Document 3J0x0mK7JEM4qyMB4Vz533X80
CG 3i/"2'
NOy 9 / 1982
("d a t e ")
_ L2vl5S a^i^^BS*
<_LOT )
( EST WT >
PROCESSES < > RT-618-D < T)
APPROVED BTT^ EWK 12/08/81
CGMTYP JOB NAME: 32RT618DMT
STB HRS_________ TIME
NON-BLEEDING
EQUIP I MENT I
| S' | NAME: WATCHUNG RED Y
I USE | LBS
PREP 1
921/
RECORD :,,._^,._,,BATCHES SINCE SPARKLER LAST |
I CLEANED* AFTER 4 BATCHES, CLEAN, DRESS
|
I | SPARKLER & PRE-COAT WITH 1 5S DICALITE
|.
| i-FILTER AID
I
\/Z\ OBTAIN FOR S11 2-CHL0R0-4-AMIN0T0LUENE-5- I
1 USULFONIC ACID
|
US^TOBTAIN FOR S24 3-HYDROXY-2-NAPHTHOIC ACID |
f ^K'lINSTALL DV & CV RECORDER & CONTROLLER CHART |
| | NOTE: NOTIFY PRESS ROOM AND ROPE OFF AREA |
1 t UNDER V-922
f,
> y*r-
l^T^RUN 10* <1O0G> WATER INTO V-Jf_&/I~& ADJ TO i
I I ACCT I N-C0DE | LBS
I----------- -I------- II iI I 777-A I ____
IJ I 740-C I
II ! 253-C |
l!
931 100 DEG F
II
DD IN 1-2 MIN* DRESINATEX
50 1 530--A | 50
STIR 2 MIN & RECORD : PH__/jML <9.5-1 0-5)
II
I STIR 20 MIN OR LONGER FOR S27
30* <620G) WATER INTO V-922
IGH IN V-926 SODIUM HYDROXIDE & RUN IN ____f
I I
I
I i
TURN ON AGITATOR & STEAM & DUMP IN FROM S2 |
I
2-CHLDRO-
LOT
100%
,,% f ' I
| 4-AMINOTOLUENE
___
I.44JLI
I -5-SULFONIC
J--ACID
_ ____ ____
I^K^KffUMP IN ACTIVATEi~CARBON
_______ 1_________ I I 40 I
LKfj^DUMP IN DICALITE FILTER AID
1 10I
Tyr \ HEAT TO 212-214 DEG F, RECORD HT________ * F, |
|
f Jr-
_______DEG F WATCH FOAM
{1
U*5 f RECORD BY3fr:_^<+>, IF NECESSARY ADJ TO +BY I
!
' U SODIUM HYDROXIDE
ASSUME 50% I________ I
f STIR 30 MIN AT 212-214 DEG F, THEN SHUT J
I
OFF STEAM
WATCH FOAM
II
NOTE: RECORD: SPARKLER PRESSURE __^.__PSI |
IF NOT ZERO, NOTIFY SUPERVISOR
1
CIRCULATE 15 MIN OR LONGER THRU SPARKLER I
| UNTIL SOL1N IS CLEAR- MAINTAIN AT 190-195 FI
| FOR SI 9 & RECORD; HT_________DEG F AND
|
RECORDER_______ _
DEG F
.. I
I RECORD: START
TOTAL MIN-- ,1
I CLARITY_Cf^^7 NOTE: SAMPLE FROM HOSE - I
SHOW TO SUPERVISOR FOR O.K*
I
I 7-D 1 178 740-C | 920
l&tStJ I
113-B I 40 777-A | 10
1 I I 7-D I
LOT8 ___ ,, CQMTYP JOB NAME = 32RT618DMT PAGE 02
EQUIP MENT
I I PAGE 2 OF 3 CG 32 CODE RT-618-D <T)
904 NJN 1 * <50G> WATER INTO V-904 4 WHEN SI 7 COMPLETE, PUMP IN V-922 THRU SPARKLER, MAINTAIN Vr922 AT 190-195 DEG F RECORD: STARTJJkB&jtdl { TOTAL MIN_/0_____
MISC 5
\2i
WEIGH IN PT FOR S35 SODIUM NITRITE , MEASURE 210j 6_UNITS INm~__V_-_9_2_8__~_F_0__RJ"3St3s37' u*
HYDROCHLORIC ACID
M__<3__ ___
CV RUN 14* <1330G) WATER INTO V-__5!r!.___
6 WEIGH IN V-926 SODIUM HYDROXIDE & RUN IN M_jfe__--
DUMP IN FROM S3
LOT
-HYDROXY-2-
___ ___
DATE PRINTED:11/04/82
USE 1 N-CODE | ACCT
LBS |
1 LBS
1l
11 1i r1
940-1 IZ-QA i
1 725-A |
1 28-D I
295 372
i 7Jt-1
1 ___ _____I
1 1 7-D | 450 253-C J
\Zth
ADJ TO 70-90 DEG F * STIR TO DISSOLVE STEAM EJECT V-921/931 INTO CV
922 WHEN SI9 COMPLETE, SHUT OFF PUMP & INSERT 7 922 FOOT PLUG RUN IN 10" (207G) WATER & HEAT TO 190-195 F CIRCULATE 15 MIN THRU SPARKLER*
PUMP V-922 THRU SPARKLER INTO V-904
AI RUN IN 5' <103G> WATER INTO V-922 & HEAT TO I 190-195 F* CIRCULATE 15 MIN THRU SPARKLER
904 y^fj^PUMP V-922 THRU SPARKLER INTO V-904
10 WHEN MTY BLOW OUT SPARKLER INTO V-904
13ST] HEAT TO 165-170 F (SMPL TO SUPVR FOR D.K*>
133-^1 RUN IN N-28-D FROM S21 IN 12-15 MIN & STIR
T J- 5 MIN AT 165-170 DEG F
vyf |*ADJ TO 129* <3409G) AT 28-30 DEG F AND
n RECORD: TEMP
,__L'SLHL___ " ICE
40X3301 57-A I
l5 I RUN IN N-725-A FROM S20 AFAP <5-10 MIN)
$. RINSE IN PT-
I
STIR 30 MIN AT 28-35 DEG F MAINTAINING
+CR, +KI F0R,S4L AND RECORD:
,
TIME STARTsSMloik, CR__dTT< + ) , KI___X._( + )
NOTE <1) IF CR-, KI-, ADD 20* AS IS IN
CREMENTS
HYDROCHLORIC ACID ASSUME 32%
28-A |______
RECORD: CR ,,< + ), KI< + )
I
<2) IF CR+, KI -, ADjD 20* AS IS INCREMENTS
IX
I
| SODIUM NITRITE*
ASSUME 33%
______| 725-A 1 _____
RECORD: CR__*___< + > , KI< + >
I1
DUP050060860
LOT-
EQUIP,I MENT/'-l
_ COMTYP JOB NAME - 32RT618DMT
** --
M. --
PAGE 03
.*. ,,
PAGE 3 OF 3 CG 32 CODE RT-618-D <T)
DATE PRINTED:1i/04/8
________ USE I ACCT LBS J LBS
SV lm^il'2)UMP INTO CV BARIUM SULFATE
H Xj&TX ADJ TO 33* <31300 AT 28-32*F
ICE
b& sstam
3301
sr 57-A l U5..S
M RECORD: TEMP_,3J2___ DEG F 6 VOLUME _^.51_r JdEJGH IN FROM DRUM AMMONIUM CHLORIDE l^o-n^riR 2-3 MIN
I! 212 I ` 165-A I
II
212
>rT IMMEDIATELY COUPLE DV THRU UNDERSURFACE
1I
I DISTRIBUTOR INTO CV IN 45-60 MIN. MA IN/LAIN
57-A
^ AT 28-32 DEG--F. RECORD: START.
OTAL MIN
.
,
42T 1 STIR 30 MIN 6 RECORD : BASE _:afc=rL_< + >,
| | DIA20 ,,~rfi<~)/PH_ZcSL,_<?.0--9.8)
\
J^PINAL TEMP________ DEG F
42n IF NECESSARY, ADJ TO PH 9.0-9.8 AND RECORD
I PH */ y SODIUM HYDROXIDE
ASSUME 50% JM&- i
7-D 4T0
J
... HYDROCHLORIC ACID
ASSUME 32%
28-D
44 I HEAT TO [&bMQbDEG F IN 65-70 MIN AND
j RECORD: HT,,_____DEG F 6 RECORDER______ DEG F
I NOTE: AT 174-176 P, OPEN WATER SPRAY
1 1/4 TURNS
902 RUN 24" <6180WATER INTO V902
12
TURN ON AGITATOR 6 STEAM & DUMP IN BARIUM
1440
16-B 1440
TO & STIR TO DISSOLVE
CV WHEN S44 COMPLETE, IMMEDIATELY STRIKE V902
13 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN
I 7-MTMIN. MAINTAIN CV AT i$kF.
j*'ttfEpORD: START__TOTAL MIN_/.&Z____________
Afj^fEAT CV TO 198-202 DEG F IN 10-12 MIN
5 MIN AT 198-202 DEG F OD TO 180x190' <+/-18,000O
5>T RECORD: PH_!w5<9.0-9.4) & STOP AGITATOR
! SHUT OFF WATER SPRAYS
1
i jTAPI
FIN
i -Jmm-
QPTR
J . ULUSMu. SUAtM 1 _^Zjh*v3r------
II
1 | WHEN INSTRUCTED BY PROCESSING AREA HALF WAY I } THRU PRESSING, DUMP IN, STIR 5 MIN 6 STOP I I AGITATOR. RESUME PRESSING. I-OCTANOL
I 10 | 588-A I 10
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