Document 3QMLeagkQVjZgeaeageow2k2D

--- LaboRrepoarttRo evirsioyn1 Analytical Report of Data for PFOS Dietary LC50 Study in Northern Bobwhite (Sera and Liver) Laboratory Report No. FACT-TOX-129 (U2723) TestingLaboratory . 3M Envir3onMmEennvti]roTnemcehntnaollLosg&byorSaaofertyy Services Fluorine Analytical2C3h6em0i9stry Team (FACT) S9U35PaBulu,shMANve5n5u1e0,6 Laboratory Contact KiBslHdagns2e3n,6.Ph0D. St PauPl.,0M/BNox5531333133331 PhFoAnXe:: ((665511))T7I7886.1670618 Revision Date: March 19, 2001 Page 1atf 7 WE oslaslor GO0663 1 Introduction 1 igottymVeD aoBeaa edese Bie Copmrp,Seo SfeeoaaAe, Thisstudywasdesignedtoquantitativelyassessperfluorooctanesulfonate(PEOS,CF:SOy, CAS #2795- _erd --iieee I avderel tada2ywpe e bSase oo trn ys onPiEPo A pa s?tt CPEhprcnin,odo5ftat3oaeaTdFevlEassCcSdprnclahdoibEeyepeoprergidsbcBseopoefrwBaPebFne,SrTmceoolr e. e Wins Ii iniabchesdrrgteo 2DvpeeleonnPO1S0.55aeWdiiehcdovpe, tgha doeoiloie. . GoFoRCFS nnherpfy gieeoraFlOSym coe my iEnay nt 2.Jl fr smI rs eiet hA -- PaAF ltghee fg ShoatytBe lm mmeaosefs dhsWelEver A sorF ry SuE edOpesing le Ni Ioidcmvmoasdeceodltdtfbo eiyoeeqyueesoboeeoseBeadPioFenSse iesceslsvctof 2 SampleReceipt 5 5 R A,ee aSEE TC hEnr virLe eboNEom oeefde 8tywar e4boa, nd 4s pcos,S19, ToheEm vCroimel cid1ive, 35toyod, 5er, di ec,recn ThEnoninilLb To eived30por ben be alsem , son6, 3059, Upc 3 Hong ` <j Theresbldg oe hes cadwi Bssre LOBSMMSsys, 2 650664 - 4 MethodsAnatantdPriparcstolry LE AnESaloyIticSal meaeothaodcs oneabOsLtiFsforyrei,sSStEooodsteypoithFshehrvoereniogclesoCeaopntp,sondnof PoAm NrYesAtB v oteto tt arFoe e oes ayObikPSr ecbipcCootnosn EE R ErirtThee aEtmeo aame ,smet OcBPs hSeereiSiaCgomtprasorn foohtiahrmhseEcOe hvoste eSmooeFy oMremrie mcsmS o mBaese CR a rag 1Ba mpt E E eT a amesPocy pin onLtiveeEest fEm TsAn e eyyic ettOwo bsFtetmo i oensLl iwvoenBes S[eRTe mREaiNRs prApapt attoys nr e REeLi nsCohEpe hr SioYeeSp gHrcea Seet:nesn y pseee cthyesrobgineiars Cen etehmam -- Ca ie. tecocof cebtsrte petryeg ees kimert omotyibRmnoBo tHE oFmEOiShe Toons PLCapt,EHSprvi pivary foie ym spanecorbneenec yteeitneepiyr reg Fen ae ba i ison eepoys i orosSSS8Fa l0r ob--eHpd--iEf Ees--eS--e mpi, rast,, otlarh, GNOB65 5 Anais : HH S1 Calibration A teecarb p yo ndcaryc p10 eirh laoiio 4n9enfn aecip.ced Qr:uraeennrcteaomoffehoeetetkeevelebreeivansgsgxhdh efispnofmrles,binlQepieipsniognfhcg1y) kvio sfbbe n Ma1l2e1a7 tyo96d570) lFOeS,spieddflosace us sty fermionviet 52 ExtranadcMetthoidBloannks AlivseiwtccRricao fetrokp,lnidnSgkiyhgropesaisewemrarncriyh cheaeehcotfed. `Bflarnksrweoretcomepltianmtifanottaragestttaineanlgytewasdetected abovethelimitofdetectionfor aspecific analyte. 53 Surrogates Teersiepmneoeaevasii,d 3sprs.Siuseleyer.Seuage eepgeewrsl 54 Matrix Spikes O5a v0e1rgt mcaobtnpeowfeieefesteeinepaypdiiSmpt0eofs4w,ei1e7p5eriesps dyxeh3tsois vprcai.ibT,eeAd0lo anmaelytbeobreciaovGeortoyoeyfarpproo1xi9m9amt.eTtlye35e0%ofdtohmeexmCpeactoedvahe.GThoeishesa mapl9esBsnademaftai sSpi1kes0we e = ct ae hove sl veyogee a 7sof becp ke. Becausethebobwhiteserawere50limited,olyfourmatrixspikesampleswereprepared.Allmatrix 55 LaboratoryControl Samples Liorory CoeSri wotsoponestof issy. 56 SampleRelated Comments Surnperctsseveswreytttoyywirosna ypstliospeardlseS li t oeaR0OS.Oathe,mancesv FEwaEs Euan, 620666 EE -- E E S P ptusS sy E oL E Tn . LSYir,s " E GA S E rpe EtT n ebe t Ai tt, T,o STR ie eT reissT in T e eR ep h fet tI e rr p ir me i + Limitsofquantitation PFOSinser is 0010pg/L;PROS i versapproximately0.070 ugg e STRt mit + Acceptableduplicateprecision - 30%,ssesedbyanalysisofteMSIMSDs. ept EEmegteni cemttyg vn r st t)sme eoryens TSa E mE E pr e ERS I E e E Et es Steoeue stsest enon reset, ok C0667 o+ Aichidmc'T?E ARAEEIEO TTTURry ++ AAttaaAB.:TTccaabblleehhooffeemmlsslooeeffevaneasrslatylt ++ AAatchaencCD::hSnammfpleeRrneocoetilptomWiki nt,LTD + AvaEEcxnchionmsodmelynicldsua Ressatf oclt GN0GE8 ThtLClpl,onA,Adviy ce o Chir Te, LtP,udrcey--l ovesig Cl neE-- 03De[e23l01 2D3e/23/01 he 3 ret Yorlalos Gn0GE9 9 Signatures |i i" Fadl Toast LL FD.4roc yee vir ocsosBseo0 TyAsteUa 6-To00 sSi oe PETE ge n0670 LaboratoryReport Analytical Report of Data for PFOS Dietary LC50 Study in Northern Bobwhite (Sera and Liver) Laboratory Report No. FACT-TOX-129 (U2723) "Attachment A "TableofResult- LiverAnalysis * DDaayy3-s7 Dy2 6008671 --_--_sor --nmnm E=tS= Boeo=e=e BESEEarh oeI s r=m BR | [=[ = TaTe Rom) [Re |c onm | o wx |m wmm | n wu | [omer| toemn |= | wn| | ETE TET re 3 4 lam[EE] 1] og eTe EEeEeTETTTL LittQueso (100PROS pointy070i. =a Do a oun,euneeoLac UUL7R --_--m ==eS= --eole EBgeBEo zBesa oh peinnie aova.oi DRBEETE a [=[ =ToT EE EE ET viinomsor = |BeseTETeTa T E EN=E EE[iT GiEET oiFR Ed |b=d eer tu(L03r 0) 1705si ie n 57s. Ere 020673 FACT-TOX-129 50874 620875 n0G76 nOG77 oo ) 650678