107.8 101.1 101.0 104.1 104.2 109.8 103.9 101.4
99.0 102.0 100.3
82.7 99.7 103.9 96.8 100.4 103.0
True
Solid (mg/kg)
Found C
Limits
--
%R
FORM VII - IN
ILM04.0 uO
DU P050 307018
U.S. EPA - CLP
8 STANDARD ADDITION RESULTS
Lab Name: LANCASTER^LABORATORIES
Lab Code
Case No
Contract: SAS No.: _________
SDG No. : FMD04
Concentration Units: ug/L
EPA Sample
No.
IDDIS IDDIS DIS2SD DIS3S
0 ADD An ABS
AS 0.003 AS 0.000 SE 0.024 SE 0.032
1 ADD CON ABS
10.00 0.019 10.00 0.023
5.00 0.035 5.00 0.041
2 ADD CON ABS
20.00 0.046 20.00 0.043 10.00 0.044 10.00 0.051
3 ADD CON ABS
30.00 0.058 30.00 0.058 15.00 0.054 15.00 0.061
Final
Cone.
rQ
1.4 0.9899 + 1.0 0.9957 12.3 0.9993 16.3 0.9997 --
FORM VIII - IN
ILM04.0
38
DUP050307019
U.S. EPA - CLP
9 ICP SERIAL DILUTIONS
Lab Name: LANCASTER__LABORATORIES____ Contract: _____
Lab Code: _________
Case No.: _____________ SAS No
Matrix (soil/water) :: WATER.
EPA SAMPLE NO.
DIS2S L
_____
SDG No.: FMD04
Level (low/med): LOW_
Analyte
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Concentration Units: ug/L
Initial Sample Result (I) C
Serial Dilution Result (S)
C
34.47 B 11.50 U
140.50 U 57.50 U
68.60 1 0.83 u 0.38 u
148528.15 2.90 u 2.30 u 9.40 u
15.50 u
71.25 B
4.15 U 1.90 U
149041.90 14.50 U 11.50 u 47.00 u 77.50 u
50105.70 14.29 B
49896.10 14.25 B
2.60 U 1541.07 B
13.00 U 1165.00 U
2.20 U 53400.07
11.00 u 52982.80
2.00 U 9.60 U
10.00 u 48.00 u
% Differ
ence 100.0
3.9
0.3
0.4 0.3
100.0
0.8
QM
P P
P P P P P P P P
P P
P P
P P
P P
FORM IX - IN
ILM04.0
37
DUP050307020
Verification of Instrument Parameters
38
DUP050307021
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
__________________
Date:
07/15/96
Flame AA ID Number: _____________
Furnace AA ID Number: ____02803
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
Aluminum^
Antimony_ Arsenic___ Barium Beryllium Cadmium Calcium Chromium_ Cobalt Copper____
Iron Lead Magnesium Manganese Mercury Nickel^___ Potassium Selenium_
silver ~ Sodium Thallium_ 276.80___ BD Vamadium_ Zinc
10
IDL (ug/L) M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 1.1 F NR NR
Comments:
FORM X - IN
ILM04.0
DUP050307022
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER._LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No. : FMD04
ICP ID Number:
____03144______
Date:
07/15/96
Flame AA ID Number: __________________
Furnace AA ID Number:
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
Aluminum 308.21
Antimony 206.83
Arsenic
Barium
493.40
Beryllium 313.04
Cadmium
Calcium 317.93
Chromium 267.71
Cobalt
228.61
Copper
324.75
Iron
259.94
Lead
Magnesium 279.07
Manganese 257.61
Mercury
Nickel
231.60
Potassium 766.49
Selenium
silver
328.06
Sodium
589.59
Thallium
Vanadium 292.40
Zinc
213.85
200 60
200 5
5000 10 50 25
100
5000 15
40 5000
10 5000
50 20
IDL (ug/L) M
28.1 P 11.5 P
NR 0.84 P 0.83 P
NR 41.1 P
2.9 P 2.3 P 9.4 P 15.5 P
NR 29.1 P
1.9 P NR
2.6 P 233 P
NR 2.2 P 84.4 P
NR 2.0 P 9.6 P
Comments:
A
FORM X - IN
ILM04.0
40
DUP050307023
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER LABORATORIES
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
__________________
Date:
07/15/96
Flame AA ID Number:
Furnace AA ID Number: ____03812
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
283.30
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
BZ
3
IDL <ug/L) M
0.84
NR NR NR
NR NR NR
NR
NR NR NR NR F_ NR NR NR NR
NR NR
NR NR
NR NR NR
Comments:
FORM X - IN
ILM04.0
41
DUP050307024
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER__LABORATORIES____
Contract:
Lab Code:
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
__________________
Date:
07/15/96
Flame AA ID Number: __________________
Furnace AA ID Number: ____04724
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
Aluminum Antimony Arsenic 193.70
Barium Beryllium Cadmium
Calcium Chromium Cobalt Copper iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium
Zinc
BZ
10
IDL (ug/L) M
1.3
NR NR F NR NR NR
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
NR
Comments:
FORM X - IN
ILM04.0
42
DUP05 0307025
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER,.LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
__________________
Date:
07/15/96
Flame AA ID Number: __________________
Furnace AA ID Number: ____04725______
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
Aluminum
Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt
Copper Iron Le<id Magnesium Manganese Mercury Nickel Potassium Selenium 196.00 Silver Sodium
Thallium Vanadium Zinc
BZ
5
IDL (g/L) M
NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR 0.70 F NR NR NR NR NR
Comments:
FORM X - IN
ILM04.0
43
DUP0503 07026
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER__LABORATORIES____
Contract: ________________
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
____05478______
Date:
07/15/96
Flame AA ID Number: __________________
Furnace AA ID Number:
.
Analyte
Wave length
(nm)
Aluminum
Antimony Arsenic
Barium Beryllium Cadmium 226.50
Cctlcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury
Nickel Potassium Selenium
silver Sodium
Thallium Vanadium Zinc
Back ground
CRDL (ug/L)
5
IDL (ug/L) M
NR NR NR NR NR 0.38 P NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
Comments:
FORM X - IN
ILM04.0
4a
DUP050307027
U.S. EPA - CLP
10 INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LANCASTER__LABORATORIES____
Contract:
t^h code: ________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number:
__________________
Date:
07/15/96
Flame AA ID Number: ____61734______
Furnace AA ID Number:
Analyte
Wave length
(nm)
Back ground
CRDL (ug/L)
IDL (ug/L) M
Aluminum_
NR
Antimony_
NR
Arsenic___
NR
Barium
NR
Beryllium
NR
Cadmium
NR
Calcium
NR
Chromium_
NR
Cobalt____
NR
Copper____
NR
Iron_______
NR
Lead
NR
Magnesium
NR
Manganese
NR
Mercury 254.00___
0.2 _0.0070 CV
Nickel___
NR
Potassium
A Selenium_
NR NR
silver____
NR
Sodium
NR
Thallium_
NR
Vanadium-
NR
Zinc
NR
comments:
FORM X - IN
ILM04.0
45
DU P05 0307028
U.S. EPA - CLP
11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER,JABORATORIES____
Contract:
Lab Code: ________
Case No.: _____________ SAS No.: ________ SDG No.: FMD04
ICP ID Number: ____ 03144 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for: A1 Ca Fe Mg
CD
Aluminum_ 308.21 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimonyl 206.83 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimony2 ___206.83 _0.0000000 _0.0000000 "0.0000000 _0.0000000 _0.0000000
Arsenic___
Barium
493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Beryllium ___313.04 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _p.0000000
Cadmium
Calcium
317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Chromium_ 267.71 0.0000000 0.0000000 -0.0000270 0.0000000 0.0000000
Cobalt____ 228.61 0.0000000 0.0000000 0.0000000 0.0000000 0.0006030
Copper Iron Leadl
324.75 0.0000000 0.0000000 -0.0001690 0.0000000 0.0000000 __ 259.94 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Lead2
Magnesium 279.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Manganese ___257.61 _0.0000000 _0.0000000 -0.0000190 _0.0000270 _0.0000000
Mercury
Nickel
231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Seleniuml
Selenium2
Silver____ 328.06 0.0000000 -0.0000180 -0.0002940 0.0000000 0.0000000
Sodium
___589.59 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Thallium
Vanadium
292.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Zinc
___213.85 _0.0000000 _0.0000000 _0.0000800 _0.0000000 _0.0000000
Comments:
FORM XI (PART 1) - IN
ILM04.0
46
DU PO 5030702 9
U.S. EPA - CLP
11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: _________
Case No.: ________
SAS No.: ________ SDG No.: FMD04
ICP ID Number: ____05478 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for: A1 Ca Fe Mg
CO
Aluminum_
Antimonyl Antimony2 Arsenic___ Barium^___ Beryllium Cadmium ___226.50 Calcium Chromium_ Cobalt Copper____ Iron Leadl Lead2 Magnesium Manganese
Mercury Nickel Potassium Seleniuml Selenium2 Silver Sodium Thallium_ Vanadium_ Zinc
-0.0000010 _0.0000000 _0.0000560 _0.0000000
-0.0001810
Comments:
FORM XI (PART 1) - IN
ILM04.0
47
DUP050307030
U.S. EPA - CLP
1XB ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number: ____03144 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for: CO CR CU MN
MO
Aluminum_ 308.21 -0.0129100 0.0000000 0.0000000 0.0000000 0.0130000
Antimonyl 206.83 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimony2 ___206.83 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Arsenic___
Barium
493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Beryllium ___313.04 _0.0000000 _0.0000000 ~0.0000000 _0.0000000 _0.0000000
Cadmium
Calcium
317.93 0.0000000 0.0004800 0.0000000 0.0000000 0.0000000
Chromium_ 267.71 -0.0001460 0.0000000 0.0000000 0.0001230 -0.0001850
Cobalt
228.61 0.0000000 0.0000890 0.0000000 0.0000000 0.0000000
Copper
324.75 -0.0014990 0.0000000 0.0000000 0.0000000 0.0003670
Iron
___259.94 _0.0000000 _o.ooooooo _0.0000000 _0.0000000 _0.0000000
Leadl
Lead2
Magnesium 279.07 0.0000000 0.0000000 0.0000000 -0.0075260 0.0000000
Manganese ___257.61 _0.0000000 _0.0000000 -0.0001800 _0.0000000 -0.0002480
Mercury
Nickel
231.60 0.0009750 0.0000000 0.0000000 0.0000000 -0.0021850
Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Seleniuml
Selenium2
Silver
328.06 0.0000000 0.0000000 0.0000000 0.0001000 0.0000000
Sodium
___589.59 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Thallium_
Vanadium_ 292.40 0.0000000 -0.0037990 0.0000000 -0.0001420 -0.0034400
Zinc
___213.85 _0.0000000 _0.0000000 _0.0020760 _0.0000000 _0.0000000
Comments:
FORM XI (PART 2) - IN
ILM04.0
48
DUP050307031
U.S. EPA - CLP
11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number: ____03144 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for: NI SB TI V
___
Aluminum_ 308.21 0.0000000 0.0000000 0.0005000 -0.0289870 0.0000000
Antimonyl 206.83 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Antimony2 ___206.83 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Arsenic___
Barium
493.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000
Beryllium ___313.04 _0.0000000 _0.0000000 _0.0000000 _0.0021580 _0.0000000
Cadmium
Calcium Chromium_
317.93 0.0000000 0.0000000 0.0000000 0.0010160 0.0000000 267.71 0.0000000 0.0000000 0.0000000 0.0003670 0.0000000
Cobalt
228.61 0.0003500 0.0000000 0.0016000 0.0000000 0.0000000
Copper
324.75 0.0000000 0.0000000 0.0003600 0.0000000 0.0000000
Iron
___259.94 _0.0000000 _0.0000000 -0.0009450 _0.0000000 _0.0000000
Leadl
Lead2
Magnesium 279.07 0.0000000 0.0000000 0.0000000 0.0010290 0.0000000 Manganese ___257.61 _0.0000000 _0.0000000 _0.0000000 -0.0000158 _0.0000000
Mercury
Nickel
231.60 0.0000000 0.0004160 0.0000000 0.0000000 0.0000000
Potassium ___766.49 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000
Seleniuml
Selenium2
Silver Sodium
328.06 0.0000000 0.0000000 -0.0002700 -0.0003600 0.0000000 ___589.59 _0.0000000 _0.0000000 _0.0050000 _0.0000000 _0.0000000
Thallium
Vanadium_ 292.40 0.0000000 0.0000000 0.0003230 0.0000000 0.0000000
Zinc
___213.85 _0.0033690 _0.0000000 _0.0000000 _0.0001280 _0.0000000
Comments:
FORM XI (PART 2) - IN
ILM04.0 49
DUP050307032
U.S. EPA - CLP
11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER._LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number: ____05478 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for: CR CU MN MO
NI
Aluminum_ Antimonyl Antimony2 Arsenic___ Barium BeryIlium Cadmium ___226.50
Calcium Chromium_ Cobalt____ Copper____ Iron Leadl Lead2 Magnesium Manganese
Mercury Nickel^___
Potassium Seleniuml Selenium2
Silver Sodium Thallium Vanadium_ Zinc
_0.0000000
_0.0000000
_0.0000000
-0.0000580
_0.0000000
Comments:
FORM XI (PART 2) - IN
ILM04.0
50
DUP050307033
U.S. EPA - CLP
11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: SAS No.: _______________________ SDG No.: FMD04
ICP ID Number: ____05478 ____
Date:
09/12/96
Analyte
Wave length
(nm)
Interelement Correction Factors for:
TI V
___
___
___
Aluminum_
Antimony! Antimony2 Arsenic___ Barium Beryllium Cadmium ___226.50 _0.0000000 _0.0000000 _0.0000000 _0.0000000 _0.0000000 Calcium Chromium_ Cobalt copper____ Iron Leadl Lead2 Magnesium Manganese Mercury___ Nickel___ Potassium Seleniuml Selenium2
Silver Sodium Thallium_ Vanadiura_ Zinc
A
Comments:
FORM XI (PART 2) - IN
ILM04.0
51
DUP050307034
U.S. EPA - CLP
12 ICP LINEAR RANGES (QUARTERLY)
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number: ____03144______
Date:
07/15/96
Analyte
Aluminum AntimonyArsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
Integ. Time
(Sec.)
7.00 7.00
7.00 7.00
7.00 7.00 7.00 7.00 7.00
7.00 7.00
7.00 7.00
7.00 7.00
7.00 7.00
Concentration (ug/L)
M
600000.0 p 200000.0 p
NR 100000.0 P
10000.0 P
NR 600000.0 P 100000.0 P 100000.0 P 100000.0 P 250000.0 P
NR 600000.0 P 100000.0 P
NR 100000.0 P 900000.0 P
NR 50000.0 P 900000.0 P
NR 100000.0 P 100000.0 P
Comments:
FORM XII - IN
ILM04.0
52
DUP050307035
U.S. EPA - CLP
12 ICP LINEAR RANGES (QUARTERLY)
Lab Name: LANCASTER_LABORATORIES____
Contract: ________________
Lab Code: _________
Case No.: _____________ SAS No.: _________ SDG No.: FMD04
ICP ID Number: ____05478______
Date:
07/15/96
Analyte
Integ. Time
(Sec.)
AluminumAntimony_ Arsenic Barium Beryllium
Cadmium Calcium Chromium Cobalt Conner Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver Sodium
Thallium Vanadium Zinc
10.00
Concentration (ug/L)
M
NR NR NR NR NR 20000.0 P_ NR NR NR NR NR NR NR NR NR NR NR NR
NR NR
NR NR NR
Comments:
FORM XII - IN
ILM04.0
53
DU P050307036
Preparation and Run Logs
54
DUP050307037
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________
Method: P
SDG No.: FMD04
EPA Sample
No.
3DDUP DIS2D DIS2S DIS2SD DIS2SS DIS3D DIS3S DIS4S FBK2D IDDIS ISDIS LCSW PBW
Preparation Date
09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96
Weight (gram)
Volume (ml)
100 100 100 100 100 100 100 100 100 100 100 100 100
FORM XIII - IN
ILM04.0
DUP0503 07038
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LANCASTER LABORATORIES
Lab Code:
Case No.
Method: F
Contract: SAS No.: _________
SDG No.: FMD04
EPA Sample
No.
3DDUP DIS2D DIS2S DIS2SD DIS2SS DIS3D DIS3S DIS4S FBK2D IDDIS ISDIS LCSW PBW
Preparation Date
09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96 09/25/96
Weight (gram)
Volume (ml)
100 100 100 100 100 100 100 100 100 100 100 100 100
FORM XIII - IN
ILM04.0
56
DUP05 0307039
U.S. EPA - CLP
13 PREPARATION LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: _____________ SAS No.: _________
Method: CV
SDG No.: FMD04
EPA Sample
No.
3DDUP DIS2D DIS2S DIS2SD DIS2SS DIS3D DIS3S DIS4S FBK2D IDDIS ISDIS LCSW PBW
Preparation Date
09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96 09/26/96
Weight (gram)
Volume (ml)
8 8 8 8 8 8 8 8 8 8 8 8 8
FORM XIII - IN
ILM04.0
57
DU P050307040
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name; LANCASTERJLABORATORIES
Contract:
Lab code: _________
Case No.;
SAS No. : _________ SDG No.: FMD04
Instrument ID Number; 03144_
Method: P_
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
As A B Bc c c c c F pMMHN K s AN TV z
LBs AE DAR0uE BGNG I E GAL N
SO S S S S ICV ICB CRI
ICSA ICSAB CCV CCB PBW LCSW DIS2S DIS2SA DIS2SD DIS2SS DIS2SL ISDIS
IDDIS DIS2D CCV CCB DIS4S DIS3S DIS3D 3DDUP FBK2D CRI ICSA ICSAB
1.00 1815 1.00 1818 1.00 1821 1.00 1824 1.00 1826 1.00 1829
1.00 1832 1.00 1835 1.00 1839 1.00 1842
1.00 1845 1.00 1848 1.00 1851 1.00 1854 1.00 1857 1.00 1900 1.00 1904 1.00 1907 5.00 1910
1.00 1913
1.00 1916 1.00 1919 1.00 1922 1.00 1926
1.00 1929 1.00 1932 1.00 1935 1.00 1938 1.00 1941 1.00 1944 1.00 1947 1.00 1951
XX X
XX X
X
XX XX
X
XX XX
XX XX XX XX XX
XX XX
X
XX XX XX XX XX XX XX
XX XX XX XX XX XX
XX XX
XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX XX
XX XX XX
zX X X X _ __
XXXXX X XX X
XXXXX XXXXX
XXX XXXXX XXXXX XXXXX XXXXX XXXXX XXXXX X XXXX
XXXXX XXXX
XXXXX XXXXX XXXXX XXXXX X XX X X XXXXX XXXXX XXXXX X XX X X XXXXX XXXXX
XXX X XX X X XXXXX
XX X
X XX XX
X XX XX XX XX XX XX XX
XX X
X XX XX X XX XX XX XX XX XX XX
XX XX
X _
X
X
X
XX XX X X -- X X ~~
X "" X X
XX XX
XX
XX--
XX XX --
XX XX
XX XX
X X " X X __ XX XX
XX X
XX
XX X XX
X X--X X X XX
--
XX XX
XX XX XX XX
XX XX XX XX
XX XX XX XX
XX XX XX XX
XX XX XX XX
XX XX
XX
X X "" X X
X X
X X
"
--
--
X X
X X
"
--
X X
X X
XX XX XX
mm.
XX--XX XX
XX XX XX
XX XX--XX XX XX
X X
X
""
X X
X X
zX X X X
FORM XIV - IN
ILM04.0
56o
DUP050307041
U.s. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Lab Code: _________
Case No.:
Instrument ID Number: 03144_
Start Date: 09/25/96
Contract: SAS No.: _________ SDG No.: FMD04 Method: P__ End Date: 09/25/96
FORM XIV - IN
ILM04.0
59
DU P050 307042
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No.:
'
SDG No. FMD04
Instrument ID Number: 05478_
Method: P_
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABB C c c c c F PMMHNKS AN TV z LBSAE DARoUE BGN GI EGAL N
SO
s
s s ICV
ICB CRI ICSA
ICSAB CCV
CCB PBW LCSW DIS2S DIS2SA
DIS2SD DIS2SS
DIS2SL ISDIS
IDDIS
DIS2D CCV
CCB DIS4S
DIS3S DIS3D 3DDUP FBK2D
CRI ICSA ICSAB
CCV
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
1.00 1.00 1.00 1.00 1.00 1.00 1.00
5.00 1.00 1.00 1.00 1.00 1.00 1.00
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
1140 1145 1149 1152 1156
1200 1205 1209 1214 1218 1222 1227 1231 1236 1240
1245 1249 1253 1258 1302 1307 1311 1316 1320
1324 1329 1333 1338 1342 1347 1351 1355
X
X
X X X X X X X X X X
X X X X X X X X X X X X X X X X X
~--
--~ ~
_-- _"
~--~
FORM XIV - IN
ILM04.0
60
DUP050307043
O.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: _ SAS No.: ______________________ SDG No.: FMD04
Instrument ID Number: 05478_
Method: P_
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBCCC C CF PMMHNKS AN TV Z LBS AE DAROU E BGN G I E GA L N
CCB
1.00 1400
X
FORM XIV - IN
ILM04.0
61
DUP050 307044
U.S. EPA - CLP 14
ANALYSIS RON LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 04724_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
A
L
s
B
A S
B A
B E
C D
C A
C R
C o
C
U
F E
P B
M G
M N
H
G
N
I
K
S E
A G
N A
T
L
V
Z N
SO
S10 S20
S40 S60 S80 ICV
ICB CRA
CCV
CCB ZZZZZZ
zzzzzz
ZZZZZZ
zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz
CCV
CCB
zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz zzzzzz
PBW PBWA LCSW
1.00 0415 1.00 0419 1.00 0424 1.00 0428 1.00 0432 1.00 0436 1.00 0440 1.00 0445
1.00 0449 1.00 0453 1.00 0457 1.00 0501 1.00 0505 1.00 0510 1.00 0514 1.00 0519 1.00 0523 1.00 0527 1.00 0532 1.00 0536 1.00 0540 1.00 0544 1.00 0548 1.00 0552 1.00 0557 1.00 0601 1.00 0605 1.00 0609 1.00 0614 1.00 0618 1.00 0622 1.00 0626
X
X X X X X X X X X X
93.2
X X X
__
_. _
~
FORM XIV - IN
ILM04.0
DU P050307045
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER..LABORATORIES.
Contract:
Lab Code: _________
Case No.:
SAS No.: _____ SDG No.: FMD04
Instrument ID Number: 04724_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASAB BC CCC c F PMMHNK S AN TV Z L BSAE DAR0U E BGN G I E GA L N
LCSWA CCV CCB DIS2S DIS2SA DIS2SD DIS2SDA DIS2SS ZZZZZZ
ISDIS ISDISA IDDIS IDDISA CCV CCB DIS2D DIS2DA DIS4S DIS4SA DIS3S
DIS3SA DIS3D
DIS3DA 3DDUP 3DDUPA CCV CCB
1.00 0630 1.00 0634 1.00 0638 1.00 0642 1.00 0646 1.00 0651 1.00 0655 1.00 0659
1.00 0703 1.00 0707 1.00 0711 1.00 0715 1.00 0719 1.00 0723 1.00 0727 1.00 0731 1.00 0736 1.00 0740 1.00 0744 1.00 0748
1.00 0752
1.00 0757
1.00 0801 1.00 0805 1.00 0810 1.00 0814 1.00 0818
98.9
91.2 97.8
117.2 49.0
103.2 70.2 88.2
127.7 64.8
X X X X X X X
X X X X X X X X X X X X X X
A
FORM XIV - IN
ILM04.0
63
DUP0503 07046
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No.: _________ SDG No. : FMD04
Instrument: ID Number: 04724_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS A BB C C C C C F PMMHNK S AN TV Z LBSAEDAROUE BGNG I E GAL N
so S10 S20 S40 S60 S80 ICV ICB CRA CCV
CCB ISDIS
ISDISA FBK2D FBK2DA CCV CCB
1.00 1138
1.00 1142 1.00 1147
1.00 1151 1.00 1155 1.00 1159 1.00 1204 1.00 1208
1.00 1212
1.00 1216
1.00 1220 1.00 1224 1.00 1229 1.00 1233 1.00 1237 1.00 1242 1.00 1246
105.4 85.8
X X X X X X X X X X X X X X X X X
FORM XIV - IN
ILM04.0
64
DUP050307047
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER__LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No. : _________ SDG No. : FMD04
Instrument ID Number: 04724_
Method: F_
Start Date: 09/26/9(5
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS ABBC C C C C F PMMHN KS AN TV Z LB SAE DAROuE B GNG I E GA L N
SO S10 S20 S40 S60 S80 ICV
ICB CRA CCV
CCB ISDIS0 ISDIS1 ISDIS2 ISDIS3 CCV CCB
1.00 1619 1.00 1621 1.00 1623
1.00 1625 1.00 1627 1.00 1630 1.00 1632
1.00 1634 1.00 1636 1.00 1638 1.00 1640 1.00 1642 1.00 1644 1.00 1647 1.00 1649 1.00 1651 1.00 1653
X X X X X X X X X X X
X X
FORM XIV - IN
ILM04.0
65
DU P 050307048
U.S. EPA - CLP 14
ANALYSIS RON LOG
Lab Name: LANCASTER__LABORATORIES____
Contract:
Lab Code: _________
Case No.: __________ SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 04724_
Method: F_
Start Date: 09/26/96
EPA Sample
No.
SO S10 S20 S40 S60 S80 ICV ICB CRA CCV CCB IDDISO IDDIS1 IDDIS2 IDDIS3 CCV CCB
D/F
Time
1.00 1724 1.00 1726 1.00 1728 1.00 1730 1.00 1732 1.00 1735 1.00 1737 1.00 1739 1.00 1741
1.00 1743 1.00 1745 1.00 1747
1.00 1750 1.00 1752 1.00 1754 1.00 1756 1.00 1758
%R
End Date: 09/26/96
Analytes
ASABBCCCC CFPMMHNKSANTVZ L B S A E D A R o TJ E B G N G I E G A L N
X X X X X X X X X X X X X X X X X
FORM XIV - IN
ILM04.0
66
DUP050307049
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_JLABORATORIES.
Contract: _______.
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 03812_
Method: F_
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS A BB C C C C C F PMMHN K S ANTV Z LB SAE DARoUE BGNG I E GAL N
SO
S5
S9
S15
S30
S60
ICV
ICB
CRA
ZZZZZZ
CCV
CCB
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
CCV
CCB
A
ZZZZZZ ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
ZZZZZZ
1.00 1625 1.00 1630
1.00 1635
1.00 1640 1.00 1645 1.00 1650 1.00 1654 1.00 1659 1.00 1704 1.00 1708 1.00 1713 1.00 1718
1.00 1722 1.00 1727 1.00 1732 5.00 1736 5.00 1741
5.00 1746 5.00 1750
5.00 1755
5.00 1800 1.00 1805
1.00 1809 1.00 1814 1.00 1818 1.00 1823 1.00 1827 1.00 1832 1.00 1837 1.00 1842 1.00 1846 5.00 1851
FORM XIV - IN
ILM04.0
67
DUP050307050
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES.
Contract: _
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 03812_
Method: F_
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS A B BC C C C C F PMM HN K S A N TV Z LB S AE DAROuE B GN G I E GA L N
ZZZZZZ ZZZZZZ CCV
CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ PBW PBWA LCSW
LCSWA CCV CCB DIS2S
DIS2SA DIS2SD DIS2SDA DIS2SS ZZZZZZ
ISDIS ISDISA IDDIS IDDISA CCV
CCB DIS2D DIS2DA DIS4S DIS4SA
1.00 1855 1.00 1900 1.00 1905
1.00 1909
1.00 1914 1.00 1918 1.00 1923 1.00 1928
1.00 1932 1.00 1937
1.00 1941 1.00 1946 1.00 1951
1.00 1955 1.00 2000 1.00 2005
1.00 2 009
1.00 2014 1.00 2019 1.00 2023 1.00 2028 1.00 2033 1.00 2037 1.00 2042 1.00 2047 1.00 2052 1.00 2056
1.00 2101 1.00 2105 1.00 2110 1.00 2115 1.00 2120
101.2 90.2
60.8 62.8
77.2 55.7
74.1 27.6
FORM XIV - IN
ILM04.0
68
DUP050307051
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANGASTER_LABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 03812_
Method: F
Start Date: 09/25/96
End Date: 09/25/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASA BB CCCC C F PMMHN KS ANTV Z LBSAE DAROuE BGNG I EGAL N
DIS3S DIS3SA DIS3D
DIS3DA 3DDUP 3DDUPA CCV CCB FBK2D FBK2DA CCV CCB
1.00 2124 1.00 2129
1.00 2134
1.00 2139 1.00 2143 1.00 2148 1.00 2153 1.00 2157 1.00 2202 1.00 2207 1.00 2211 1.00 2216
64.1 61.4 72.6
107.1
FORM XIV - IN
ILM04.0
69
DU P050307052
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES
Contract:
code: _________
Case No. :
SAS No.: _________ SDG No. FMD04
Instrument ID Number: 03812_
Method: F_
Start Date: 09/25/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS A BBCCC C C F PMMHNKS ANTVZ LBS AE DAR0UE BGNGI E GAL N
SO S3 S9 S15 S30 S60 ICV ICB CRA ZZZZZZ ccv CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ PBW PBWA ccv CCB LCSW LCSWA DIS2S DIS2SA DIS2SD DIS2SDA DIS2SS ZZZZZZ
1.00 2334 1.00 2339 1.00 2344
1.00 2348 1.00 2353 1.00 2358 1.00 0003 1.00 0007 1.00 0012 1.00 0017 1.00 0021 1.00 0026 5.00 0031 5.00 0035 1.00 0040 1.00 0045 1.00 0049 1.00 0054 1.00 0059 1.00 0104 1.00 0108
1.00 0113 1.00 0117
1.00 0122 1.00 0127 1.00 0131 1.00 0136 1.00 0141 1.00 0145
1.00 0150 1.00 0154 1.00 0159
103.2
98.6 68.6 69.6
X X X X X X X X X
X X
X X X X X X X X X X X
FORM XIV - IN
ILM04.0
70
DUP050307053
U.S. EPA - CLP
14
ANALYSIS RUN LOG
Lab Name: LANCASTERJLABORATORIES
Contract: _______________
Lab Code: _________
Case No.:
SAS No.: _________ SDG No. FMD04
Instrument ID Number: 03812_
Method: F_
Start Date: 09/25/96
End Date: 09/26/96
EPA Sample
No.
ISDIS
ISDISA CCV CCB IDDIS IDDISA DIS2D DIS2DA
DIS4SA DIS3S DIS3SA DIS3D DIS3DA CCV
CCB 3DDTJF 3DDUPA FBK2D FBK2DA
CCV CCB
~
D/F
Time
1.00 0203 1.00 0208
1. 00 0213 1.00 0217 1.00 0222 1.00 02 27 1.00 0231 1.00 0236 5.00 0240 5.00 0245
1.00 0250 1.00 0254 1.00 0259 1.00 0304 1.00 0308
1. 00 0313 1.00 0318 1.00 0322 1. 00 0327 1.00 0332
1.00 0336 1.00 0341
%R
Analytes A S A B B C C C C C F P M. M H N K S A N T? V z LB SAEDAROUEB GNG I EGAL N
76.0
47.8 74.2 79.0 76.0 75.3
67.9 W7Z
X
X X X X X X X X
X X X X X X
--
X X X X
X X
~ ~ ""
--* ""
-- _
---- "" -- --
"" "" -- --
----
1 *-- --
FORM XIV - IN
ILM04.0
71
DU P050 307054
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES___ _
Contract:
Lab Code: _________
Case No.: SAS No.:
' SDG No.: FMD04
Instrument ID Number: 04725_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
AS AB B C C C C C F PMMHN KS AN TV z LBSAE DARoUEB GNG I E GA L N
SO S5 S15 S25
S40
S50
ICV
ICB
CRA CCV
CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV
CCB
ZZZZZZ A ZZZZZZ
ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ
ZZZZZZ ZZZZZZ ZZZZZZ
1.00 1.00 1.00 1.00 1.00 1.00
1.00 1.00
1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 5.00 5.00 5.00 5.00 5.00
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00
1546 1550 1554 1558 1602 1606
1610
1614 1618 1622 1626 1630 1635 1639 1643 1647 1651 1656 1700 1704 1708 1712 1716
1720 1724
1728 1732 1736 1740 1745 1749 1753
__ _ _
_
X X X
X X X X~
X
X X X
--~
X X
--
FORM XIV - IN
IIM04.0
72
DU P0 50307055
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES.
Contract:
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: FMD04
Instrument ID Number: 04725_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASAB BC CC C c F PMMH N K S AN T V z LBSAE DARODE BGNG I E GA L N
ZZZZZZ CCV
CCB ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ PBW PBWA LCSW LCSWA CCV CCB DIS2S DIS2SA DIS2SD DIS2SDA DIS2SS
ZZZZZZ ISDIS ISDISA IDDIS
IDDISA CCV CCB DIS2D DIS2DA DIS4S DIS4SA DIS3S
5.00 1757
1.00 1801
1.00 1805
1.00 1808
1.00 1812
1.00 1817
1.00 1820
1.00 1825
1.00 1829
1.00 1833
1.00 1837 109.8
.1.00 1841
1.00 1845 120.2
1.00 1849
1.00 1853
1.00 1857
1.00 1901 -9999.9
1.00 1905
1.00 1909 -9999.9
1.00 1914
1.00 1918
1.00 1922
1.00 1926 107.9
1.00 1930
1.00 1935
88.0
1.00 1939
1.00 1943
1.00 1947
1.00 1951 102.7
1.00 1955
1.00 1959
97.7
1.00 2003
X X
X X X
X X X
"------
X
X X X X X
X X X X
-- --
FORM XIV - IN
ILM04.0
73
DUPO 50307056
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTERJLABORATORIES____
Contract:
Lab Code: _________
Case No.: SAS No.: _______________________ SDG No.: FMD04
Instrument ID Number: 04725_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBCC CCC FPMMHNKS ANTVZ LBSAE DAR0UE BGNG I E G AL N
DIS3SA
DIS3D DIS3DA
3DDUP 3DDUPA CCV CCB FBK2D FBK2DA CCV
CCB
1.00 2008 -9999.9
1.00 2012 1.00 2016 113.6 1.00 2020 1.00 2024 121.0 1.00 2028 1.00 2032 1.00 2036 1.00 2040 126.4 1.00 2044
1.00 2048
X X X X X X X X X X
FORM XIV - IN
ILM04.0
74
DUP050307057
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER__LABORATORIES
Contract:
Lab Code
Case No
SAS NO.: _________ SDG NO.: FMD04
Instrument ID Number: 04725
Method: F
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
so
S5 S15 S25 S40 S50 ICV ICB CRA CCV CCB ZZZZZZ
zzzzzz
DIS2S DIS2SA DIS2SD DIS2SDA DIS2SS ZZZZZZ DIS3S DIS3SA CCV CCB
Analytes
D/F
Time
%R
ASABBCC CC cF PMMHNKSANTVZ LBSAE DAR0uE BGNG I EGAL N
1.00 2213 1.00 2217 1.00 2221 1.00 2225 1.00 2229
1.00 2233 1.00 2237 1.00 2241 1.00 2245 1.00 2249 1.00 2253 2.00 2257 2.00 2301 5.00 2306 5.00 2310 111.6 5.00 2314 5.00 2318 ___116.3 5.00 2322 5.00 2326 5.00 2331 5.00 2335 115.1 1.00 2339 1.00 2343
____
X X X X X X X X X X X
X X
X
X X
A
FORM XIV - IN
ILM04.0
A
75
DUP050307058
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_JLABORATORIES
Contract:
Lab Code: _________
Case No.:
SAS No. : _________ SDG No.: FMD04
Instrument ID Number: 04725_
Method: F_
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABBCCCC cFPMMHNKSANTVZ LB SAE DAR0uE BGNG I E GAL N
SO S5 S15 S25 S40
S50 ICV ICB CRA CCV CCB ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1
ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 ZZZZZZO ZZZZZZ1 ZZZZZZ2 ZZZZZZ3 DIS2SD0 DIS2SD1 DIS2SD2 DIS2SD3 CCV
1.00 0112 1.00 0114 1.00 0116 1.00 0118 1.00 0120
1.00 0122 1.00 0125 1.00 0127 1.00 0129 1.00 0131 1.00 0133 10.00 0135 10.00 0137 10.00 0139 10.00 0141 5.00 0143 5.00 0145
5.00 0147
5.00 0149 5.00 0151 5.00 0153 5.00 0155 5.00 0157 5.00 0159 5.00 0200 5.00 0202 5.00 0204 10.00 0206 10.00 0208 10.00 0211 10.00 0213 1.00 0215
X X X X
X
X X X X X X
X X X X X
FORM XIV - IN
ILM04.0
76
DU P0 50307059
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES_
Contract:
Lab Code: ________
Case No.:
SAS No.: _________ SDG No. FMD04
Instrument ID Number: 04725
Method: F
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
A SA B BC C CC C F PMMHN KS AN TV Z LBSAE DAR0UE BGNG I EGAL N
CCB DIS3S0 DIS3S1 DIS3S2 DIS3S3 CCV CCB
1.00 0217 10.00 0219 10.00 0221 10.00 0223 10.00 0225
1.00 0227 1.00 0229
X X X X X X X
FORM XIV - IN
ILM04.0
77
DUP050307060
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER,LABORATORIES.
Contract:
Lab Code: _________
Case No.:
SAS No. : ______ __ SDG No.: FMD04
Instrument ID Number: 02803_
Method: F_
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes ASAB BCC CC CFPMMHNKS ANTV z LBS AE DAROuE B GNG I E GA L N
SO 1.00 0344
S10
1.00 0348
S20
1.00 0351
S40
1.00 0355
S60
1.00 0359
S80
1.00 0402
ICV
1.00 0406
ICB
1.00 0409
CRA
1.00 0412
ZZZZZZ
1.00 0416
CCV
1.00 0419
CCB
1.00 0423
PBW
1.00 0426
PBWA
1.00 0430 106.6
LCSW
1.00 0433
LCSWA
1.00 0436 106.3
DIS2S
1.00 0440
DIS2SA
1.00 0443
91.8
DIS2SD
1.00 0446
DIS2SDA
1.00 0450 102.3
DIS2SS
1.00 0453
ZZZZZZ
1.00 0457
A CCV
CCB
1.00 0500 1.00 0503
ISDIS
1.00 0507
ISDISA
1.00 0510
95.8
IDDIS
1.00 0513
IDDISA
1.00 0517
94.0
DIS2D
1.00 0520
DIS2DA
1.00 0523
94.4
DIS4S
1.00 0527
DIS4SA
1.00 0530
88.2
X X X X X X X X X
X X X X X X X X X X X
X X X X X X X X X X
FORM XIV - IN
ILM04.0
78
DUP050307061
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER .LABORATORIES,
Contract:
Lab Code:
Case No
SAS No.: ______ __ SDG No.: FMD04
Instrument ID Number: 02803
Method: F
Start Date: 09/26/96
End Date: 09/26/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASABB C C C C c F PMMHN KS ANTV z LBSAE DAR0uE BGNG I E GAL N
DIS3S
DIS3SA
CCV
CCB DIS3D DIS3DA 3DDUP 3DDUPA FBK2D FBK2DA CCV CCB
1.00 0533 1.00 0537
1.00 0540
1.00 0543 1.00 0547 1.00 0550 1.00 0553 1.00 0557 1.00 0600 1.00 0604 1.00 0607 1.00 0611
97.0
100.0 101.4 117.1
X
X X X X X X X X X X X
FORM XIV - IN
ILM04.0
A
79
DUP0503 07062
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES.
Contract:
Lab Code: _________
Case No.:
SAS No.: _________ SDG No.: HMD04
Instrument ID Number: 61734_
Method: CV
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASAB BC C CC c F pMMHNKSANTVZ
LB S AEDAR0 UE BGNG I E GAL N
SO 1.00 1209
SO. 2
1.00 1211
SO.5
1.00 1214
S1.0
1.00 1216
S2.5
1.00 1219
ICV
1.00 1222
ICB
1.00 1225
CRA
1.00 1227
CCV
1.00 1229
CCB
1.00 1232
PBW
1.00 1234
LCSW
1.00 1236
ISDIS
1.00 1239
IDDIS
1.00 1241
DIS2D
1.00 1244
A DIS2S
1.00 1246
DIS2SD
1.00 1248
DIS2SS
1.00 1250
DIS4S
1.00 1253
DIS3S
1.00 1255
CCV
1.00 1257
CCB
1.00 1300
DIS3D
1.00 1302
3DDUP
1.00 1304
FBK2D
1.00 1307
ZZZZZZ
1.00 1309
ZZZZZZ
1.00 1311
ZZZZZZ
1.00 1313
ZZZZZZ
1.00 1316
ZZZZZZ
5.00 1319
ZZZZZZ
1.00 1321
CCV
1.00 1324
X X X X X X X X X X X X X X X X X X X X X X X X X
X
FORM XIV - IN
ILM04.0
80
DUP050307063
U.S. EPA - CLP 14
ANALYSIS RUN LOG
Lab Name: LANCASTER_LABORATORIES____
Contract:
Lab Code: _________
Case No.: SAS No.: ______________________ SDG No.: FMD04
Instrument ID Number: 61734_
Method: CV
Start Date: 09/27/96
End Date: 09/27/96
EPA Sample
No.
D/F
Time
%R
Analytes
ASAB BC C CC C F PMMHNKS ANTV Z LBS AE DAR0UE BGNG I EGAL N
CCB
1.00 1326
X
FORM XIV - IN
ILM04.0
81
DUP0503 07064
Raw Data
82
DUP050307065
ICP Data
83
DUP050307066
page:
LANCASTER LABORATORIES -
Run.Name: 9626903161.
... . INSTRUMENT ID: 03144
Tube: 1 SO
09/25/96
18:15 '
, -. ELEM
CQNC (ppm)
AVG INTENSITY (COUNTS)
%RSD
/ #1 '_
INTEGRATIONS #2
#3
Ac 0.000
___Ai .
0.000 .
As. ' 0.000 .
"___B*
0.000
.___Ba . . 0.000
' __.Be
0.000
Ca V 0.000
___Cd
0.000 '
Co 0.000
__Or.
0.060 -
; Cu
6.000
Fe' , 0.000
'
0.000
Fla 0.000
tin 0.060
' ` Mo
0.000
;__Na
0.000 .
___Ni-'
0.000
. Pb j 0/.000
5,66666 44,41 . ' 6.00000
. 10.00000 52.91
8.00000
-12.00000 221 ;s
-40.00000
2i66666 216.5;
6.00000
0.00000 O'
b.j00000
2.00000 0
2.00000
' .4.00000- ' 132.2. -.../ 0.00000, '
; -O '. 33333 173.2
0.00000
--0,66666 . 173.2
.0.00000.
1 ..33333 86.60
2.obooo
0.. 33333' 754.9
-. 0.00000
10.66666 "19,-51
. 13.00000
5.00000 34.64
. 6.00000
' 19.33333 20'. 90-
-17.00000
. 2.00000 0 . '
2.00000
1.66666 91.65 :.
3.00000
--36.66666 35.06 -42.OOOOO
,3.66666 56.77
6.00000.
. ; 2.66666 . 169.. 0
3.00000
3.00000 16.00000 -9.00000
6.00000 0.00000 ,.2.00000
lO.'OOOOO . -1 .000.00
-2.00000 '2.00000 -2 . OOOOO19.00000 3.OOOOO '24.00000 ' 2.00000 . 2.00000 -46-. OOOOO . 2.00000 -2.00000
8.00000 '6.00000 13.0.0000 -4.00000
0.OOOOO ' 2.00000
2.00000 0'.OOOOO 0.00000 0.00000 .3.00000 . 10.00000 6.00000 17.OOOOO 2.OOOOO 0.00000 -22.OOOOO .3.00000 7.00000
__:Sb " . 0.000
' -8.66666 .259.3
-14;OOOOO
-2.8.00000 .
16.00000
A;i_Se r , 6-.000 : '
10.66666 ".156.1
-16.00000..- , 24.00000 -, - .-Q.00000
__Si ' '0,000.
23.33333 17.84 \'20..QOOOa : " .22.00000 . 28.00000
;;:_Sn
0,000'
0.66666 173.2- .
0.00000
2.00000
0,00000
-.1 -'Sr'. 0.000 .-" *' . O.OQOOO O
0.00000
0.00000.
0.00000
. __Ti : ' 0.000.,
8.66666. ,24.01 .
7.00000
8.00000
11'.00000
' Ti
'0.000
2.66666 43.30
2.00000
2.00000
" 4.00000
'7. 0.000
3.33333 '34.64
- 4.00000-
2100000 . ' -4.00000
' ;zn: 0.000
' 3.66666 13..74
4.00000 '
4.00000
3.*00000
', . - `i'
L '- j
'! ;
84
DUP050307067
UANCftSTtR tftBQRAVOAIfctt
; Name:
9626903161 s'l b
09/25/96 '
18:18
INSTRUMENT ID: 03144
AVG
,00 NC
INTENSITY
;M
(ppm)
(COUNTS)
%.RSD '
#i
INTEGRATIONS
#2-
'
#3
10.000
16132.00000 0.833 15985,00000
16162,00000
16249.00000
10.000
26537.00000 0.564 26369,OOOOO 26657.00000 26585.00000
10.000 .
6192.33349 1.082
6121.00000
620,2.00000
6234.00000
V 10.000 10.000
10359.00000 1.008 16-430.00000 0.988-
10249.00000 16259.00000
10371.00000 16449.00000
10457.00000 16582.0.0000
111 10.000
6394.33349 1.032 -6324.00000
6404.00000
6455.00000
ic 50.000
66106.33593 0.939 65394.00000 66393.00000 66532.00000
20.000
20791.33398 0.940 . 20580.00000 20828.00000 20966.00000
SOI000
. 25445.66601 0.983 .25182.00000 25475.00000
25680.00000
10.000-
20369.66601 1.003 ' 20148-. OOOOO 20410.00000 20551.00000
8.5
DUP0503 07068
page: l .
LANCA8T Eft LABORATORIES
Run feme: 9626903161
INSTRUMENT Ip: 0314l
Tube: 3
S2 5
09/25/96
18:21
E.LEM
' CO NO ( ppm )
AS 5.00b
__.Be
1.000
Co 2.000
__Sb 10.000 --
Se 5.000
;__Si . 5.000
Sn 10.000
___Sr ; l.ooo .
....Ti
5.000
___T i 10.000.
V '' ' 5.000
' AVG INTENSITY
(COUNTS)
%RSD
" #1
INTEGRATIONS #2
#3
S188.00000. 1'. 134 977.66668 0.413
'1508.00000 0.303 17165.00000 Oi 627 - 5325.00000 0.379
6118.66650' . 0.287 1425.66662 0.359 11037.66699' ' 0.317 5561.66650 0.340
579.OOOOO 0.456 8303.33300 ' 0.248
8294 J00000 980.00000
1512.00000 17137.00000 ; '5340.00000 . 6135.00000
1430.00000 -11072.00000 "
5575.00000 .581,00000 ' . 8311.00000,
8121.00000 980.00000
1509.00000 17284.00000
5333.OOQOO ' 6121.00000 1427.00000 11039.00000 5570.00000
580.OOOOQ 8319.00000
8149.00000 973.00000 1503.00000
17074.00000 5302.OOOOO 6100.00000 1'420. OOpOO
11002.00000 5540.00000 576.00000 8280.OOOOO
86
DUPO 50307069
LANCttS'l ER LABO&H 'I ORI tS
-i Name: 9626903161
INSTRUMENT ID: 03144
4 S3 S
09/ 25 796
18:24
CONC ... ( ppm )
AVG INTENSITY (COUNTS)
. %RSD
#1
INTEGRATIONS .82
- . 83
862.00000 0.232 -
862.00000 . . 864.00000
3600.66674 0.4S2 ' -3612 ..00000
3582.00000
. 860.00000 . 3608.00000
\
87
DUP050307070
LANCASTER LABORATORIES
Run Name: , 9626903161
Tube: 5
S'4 5"
09/25/96
18:26
) : 03144
ELEM
CONC (.ppm)
__A1ca K
___Mg ___NA
50.000 100.000
500.000 100i000 590.000.
AVS INTENSITY (COUNTS);
:. %RSD
#1 .
22692,00000 . 1.299 113682.33593 1.254
8440.66699' 1.510 41245'. OOOOO '1.202
349716.34375 1.231
*'22356.00.000 112063.00000 8295.00000 40661.00000 344852.00000
INTEGRATIONS
42
43'
22812.00000 114234.00000.
8495.00000 41367.00000 351258.00000
22908.00000 114750.00000
8532.OOOOO 41617.00000 353039.00000
. . ' -
r .
*-V: :v . I.-V
88
DUP050307071
Page :
LANCASTER LABORATORIES
f
.Run Name-: Tube: 6
9626903161 ICV
09/25/96
18:29
INSTRUMENT ID: 0614*3
ELEM-
AVG. (.ppm.).
%RSD
INTEGRATIONS
#1
: #2
#3 "
REREAD REDIG
Aa
AL As e ' Ba Be ;__Ca .. Cd ;' ' Co.. ; " Cr ` Cu
' Fe K.
-. .Mg Mn' '
___Mo Na Ni ..
___Pb . Sb '
_i.Se __Si Sn -
Sr '
..___Ti ___Tl-
__y __Zn
0.57014 0.720 .
; 0.57052 -
30.68478 0.289
30.60288 "
2.28607 1.193 ,
2.31041
. 1.36032 0.2/5 .
1' 135600 -
. 5.83684 0.139
5.82940
0.58594 0.200
0.58525- .
62.58642 0.231
62.45800
. 5.76820' 0.255
. 5.78340 '
1.13968 0.464
1:14498
5.86706 0.244 '
5.85575 .
5.90962 0.210 .
5.90449
5.89470 0.236
: 5.88759 :
61.52447 0.481
'61.22811
30.94850 0. 198
30.93713 '
5.84269 0.218
5.83695
29.79819 0.092
29.77349
61.93701' 0.212 .
. 6i.90985
11.60525 0.179
11.59268
29.12100' 0.191 . 29.09490
. -5.89179 0.314- ..... "5:88964 :
' 2.32791 0.420. ..
2..33105
4.85934 4.246
- ' 4.63858..
. 5.75691 0.494
5-. 72640
1.18977 0.194
1.18956
2.38819 0.135
.. 2.38729
' 6.09858 0.866 '
6.14542
2.36581 0.177
2.36608
3.87096 0.203
5.85940
0.56585
0.57404
30.67245
30.77902
2.29124 -..
2.25657
' 1.36215 ..... * 1.36279
5.84552
5.83560
0.58526
0.58730
- 62.- 55740
62.74388
5.75401
5.76720
1.13439
1.13966
.5.86222-
5.88321
5.90059
5;92378
5'. 88576: .
5.91074-
61.52447
.61.82083
30.89342
31.01496
5.83383
5.85729
- - 29.827.94
29.79315
. 61.82123
62.07995
IT . 59376-
- 11.62929
. 29.08300
' 29;18511
. 5.91133 . / 5.8.7440 ; -
. 2.31693 ' ' : '2.'33575.' '
/ 4.89210
5.04732
r-
5.78281
'5.76152-
1.18756
; 1..19219
2.38549 '
2:39180 .-
' 6,04129
.6.10903
2.36148
;2.36987
5.87020
5.88329
...89
DUP050307072
Page: 8
LANCASTER LABORATORIES
Run Name: 9626903161 Tube : 7- ICB
09/25/96
18:32
INSTRUMENT lb:. 03144
ELEM
AVG .(.ppm}
' %RSD
-' . #1
INTEGRATIONS #2
'Aa
-0.00194 119.8
0.00038' ' -0.00428
___Al
0.02472 13.59
0.02174-
0.02836
___As
0.00072 2054. .
0:01700
-0.00253
B' ' -
0.'60924. .24.17 1
0.01127
.. 0.00962
___Ba
0.00185 57.73-
0.00309
0.. 00123
' 6e
0.00000 52.79
0,00000'.
0.00000
___Ca-
0.03548 12.72 '
0.04047
0.03431
__Cd '
0.00213 -81:49
0.00.314
. 0:00314`
;___Co . ' - : 0.00354 74.80
0.00619
0.00089
__Cr ' . ; -0.00214150.2
-0.00537
-0.00214-
... Cu.
: . 0100772 7.244
0.00836
0.00739
. Fe-' ^
' -O..00122 57.42
-0.00163
-0.00041,
___K
-
0.07902 263.3
-0.ii854
0.05927
___Ma
'iv ' 0.02025 54.14
6.03078 ' .
0.021-06
_Mn-
0,00261 91 .,47
.0.00469
- 0.00313
'___Mo
. 0.01991 17.40
0.02369
0.01916'
__Na -
0.07246.51.59 0-.09819 -
0.08962
N1 ,, :..
,-0.66228'84-.33
0.004.20': .
0.00228
' -Pb-
> 6.01311 75.38
0.01445
0.02226'
:i,^fir---:YQi00748 193.9 i
0.Q2367 . .... ,0.00318
: _j3i- . >
_Sn..
, 0.00752- 208.1 Hr '0 i 05110 28.12 '
-0.01392 58! 53
0.01254
0.06611 -0.00451 -.
/ -0.01003
, 6..04973 "-0.01861
:_Sr -. ' ' v 0.00024. 43.30
0.00036
0.00018
" '' f i ' -
-61.0.0690 0. '
-0.00690
-0.00690
' __T1 . `
___V,
.
-0.06947 103.9
-0.01172
-6.0017452.79 -0.00254
-0.15044 -0.00194
' _L_Zn -
0.0017731.56 0.00209
0.00210
#3 REREAD REDIG
. -0.00194'__; 0.02405 __
-0.01229 ___ 0.00684'__ 0.00123 __ t>. 00000 =__
. 0.03166 __. .0.00012 __ 0.00354 _ 0.00108 0.00740- __l
, -0.00163 0.29636___ 0.00890 0.00000 __ 0.01689.. __ 0.02957'__ 0.00035 __ 0.00262 _
-O.0644O __ 0.02007 _ . 0.03/46__ '..-0,01864 __ ' 0.00018 -0.0069.0 __ -0.0462S __ -0.00073 __
0.00112
90
DUP050307073
!
LANCASTER LA BO RA T 0 RIE S
Run Name; . 9626903161 8 OR I
09/25/96
18:35
INSTRUMENT ID: 03144
i .'*1
- AVG (ppm )
%RSD
#.1
INTEGRATIONS. #2
#3 . REREAD REDIG
,0l02143 10.89
O.02377
.
0.00494 156.2
0.01299
Mcf.
0.01653 52.78
0.00898
0.00687 40.70
0.00391,
0.00061 100
0.00061
;e
' - 0.01003 0.014'
. 0.01002
/
0> 0078Q 40.63
. 0.01044
i ;a ' 6.01018 8.547
0.01068
c>
0.10337 1:480 .
0.10160
. r .
,, 0.01828 10.20 .*
'0.01720
\;u ' 6.05582 1.728
0.05582
e - ' ' -0.00467 22.57
-0.00406
is .. . ' 0.01975 346,4
-0.05927
pg
0.01550 54.98
0.01631
;_rHn : 0.03131 . 0.001
0.03131
..... Mo . . - 0.00479 31.57
0.00&30
M.-js
0.01432 46.06.
0.01814
r-1 i
0.08259 4.092
.0.08292:
H b . 0.00861 69.56 Oi 01514
"....Sb M.' 6.12912 O'. 822 . ;
0.12980
*S'' ** ~ Si" ' '
0.02069 164.-1,. . 6.02150 15.96' :
0.01348 0.02039
__Sn
-0.00432 32510
0.00972
__Sr `
' 0.00012 43.30.
. 0.00009
T i -0.00630 16.49 : v -0:.00690
I
-0.02716 195.6
' -0.01561
0.10129 0.680
0.10170
Vi
0.04132 1.401'
0.04100
0.01910 -0.00241
' 0.02143 _________________
0-00425
_'
0.01453
0.02609
, O1.00947'
' 0.00724 ______ ________
0.00123
0.00000 _________ ________
0.01003
0.01002 __
. 0.00868
0.00428 __________________
0.00917
0.01068 6
. 0.10425 0.02043' '
0.10426 0.01720 ' '
'
0.05679
0.05486 _________ ________
-0.00406 , -6.00589__
0.05927 -
.0.05927 _______
> O;.02-359. ' ' 6.03131
0.00660 ;_________ 0.03131 . .
' -
' 0.00479
0.00327
. .0:01813
0.00670 _______
0.08580 '0-00731 .
0..07906 0.00337
,_______
' O. 12967 . ,0.05770 .0.02535 ;
O'. 12790 -0.0690*9
0.01875 -
________
-0.00432 ;
o.00009
-0.01836 ' _____
. oroooie
,
-0.00510 -0.08515
0.10050
-0.00690 _______ ________ 0.01926 ' - " - .
' 0.10168 ________ ______
0.04098
0.04199 ______
A
DUP050307074
Page: 10
LANCASTER- LABORATORIES
Run Name: Tube: 9
9626903161 ICSA "
'
\ - 09/25/96 \
'. INSTRUMENT - ID:* 03144 18:39
ELEM
" AVG (.ppm)
' %RSD
#1
INTEGRATIONS ' #2 .
#3 REREAD'REDIG
__Aa:-.
-0:00884 15.64
--0.00914
"-O.00733
-0.01004
___A1
506.16058 0.596
503.06185
509.09542
506.32446
___As' '
-0.2-1023 1.9.37
-0.17653
-O'.25551
-6.-19867-
^.
, O'.08886'.2.179-0.0866:3 .-. ,0.09017- . - 0.08977
___Ba
' 0.00702 10.18 '.
0.00743
0.00743
'0.00619
J_Be :
'-0:60204' 0,219
. Ca . .-T - . 4$1.00122- 0.612-
-0.00204. 487.88891
-0.00205 493.89270
-0.00204 491.22201
....Cd -
-0:00159 103; 6 '..,-0.00117
' -6.00342
' -0.00019
- 4 . Co
-0.00131-325.2
-0.,0044.0.
.. -0.00307
0.00355 -
'___Or
^ , 0.00229 801.33
Cu `
1 ` O.:06'484. 7i .24
- r 184.80996 0.497 '
. 0.00442 . O . 00759
183.96868
0.00124 0.00597 .185'. 79275-
' 0.00121 0:00097
184.66847
K /-'
0.01975' 916.5 ' '
0.05927
0.-17.781
-0.17781
' ' Mg ** ' 'T 51858941 0.480 -
516.23315
521-.-19970 - 518.-33532 "
Hn 1
- Mb
-
-0.00423 1.177-0106554 20.82
-0.00418 -O'. 00428
-0.00428 -0.00579
-0.00423 .-0.00655
Na
0.08008 23.02
'0.08532
0.09533'
0.05960 -
. . Ni-' W-* .-0..01122 14.93 ' -0.01025 .'
-0.01026
-0.01316
-__Pb
v . ' 0.00190 988.5
: O'. 01410 .
0.0.1137
" -0.01976
,{>*&
85.92./ -, . -0.02284
-0.0i.799. .- --0.00039
0-3365-. 60.85- - -0.02414 ..... . -6.. 01.965
-0.05715
' Si c"
-. 0.18836 1.167 /. / 6.-19058
0.18618
0.18832/
A - Sn Sr .
~ /0:00930 150.5 .0101884 6.96i ... ...
0.02332. ' , 0.01866 .'.
0-. 00929 0.01902
, -0.00469, 0:01884
--'Ti, '
, j-0.00660 7.872
- -0.00600'
-0.00690
-0.00690
. ___T1 . V-
0.16247 70.06. -0 ..00081 256.4
0.04097 -0.00200 .
O:17977' ' -0.00159
0.26667 -0.Q0202
_____ Zn
0.01689-
' 0.01674
0.01685
93
DUP050307075
i)
LANCASTER LABORATORIES
hi in Name:. -9626903161 IO TCSAB
09/25/96
INSTRUMENT ID: 0314-4 18:42 ..
AVG
INTEGRATIONS
:M
(ppm.)
%RSD
41
42 . ' ..
43
'REREAD
. 0.18619 0.933
0.18820
0.18512
0.18526
<
503,979.52 0.397
501.74346
504.58734
505.60772
; > --.
-0.10686 27.77
-6.13947.,
-0.09970
-0.08141
i/j
0.05539 1; 529 .
0.05630
0.05523
0.05463.
0.-48805 0.. 480
. ' 0.48537
0.48970
0.48908
:.!"#
0.47762- -0.643
' 0.47454
0.47761
0.48070
: -ci
490.84335 0.453'
- 488.39666 '
491.37701 '
492.75634
r:a
0.87981 - 0.242
0.87736 `
-0.88126
0.88081
-O
0.43427 0.167
' 0.45339
'0.45471
0.45471 .
r ' Q..47269 0.908
0:46782
O'. 47593
0.47433
Ju
0.48269 0.637-
o:47930. J - 0.48531
0.48344
7.
184.46424 0.467
.183.49424 -
184.75495.'
185.14352
-0.05927 200\ 0
-0.05927--
-0117781 ' ' 0.05927 - -
_.M'a
.516.66748 0.-327'.- - 514.. 72625 -
517.42565
517.85046
Mn
0.46424 -0.382
0.46218
'0.46526 - -
0.46526
Mo .
-0.00655' 52.87
-0.00579
-0.01033
-0.00352 '
Ra . -:
0.05293 38.31
0.05674'
. 0.07103
0.03101 - 1 .
H i . 0.89855 0.696 - ' 0.. 89246
,0.89822
0.90496 `
. iJb
0.04997 8.775
0104585
0-. 04947
0.05458 -
3 b ' ' . Se;
0;57936 3.558- - . O'. 57067-:.';. . ` 0.56450 ,
0.'02503 39.43
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0.60290 ,- 0.03405
-
Si '
6.08466 6.822 ,, , 0:08693- ' 0108896. " . 0-.07810 '
L_Sn SrVi :
-0.00320 22Q.5 0.01830 0.495
-0.00750 6.928 -
-v . ,-0.00322- 6.; 01830.
-6;007.80
TO.01028 0.01839 .
-0.00690 .
0.00388 0.01821 -0:00780
i. ' .
0,17185 52.45
0.22419
0.06775
0.22362
V
- 0.47513 0.552
0.47391
0.47814
0:47334 '
:n
0.96530 0.843
. 0.95608
0.96822
0.97161
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DUP050307076
V: 1-2
LANCASTER LABORATORIES
Run Name.:.*; 9626903161 .Tube: 11. CCV ;
` j. 09/25/96
18:45
INSTRUMENT ID: 03144
EL EM
. ' AVG (ppm.)
%RSD ' , - #i
INTEGRATIONS '*2
43 ' REREAO REDIG
a-
0.4831-7 0.282
0.48238
0.48474
0.48238
25.99057 0.461
25.95671
26.12373
25.89126
:-.s 'i
73 '; r"' "
1.97426 0.830 1'. 25311 1.198 ` 4.88821 0:545 0.49759 0,424" . ' 53.26701 .0.396 .'
1.96024.
T.239707 4.86114 0.49590 53.11924'
7 1.99229 . 1-'. 26934 . .
-'4.91445 0.49996
53.50890
1.97024 ' ' 1.25028.
4.88904 0.49691 53.17290
:a
4.90976 0.529'
4.88439
4:93637'
4.90851.
. r ;
0.98986 0.204
0.9.9166 -
0.99025'
0.98768
5.08198 0.488
5.06527
5.. 11'054 .
5.07014
i
7 5.06177 '0.386
5.04862-
5.08425
. 5.05244
j- r~i -'5.07460 0.450
1/ 7 50708495 0.626
:5:06140. 49.96641
.5.10100 50.440S8 .
5.06140 49:84786 ' '
A7 26.07051 0.353
' 25.97163 .
26.15405 . =
26.08585
Mn . 7.7" ',-7 4.97746 0,511 Mo-. 7777- 25.44953 0.488' a 7 7- - .. 51.83114 0.377
-
' 4.95501 25.32599 51.74727
' 5.00513 25.57484 52.05458
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4.97224 25.44777 51:69157
rti
9,.86219 0.557
9.81991
9.92435..:
9.84231
.
A 1 25.04262 0.' 306
24.97847'' ' ' 25.12768
25.02172" '
' '"
" .Sb;."v 5:07027 0.434
'5:05552.
5.09558.7
5.05990
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4 27014,70' 0.257
2.:02066
2.01125'.. .
2.01220. 7.
..
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6.28469 1.869
6.15521
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'6.38447
6.31440:'
r
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i - 4.`86535 0.-29.9
4.85078
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'- Sr .- t .r O'...99341 0.498 '
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.; 2.04033 0.530
. 6.98915 . 2.03973 ' ' ='
0.99885 ' - 0.992237
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2.02983
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5.02315 1.396
4.94412- ' 5.07810 ' 5.04723
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1.97849
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1.99699
1.98195 "
7
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: 5.02385 0.406
5:00995
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5.01428 .
i
94
DUP050307077
i
Page: 2 3
LPNUASIEH LABORATORIES
Run.Name: 9626903161 Tube: 12 CCS
1____ - . E I/'EM
Aa
__ A.l __ As
B .Ba .Be ca _Cb .Co .Or-
Cu Fe
__ Mg in
_Mo
Na Ni
Sb:.
Si
.Sn
__Sr'
V Zn
AV6 ' (ppm/ ,
%RSD
-0.00194 60.33 0.05859 22.92 0.01297 98/66 0.01317 23.26 ' 0.00144 24.74
. 0100000 45.26 ' 0.06803 16.82.
.0.00137 63.01 0.00177 86.45
.-0.00214 0.032 0;00386 28.75-
CL 02212 23. . S3 -0.01975 458.2 '
0.03803 62.86 .0.00052 172.3 ,
0.01336 34.58 > 0.03052.84.94 0.00098 225.8 0.01700:' 13.29 "0/00408 227.2 6.00733 216.3 .
- v. 0:03496- 12.40 .u.O/00240 291.a
0.00012 86.60 -0.00510 91.69"-6 .'23715 19-.33 -0.00156 45.26
0.0017.8 31.34
09/25/96 '
i8:48
INSTRUMENT ID: .03144
INTEGRATIONS ,
tt 1
:' #2 '
. . #3
REREA6 REDIG '
-O'. 00076 ' 0.07029
0.02532 10.01466
"
-0.00194
' $%$&'((
;
)*+***,-
./0/123/ 4
0.00123 0.00000 0.07917 0.00237 ` 0/00088 -0.00214 0 ,.00450
` 0.00185 . 6.00000 . 0.66861 0.00037
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-0.00214
0.00258,
0.02761 . -6.11854'
6.04532 - 0.00156-
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0.04102 ' 0.00227 0.01831 .
' 0.00970 0.02i94.:
p'.63988 -
.,-0,00662/. 0.01254'. . 6.03332 `
0.00243 : 0.00018 '
-0.00463' J : - 0.00018
0.00030 ..
-6.00780 -
r0.18517 -0.00074
0.00210
-0.27190 . -0/00197
0.00211
-0,00311 ___ 0.04392 ___
0.01385 -___ 0.00965 ___: 0.00123 __ 0.00000 ___ 0.05630 ___ . 0/00087 . 0.00089___ -0.. 00215 ___ ,0.00450 ___ 0.01724 __ 0.05.927 0.01133 _ 0.00000 ___ 0.00932 0.000,99 __ -0.00158
0.01439 _ 0.00917- _ -0.010.97
, o'.oaieaf/ii
' 0.00942 0.00000 _
-o. 00780 /I -0/25437 -0.00198 _
0.00114 _
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DUP050307078
-LANCASTER. LABORATORIES
.'Run Name: 9626903161 "
Tuber 13 , PBW
.
.****, 100-100, OF 1,9,62695720002,8,
. 09/25/96
18:51
INSTRUMENT ID: 03144
ELEM .
AVG '':
567(ppm.) . /
)
INTEGRATIONS . .
#1
42 .
.43 :
REREAD REDIO
0^00038 599.5
0.000.39
. 0.02269 49.89
0.01314
; AS -'/ : -
0100581 .'208.0 ' ' --0.00736r-'
0,0161211.03
' ' O'. 01409 ' .
0.00272
:0.03519 0.00839 0:01686
-0.00194 ' ' ' ________
0.01973 _______. :0.01639- . '
0.01742
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31Be..
' / Ca'
'
' 0,00.020 346,4 ' 0.00061
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0.O278S 31.62 '
0.03782
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' 0.02463
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0.00087 .
-0.00062 T7~ '
' Cd ' ./' ..:O'.00050 198.4 O.OOC45 168.4
0.00125 6.00089"
0.00089 -0.00042
' -0.00107 173.4 .
, 0.00107
-0,00215
' -0.00215 _____________
-''0.00354-54;..47 ,0.00851 21.83
0.00161. 0.01054
0.00547 '. ' v6";6oail
0.0035.4 0.00689 '_________
_ "
' '.-0.01975 9i6.5
" 0.17781
. -0/05927 . -0.17781
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0.01375 30.56
0.01618
0.00890
0,01618 __;
' 0.00000' 67.05
0.00000
: 0,00000 -
O-.OOOOO.________ - '
; - V O,00378: 23.09
0.00327 .
0.00479.
. 0.00327 ___ ____
1 : . " -.0.02.".00. 122l4 ' 0.02100-;.
"0.04673
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.. `0.00096 3.03.2 -v^l-^7 ' 0;00260 260,6
. 6.00658 224.-2
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0.00002 60301
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-6.06750 '6.'928
-0.10990 74.61
-0,00159 43.56
6.00997 0.130
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0.03500 '. 0.00938
-0.00009. -0.00780 .-0,20241 -O.00199
0.00997
0.030R7 ' " . 0.00938:'" ; V 6.00000
'-0.00690
-0.08113 . -0.00079
0.00995
0.02923
-0.01868 . , .______
0.00000 - ' . ______
' -0.00780
______
-0.04616
-0.00200 ___
' 0.00998
DUP050307079
LANCASTER LABORATORIES
*-*if Name:-; "9626903161
V , . INSTRUMENT 1 ID: 03144
,o: 1`4 ' LCSW - - t;v. i -i , RF1,962695720002,8 > j .
;* -
. AVG (ppm.)
%RSD
09/25/96 . 18:54
#1
INTEGRATIONS " '#2'.
43.
REREAD REDIG
J : 0.04983 3.578
2.09452 0.106
" 2.07399 1.298
M 2.08059 0.347
\":a , Re
2.00553 .0.210 0.05016 0.005
./; .a ' v "v ' ' 4: 311655 0.288
i.:d 0.05057 2.275
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0,20214 '0.461 ' . 0.26014 0.7/42
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.1,04179 0.221-
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0.50693 6.1-78 ,
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: 0.51017 0.378
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n
0.51377' 0:441 '
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, --Se
1..99793 1.291 .
J-IIsn-. ..-? /
: 4.88506 0.519 3; 98967 0 - 766
;___Sr . ,\- . , 1.02005 0.261
. Ti
1.00126 0.051
J i 2.00768 3.461
0.50219 0.250
,/Zn
0.51479 0.251
0.05021
0.05138
2.09229
2.09675
2.04291 .
2.08861.
2.07225
2.08503 -
2.00409
. 2100223 '
0,05016.
.0.05016
4.29748
4.31859
0.05082
0.04931
0.50413
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0.20321
' " 0.20160- '
0.25821
0.26207...
1-.04016
1.04077
4.08977
3.97123 -
.2.06339- .
2;073Q9
0.50745
0.50745
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2.06364
4.14172
4.17746
0,50824
0.5-1017 .
0.S1508 .
0.5570^, ;7,:V 1.96845 '
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0,51509
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3.95457 ' .. 4.01073
1.01715
1.02039
1.00156
1.00156
2:07717
2.00768
0.S0078
. 0.50259
0.51382 .
0,51626-
0.04788
2,09451
. 2.090.44-
2.08448
2.01029
0.05016
4.31947"
6.05157 Is
- 0.50546
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1.04443
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3.97123
2.09978 0.50589 1 '2.06818
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4.14888
0.51211 '
0.51115 = 0;. 55036--, .... ... ..
2.01643': '
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4.00370
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DUP050307080
Rage: 16
LANCASTER LABORATORIES
Run. Name: 9626903I61: 'V ;, '-
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Tube: 15
258529.0
U***,100-100,DEI,962695720002,8,
09/25/96
18:57
INSTRUMENT ID: 03144
,ELEM
AVG " (.ppm).
%RSD
-0.00083. 405.2 : .0.034-47 13.54'
0.0061.6 86.81 ' } 0.03316 8; 425
i7- - o .;o686ti '' *>043
i^-a.ooooo. 151.3 ;i'-;.r48;.528t5'. OY29
. 0.00062 69 .'46 , , o. oooaa ,299.8 "
<" -0.00161 57.69 0.^00128 302.8 0.00344 20.29 '
-. X; , i:l'l 54107 3.846.. : R. 50. . 10570 0.241
7 'AR5' -,0.01429 .0.027 ' ` ' o'. 00378 61.10 53:40007 0.100
' .^^'t'-O^OOOOO 26351'0A'60063l' 534'. 9
231/.3*'
" 6/10223 is:43
' 14.06347- 0:249 6:66236 296.8
"/IV .0.45574 .0.159
v 't v -0/661. so' 292'. 9
V - -o; 16193 53.89 >0.00079 151 .3
- 0.00801 0.161
INtEGRATIONS
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0.00305 7 `
-0.00277
-0:00277
0.03069 .
Q.03969
0.03303
-6.01208'' 0.03354
0.06942
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148.31146
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14.02436. , 0-. 00235 '
0.45493 ... 0.00030 :
14.09244 ...14.07359 _______
-0.00465., . ' 0.00940 _____;
0.45643 1' '0.45580- ;________
-0.00780
0.00210
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-0.08102 -0.00199'
-0.15036 0-. 00040
-0.25441 -0.00079
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0.00800 .
0.00801
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.-.Run Name; -9626903161
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'Tube:' 16' 2585290
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UP**.100-100,OF1 -962695720002.8,,
. ' 09/25/96
,. 19:00
INSTRUMENT ID:. 03144 .
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INTEGRATIONS . #2
#3 ' REREAD REDIG :
ct : \>
v-..-:
b afee Oa ( 'b
: ro C rCu
____Fe K Ma Mn'T IIP ; Na
__Ni - Pb
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0.01831 6.419
0.01712
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0.03888.
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0.23729 1/178
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0.46243
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'0.01003 0.032 .
0.01004
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T 145'. 78033 0/711
' 144.85774 >' 146/90299 "
0.01003 145.58084
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'.0/00922 6.245
0.00985
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- 0.00871 '
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0.10011
0.09613
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- , , 0.01832 10.18
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. 0.05156 2.856 :. ' ' ' 0:. 05284
0.05187
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`0.20310
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. 0.20737
r,' 3.3389.9' 3.695 '
3.20069
. / 3.43778
3.37851
49.90760 0.764
49.60903.
50.33725
49.77651.
0.04566 0.021
6:04566
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0.04565 . . 6.19993
0.04566 0.19766
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54-. 25205 0.761 ...
53.85558
. 54.68045
1 54.22012 -
0.07693 1.451 .
,0.07564'
0,07758
0.07757-
0.00425 106:6
-0.00098 :
: -.. 0.00686 /, 0.00688, - . : /
''0,11415- 2.827., 0.08967 4.808
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14.15682 0.643
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0,52960 0.001 .0.46.474 0.800
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0.03639 0.09629. 0.04985
0.03630 0.09752 ' 0.05083
- 0.19246 0.09931 0.05083
. V/
99 DUP050307082
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LANCASTER LABORATORIES
Run Name: 9626903161. :.
.. -
Tube: 17 ' 2585290'
0-***. 100-100,DF1.962695720002,8, ,
,i
` "':' '09/25/96**'
INSTRUMENT ID: - 19:04 .
03144 ;
l 89
-
(ppm.j
%RSD
: ./INTEGRATIONS
#1 ' #2
' #3
REREAD REDIG
' -0 ..00515 60.01 O.00950 67.33 O ; 00728:180.2 O .'03396 - 70 378
.0 ..06674- I ;418 6.00000 14622,i 46.36326 '61236
-0.00188 188;9 0.00000 '13656 :
-0.00215 0.000'' , 0.00096 T15.1 ' 0.60121''57.65
; 11; 32374 5`.170 49.53687 0.394 0.01378 6.526, , 0.00327 46.15 52.76628- 0,342'.' -0.00096 115.2 -0.00458/ 236-. 1.. T-;:Q. 01219735.70;<: ' 6 .'09094 5.368 , -.13:88519 6.453.
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0.00000 14622
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0.60211-
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- 0.00792 0.03409
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0.06.570 ___ 0.00000 ' -
146,15274 - > 146176322
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-0.00062
. 146.17384-" 0.00087 ~T_s
0.00353 - ' ' -0,00176
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0.01587 _______^
DUP050307083
Page: 19
'
LANCASTER LABORATORIES
Run Name:.. 9626903-161
,
. f>rsas 5
rube: IS
2585290
R;:;;< iOO-rlOO.-DFl .962695720002.8, .
* 09/25/96
19:07
INSTRUMENT ID: 03144
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AVG '
ELEM ,
-(.ppm.)
' %RSD
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;
INTEGRATIONS' . #2
#3'
REREAD REDIG
i/Aq
0.04694 4.325
0.04928
0.04578 ' ' 0.04575 ;
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., V:-'-' ' '' '
V
2:05365 .1..683 0.04727 34.82
2.04311 -0.319 2.01359 0.239,
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0.04815 0.000
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148. 1 <4666 0.446- 148.58885
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0.47499 0.740. '
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1 50189616 -.0.49985. 1-.98644' 56.39718'.
50.89371-..0.49672 . ' 1.97590 ' 56:32141,
50.66792 0.49203 1.96683'
55.99267
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3:9.8688 1.118
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4:03839
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0.99555 0.810
. 0.99975 -
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6.04273 204.3 0.48478 0.007
0-03107 ... 0.48482
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0.13532 0.48474
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0.49300 0.150 ' .
0.49381
0.49284
0.49236
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101 DUP050307084
Page: 20
LANCASTER LABORATORIES
;R'yn>NamA:.-v 9626903161,.
...................
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Tube:- 19 2585290
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09/25/96 . 19:10
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'INSTRUMENT ID:. 03144
.
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-0.00219 123.1 . . -0.00375
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.
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- 0.01487
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1 /0.00000, 42.42 .
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0.00000
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-- ` 29:80838'O'.385 ' : ' .29.69431'.'
29.192391
' 29.80691
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0.00037. 115.0 .0/boo 01 >2495 , -6/00161: 208;'2
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0.23708
6.00064 -0.00041 -'0.23708
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9.97922 0.504 0.00285 0.064 '
9.92501 0.00286
.
10.02454
9.98812
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V Mo . , ; - 0.0,6352. 53/92
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0.00327
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; l^lNa /
10; 59656 0.277 .'
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10.62706
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-0.00464 0.372 . 6> 09656 0.757 v-0.60750 6.928
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102
DUP050307085
LANCASTER, LABORATORIES
MNOi .Name:. 96-26903I6I
Tube: 20
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r. _ 1 00- ioO jDp 1. r 962695720002...8, .
09/25/96 '
.19:13'
INSTRUMENT ID: 03144
t'. t:M
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INTEGRATIONS 'ft2
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REREAD REDIG
>i
-0.00320.55.58-
-0.00476 .
-0.00126
Vl i
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0.02633
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0.08451 0.423 :
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0.65199
37.59380 0.437. - " 37.55172-
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0.00226 38'.49 '
0.00176 ' '
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29.40841 0.553,
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; -0.02687. `'f-;. ',-0.00133
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8.46437 0.454 . . '8..47507
8.49636
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0.03241 0.884
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0.00101 0.03258
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0.08430
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DUP050307086
Page: 22
LANCASTER...LABORATORIES .
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Run . Name :: 1 . 962690-3161..
v. .
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Tube: 21
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**** 11QQ-100D F.1962695.720002 , S ,
09/25/96
19:16
INSTRUMENT. ID: 03144
EL EM
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%RSD
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#3 REREAD. REDIG
, V_Mg TXlMn
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Xv ; ;X-Zn
-0.00201 87.57
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00575 "47.96;
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4.68249 '.- t 4144541. -
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37.94625 ' 1 .-78862
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0.00857 , 77.96458 '
0.00781 , 79.51567.
0.00479 - 78.64505
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0,14421 -.0.00113
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0.00845
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DUP050307087
j1 t - ; `23
..LANCASTER LABORATORIES
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' 5 3-0 '
1 i,,.-e: 22. 258-5289'
* ***. 100-100; DF1 ,,962695720*002,8, r '"
09/25/96
'19:19
INSTRUMENT ID: 03144
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"0.0036.5 37.21
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