Document 3QMnkKkXaBr2oMv6aZ36Rq2aa

02/28/2001 ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT B A C K T O MAIN LAB REQUEST NO. 8442 REQUESTOR NAME: EAR DEPARTMENT: 0535 PROJECT NO: 9970012600 DATE RECEIVED: 09/07/1982 DESC: ENVIRONMENTAL SCREEN ON L-6778 CONTRACT LAB(S): EXP COMP DATE: 11/12/1982 DATE COMPLETED: 11/09/1982 PROJECT LEAD: PHONE NO: 3M FAX NO: 651-778-6176 EVAPORATE TO DRYNESS UNDER AIR OR N2. PRODUCT CONTAINS 40% WATER SO HEAT TO ABOUT 40 DEGREES C IN WATER BATH OR BY OTHER METHOD TO INCREASE EVAPORATION RATE- MO HAS SAMPLES SAMPLE DATE CODE DESCRIPTION RESULT MDL or (95% C.I .) TOTAL PROD. 96-HR-LC50 BOD-05 BOD-10 BOD-20 COD SLUDGE-TOX FISH ACUTE TEST - 96 HOUR BOD-05 BOD-10 BOD-20 COD SLUDGE TOXICITY SOLIDS 96-HR-LC50 BOD-05 BOD-15 BOD-28 COD SLUDGE-TOX FISH ACUTE TEST - 96 HOUR BOD-05 BOD-15 BOD-28 COD SLUDGE TOXICITY >1000 MG/L 220000 MG/KG 270000 MG/KG 330000 MG/KG 530000 MG/KG SEE ATTACHED REPORT >1000 MG/L <8800 MG/KG <8800 MG/KG SEE ATTACHED REPORT 280000 MG/KG NOT ANALYZED Enter Carriage Return to continue: - tp* Environmental Laboratory B O D Work Sheet - Samples UCT. * 0 D A vizpQ B A C K TO MAIN Cab Req. No. 1 A n alyst O at Started _____________ ____________________________________ 9-/0 -<SZ. BOD Run No.t ~ jf'X. A n a lyst Day BOD Readings , OP 6*^ D a ta 9 -i s -%2 S am p le D escrip tion Initial Dilution 5f1Ll ' 2 ' - ' 2 0C - V r . ` fiifV q . Ehv. 'Scn iJ o k L - 6 7 7 $ . . : of Sample diluted to Jq q ml with D1water > Initial Dilution Factor (Dilution factor = 1 if undiluted) Bottle No. S r/ 70 /I /5' 7/ Cone, of Sample1 Sample Size3 Initial D.O. (0,1 Present 0 .0 . <D2) 0-5' A i-O 2,o HO %>'0 to o voo % .?o V 'D b % SO %./c %'/0 %` f t r 7 .7 0 7 .7 0 Total 0 .0 . Depletion IDj Oj I C. SC : : 0- C 7> a - ^ s * /,o o i.io /. 60 Depletion Due To Sample Dev BOO 6 '. 7 0 G- .(S' O'Hl 0, s7 / -o3 Hoc fi, C O a: y30 7 ,/ fO V, S J& 9 SATO Average S 3 __________ -Day BOD < % 9 p b /(j . ' - Note: 1. Cone. = Concentration of sample (ml/l or mg/l) in BOD bottles. ta) Laboratory fttork Shaat Sampla* Lab Req. No. | Xn*iv*t . CW ^ : :-J B A C K TO MAIN '$;<***>' '''H V \ 'i ^ r * *.*; ! ; ylA^*--g^-a-*A--L----- :-*------- ------------------- *-- ------- ---- ,\, *:.". V, . ' v ' .-> *.:' *--. --.-- --.--........... " ----"*^A--.*--, ly v ^ .* T----- ------------- 'V V"` -- *--*- - ------------- - .. K p H y i ; ,.- 4 !;i.,v W f e .' '* .t . <7*:%'..*> ' - . . y , - .- ^ I * ___ - -__ ____ ' "*- ____ V4 * S '^ '. 6 0 0 R u n N o .l - ' .;; - 7 ` '. : .--.yk Dote iu irted ^ fc O 'S X ~ S ' Aneiytr _ ` P a y 6 0 0 Reading . \ ' Oste (tem ple D escrip tio n t Initial Dilution Initial Dilution Factor w * -a E b u se a e < ?iJ oM L - 6 T 7 0 "} ? o . ix s m ^ of Sample diluted to / (X ) mi with Dl water V ? " .............................. J. I '! ....................................................................... * ........ ".J ' ,. '" '.7 (Dilution factor f if undiluted) -- -- -- -- , Botti* No. Cone, of tempi*1 #37 :* Po 71 75' 2/ r lampi* 1tee* c -r Q Xo HO 76 Initit 0 .0 . (Ot I Preaent 0 0 .(0 ,) Total 0 ,0. Depletion 6 r0 }l <5670 ? .? o 7 $0 % $ "7 . 7 0 * 7 ,7 6 X SO 7 /7 0 *7-/0 ^ V v- / .T P f.zo 1.10 f.S 170 si DepletionOu* . To topie.'... . 4 v ' s i ' 4 `i /< T *Dev BOO PTf Q 7/JT 0. 'ZXNoO ; 0 , Zoo : JZ.OiO 0 V/; 0 '6 7 . LSI SffiO h4 C H :: ' 4 . ' <r o*v BOO -. j- V - 4 .' r 4 . ', ''S ;- , ' ' ` - Mot*: t . Cone = C oncentration o f sample |m l/l or mg/1) in B O D bottles. 2. Sample Size = ml or g of sample or diluted sample added to BOO Bottle. Comments Cj5 0 - Ztt.C C O ,* ' ; .- 4' .' : '`.4;: v, .'.;.44 '7'<-, c-.- /.'.t-* :`v. A'' ' N','7 ' 'X ' ;r. r.r ,'ip--; ': `` ''. .'-X-S' s0\*yp 'TVV ... .' "- :- *'...4V,>=.:-4iv.*r.^;T'. *Vv.^f, ':vf.-;;- ' ' i. '- ",* ' '> , ;,/.;.'.?:",r 'y V'.:;|7 V\ : ' :\V;4"<-V;->'4;:.; - :: .**.*:**%,v;i*.v ' . '. 4;v7; ' 4 - y'"-..e; ./' . '4, . '\r ,,V.-'iv4;.*;,...V..,ij'i-l-ilu;i.l.1. ./.'.'. . ,L.?. :v<;.* \yV*?> .-ivV.'ri;,t*y.! 4 "C '.',;V .''i:s*4 Vr>'X ' ',v4./; '4 ' K tab Req. I rUeivfi V- . lampla bawr Iptlon W Initial Dilution Initial Dilution Factor v.*-I.:-'. .7;>i.;SW1'5'--'", B S 9 i(irW ' *> **> g ? , ? * ' ' ", <`v : V'-. v.'-.' x.[ .v-."v*r-'' ^ rn, ; 4 S r V .:c x r s if s ,T .-i- .? .... < 9 ^ G ^ r........ *?""?. :* f ::. : -m & & 1.^-k v ew% : 2 ow a^ g E h u scnegiJ o n > L z & g jm ... of Sample diluted to f p Q ml with DI water ;>ii.. -*~+ (Dilution factor 1 If undiluted) B o ttle - M e . .. P #> 7J Jl C one, o f S e m o fe 1 . . Wt n99lJr 9i Pa l; . F row n ' s h S * -.;. 0 . 0 . ( P t I x 0 0 . 1 0 , 1 T o t a l 0 .0 . D a p ta to a ( o ,O j) O e p te d o n O iM T g jtw p ia . 0 -6" / .0 3 -0 ^ O <3 * 9 0 .: ? .? 6 Si 9 0 % ?0 fr o :: ? * 0 76 ? fC t jS & -- ,W c W- / ..S 2 s-% Z -K , C `G O 230 1 .y i v ;: 3 .S T > r .3 o 3^ c 3 -/T ^ > 5 r0 0 / 7 6 H( 2 8 ^ *D e y ' .'.- ' D O . . . : < 3^ V P 0 - . A w rage - -tW v . . . . . .. r*-r-- * ' ; : ,;.V 7 W . '^ - 'V ' ; ; : l 6 t ,0 0 Q S 2, 2 o o Z S .Z O O , . ; . . . ;... / 8 . f 0 ih m : < *? ' - ` - f ' - V : . r ; . ;, .- 1. Cone. = Concentration o f sample (ml/l or mg/l) in B O D bottles. 2. Sample Size = ml or q of sample or diluted sample added to BOD Bottle. fSSmintr C S & 1 .-3 2 & X Q .M i /. % fetm 1*766 pwo - W *- -'-V r B A C K TO MAIN Environmental Laboratory BOD Work Shoat - Blanks, Controls,`and Standards Lab Request No. ^ A n alyat L^ Seed T y p t &Source S 10 '5" -'-' u l t . 2o r ^ v f o o 3M O at* Startad c/ - / - v . Seed C o n cen tratio n . `" BOD Run No. | <7. <Q u,.-. , J - ---- <S - Day BOD Readings A n alyat ^ u . / . / __________________ ' " tc iv.y<r 1-- " . r :----------------- a ta c? - f S - X ? Nonseeded Dilution Water Blank Bottle No. ;>.` -' ffe - no m o .9 Initial 0.0. lAi> Present D.O. (A2) s?vr 0.0. Depletion (At -A2) O 'tO . O 'fcO . ' i> 60 Average 0.0. Depletion (A, 2) P ' O Seeded Dilution -Water Blank (optional) Bottle No. V Y "($ n' n Initial D.O. <C,I ^ 9o X '$ % iT Present 0.0. (Cal # '3 0 % '9o % at 0.0. Depletion (C, -C2> O i . O 6 6 ; O ' 6^ Average D.O. Depletion <5i - Cj) 0 -6 0 Seed Controls Bottle No. SampleSize Initial 0.0. (Bt ) Prtant D.O. (Bal 0.0. Depletion (BfBal 7 5 '' w > 65V v 6 v .6^17 i KO Ib O _____ __ %<5 $6 7 5 ' % cO 7 .7 0 V ' ?V0 #-C0 ` 7-60 6 'v & - ; -. r 0 -7 0 0 -7 .5 ' 6 -& > /.C5T , L--G--l-u--c--o--s-e-----G- lutamic Acid Standard Bottle No. SampleSize Initial D.O. (D,l 77 -7 /> 7 < io . ai*.'" rs. y 70 *0 3 ^0 Present D.O. . (D2) Total D.O. Depletion (Dt - D2) b . S ,^ ; 250 VYo y.C o H .6 Depletion Due 5 -Dav To Standard . BOD .111 111 6 76 Y ? ' ^Average 's,/ 0 -Day BOD :: Si /70~y jX Potassium Hydrogen Phthalata Standard (optional) Bottle No. SampleSize Initial D.O. (DtI Present D.O. (D2I Total D.O. Depletion (Dt -0 2) DepletionDue To Standard Day BOD Average -Da BOD Fo rm 19760 PWO " ...' : V *. . < - . r vUVi ' ' . > . . l . - . u - ' : V r : ' .-V ; . t Y-Y ' V- ; 7. Vi'*' Vi*V"' ,-* . - .tr- B A C K TO MAIN stim ai Laboratory - /fork Shoot - Blanks, ,w ol, an0 Standards -w .q iy fo Q ,, y, -y Lab Request No. | Analyst .SMd Type* Sourca . [Cm tttrM ,Saad , onwnintfiw1, ---- S - 0 i \ k . + j j , - ___ Nonsaadgd Dilution - Water Blank BOO Run No. | g g , -jQ 9. Analyst I f ') ; 0Y BOO Readings . sn /lO . bata BotUaNo. liO 7 \ v . : 7 :;. Initial D.O. lA, f?S (0 ri . t iadad Dilution Water Blank (optional} /-:;.;5^ \''s''.'` '? '` ^:> ioni No. ' W W .;' . fc,) 7 6? & 9 o % 1U /7 " Saad Controls : 8 ^ fraasnt D.O. <**> ; - ~?~90 7 g o ' Praaant 0 .0 . (C ,) -7 *?d &od D.O. Captation (A, A ji o -?s 0> 9s~ ' % < ...... . ..............T -T?.-" D.O. Depletion v (C, d, f:o 6:) O SO ' M l Avaraga D.O. Dspfation i*t-*a > : , 0<9$ : . Avaraga 049-; - PteMon.. 0-9/ Conta No. StMUpIftftlt . '7 7 ^ ' '.w v6 /. <90 io m . Jho . Glueosa Glutamic Acid Standard . Y :S . Initial 0.0. 1 :% .<60 7 .7 0 v Praaant D.O. a 7 ,7 0 7~7> .9 5 r ^ 7o _ D.O. Daplation ; (8 , - 83) A/0 /3 r /. S - oi> - B o t ila N o . B t flip IC M lt 7? >**/ v- so 70 W U e i D .O . ( 0 ,) P ra a a n t D A * (D a ) 7^ ' >5 - / 7 0 : g -g o 5 $ 50 T o ta l 0 .0 . D a p ta tk m (Q ,- O a > 3 l 9 .s 0 g ,0 Q D a p la t io n D u s ;.T d .B s i w lp r d 9 .' ** *t.` , . * ' ' 2 J Cr 3 -6 1 S . / 1, s /O BO O . D av /T - 4 v bo o a il: a . B o ttla N o . ; 3B(nf4i Six# _`; r ' .. `r.t form tg7BB PWO fa W a ip .a .i'lO a 'i W a a a n tP .0 . 7- P *> S Total 0 JO . D ap latio n (O fv D ,) O teM tonO u* I -D ay .To B tam N rtf' ;; ' B o a : ; ' : / m i -V. - . A v a ra g a .:.:.:-. ' 'P a y 1S5d ~ ^ - *..*' V *-7 .;- ' ..Jr."'.*.v- B A C K TO MAIN Itaf Laborttory Shgat - Blanks, i|, and Standards S.iQ 'S ^ O* ULT. O C ttV fo O .*':vh-hV-.'&P.p-.-. - --------------------------------- :------------ ------------ --------- - Lab Request No. | ; BOD Run No. # < ^ 7 .- Q -' t . A n alyst _______j f ( 6 ^ &S a a d T y g S o u r c a . D ata Startad 9 /o -v. Se e d Concentration A n a ly st -Day BOD Readings , ^'5' D ata Q o r - z ,:; Nonsaedad Dilution Water Blank Bottta No. Initial D.O. (A,) m m :- . - ' : . : - & # r 7 7 7 7 7 ... , * 7 7 -> 7 Saadad Dilution - Water Blank (optional) Bont No. Initial D A (C,) 6 9 : 59*90 si >9 - y / 7 S' - .7 " Present D.O. <a 2> 7-^ 0 7 7T 7 .*sT . ' '. y v- . ... Present 0 .0 . (Ca) 70 7 -SO ~7'9o D.O. Depletion (Af rA2) 1-^ 0 V < '6 - 7 7 te-j -Cjf '- /-7 'O. Average D.O. Depletion ; (f - jl ; V*- ' - : : ' * r <>^'77*y4>X1; '* * v vit Average 0 .0 . /. Depletion. (5l -C jl /.. /-O S' ' Saad Controls B o ttle N o . S n n p l i 3face In it ia l D .O . ( B ,) P rsa a n t 0 .0 . (B a i D .O . D e p le tio n IB / .B a ) -7<' ' 65" 6 .^ D Yo GO m !> GIuoom Glutamic Add Standard Bottle No. CajbmIa ^PtMi Btltiei D A (Of) <Z > ^ <7 s T 7 7 .7 0 Present D.O. (Dg) 7? :^ /.W .5 0 7D :S .r .y r 4 /fc f 7* 390 /: 7. - 7 6 . 7 / 6 ': 6'375 S -/0 7- 7 -3 3 7 7; ;- b 5 * / .T O ' -/ .; . 5; , 7 : Total D.O. (Df Ih ) < /.9 r -0 *: i 7;_ Depletkm Dve To Standard /-S T ' Dev - BOO m w i 7^3i Z 3 i" 23o ^ :B O O *v ' ; .,k*?; Bont No. iAt ' M i a i 0 . 0 . V7 . ; t i. -5 Present D.O. Tgtal D p . ' Depletion (D t` O il - Dev . -j;-7 : A f f * 5- 7" T s * t a r 7 , , , 7 | p | ; > 3 | *.7. -f*``ii/.t ; .7 -.7 ''.:4 : '3 i7:v- *.r7* . . 7 5 '*: ' v ; . 5 . / ; . 5 & 7 7 - - i - .:-':*' . *. '>.** :. 7 7 . 7 7 : ' 7 :7 ; ; ;v-</ ; .. ; ;Vv. O:'* . >5 ; ;*'. V-. " ; 7 r.9.- SS ri ;C*;. .t_*` ... .7.-.:.-;fyj c;.w^K~ swsB>iti<.v v' .7 7AA7V'>^V^';<v-:-V.-7.a.V^.a>fy:'; tVA'nti Ml Laboratory Shoot *Blanks, ift, and Standards L U X -3c> n f v f o O ~ -- --- --- -------------------;--- " -- --Lab Request No. t ----- ---- ------ B_ O_ _D R_ un No. fa Analytt Data Started ^<0 Seed Tvpfc &Sourca ^ Seed Concentration Analyst SCt-Lii A-- Nonsaadad Dilution -Water Blank B A C K TO M AN s.-^ 't'isV : if.-;*, ' ?%;; .v.V'? ; ~ : ;....' r .'i : ' - Oay BOD Readings Data 9-33-^ . . Botti* No.. . . . ; Initiai D.O. , (A ,) - b ; Seadad Dilution -Water Blank (optional) Prawnt D.O. (A2) - - - 7 .5 0 ` > 7 * .s r ~ 7 -> S O V- D.O. Captation (At A j) /3 Q 7- A**r*g* D.O. Depletion : (At -2) ; . 7 3 0 7 V: ^ * *-. - .1'* *\'c 'r : 7 ? . s 7 - 7 ' ":. ' . y .- ` . .,t*. * -te. . Botti* No. 7 it // Scad Controls Initial 6.0. (C ,) -*p r'-O'! y .vo * Frasant D.O. IC2) "7 S T ' 7^ 0 n-vjsr `7 0 D.O. OdplBtion (C| * 2) I.3S 1.20 hi : *-:7 r*' -, y y " - Average 0 .0 . Depletion. (Ci e2> '. ' / 22 ' ... Botti* No. Sampt* Size Initial D.O. (8,1 Prwent D.O. 3 D.O-Depletion (Bj -B j) y9 V- ^ > : ' *70 YjO : : X V4.C/0 . 7 \ 7c > "7 .2 0 V '' C .8 ; ": 7 ' ' '-'V -/> i W 7 - 7 'V.> ' : - : ' ; { . : V .& - . . : - , :/ ; ; Glucosa Glutamic Acid Standard Botti* No. Sampi* S* Initiai D.O. tt>t> ' Pr*e*nt D.O. " ID2) ;i4 .. . /W tV C / C-! . ' %s o : s . t o *3,S O f5> ; i ? 6 Potassium Hydrogen Phthalete Stendard (optionl) Semple Stee MtW D.O. Frwant D.O. . ID jI ' . ',' v ;V ' : Form W 7S5 FVVO Total D.O. Daplation (D, -Dj S7 s. 30 '_r . / * Total 0 .0 . Daplation (Ot> 0 3 ) Daplation bu* Te Standard . -Day . 800 sm 9 ./ - 3M T S <r ^V - . Avng.'tS j2Q -Pay BOD J DaptettePua ' Oay . Te w w , * .f. ;.:.. .800 _ '.y'*.";. ; V-t '1='" - c ;V_r l'y V ''Srz'y>'r.V:':7l r\./P.*;rV'--* ,:T 4 v ' : r''^ : :':`{v;l^ 'Z-sS-rt' - J: Ji-J--j ; 'Averege.V.'- ' *; -Dey -BpiD/i:,--. B A C K TO MAIN tal Laboratory Shaat Blanks, 'and Standards S,* > , ( $ ' . u l t . <? m ^ V Q Lab Request N o. p Analyst . -Vr:" '.'-V.'- ' Data Started Seed Typ e & Source . Sfd. Concentration t li.- A A ~ * . j 2 .b p M / . 1 Nonseaded Dilution - Water Blank :- . BOD Run No. % Q l . ^ O .'A '.t V l H->u: A nalyst - . - D a y B O D R ead in g s rc .i ;' ' ' . ' 1- _ Data Bottle No. Initial DO. (Ail Prsent D.O. (Aa) D.O. Depletion lAv-Aa) ito . : ! ' V/ ;;i ' b ' . r : '/ ' V - 7 * 7 "Z p2 * -yy : . - : , 7 , 3Q Seeded Dilution - Water Blank (optional) 1' . ' ' -' Bottle No. In itia l D O . <C,> Prtant D .O . IC j) > .Q D ' 1 'S O ."j D .O . Depletion (C, '.C l ' 6% a : /? Seed Controls >>` J 7 2 if - /,7 :; : 7 .3 0 -7-YO -7-SS' v-'v y .6 0 Mo ' /* 3 0 Average D.O. . ! Depletion : 7 M 9 k il %V- * , , Average D .O , Depletion -V t , -C al .. v". : ' ; ' *' * -: 1-13 Bottle No. Sempla Sfate Initial DO. IB,) Preaept D.O. 182 D.O. Depletion <8 , 83) `.'-'y *0 v' ~ ' ' ' 6V f v / t;0 . S -s6 "77 '*> HO 7 7.70. Z.S Oi-O: 'S 'J O ; :y 3". ? p H. S j 7 ,;. ^Glucose - Glutamic Acid Standard Bottle No. Sample Size 7*7 , ^ O ; 7 7 / -. - 7 7 . V: / V f r MtM D.O. ID ,! ' Present D O . " lb2 3^ 0 S7 & ? :; V.SO "3 . / o /7 Total D.O. Depletion (Of - D jI Hoo S .7 Q 7 ,/ 0 Deplfon'Ptie';, To BjeotNnl.v ^ ^ BOO -N ; _Avereee ^ 7 : -Dev BOP 7 . y; y 2 ^. JT .7 0 7W . c/^ , - . ? 7 Bottle No. Sample S ix* Ini* DO. Present D.O. IDjI Total DO. Depletion (Di -Dal Depletion Due To Standard Day I D AyerepeJ^';' v.-Oay ...b o o ,