Document 3N9z6p8XdYj9o01VjXVQ0mvG0

AA'Wfe -' * y x December 12, 1990 Mark Hross Gary Jones Mike Marshall Attached are copies of handouts from the 12/10/90 TCC meeting. Please have your comments to me on the Generic Product Stewardship System Requirements section by December 14. R. K. Hinderer 1212-1/jp 20893001 BFG07791 BHFQoodrich 3925 Embaay Partcway Akron, OMo 44333-1799 Telephone: 216-374^366 Fax; 216-374-2238 The BFGoodrteh Company Environmental Heotth 6 Safety Management Systems TELECOPY COVER SHEET f W_}) DATE: TIME: NUMBER OF PAGES: (INCLUDING THE COVER) p.`3& JO; T2y*(JiL> -T^/zn StL OF: fax# ___________ --2 92 - 'fdQ ! FROM: TBoS> OF: _______________________________ COMMENTS: zoocssoz T BFG07792 GENERIC PRODUCT STEWARDSHIP SYSTEM REQUIREMENTS RAW MATERIALS A. RESEARCH AND DEVELOPMENT 1. ACQUISITION - R & D CHEMIST REQUESTS SAMPLES. - SALESMEN VOLUNTARILY SUBMIT SAMPLES. 2. REQUIREMENTS - MATERIAL SAFETY DATA SHEET (MSDS) MUST BE ACQUIRED FOR ALL MATERIALS, EITHER BY: CHEMISTS R & D HAZARD COMMUNICATION COORDINATOR MAINTAINED BY BOTH - TSCA INVENTORY CONFIRMATION NOT REQUIRED, BUT IF RECEIVED WITH SAMPLE, MUST DESIGNATE WHETHER KNOWN OR UNKNOWN STATUS. 3. RULES - NO MATERIAL MAY BE USED IN R & D WITHOUT AN MSDS. - CENTRAL R & D CHEMICAL TRACKING SYSTEM MUST INCLUDE: CHEMIST'S NAME DATE RECEIVED MSDS YES/NO TSCA - STATUS KNOWN YES/NO ON INVENTORY - UNKNOWN TRADE NAME CHEMICAL NAME SUPPLIER CAS NUMBER OF SUB-INGREDIENTS 20893003 BFG07793 B. PILOT PLANT AND FULL-SCALE PRODUCTION REQUIREMENTS 1. RULES - MUST CONFIRM HAZARD COMMUNICATION COMPLIANCE. MSDS MUST BE TRANSFERRED TO PILOT PUNT. EVALUATE FOR INTERNAL UBEL SYSTEM, I.E. HMIS/NFPA/OTHER. IDENTIFY SUB-INGREDIENTS FOR MSDS WRITING SYSTEM AND LOAD ONTO DATABASE. - HAZARDOUS WASTE STATUS MUST BE DETERMINED. TSCA INVENTORY CONFIRMATION IS REQUIRED. YES/NO IF NO, MUST CONFIRM R & D RECORDKEEPING IS IN PUCE. - MANDATORY^CERTIFICATION LETTERS ARE REQUIRED FROM EACH QUALIFIED SUPPLIER FOR EACH RAW MATERIAL. THE DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT MUST CERTIFY TO PURCHASING AUTHORITY TO PURCHASE BY ADDITION TO QUALIFIED SUPPLIER LIST. PURCHASING MAY NOT PURCHASE ANY RAW MATERIALS FOR PILOT PUNT OR FULL-SCALE PRODUCTION WITHOUT AUTHORIZATION FROM HS&E DEPARTMENT. IENTS - RESEARCH AND DEVELOPMENT, PILOT PUNT OR FULL-SCALE MANUFACTURING ;t DETERMINE TSCA INVENTORY status, yes/no IF NO, MUST SEND R & D TSCA NOTICE TO RECEIVER. MUST ALSO CONFIRM R & D RECORDS. - SEND MSDS AND CONFIRM LABEL. 05 CS5 Co BFG07794 nPMiil ATIONS (INTERMEDIATES AND FINISHED GOODS) A. RESEARCH AND DEVELOPMENT 1. MINIMUM RECORDKEEPING REQUIREMENT, EITHER CHEMIST OR CENTRAL. - IF NEW CHEMICAL IS CREATED (I.E. SYNTHESIZED), THE FOLLOWING RECORDS MUST BE MAINTAINED AND CONFIRMED: (A) COPIES OF OR CITATIONS TO INFORMATION REVIEWED TO DETER MINE THE RISK OF NEW SUBSTANCE. (B) COPIES OF NOTICES OF RISK (I.E. LABELS, MSDS, OTHER). (c) DOCUMENTATION OF PRUDENT LABORATORY PRACTICES. (o) NAMES AND ADDRESSES OF PERSONS TO WHOM SUBSTANCE IS DISTRIBUTED. IDENTITY OF SUBSTANCE TO EXTENT KNOWN. AMOUNT DISTRIBUTED. COPIES OF NOTIFICATIONS (I.E. LABELS, MSDS, OTHER). - IF NEW CHEMICAL IS MANUFACTURED AT GREATER THAN 100 KG PER YEAR, MUST MAINTAIN: IDENTITY OF SUBSTANCE TO EXTENT KNOWN. PRODUCTION VOLUME OF SUBSTANCE. DISPOSITION OF SUBSTANCE. 2. SHIPPING REQUIREMENTS DETERMINE TSCA INVENTORY STATUS OF ALL INGREDIENTS. YES/NO / IF NO, MUST SEND R & D TSCA NOTICE AND CONFIRM TSCA R & D RECORD MAINTENANCE. - SEND MSDS AND CREATE LABEL. - CONFIRM DOT COMPLIANCE. ') N 3 BFG07795 $002680 PILOT PLANT and full-scale production new formulations - CREATED by R & D, manufactured by pilot plant or full-scale production. rules - ALL FORMULATIONS MUST BE REVIEWED BY DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT, CONFIRMING THE FOLLOWING: TSCA COMPLIANCE HAZARD COMMUNICATION COMPLIANCE ENVIRONMENTAL COMPLIANCE FDATCOMPLIANCE Kafr, - IT IS SUGGESTED THAT A PIP/FORMULATION REVIEW SYSTEM BE IMPLE MENTED. .2 ALL FORMULATIONS MUST BE APPROVED AND CERTIFIED BY HEALTH, SAFETY AND ENVIRONMENTAL FOR THE FOLLOWING: - ALL INGREDIENTS ARE ON THE TSCA INVENTORY. - ALL INTERNAL REACTIONS ARE ON THE TSCA INVENTORY. - THE CHEMICALS ON REPORTING RULES (CORR) MUST BE REVIEWED AND COMPLIANCE CONFIRMED. - MSDS MUST BE CREATED. - LABEL MUST BE CREATED. - ENVIRONMENTAL STATUS MUST BE DETERMINED (I.E. HAZARDOUS WASTE STATUS, PROPOSITION 65 STATUS, CERCLA STATUS, ETC.). ANY TOXICITY TESTING MUST BE CONFIRMED. - TME'S, PMN'S, ETC. .. 3. MANUFACTURING FACILITIES ARE NOT AUTHORIZED TO PRODUCE ANY FORMU LATIONS WITHOUT A DIVISIONAL HS&E DEPARTMENT CERTIFICATION ON OR WITH THE FORMULATION (I.E. RECIPE AND INVENTORY CONTROL CARD). 2O893O0G 4 I BFG07796 4. PROCEDURE a. R & D SUBMITS FORMULATION TO DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT FOR REVIEW. B. DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT PERFORMS REVIEW. c. DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT APPROVES FORMULATION AND CERTIFIES TO INVENTORY CONTROL ON THE FORMULATION RECIPE. o. MANUFACTURING IS THEN AUTHORIZED BY INVENTORY CONTROL TO PRODUCE. 5. MODIFIED FORMULATIONS - R & D GENERATED MODIFICATIONS - MANUFACTURING GENERATED MODIFICATIONS RULES A. ALL MANUFACTURING MODIFIED FORMULATIONS MUST BE REVIEWED AND APPROVED BY A RESPONSIBLE R & 0 CHEMIST. B. ALL R & D MODIFIED FORMULATIONS MUST BE APPROVED BY PLANT PROCESS ENGINEERING AT MANUFACTURING. C. ALL MODIFIED FORMULATIONS MUST BE ROUTED THROUGH THE NEW FORMULATION REVIEW PROCEDURES OUTLINED ABOVE. 6. SHIPPING REQUIREMENTS S*- CONFIRM TSCA COMPLIANCE. YES/NO ( IF NO, SEND R & D NOTICE AND CONFIRM R & D TSCA RECORDS. 1 - CONFIRM MSDS AND LABEL. \ - CONFIRM DOT PROCEDURES.^ V A\ - CONFIRM FDA-AND USDA,PROCEDURES. ) // 20833007 - 5 BFG07797 C. PURCHASE FOR RESALE 1. RULES TSQMj /=>*; / / A. MUST OBTAIN MSDS, LABEL AND TSCA CERTIFICATION FROM SUPPLIER AND SUBMIT TO DIVISIONAL HEALTH, SAFETy AND ENVIRONMENTAL DEPARTMENT. / B. HEALTH, SAFETY AND ENVIRONMENTAL DEPARTMENT MUST CREATE MSDS AND LABEL, PERFORM ENVIRONMENTALCFDA AND TSCA^REVIEW, AND CERTIFY AUTHORIZATION TO PURCHASING: ( alu-^xSGrtPs. c. PURCHASING MAY NOT PURCHASE ANY PURCHASE FOR RESALE UNTIL ^ AUTHORIZED BY DIVISIONAL HEALTH, SAFETY AND ENVIRONMENTAL ? DEPARTMENT. D. BY-PRODUCTS OR WASTESTREAMS USED OR DISTRIBUTED FOR COMMERCIAL PUR POSES OTHER THAN DISPOSAL. - PROCEDURES FOR MODIFIED FORMULATIONS MUST BE FOLLOWED AS IF INITI ATED BY MANUFACTURING PLANT (I.E. THESE MATERIALS REQUIRE HAZARD COMMUNICATION COMPLIANCE, TSCA COMPLIANCE, ETC.). IMPORTS A. RULES 1. ALL PERSONS AUTHORIZED TO IMPORT MUST BE IDENTIFIED. 2. ALL OTHER PERSONS MUST BE INFORMED THAT NO IMPORTS ARE AUTHOR IZED. 3. ALL IMPORTS MUST BE REVIEWED AND CONFIRMED FOR THE FOLLOWING: ALL INGREDIENTS ARE ON THE TSCA INVENTORY. REVIEW THE CHEMICALS ON REPORTING RULES LIST (CORR) FOR REPORTING RULES. U.S. MSDS ANO LABELS MUST BE CONFIRMED AND/OR PREPARED. CONFIRM FDA/USDA/v^ , 5* CS CJ 86 ou BFG07798 &QBtt A. RULES 1. ALL PERSONS AUTHORIZED TO EXPORT MUST BE IDENTIFIED. 2. ALL OTHER PERSONS MUST BE INFORMED THEY ARE NOT AUTHORIZED TO EXPORT. 3. ALL EXPORTS MUST BE REVIEWED AND CONFIRMED FOR THE FOLLOWING: ALL INGREDIENTS MUST BE IDENTIFIED. REVIEW TSCA 12(b) EXPORT REPORTING LIST. IF ANY OF THE INGREDIENTS ARE LISTED ON THE 12(b) EXPORT LIST, THEN NOTICE MUST BE SENT TO EPA PRIOR TO THE TIME OF EXPORT. FOREIGN TSCA, HAZARD COMMUNICATION AND FDA EQUIVALENT LAWS AND REGULATIONS MUST BE CONFIRMED ON ALL EXPORTS79u NON-INVENTORY CHEMICALS A. EXAMPLES - LAB SUPPLIES, JANITORIAL SUPPLIES, MAINTENANCE SUPPLIES. 1. THE USING FACILITY MUST MAINTAIN MSDS FOR ALL COMPOUNDS. 2. THE USING FACILITY MUST MAINTAIN THE INGREDIENTS FOR ALL COM POUNDS FOR SARA TITLE III REPORTING PURPOSES. M 7 BFG07799 G00CG80; RECOMMENDED IMPLEMENTATION TIME LINES CORPORATE AUDIT FOR TSCA COMPLI ANCE O UJ o boi til >=3 Ot 3 2: a. 20893010 oLU a uo UJ (/) til < ui CSI c<rn >- < Q a. < Q * X (1--/) z su:] *z--i to WZh (/) hi zH Z uj (<llOL/I) tZH--o z13U--J <_UoJl <<(9C CUaJJ: ss io-- a uj UJ HLU HUJ >Mh-- tZU-J CZLkJl CUCOaoSJJ:JQeOUHc. uWWUUO.I ' CUJJ t--11 U1J Z< ZHKH (1Q//1i Z iH/-i =aUa>J < Ut--J CtzJ--il1 Uzt--J co<QOOc. <c KI=OH3- tt>ooZ tZUoJ- CJ < Z Z <C "3 BFG07800 TSCA & HAZARD COMMUNICATION COMPLIANCE PROGRAM SUMMARY BFG07801 20893011 RAW MATERIAL TRACKING SYSTEM CHEMICALS ARE RECEIVED INTO R&D BY THE LAB AIDE, WHO IMMEDIATELY NOTIFIES THE RECEIVING CHEMIST AND REQUIRES A "RECEIPT OF CHEMICAL" FORM BE COMPLETED BEFORE RELEASING THE MATERIAL TO THE CHEMIST. THIS FORM IS SUBMITTED TO ENVIRONMENTAL ALONG WITH A MATERIAL SAFETY DATA SHEET (MSDS). IF AN MSDS IS NOT RECEIVED WITH THE MATERIAL, ENVIRONMENTAL WILL IMMEDIATELY REQUEST ONE FROM THE SUPPLIER. AN R&D CODE NUMBER IS ASSIGNED BY ENVIRONMENTAL AND ALL CHEMICAL INFORMATION ADDED INTO THE COMPUTER, IE., TRADE NAME, CHEMICAL NAME, SUPPLIER, CAS NUMBER. AN EXPERIMENTAL (99 SERIES) CODE NUMBER IS ASSIGNED FOR ALL RAW MATERIALS BEING USED IN EXPERIMENTAL BATCHES AT THE PILOT PLANT OR THE MANUFACTURING PLANTS.' UPON ASSIGNMENT OF A 99 NUMBER A RAW MATERIAL SPEC SHEET IS WRITTEN BY THE CHEMIST AND SENT TO THE SUPPLIER FOR CONFIRMATION. A RAW MATERIAL EVALUATION FORM IS CIRCULATED IN ENVIRONMENTAL WHICH REQUIRES HMIS RATINGS, HAZARDOUS WASTE INFORMATION AND A BREAK DOWN OF THE SUB-INGREDIENTS IN THE RAW MATERIAL. ALL THIS INFORMATION IS ADDED TO OUR CHEM-LINK DATA BASE. A TSCA CERTIFICATION LETTER IS IMMEDIATELY SENT TO THE SUPPLIER TO ENSURE TSCA COMPLIANCE. WHEN A RAW MATERIAL IS GOING TO BE USED IN AN IN-LINE PRODUCT, A PERMANENT (50-58 SERIES) CODE NUMBER IS ASSIGNED. IF THE PRODUCT DID NOT PREVIOUSLY HAVE A 99 NUMBER, ALL INFORMATION NOTED ABOVE WILL BE COMPLETED. BATCHCARDS WILL NOT BE RELEASED FOR PRODUCTION AT THE MANUFACTURING LEVEL WITHOUT TSCA CERTIFICATION. BFG07802 20893012 RAW MATERIAL TRACKING SYSTEM BFG0T803 20833013 TO:' ENVIRONMENTAL AFFAIRS REPORT OF RECEIPT OF CHEMICAL SUPPLIES 3ECEIVED BY CHEMIST APPROVED BY GROUP MANAGER SUPPLIER NAME _____________ ADDRESS _____________ Code No. Akkigned Amt Rec Description DATE RECEIVED The chemical(s) listed below have been reviewed to ensure the following: 1. Minimum quantity necessary has been ordered. 2 MSDS and label have been reviewed. 3. Safe work practices established and appropriate personal protection is available. Chemical Name MSDS Rec ' Note: Attach MSDS, TSCA information and any other Environmental or Health information available. 000-118 Rev. 1/88 BFG07804 3735 GREEN ROAO BEACMWOOO. OHIO 44122 216/292*5000 DIRECT DIAL NUMBER Re: Material Safety Data Sheet Request/ Toxic Substance Control Act (TSCA) 15 use 2601 et. sea. Compliance Activities Dear Sir or Madam: As a supplier of raw material chemicals to Tremco, Inc., it is important that you answer all the following questions in order to insure that the raw materials which you are supplying are in compliance with specific provisions of the Toxic Substances Control Act (TSCA) 15 USC 2 601. et. sea. A list of the raw material(s) that we are inquiring about is attached. For each raw material listed on the attached, please answer the following: 1. For chemical substances: Is the substance registered with the EPA on the list or "inventory" of existing chemical substances either by inclusion on the initial inventory or by submitting a Premanufacture Notification (PMN) after July 1, 1979, to the EPA? 2. For mixtures of chemical substances: Are all components of the mixture on the list or "inventory" of existing chemical substances either by inclusion on the initial inventory or by submitting a Preraanufacture .Notification (PMN) after July 1, 1979, to the EPA? 3. To the best of your knowledge, has a "substantial risk" notification been submitted to the EPA on the raw material(s) under Section 8(e) of the act? 4. Has the EPA proposed or promulgated "significant new use" rules or regulations under Section 5(a)(1)(B) or 5(a)(2) of the act for any product on the attached list? BFG07805 t/T 2083301 Page 2 uwmm 3735 GREEN ROAQ 8EACHWOOO. OHIO 44122 216/292*5000 DIRECT DIAL NUMBER Your cooperation, in promptly answering the above questions regarding the Tremco TSCA compliance activities, will be appreciated and will enable Tremco to purchase these raw materials from your company in the future. In addition to the above, please forward the most recent Material Safety Data Sheet (MSDS) for each product listed in order that Tremco may insure compliance with the Federal OSHA Hazard Communication Regulations at 29 CFR 1910.1200. Your cooperation in this matter will be appreciated. Please return a copy of this letter with your response to my attention. If you have any questions or comments concerning the above, please contact me or Mr. David Trimble, Corporate Manager, Environmental Affairs at 216/765-6734. Very truly yours. Administrative Manager Raw Material Code Number 0893016 TREMCO RAW MATERIAL SPECIFICATIONS GENERIC TYPE/TRADE NAHE_ SUPPLIER CHEMICAL NAME/MATERIAL NAME Composition CAS No. Physical/Chemical Properties Sp. Gc. C ' F3- Wt ./Gal.] Color_>___________________________ Viscosity Flash Point-OC/CC______________ Auto. Ign. Temp._______________ Acid No._____________________ Saponification No. P______ ,__________________________ Melt Point Distillation _______________ IBP 10% 50% 90% ______________________ Dry Point API Gravity_____________________ KB No.____________________________ % Water___________________________ Sol. in Water_________________ Sol. of Water in % Non-Volatile__________________ Iodine No. Storage Requirements^ % % % % % % % S. T. NO. IN-LINE CODE NO K & D NO. 99. NO. DATE %Unsaturation Oil Absorption Mass Tone______ ' Let Down Fineness (Av. Part. Size) % Retained on #10 % Retained on #20 % Retained on #30 % Retained on #40 % Retained on #50 % Retained on #70 % Retained on #100 % Retained on #200 % Retained on #325 % Retained in Pan % Water Sol. Salts . ________ Additional Physical/Chemical Properties Toxicity & Handling Precautions -- G .--____________nr> ur~ -- ----------------------------------------------------------------------- ---------------------------------------------------------------------------------------------------- NOTES: _________________ _________________ By___________________________ - . .1. Ensure that all supplier technical data sheet specifications are indicated above. 2 All Q.C. testing to be performed must be indicated by placing Tremco Standard Test Number above. 3. Are supplier provided specifications the same as Trem Q.C specifications? If not, you must notify Purchasing and the supplier to ensure specifications - can be met. 001-207 Rev. 6/86 BFG07806 CODE NUMBER; DATE: CHEMICAL NAME RAW MATERIAL DATABASE EXEMPT (Y/N): SUDDEN RELEASE PRESS (Y/N): EXEMPT DESIGNATOR: IMMEDIATE HEALTH (Y/N): HEALTH: DELAYED HEALTH (Y/N): FLAMMABILITY: FIRE HAZARD (Y/N): REACTIVITY: REACTIVITY HAZARD (Y/N): PERSONAL PROTECTION EQUIPMENT: HAZARDOUS WASTE DATABASE NUN-HAZARDOUS RCRA (4QCFR261)(Y/N): HASTE DOT PROPER SHIP. 'G NAME: SPILL RESIDUE: WASTE DOT/EEA REPORTABLE QUANTITY: SPILL RESIDUE NUMBER: WASTE DOT REQUIRED LABELS: HAZARDOUS WASTE CODE: WASTE DOT HAZARD CLASS: HAZARDOUS WASTE NUMBER: WASTE DOT I.D. NUMBER: COMPATIBILITY GROUP: WASTE DOT PACKAGING REG'S: SUB-INGREDIENTS DATABASE IS THIS AN ALTERNATE SOURCE OF AN EXISTING RAW MATERIAL? O YES Q KD IF YES, ARE THERE ANY CHANGES TO BE MADE TO THE SUB-INGREDIENTS DATA? |_J YES LIST NEW CHEMICALS (SUB--INGREDIENTS) OR REVERSE SIDE Q 150 TREMOO DRTO T.TNKg CHEMICAL NAME CAS NUMBER FORM % (WT) y BFG07807 NEW CHEMICAL CHEM LINK# CHEMICAL NAME CHEMICAL DATABASE NEW CHEMICAL CHEM LINK# CHEMICAL NAME CONFIDENTIAL NAME CONFIDENTIAL NAME CAS NUMBER TOXIC EXPOSURE DATA CAS NUMBER TOXIC EXPOSURE DATA OTHER TOXIC DATA IARC NTP OSHA ACGIH TPQ SARA 313 TCLP SARA 302 PROP 65 ' KENTUCKY AIR TOXIC CERCIA RCRA TSCA-12 (b) IARC NTP OSHA ACGIH TPQ SARA 313 SARA 302 PROP 65 TCLP KENTUCKY AIR TOXIC CERCIA RCRA TSCA-12 (b) NET? CHEMICAL CHEM LINK# CHEMICAL NAME NEW CHEMICAL CHEM LINK# CHEMICAL NAME CONFIDENTIAL NAME CONFIDENTIAL NAME CAS NUMBER TOXIC EXPOSURE DATA CAS NUMBER TOXIC EXPOSURE DATA OTHER TOXIC DATA IARC NTP OSHA ACGIH TPQ SARA 313 SARA 302 PROP 65 TCLP KENTUCKY AIR TOXIC CERCIA RCRA TSCA-12 (b) |Tob6 ()^ IARC NTP SARA 313 TCLP OSHA SARA 302 ACGIH TPO , . N PROP 65 KENTUCKY AIR TOXIC fc--c CERCIA RCRA TSCA-12 (t>) h* -- BFG07808 INTERMEDIATES/FINISHED GOODS TSCA CONTROLS o R&D EXPERIMENTAL MATERIAL (EXEMPT) TO BE SHIPPED o PIP WITH LABBOOK NUMBER* SUBMITTED TO BATCHCARD COORDINATOR o CHECK FOR TSCA CERTIFICATION ON ALL RAW MATERIALS o REQUEST VERIFICATION VIA FAX FROM SUPPLIER IF NECESSARY (PIP NOT PROCESSED UNTIL TSCA VERIFICATION RECEIVED) o COMPLETE ENVIRONMENTAL COORDINATOR PORTION OF PIP (INCLUDES TSCA VERIFICATION QUESTIONS) PIP SUBMITTED TO PRODUCT SAFETY SPECIALIST o "TSCA OK" INDICATED ON MSDS IF ALL COMPONENTS OF FINISHED PRODUCT ARE ON TSCA INVENTORY o "R&D USE ONLY" INDICATED ON MSDS IF ANY COMPONENT OF FINISHED PRODUCT IS NOT ON THE TSCA INVENTORY o PIP,MSDS,HAZARD WARNING SUBMITTED TO ENVIRONMENTAL MANAGER o CHECK REACTION CHEMISTRY FOR TSCA VERIFICATION o PMN FILED ON REACTION PRODUCT(S) IF NECESSARY o COMPLETE ENVIRONMENTAL MANAGER PORTION OF PIP (INCLUDES QUESTIONS ON TSCA VERIFICATION FOR REACTION PRODUCT(S)) o R&D EXPERIMENTAL MAY BE SHIPPED o SPECIAL RECORDKEEPING PROCEDURES ARE INITIATED, IF NECESSARY o QUANTITY OF'MATERIAL SHIPPED MUST BE RECORDED o RECEIVER OF MATERIAL SHIPPED MUST BE RECORDED o RECEIVER OF MATERIAL MUST BE NOTIFIED OF TSCA STATUS LABBOOK NUMBER ASSIGNED (FORMAT: AAAA-BB-CC-D) A-SPECIFIC NUMBERED LABBOOK B-SPECIFIC DEVELOPMENT CHEMIST ALPHA CODE C-SPECIFIC PAGE NUMBER D-ALPHA SEQUENCE IF MORE THAN ONE FORMULATION OR VARIATION PER PAGE BFG07809 0Z0E680Z INTERMEDIATES/FINISHED GOODS TSCA CONTROLS PILOT PLANT AND MANUFACTURING PLANTS PROCESSING OF BATCHCARD FOR MATERIAL TO BE PRODUCED o BATCHCARD AND PIP SUBMITTED TO BATCHCARD COORDINATOR (PILOT PLANT CARD USES LABBOOK NUMBER o MANUFACTURING PLANT CARD USES EXPERIMENTAL OR IN-LINE CODE NUMBER o CHECK FOR TSCA CERTIFICATION ON ALL RAW MATERIALS o REQUEST VERIFICATION VIA FAX FROM SUPPLIER IF NECESSARY (BATCHCARD PIP NOT PROCESSED UNTIL TSCA VERIFICATION RECEIVED) o COMPLETE ENVIRONMENTAL COORDINATOR PORTION OF PIP (INCLUDES TSCA VERIFICATION QUESTIONS) o BATCHCARD AND PIP SUBMITTED TO PRODUCT SAFETY SPECIALIST o "TSCA OK" INDICATED ON MSDS IF ALL COMPONENTS OF FINISHED PRODUCT ARE ON TSCA INVENTORY o "R&D USE ONLY" INDICATED ON MSDS AND LABEL IF ANY COMPONENT OF FINISHED PRODUCT IS NOT ON THE TSCA INVENTORY o BATCHCARD, PIP, MSDS AND HAZARD WARNING SUBMITTED TO ENVIRONMENTAL MANAGER o CHECK REACTION CHEMISTRY FOR TSCA VERIFICATION o PMN FILED ON REACTION PRODUCT(S) IF NECESSARY o COMPLETE ENVIRONMENTAL MANAGER PORTION OF PIP (INCLUDES QUESTIONS ON TSCA`VERIFICATION FOR REACTION PRODUCT(S)) o BATCHCARD STAMPED AS REVIEWED FOR TSCA REQUIREMENTS o STAMPED INDICATING PMN FILED IF NECESSARY o MANUFACTURING PLANT BATCHCARDS SUBMITTED TO COST FOR ENTRY TO DATA BASE (THIS STEP IS OMITTED FOR PILOT PLANT BATCHCARDS) o BATCHCARD IS SENT TO PLANT READY FOR PRODUCTION o SPECIAL RECORDKEEPING PROCEDURES ARE INITIATED, IF NECESSARY o QUANTITY OF MATERIAL SHIPPED MUST BE RECORDED o RECEIVER OF MATERIAL SHIPPED MUST BE RECORDED o RECEIVER OF MATERIAL MUST BE NOTIFIED OF TSCA STATUS BFG07810 20893021 INTERMEDIATES/FINISHED GOODS TSCA CONTROLS 'Z Z 0 C 6 8 0 to LABBOOK NUMBER ASSIGNED (FORMAT: AAAA-BB-CC-D) BFG07811 PRODUCT INFORMATION PROFILE TREMCO Product Code No. TREHCO Product Registry No. Batchcard Priority RUSH [] 1. Development Chemist NORMAL [] If rush, state date required SIGNATURE DATE COMPLETED _______________________________________ _____________________ 2. Group Manager _______________________________________ _____________________ 3. Batchcard Coordinator _______________________________________ _____________________ 4. Product Safety Specialist _______________________________________ _____________________ 4a. Plant D.O.T. Specialist _____________________ 5. Batchcard Coordinator _______________________________________ _____________________ 6. Industrial Hygienist _______________________________________ _____________________ 7. Batchcard Coordinator _______________________________________ _____________________ 8. Manager-Environmental Affairs _____________________ 9. Batchcard Coordinator _______________________________________ _____________________ Chemist Name Lab Book Number Card Issue Date Product Name (per Marketing) Product Class (Flooring, Coating, etc) Application (Brush, Spray .etc) Previous TREMCO Experimental Code Number (If applicable) __________________________ Actual Production Location(s): I. DEVELOPMENT CHEMIST SECTION A. Indicate type of card: Pilot Plant Card [] White Card [] Experimental Card [] Pink Card [] Alternate Card [] Purchase for Resale [] Indicate below the reason for issuing this batchcard. This reason is also to be indicated on the batchcard in the Remarks/Special Remarks Section of batchcard. B. Does the formulation include intermediates? (If no, go to Question F) Yes [] No [] C. Do the intermediates involve a chemical reaction? (If no, go to Question E) Yes [] No [] D. List the Intermediate Code Numbers below and in Section V.A. which involve chemical reactions: 0893023 i BFG07812 E. List any special storage conditions required for any of the Intermediates. F. Does a chemical reaction occur in this formulation on this batchcard? (If no, go to Question H) Yes [] No [] G. List the Raw Material/Intermediate Reactant Code Numbers and describe reaction chemistry below and in Section V.C. H. List any special storage conditions required for any of the raw materials. I. Are there Raw Material Spec Sheets for all raw materials in this formulation and are these appropriate? Yes [] No [] (If yes, go to Question J) If no, a new code number must be obtained and a new raw materials spec sheet must be prepared and given to the Environmental Administrator. J. List any special storage conditions required for the product. K. Are the Quality Control Procedures and Specifications established in the Q.C. Section of the batchcard and are these correct? Yes [] No [] (If revised card, ensure Q.C. specifications have not changed.) L. Indicate the old stock check period for the product. M. What is the product maximum shelf life from date of packaging? c os o 2 BFG07813 N. Indicate the following physical/chemical characteristics. All information must be generated by the development chemist or by the Technical Services Group. ALL BLANKS MUST BE COMPLETED (* - complete if flashpoint <140*F) Weight/Gallon _______________ Color ___________ Specific Gravity _______________ Physical State Melting Point _______________ Evaporation Rate Boiling Point _______________ Odor Freezing Point _______________ Flashpoint Softening Point _______________ Method(TAG,SETA,etc.) Vapor Pressure _______________ Upper Explosive Limit(UEL)_ *Vapor Pressure @ 55C__________ mm Corrosive to Skin [] Yes [] No *Viscous Liquids Only Burn Rate Test (Potential Flammable Viscosity Test ISO 2431-72. ____________ Solids only)______ Solvent Separation Test ISO R1523-73 Vapor Density (Air-1) Lower Explosive Limit(LEL). pH (Aqueous) _____________________ Decomposition Temperature Solubility in Water_________________ Autoignition Temperature % Volatile By Weight Molecular Weight (If single substance) Comments: ______________________________________ O. Does the batchcard show: Issue Date Yes [] Weight/Gallon Yes [] No [] No [] Flashpoint (Liquids Only) Chemist Initials Yes [] Yes [] No [ ] No [] If no, state reason: P. Is this product potentially: (1) Ignitable Yes [] No [] ,(40 CFR 261.21)(D001) (Liquid @ 100*F - Flashpoint < 140'F) (Solid @ 100'F - Burns "vigorously and persistently") (2) Corrosive Yes [] No [] (40 CFR 261.22)(D002) (pH <2.0 or pH >12.5 for aqueous products) (Corrosive to SAE 1020 Steel >2.35 mm/year)(ie., DOT Corrosive Liquids) (Does NOT include DOT skin corrosives) (3) Water Reactive Yes [] No [] (40 CFR 261.23)(D003) (Does product react violently with water or generate toxic gases or fumes on addition of water?)(Does NOT include moisture sensitive polyurethanes) (4) TCLP (Toxicity Characteristic Leaching Procedure) Does the product contain any of the following: Yes [] No (] (Indicate total contents down to 0.1 ppm.) CAS NO. D004--Arsenic..................................................................................... D005--Barium........................................................................................ D018--Benzene..................................................................................... D006--Cadmium..................................................................................... D019--Carbon tetrachloride...................................................... 7440-38-2 7440-39-3 71-43-2 7440-43-9 56-23-5 20893025 3 BFG07814 D020--Chlordane............................................................................... D021--Chlorobenzene...................................................................... D022 --Chloroform............................................................................. D007--Chromium.................................................................................. D023- -o-Cresol*............................................................................... D024--ra-Cresol*............................................................................... D025--p-Cresol*............................................................................... D026--Cresol....................................................................................... D016- - 2,4-D......................................................................................... D027- -1,4-Dichlorobenzene....................................................... D028 - -1,2-Dichloroethane.......................................................... D029- -1,1-Dichloroethylene..................................................... D030--2,4-Dinitrotoluene.......................................................... D012- -Endrin....................................................................................... D031--Heptachlor (and its hydroxide)............................. D032- -Hexachlorobenzene............................................................ D033- -Hexachlorobutadiene....................................................... D034--Hexachloroethane............................................................... D008- - Lead............................................................................................ D013--Lindane.................................................................................... D009--Mercury.................................................................................... D014--Methoxychlor........................................................................ D035--Methyl ethyl ketone....................................................... D036--Nitrobenzene........................................................................ D037--Pentachlorophenol............................................................ D038--Pyridine.................................................................................. D010--Selenium.................................................................................. D011--Silver....................................................................................... D039- -Tetrachloroethylene....................................................... D015--Toxaphene................................................................................ D040--Trichloroethylene............................................................ D041 - -2,4,5 -Tr ichlorophenol................................................... D042- - 2,4,6-Trichlorophenol................................................... D017--2.4.5-TP (Silvex)............................................................ D043--Vinyl chloride................................................................... CAS NO. 57-74-9 108-90-7 67-66-3 7440-47-3 95-48-7 108-39-4 106-44-5 94-75-7 106-46-7 107-06-2 75-35-4 121-14-2 72-20-8 76-44-8 118-74-8 87-68-3 67-72-1 7439-92-1 58-89-9 7439-97-6 72-43-5 78-93-3 98-95-3 87-86-5 110-86-1 7782-49-2 7440-22-4 127-18-4 8001-35-2 79-01-6 95-95-4 88-06-2 93-72-1 75-01-4 (5) Is this compound specifically on either the 40 CFR 261.33 (e) or (f) list: (This question only applies to single specific chemical substances.) Yes[] No [] Q. Based on your review of raw materials and intermediates MSDS's, list any known health hazards: R. List any special handling requirements including safety or handling procedures, personal protective equipment, etc... <30893026 4 BFG07815 S. List any of the raw materials or intermediates contained in this formulation which are received with DOT markings or labels: Code # DOT Marking or Label Wording T. To the best of your knowledge, during production precesses are there: (1) Wastewaters? (Water cleanouts or azeotropes) (2) Waste Solvents? (Cleanout solvents or azeotropes) (3) Air Emissions? (Vented or fugitive) (4) Waste Products? (Mixer cleanout, scrap, etc.) (5) Personnel Exposures? (Uncontrolled or controlled) Yes Yes Yes Yes Yes [] U [] [] [] No [] No [] No [] No [] No [] Please consult with plant process engineering and explain details of any items marked "Yes" above. Be specific about quantities, types and ultimate emission or discharge location: U. Complete 100% formulation in Sections VI and VII and indicate components which should be maintained as confidential. If confidential, give maximum weight percent and generic names to be used on MSDS and label. If SARA 313 chemical, complete SARA substantiation form. If any of the individual components react, indicate in Section V.B. See Environmental Affairs Group for assistance in completing this section. V. List here and in Section II.C. all packaging requirements for this product (Include container code numbers specifications and sizes to be packaged as indicated by Marketing Product Manager and approved by Plant): Code Number Package Size Spec (-257,-278,etc) (17H,17E,etc.) (Metal,Lined,etc. ) W. Please state any other special conditions of which the plant should be aware. 2.Z0E G 802 5 BFG07816 X. voc (1) Does this product contain VOC? Yes [] No [] (If no, go to Question Y) (2) Is this an architectural coating under SCAQMD Rule 1113? Yes [] No [] (If yes, go to Question X (4)). (3) What is level of "VOC"(g/L) (4) What is level of "VOC Less Water Less Exempt Solvent"(g/L) (5) Coating Type: [] Concrete curing compound [] Fire retardant coating [ Primer, sealer or undercoater Quickdry primer, sealer (opaque) or undercoater [] Fire retardant coating (transparent or translucent) [] Industrial maintenance primer or topcoat [] Mastics texture coating [] Roof coating [] Tile-like glaze coating N Traffic coating U Urethane coating u Waterproofing mastic coating [] Metallic pigmented coating [] Other N Waterproofing sealer (6) Is this material photocheraically reactive? Yes [] No [] OR Is this product exempt? Yes [] No [] If exempt, list exemption OR Is this product regulated under Rule 1168 as an adhesive? Yes [] No [] Y. If a pilot plant card, an experimental card or a pink card, must R&D monitor batch? Yes [] No [] N/A [] If yes, give name: Z. Date required to be available for shipment (If ASAP, Inventory Control must advise Field Service as to the estimated date the material will be available for shipment): Chemist's Signature Group Manager's Signature Date Date 8Z0C G 802 6 BFG07817 II. PRODUCT SAFETY SPECIALIST/INDUSTRIAL HYGIENIST A. (1) Complete Material Safety Data Sheet worksheet in Section VII. (2) Have Material Safety Data Sheets (MSDS's) been written on intermediates and given to Batchcard Coordinator? Yes [] No [] No Intermediates [] (3) Have MSDS's been written on this formulation and been given to the Batchcard Coordinator? Yes [] Give issue date:___________________ No [] (4) If no, does a current MSDS cover this product? Yes [] Give code number:__________________ Give issue date: No [] (5) Does this MSDS indicate this additional coverage? Yes [] No [ ] (6) If no to 4 or 5 above, attached new or revised MSDS. (7) Compete MSDS Association Table. B. Please complete HMIS ratings for raw materials and this formulation in Section VI. Place HMIS rating for this formulation on batchcard. C. Indicate below the package specification code number suffix (-257,-278,-202,etc.) indicated by Marketing, Engineering Services and productions facilities for each intermediate and finished good: Code Number Package Size Spec (-257,-278,etc.) (17H,17E,etc.) (Metal,Lined,etc.) Label Necessary Yes [] No [] ________________________________________________________ Yes [] No [] Yes [] No [] To be determined by:; D. For each package size indicated above, where labels are necessary, are labels on file with Divisional Label Coordinator, and are the precautionary statements correct? Yes [] No [] Use Experimental Label[] Use HMIS Label [] ' E. If no, has Divisional Label Coordinator been contacted and has a Label Change Form been initiated? Yes [] No [ ] F. Are formats and labels correct? Yes [] No [ ] Product Safety Specialist's Signature Date 0833029 7 BFG07818 III. PLANT D.O.T. SPECIALIST A. Complete DOT Shipping Information: Product Proper Shipping Name_______________________ Product Required Labels_____________________________ Product Hazard Class Product UN/NA Number Product Limited Quantity Exclusions_____________ Product Packaging Reg.'s____________________________ Product Emergency Response Guide Sheet Number Product Red Label Rating* Product UN Shipping Name____________________________ Product UN Hazard Class_____________________________ Product UN Packaging Group Product Additional IATA Packaging Group________ Product Marine Pollutant [] YES [] NO Product Uniform Freight Name_______________________ Product Freight Classification Number___________ Product Freight Packaging Class___________________ Waste Proper Shipping Name_______________________ Waste Required Labels________________________________ Waste Hazard Class____________________________________ Waste UN/NA Number Waste Reportable Quantity Waste I.D. Number Waste Packaging Reg.'s______________________________ *Red Label Ratings: 0-Non-Regulated DOT 1-Flammable Liquid (Flammable Liquid Label Required) 2-Flammable Liquid, Limited Quantity (No Flammable Liquid Label Required) 3-Poison B, Liquid, NOS UN2810 (Poison Label Required)(Only applies to Tremstrip 20) 4-Corrosive Liquid, Limited Quantity (No Corrosive Liquid Label Required) 5-Corrosive Liquid (Corrosive Liquid Label Required) 6-Flammable Liquid, Corrosive, NOS UN2924 (Both a Corrosive Liquid and Flammable Liquid Label Required)(Only applies to Tropical Grade THC-900) Plant D.O.T. Specialist's Signature 8 Date BFG07819 IV. ENVIRONMENTAL. COORDINATOR SECTION A. Have MSDS's for 99-numbered compounds been forwarded to the Production Plant Q.C. Laboratory and Pilot Plant? Yes [] No [] N/A [] If no, are these attached: Yes [] If no, state reason: No [] B. Have MSDS's for permanent raw material code numbered compounds been sent to Distribution Lists for indicated production facilities? Yes [] No [] If no, are these attached: Yes [] No [] If no, state reason:__________________________________________________________________________ C. Have Raw Material Spec Sheets been received from Chemist and forwarded to Purchasing Departments and Q.C. Departments on all raw materials? Yes [] No [] If no, are these attached? Yes [] No [] If no, state reason:______________________________________________________________________________ D. Have TSCA Certification Letters been received on all raw materials? Yes [] No [] If no, list code numbers and reasons: E. Have MSDS's been written and distributed on all Intermediates in this formulation? Yes [] No [] No Intermediates [] F. Has a MSDS been written and distributed on this formulation? Yes [] No [] If no, are-these attached: Yes [] No [] If no, state reason:. G. Does this product contain chemicals on the Kentucky Air Toxic listing (401 KAR 63:022)? Yes {] No [] If yes, list in Section V.G. H. Does this product contain chemicals identified in Section 302 (40 CFR 355) or Section 313 (40 CFR 372) of SARA Title III? Yes [] No [] If yes, list in Section V.H. and/or V.I. I. Does this product contain a CERCEA hazardous substance (40CFR302.4)? Yes [] No [J If yes, list in Section V.J. J. Does this product contain chemicals identified in Proposition 65? Yes [] No (] If yes, list in Section V.K. Environmental Coordinator's Signature Date GG C CO o CJ 9 BFG07820 V. ENVIRONMENTAL AFFAIRS SECTION A. The following Intermediates are reaction products: (To be completed by Chemist) Intermediates -------------------------------------- -------------------------------------- -------------------------------------- N/A [] Approved Manager - Environmental Affairs If N/A, go to "C" below. B. Are all of above Intermediates registered on EPA/TSCA Inventory? Yes [] No [] CAS# If no, give the date of PMN submission and date production may potentially begin if PMN clears EPA or give reason for experimental production: PMN Submission Date: Proposed Production Date: Reason for Experimental Production: NOTE: If experimental, production requirements of TSCA Research and Development Exemption outlined in the September 6, 1986, memo must be complied with. C. The following Raw Material/Intermediate Code Numbers react by the following chemistry in the product: N/A [] App roved Manager - Environmental Affairs If N/A, go to "E". D. Is the reaction product on the EPA/TSCA Inventory? Yes [] No [] CAS#_________ If no, give the date of PMN submission and date production may potentially begin if PMN clears EPA or give reason for experimental production: PMN Submission Date: Proposed Production Date: __________________________ Reason for Experimental Production:____ NOTE: If experimental, production requirements of TSCA Research and Development Exemption outlined in the September 6, 1986, memo must be complied with. E. From information given in Section I.P., list below the RCRA Hazardous Waste characteristics and the Tremco compatibility group for disposal purposes: Hazardous Waste Code: ____ Hazardous Waste Number:____ TREMCO Compatibility Group, ZCOEGROZ 10 BFG07821 Is testing necessary? Yes [] No [] If yes, have samples been submitted? Yes [] No [] Place compatibility groups on batchcard. F. Based on Section I.T. above, are there special procedures that need to be implemented into current plant environmental programs (i.e., wastewater analyses, personnel exposure monitoring, etc.)? Yes [] No [] Comments:___________________________________________ G. Kentucky Air Toxic listing (401 KAR 63:022): Chemical Name % (WT) CAS # H. Section 302 (40 CFR 355) of SARA Title III: Chemical Name % (WT) CAS # RQ TPQ I. Section 313 (40 CFR 372) of SARA Title III: Chemical Name %,(WT) CAS # J. CERCLA Hazardous Substances (40 CFR 302.4): Chemical Name % (WT) CAS # 11 RQ BFG07822 MC 05 Cfi CJ CJ u K. Proposition 65): Chemical Name % (WT) CAS # Manager - Environmental Affairs Signature Date PIP.FRM 20893034 12 BFG07823 VI. 100% FORMULATION Product Code Number Product Name A. Development Chemist Tremco Code Number 100% Formulation Date Product Safety Specialist HMIS H F R PP Total 100.00 B. Internal Reaction Products 1. FORMULATION RATING: 3. TOTAL 2. TOTAL TOTAL 4. r; TOTAL 13 BFG07824 083303S - S e c tio n 313 T o x ic c h e m ic a l, must pass s u b s ta n tia tio n te s t and s u b s ta n tia tio n form must be a tta c h e d . Uuuuu 43 uuo H<D oaBCL <>u H0 4J Xc *4 J4 ea; Xo Ma> to <o g 3 z *H *OC4 r**CyH4O 4J a) <0 CL LSi W <O44 4>J> V f-co4O *>o1 r4 s0) X *4 <co44 oa sHu faJ XCO o X QCoOo hC-1 404) CcOO cU -J 0 '3 XO60) CLoli I CQ o 44 La>i e0) o 'wr4' z<eCuO 1 f-4 4-1 o*Koc *Cr4O L> 00d) ZZZZZZZZZZZZZZ X * * MI fust q u a lif y asI I Itra d e s e c re t under 0SHA "back e n g in e e rin g " t e s t , and * F or s p e c if ic c h e m ic a l name and q u a lif ie d s u p p lie r s , see raw m a te r ia l spec s h e e ts . w QHC o00ao> ja >s c 44 A3 1 o 0> <# 50 d 0) H z CO c <44 4J CO 0 c O 0) i4 X o -4 Li 44 CO V CL z /*> C4 e CO CO <44 >%/o a> 0) 0) H4 o 44 44 Li 0> CO * 4> r4 *4 CO -O 2 O0 MH e.T> eo 0a o Li CO 3 3 0) to P<*O>| > << zZZz ZZZZZZZZZZZZ H 0) r-4 4) 44 o i4 f-4 o e > 4-1 O 3 *t4 S c p4 ^4 H o 44 cbe O o *d o e z z Z T3 c e * 4) M X *f-4 CO o * d , CO W H iJ 4> w Li a< 1* 44 ^4 CO 3 M CQ (Q CO i-4 a aH *-4 H 3 Li e Z C Li O 0 44 w o V 0) Li bL i4 p Q M X O 44 a * UJ H4 U o CO <44 44 CO w CQ b tfl z i-4 i X Z r-4 44 Li O 3 c 3 3 #> Z a o e Q> CO O au Li CLU3 b3 a o <44a a Ut O ^4 o o >4) f-4 ^4 *4 X i * o HU zQ O0a4. o HOaozoO4t Otf * t--1 > 4P oO f-4 l . < a0>0)) CQ 44 O (2 oo e0) Li H z0 0d> no i BFG07825 SARA T i t l e MINOR MODIFICATION FORM Product Line Code_Original Product Registry Number TREMCO Product Name________ oBatchcard Priority: Normal Q Rush (If Rush, state date required) Issue Date Lab# Previous Experimental# Production Locations I. A. Type of card: Q Pilot Plant Q Experimental Q White Q Pink B. Type of Modification: Process change only (hold times, mixing speeds, orders of addition, etc.) | | New raw material (<0.1%)* | | Alternate supplier of existing raw material (<0.1% impurities)* | | Small "tweeking" (<1.0% change of total batch) of existing raw materials** *If >0.1% change, a new PIP must be filed **If >1.0% change, a new PIP must be filed C. Are there any changes in the existing chemistry (i.e., 100% formulation on MSDS) oor reaction chemistry occurring? No Yes (If 'Yes', you cannot use this form; a new PIP must be filed) D. List all changes you are making to the original recipe (i.e., batchcard): Chemist Signature Group Manager Signature Batchcard Coordinator 100% Formulation A. RM Code # % Formulation Date Date Date B. Internal, Reaction Chemistry 1. Total 2. Total 3. Total BFG07826 C0680 CARD TYPES I. PILOT PLANT CARD A. Uses lab book number and PPK (Pilot Plant Kinsman) number only. B. Assigned and controlled through R&D Department. C. Used for pilot plant production only (R&D lab production will be done in R&D lab book). D. The card must be stamoed PILOT PLANT CARD. E. All raw materials are expensed to R&D account. F. Will not be inventoried. G. Will not be set up on data base. H. The reason for usine a PILOT PLANT CARD formulation must be stated in the remarks section of the card. II. EXPERIMENTAL CARD A. First time experimental formulations only (Limited number of batches. Subsequent production of modified formulations will be on PINK card ONLY). B. All raw materials, intermediates and finished goods be inventoried. C. Formula number will be set up on data base. D. Must be converted to in-line code to be sold beyond experimental quantities (See Formula Number Assignment section). E. May contain '99' numbers. F. The card must be stanroed EXPERIMENTAL CARD. G. Requires special formula number designation (See Formula Number Assignment section). H. The reason for usine an EXPERIMENTAL CARD formulation must be stated in the remarks section of the card. III. PINK CARD A. Used for a modified formulation of an existing WHITE or EXPERIMENTAL card if, and only if, the difference in the formulation does not require a revision to the existing MSDS or label. (Should a revision be necessary, the card must be processed as an EXPERIMENTAL card or a different WHITE card, so that a unique 'rf code number will distinguish it from the existing EXPERIMENTAL or WHITE card. CO B. The formula number and issue date remains the same as the related WHITE or ^ EXPERIMENTAL card. rA ' 03 1 BFG07827 8C0C680 C. Will not be set up on data base. D. Inventory must be segregated using batch number (if necessary). E. May enter production manually using non-standard production inventory transactions or as standard production with miscellaneous inventory adjustments for differences in component usages. F. The card must be stamped PINK CARD. G. Should be used whenever the modified formulation will be sold under the existing formula number. H. May be used to test as many different formulations as needed. I. The reason for using a PINK CARD formulation must be stated in the remarks section of the card. ALTERNATE CARD (PROCESSED AT PLANT LEVEL. AFFAIRS GROUP) THIS CARD IS NOT ROUTED THROUGH THE ENVIRONMENTAL A. Used for final or in-line formulation of product for a scaled batch size of an existing WHITE or EXPERIMENTAL card or for use of non-standard production equipment. B. The formula number remains the same as the related WHITE or EXPERIMENTAL card. C. Will not be set up on data base. D. Enter as standard production with miscellaneous inventory adjustments for differences in component usages due to computer scaling. These adjustments should be summarized at bottom of card. E. The card must be stamped ALTERNATE CARD. F. Should be used whenever the scaled formulation will be sold under the existing formula number. G. The reason for using an ALTERNATE CARD formulation must be stated in the remarks section of the card. WHITE CARDS A. Used for final or in-line formulation of product for full scale production on standard equipment. 20893039 2 BFG07828 CARD AUTHORIZATION REQUIREMENTS WHITE, EXPERIMENTAL, PINK CARDS A. Plant approval of faxed handwritten draft will be as follows: 1. Kinsman - Process Engineering Manager 2. Vernon - Plant Manager 3. Columbus - P.&I,C. Manager 4. Barbourville - P.&I.C. Manager 5. Felt - Process Engineer B. R&D Signatures 1. Originating Chemist 2. Group Manager 3. Product Safety Specialist 4. Industrial Hygienist 5. Division Manager, Environmental Affairs Group C. Plant signatures for final, typed copies will be as follows (If a designated representative signs instead of one of the below, it should be indicated for whom they are signing): 1. Kinsman - Process Engineer or Plant Manager 2. Vernon - Process Engineer or Plant Manager 3. Columbus - Process Engineer and Plant Manager 4. Barbourville - Process Engineer and Plant Manager 5. Felt - Department Manager or Plant Manager or Division Manufacturing Manager or Inventory Control Manager or Quality Control Supervisor D. Cost Department PILOT PLANT CARD A. Signatures will be as follows (If a designated representative signs instead of one of the below, it should be indicated for whom they are signing): 1. Originating Chemist 2. Group Manager 3. Pilot Plant Manager 4. Product Safety Specialist 5. Industrial Hygienist 6. Division Manager, Environmental Affairs Group 3 BFG07829 20893040 FORMULA NUMBER CODE ASSIGNMENTS I. RAW MATERIALS A. Experimental codes (99 numbers) 1. Requested through the EAG Environmental Administrator. 2. Requester must supply all required information before code is issued. B. Permanent Raw Material Code Numbers 1. Requested through the EAG Environmental Administrator. 2. Requester must supply all required information before code is issued. 3. Raw Material Spec Sheet must be completed and given to the Environmental Administrator before a code number will be given out for chemical raw materials. For non-chemical raw materials, the Environmental Administrator will contact the respective Purchasing Department in order to insure Purchasing has the necessary information and paper work on file. 4. When ready to assign a permanent code for a previous 99 number code, the Environmental Administrator will request a current 'Where Used' listing and notify appropriate batchcard and format personnel. New cards must be issued reflecting new permanent raw material code number. This applies only to the cards expected to be active again. II. FINISHED GOODS, INTERMEDIATES AND PURCHASE FOR RESALE ITEMS A. Finished Goods and Purchase for Resale items. 1. Requested through designated divisional personnel who, in turn, request through the Cost Department Data Base Coordinator. 2. Divisional Coordinator a. Michelle Mikol - Roofing b. Ruth Prokop - Sealants, Automotive Aftermarket c. Susan Stringer - International B. Intermediates 1. Requested through the Cost Department Data Base Coordinator. III. EXPERIMENTAL CODES A. Requested through designated divisional personnel who in turn request through the Cost Department Data Base Coordinator. B. A special series is used which identifies this formula number as experimental and the plant location. 1. Kinsman - Line #-XK01-Package Code (ie., 361-XK01-996) 2. Vernon * Line #-XL01-Package Code (ie., 364-XL01-996) 3. Barbourville - Line #-XB01-Package Code (ie., 897-XB01-996) 4. Columbus - Line #-XA01-Package Code (ie., 950-XA01-996) 5. Felt - Line #-XE01-Package Code (ie. , 036-XE01-996) fv C. Must be assigned an in-line code to be sold beyond experimental quantities. tH >C 680: 4 BFG07830 I. PILOT PLANT CARD PREPARATION AND ROUTING A. Handwritten card prepared by Originating Chemist in conjunction with Pilot Plant Operator and Pilot Plant Manager, or prepared by the Pilot Plant Manager and/or the Divisional Plant Process Engineer in conjunction with R&D Chemist and forwarded to R&D Chemist. B. Card initialed by Originating Chemist and Group Manager. Originating Chemist will submit Product Information Profile (PIP.completed by Chemist) and initialed batchcard to Designated Typist*, who will then submit all paperwork to Batchcard Coordinator at least ten days prior to proposed first production date. C. Batchcard Coordinator will make copies and complete routing for EAG and Pilot Plant approvals (See CARD AUTHORIZATION REQUIREMENTS). D. Upon obtaining Pilot Plant and EAG approvals, the Batchcard Coordinator will distribute batchcards as follows: 1. Pilot Plant (with copy of PIP) 2. Pilot Plant Manager 3. Originating Chemist 4. EAG files II. WHITE AND EXPERIMENTAL CARDS A. Handwritten draft prepared by Originating Chemist, who submits it to Designated Typist to fax to production plant for review/changes. B. Upon completion of review, plant faxes approved/changed draft back to Designated Typist to submit to Originating Chemist for review (Steps A and B will continue until draft is satisfactory to plant and Originating Chemist). C. Originating Chemist submits approved draft to Designated Typist, who types the batchcard and returns both to Originating Chemist for his/her initials, as well as the initials of the Group Manager. ' D. PIP 1. (Chemist Section) will be completed by Originating Chemist. WHITE CARDS a. A new PIP must be completed for a WHITE card if a batchcard Checklist or a PIP is currently not on file, 0 where in the "best professional judgment" of the chemist, the modification from the original formulation has increased the hazards from the existing formulation to the new modified formulation. b. If a new PIP is not required, a "Minor Modification" form (MMF) must be completed to accompany the WHITE card through the system. c. The 100% formulation and MSDS worksheet must be completed for each PIP submitted (with MMF, only 100% formulation required). d. The PIP/MMF must also be signed by the Group Manager. n Designated Typist - Mary Coleman, Sealants/ Bea Williams, Roofing t-o e s s o : BFG07831 2. EXPERIMENTAL CARDS a. A. new PIP must be completed for all EXPERIMENTAL cards. PIP/MMF, batchcard and approved draft copy should be given to Designated Typist, who will then submit all paperwork to Batchcard Coordinator at least ten days prior to proposed first production date. Batchcard Coordinator will route PIP/MMF and five copies of the batchcard for EAG approvals. Upon completion of EAG approvals, Batchcard Coordinator will forward five batchcards to production plant for signatures. After all plant signatures are obtained, plant will return all five batchcards to Batchcard Coordinator. Batchcard Coordinator will forward four batchcards to Cost, and one copy of PIP/MMF to designated plant personnel. Batchcard Coordinator will maintain original PIP/MMF and one copy of batchcard for EAG files. The Cost Department Data Base Coordinator will load batchcard on data base, generally within two days, and Cost will distribute stamped batchcards for Sealant and Roofing Divisions as follows: 1. Cost Department 2. Inventory Control 3. Process Engineering 4. Batchcard Coordinator for EAG files CARDS Handwritten draft prepared by Originating Chemist, who submits it to Designated Typist to fax to production plant for review/changes. Upon completion of review, plant faxes approved/changed draft back to Designated Typist to submit to Originating Chemist for review (Steps A and B will continue until draft is satisfactory to plant and Originating Chemist). Originating Chemist submits approved draft to Designated Typist who types the batchcard and returns both to Originating Chemist for his/her initials, as well as the initials of the Group Manager. PIP/MMF (Chemist Section) will be completed by Chemist. 1. A new PIP must be completed for a PINK card if a batchcard Checklist or a PIP is currently not on file, or where in the "best professional judgment" of the chemist, the modification from the original formulation has increased the hazards from the existing formulation to the new modified formulation. 2. If a new PIP is not required, a MMF must be completed to accompany the PINK card through the system. 3. The 100% formulation and MSDS worksheet must be completed for each PIP submitted (with MMF, only 100% formulation required). 4. PIP/MMF must be signed by Group Manager. 6 0833043 E. PIP/MMF, batchcard and approved draft copy should be given to the Designated Typist who will submit all paper to Batchcard Coordinator at least ten days prior to proposed first production date. F. Batchcard Coordinator will route PIP/MMF and three batchcards for remaining EAG approvals. G. Upon completion of EAG approvals, Batchcard Coordinator will forward three batchcards to production plant for signatures and a completed copy of PIP/ MMF to designated plant personnel. H. After all plant signatures are obtained, plant will distribute as follows: 1. Inventory Control (with copy of PIP/MMF) 2. Process Engineering 3. Batchcard Coordinator for EAG files 7 BFG07833 20833044 EXCEPTIONS TO PREPARATION AND ROUTING PROCEDURES I. ARTICLE EXEMPTIONS (FELT PLANT) A. Includes the following: 008-line 038-line 014-line 407-325-601 024-line 407-329-601 028-line 407-329S-601 034-line 407-425-601 036-line 407-425S-601 037-line 407-429-601 B. Draft prepared by Originating Chemist in conjunction with Roofing Division Plant Manager or Felt Process Engineer, or prepared by Roofing Division Plant Manager or Felt Process Engineer in conjunction with R&D Chemist and forwarded to R&D Chemist. C. Draft submitted to Divisional Secretary, who types batchcard and returns typed card and draft to Chemist. If card has been typed by Plant, this step is omitted. D. Card is approved and initialed by Chemist and Group Manager. Batchcard is then submitted to plant by R&D Chemist. E. Upon obtaining plant signatures, batchcards are returned to R&D Chemist. F. R&D Chemist submits approved typed batchcards to Batchcard Coordinator. G. Batchcard Coordinator will stamp cards "ARTICLE - EXEMPT" and forward four batchcards to Cost. Batchcard Coordinator will maintain one copy of batchcard for EAG files. H. ' The Cost Department Data Base Coordinator will load batchcard on data base, generally within two days, and Cost will distribute batchcards as follows: 1. Cost Department 2. Inventory Control 3. Process Engineering 4. Batchcard Coordinator for EAG files II. 159-LINE INTERMEDIATES (FELT PLANT) A. Handwritten draft prepared by Originating Chemist, who submits it to Divisional Secretary to fax to production plant for review/changes. B. Upon completion of review, plant faxes approved/changed draft back to Divisional Secretary to submit to Originating Chemist for review (Steps A and B will continue until draft is satisfactory to plant and Originating Chemist). C. Originating Chemist submits approved draft to Divisional Secretary who types the batchcard and returns both to Originating Chemist for his/her initials, as well as the initials of the Group Manager. D. Batchcard and approved draft copy should be given to Divisional Secretary, who \ 8 BFG07834 c frn rn ftn ? ! will submit all paperwork to Batchcard Coordinator at least five days prior to proposed first production date. E. Batchcard Coordinator (as designated personnel) will generate copies, stamp remaining EAG approvals on batchcards and forward five batchcards to plant for signatures. F. Upon completion of plant signatures, cards will be returned to Batchcard Coordinator, who will then send four copies of batchcard to Cost Department and one copy of PIP/MMF to designated plant personnel. Batchcard Coordinator will maintain one copy of batchcard for EAG files. G. The Cost Department Data Base Coordinator will load batchcard on data base, generally within two days, and Cost will distribute batchcards as follows: 1. Cost Department 2. Inventory Control 3. Process Engineering 4. Batchcard Coordinator for EAG files III. PURCHASE FOR RESALE (NOTE: Initiator - person bringing a purchase for resale into the Company) A. Prior to purchase of material for resale, initiator is required to notify Corporate Safety Specialist (who will complete a PIP for the purchase for resale item) and the respective Purchasing Department (who will obtain supplier's MSDS, TSCA certification and any other pertinent information on purchase for resale material). B. The PIP (Chemist and Safety Specialist Sections completed) will be forwarded to the Batchcard Coordinator by the Safety Specialist, along with the supplier's MSDS for the purchase for resale product. C. The Batchcard Coordinator will route the PIP for EAG approvals. Upon obtaining EAG approvals, the Batchcard Coordinator will notify the respective Purchasing Department of authorization for purchase by the Company and maintain the PIP for EAG files. IV. SPECIAL COLORS - SPECTREM 1 AND SPEtTREM 2 A. R&D Chemist will notify Batchcard Coordinator of for batchcard for special color and provide the information necessary to complete the batchcard. B. The Batchcard Coordinator will fill in the generic batchcard (which shows previously obtained plant signatures) with the specific information for the special color and, as designated personnel, stamp EAG approvals on the batchcards. C. Upon completing EAG approvals, the Batchcard Coordinator will generate copies, sending four batchcards to Cost and copy of pre-approved PIP to designated plant personnel. The Batchcard Coordinator will maintain a copy of the batchcard and PIP for EAG files. D. The Cost Department Data Base Coordinator will stamp the cards and distribute as follows: 1. Cost Department 9 BFG07835 2. Inventory Control 3. Process Engineering 4. Batchcard Coordinator for EAG files V.ADHESIVES SYSTEM DIVISION - BFG A. Batchcard is typed at BFG and approved by Originating BFG Chemist prior to submittal to the Batchcard Coordinator. B. Originating BFG Chemist will complete PIP (Chemist Section) and submit to Batchcard Coordinator, along with batchcard and raw material MSDS backup for the batchcard. C. Batchcard Coordinator will route for Pilot Plant and EAG approvals (See CARD AUTHORIZATION REQUIREMENTS for PILOT PLANT cards). D. Upon obtaining Pilot Plant and EAG approvals, the Batchcard Coordinator will distribute batchcards as follows: 1. Pilot Plant (with copy of PIP) 2. Pilot Plant Manager 3. Originating BFG Chemist 4. EAG files BCPROC.MSD REV 12/04/90 n 10 BFG07836 0893047