Document 3Q9bg2mOBwDJjy4kvyGGNagm0
3M SpecialtyMaterials
May 23,2000
3M Center St.Paul,MN 55144-1000 651733 1100
Dr.CharlesAuer,Director Chemical ControlDivision OfficeofPollutionPreventionand Toxics UnitedStatesEnvironmentalProtectioAngency 401 M StreetS,outhwest Room 403,EastTower (MailCode 7405) Washington,D.C. 20460
Re: Informationon PerfluorooetanSeulfonates and RelatedCompounds - AdditionalInformation
Dear Charlie:
Iam enclosingadditionailnformationthatdidnotgetsubmittedwiththerecentMay 18,2000 submittaltoyou on perfluorooctanseulfonateasnd relatedcompounds. This informationincludes:
1. An additionaslummary and reporton N-ethylperfluorooctasnuelfonamidoethano(lNETFOSE Alcohol) and a revisedN-ETFOSE AlcoholBibliographySheetthatincludes thisreport.
2. Informationon N-methylperfluorooctanesulfonamidoeatchryyllat(eMeFOSEA).
3. Informationon PerfluorodecanesulfonaAtmem,onium Salt(PFDS).
4. Informationon Perfluorooctanseulfonylamido(ethyla)cetate(PFOSAA) and a revised PFOSAA BibliographySheetthatreferencesFC- 127 as anothersynonym forthis compound.
5. Informationon N-ethylperfluorooctanesulfanamidoetahcyrlylate(ETFOSEA) and a revisedETFOSEA BibliographySheetthatreferencesa studynot includedon thebibliographysheetlastweek.
The BibliographySheetsforMEFOSEA and PFDS were includedas partofthe May 18'hsubmittal and remain unchanged.
Very trulyyours,
WilliamA. Weppner, Directorof Environmental,Health,Safety And RegulatoryAffairs SpecialtyMaterialsMarkets 3M Center,Bldg.236-IB-10 (651)733-6374(phone) (651)733-1958(fax) E-mail: waweppner@,numn.com
N-ETFOSEAlcoholBibliography
Synonyms: FM 3422, FM 39M, FM 4635,FM 4120,F 9=, FC-10
PhysicaUChemical Properties rdle
Water solubility LetterReport. BoilingPoirdInformaDon DeterminationofVapor PressureCurve by Dynamic Method forU1463 (EtFOSE) llntemalMemo -Merdng PointofFM-= N-EthylFOSE Ak*W
Laboratoryor Author
Date Completed
3M Env. Lab
11/15/77
ASel
11/30/98
ASci 3M SMMD Analytical
Lab
1
11/6/98 11/22/99
Type
Robust summary, relevantpages from
"Anoy&W Methodology on FM
34= Robust summary, Wwroport
Robust summary, firkwreport
Robust summary, War report
EnvironrrwntalFate and Transport Title
Tech Report-BiodegradatioSntudiesofFkwocarbons, Request forLaboratory work - BOD/COD, Mmm - Chronolog!cW Review of BiodegradationStudieson FM3422, Tech Report - BiodegradationStudiesof Fluorocarbons- 11.(Robust summary for4 documents)
Tech Report - Bk)ooncentraUonof FM3422 In BluagilSlunfishand InChanrol Catfr.h,Tech Report - AquaticFate ofa FluorocherrdealF:M 3422 Tech Notebook copies- AriaVicalfrom fishbwconcentrationdwies
Alkalinehydrolysis
Laboratory or Author
Completion Date
Type
3M Env. Lab
8/12/76, July,1977,
8/12177, 1/g/78
Robust summary, 2 technkw reports, work request,review
document
3M Env. Lab G. Vraspir
3M Env. Lab
5/17/1977, 10/14/77,
3/8/93 1/15f76 -
2/l/78
11/15/77
Robust summary, 2 technicalreports, critiqubey i.w.
GIIWft(Comal)
??? Robust summary, rowmt pages from
"Anoydeal Methodology on FM
34=
Pilotstudieson soU adsorption Evaluationof the Bbwneentration Potentiaolf FM 3422 ITech Report - Adsorpfionof FM-3422 on Soil
3M Env. Lab 3M Env. Lab 3M Env. Lab
10,13,78. 5/19/93, l2/3Of75. 3/7f77,
Robust summary, page from technical notabook ai8que from S. Boyd (MSU)
4/12177, oW 2 pages of data
5/gf77
summaries.
Robust summary.
8/16/78
cduque from G.W. Glktt (CornelQ, technicalreport
Robust summary, critiquferom S.
gIlf78
Boyd (MSU), 1 technicalreport
EnvironmentFaalteandTransport Title
Tech Report-AnalysisforFluorochomicalIsnBluegilFlish
Tech Report-BioaccumulationofFluorochomicalIsnTenn. RiverT,ech ReportFluorochemicalsInTenneessee RiverFish.
TechnicalReport-Photolos ofFM 3422 on Sol Tech Report- FM-3422 Phatolos SbxlyusingSimulatedSunlight Tech Report- Determinatioonfthe PanftionCoefficien(tN-Octano&Water)ofFM 3422
Laboratoryor Author
3M Env. Lab
Completion Date
5/l/79
Type
Robustsummary, critiquferomJ.W. Gillet(tComeU), technicarleport
3M Erw. Lab
3M Env. Lab 3M Ag. ProductsLab
NOTOX Safety& Environmental Research
5/22179, 12128/79.
318/93
12/10/79 8/11/81
Robust summary, 2 technicarleports, cirftquferomJ.W. Giik#(Comd)
Robust summary, technicarleport critiquferom S.
Boyd,MSU Robust summary, technicarleport
6/2/94
Robust summary, technicarleport
Sunwnary Reports Title
Laboratoryor Author
3M Env.Lab
Completion Date
11/15177
Type
Technicalreport, CriUqueby S. Boyd (MSU) Exerptsfrom thisreportappended
tosolublutaynd alkalinheydrolysis robustsummaries.
Tech Report-AnalyUcalMethodologyon FM 3422
Tech Report-AnalyticaMleftiodok)gaynd Support Tech Report-FinalcomprehensiveReporton FM 3422
3M Env.Lab 3M Env.Lab
1/17/79
2/7/1979, 3/8/93
Technicalreport.
Exerptsfromthis reportappended to solubilitayl,kaline
hydro"s,voWUlty, distribution
coefficiensto,il adsorption,
biodegradationa,nd fishchronictoxicity robustsummaries.
TechnicalReport, crrdquebyi.w. GllkM(ComeiQ
EcotoxicftyElements Title
Laboratoryor Completion
Type
Author
Date
The EffectsofContinuousAquems Exposureto78.01 on HatchabiliotfyEggs and Growth and SurvkM ofFryofFatioadMinnow (PimgRbliesRMDIM ,Summary of HistopathologicEaxlaminabons of FaVioadMknm (PkmphoWs promelas)Exposed to78.01for30 Dap-.
EG&G BWnomics
Tech Report- Mufti-PhaseAlgalAssay Test MeUwd.
3M Erw. Lab
June, 1978, Sept. 1978
12130/81
Robust summary, 2 technIcArepoftb, exerptfromTech Report- Anaoc&J Methodologyand Support(1/17179)
Robust summa technicarleport.
Perfluorooctane sulfonylamido(ethyl)acetate PFOSAA
Synonyms: FC-109, FC-109-X, FC-127, FC128, FC-129, E2113, E2566-2, R1904
Physical/ChemicalProperties Title
Laboratoryor I Author
Date Completed
Environmental Fate and Transport Title
Tech. Report Fateof Fluorochemicalsinthe Environmenta-l(sic)(Warburg respirometemrethod forbiodegradatioonf FC-128) Ready Biodegradabiliotfy FC-128 - BOD/COD
Laboratoryor Author
3M Env. Lab
3M Env. Lab
Tech report-AnalysisforFluorochemicalsinBluegill 3M Env. Lab
Fish Ready biodegradabiliotfyFC-127 - BOD/COD
3M Env.Lab
Date Completed
8/lZ76
7/8177 5/l/79 8/19181
Ready biodegradabiliotfyFC-109-X - BOD/COD
Pace Laboratories, Minneapolis,MN
12/31/87
Type
Type
Robust summary, technical report
Robust summary, copiesof date sheets
Robust summary, technical report
Robust summary, copiesof data sheets
Robust summary, copy of computer resultfsrom archives
Summary Reports Title
Laboratoryor
Date
Type
Author
Completed
EcotoxicityElements Title
Acute toxicitoyf FC-128 tofatheadminnow
Acute toxicitoyf FC-128 tofathead minnow
Acute toxicitoyf FC-1 28 to fatheadminnow
Acute toxicitoyf FC-1 27 to fatheadminnow Toxicityof FC-127 to activatedsludge @respiration
Laboratoryor Author
3M Env.Lab 3M Env.Lab 3M Env.Lab 3M Env.Lab 3M Env.Lab
Completion Date
5/18/74
6/29/74
8/26/77
7/24/81 8/14/81
Type
Robust summary, copiesof data sheets
Robust summary, copiesof data sheets
Robust summary, copiesof data sheets
Robust summary, copies of data sheets
Robust summary, copies of data sheets
Ready Biodegradability":ModifiedOECD Screening Test"forFluorad FC-129 MicrobicsMicrotoxToxicityTest - FC-109-X ActivatedSludge RespirationInhibitio-nFC109-X
Acute Toxicityof E2566-2 to Daphnia magna Acute Toxicityof E2566-2 to Fathead Minnow (Pimephales promelas)
Biodegradation(methyleneblue active substance)
Acute ToxicityofRi 9D4 to Daphnia magna Growth Inhibitioonf Ri 904 forGreen Alga (Selenastrum capricomutum) Acute Toxicityof Rl 904 to Fathead Minnow (Pimephales promelas)
MicrobicsMicrotoxToxicityTest - FC-129 Inhibitioonf Rl 904 forActivatedSludge Respiration
Rl 904 BOD Report for3M Company
RCC, Itingen, Sm(itzeriand
3M Env.Lab
3M Env.Lab ABC
Laboratory, Columbia, MO
ABC Laboratory, Columbia, MO
Pace Laboratories,
Inc., Minneapolis,
MN ASci Corporation, Duluth,MN ASci Corporation, Duluth,MN ASci Corporation, Duluth,MN ASci Corporation, Duluth,MN AScl Corporation, Duluth,MN AScl Corporation, Duluth,MN
9/19/84 10/15/87 10/30/87 1/9/88 1/12/88
2/15/89 6/17/97 6/18/97 6/27/97 7/g/97 7/10/97 Jul-97
Robust summary, memo about study reliabiliftiyn,al
report Robust summary, copies of
data sheets Robust summary, copies of
data sheets
Robust summary, final report
Robust summary, final report
Robust summary, computer report,copies of
data sheets
Robust summary, final re rt
Robust summary, final report
Robust summary, final report
Robust summary, copiesof data sheets
Robust summary, final report
Robust summary, final report
EthylFOSEA
Synonyms: FX-13, B1228. D-1
Physical/ChemicaPlroperties Title
Determinatioonf Physico-chemicaPlropertieosf isample D-1 EnvironmentalFateand Transport Title Ready biodegradabiliotfFyX-13 (BOD/COD)
Ready BiodegradabilitTyestof D-1
BioaccumulationStudy ofSample D-1 with icarp (gykn@nuscarpio
Laboratoryor Author Mitsubishi
Chemical Safety InstituLtted., Yokohama,
I Japan 1
Date Completed
2/14/96
Type 1Robust summ.ary,finarleportj
Laboratoryor Author
3M Env.Lab
Mitsubishi Chemical Safety
InstitutLetd., Yokohama,
Japan Mitsubishi ChemicalSafety InstitutLetd., Yokohama,
Japan 1
Completion Date
4/26/84
Type
Robustsummary, copiesof data sheets
10/31/95
Robust summary, final report
Robust summary, final
11/30/95 1
report
EcotoxicitEylements Title
Laboratoryor Author
Acute toxicitoyf FX-13 tofatheadminnow
3M Env.Lab
ActivatedSludge RespirationInhibitioTnest-
IFX-13
I 3M Env.Lab
Completion Date
4/1/84
5/17/84
Type
Robust summary, copiesof data sheets
Robust summary, copie data sheets