Document 3DvMRbxVj7DEV7DykqKGJJqJ

WRITTEN BY: 3 .M.S. APPROVED BY: DATE: 8/90 REVIEWED: 3PS DATE: 10-9! OPERATOR'S NAME: DATE CHECK ACTION STEPS (Capital.letters) and Comments (Small letters) 1. REVIEW JOB SAFETY INSTRUCTIONS. THE OPERATOR AND THE TRUCK DRIVER SHOULD NOT LEAVE THE DELIVERY TRUCK UNATTENDED WHILE THE TRUCK IS BEING UNLOADED. NO VEHICLE OR TRAFFIC SHOULD BE IN THE AREA WHEN UNLOADING. THE DELIVERY TRUCK IS NOT TO BE LEFT RUNNING WHILE IT IS BEING UNLOADED. THE TRUCK DRIVER SHOULD BE AWARE OF EVACUATION PROCEDURE. 2. INSURE THAT YOU ARE WEARING PROPER SAFETY EQUIPMENT. BE SURE THAT YOU ARE WEARING GOGGLES AND GLOVES WHEN CATCHING SAMPLES OR HANDLING THE PRODUCT. A COMFO II MASK IS REQUIRED WHEN AIR SPACING A TANK OR CATCHING A SAMPLE FROM AN OPEN DOME ON A DELIVERY TRUCK. 3. CATCH A 1/ OUNCE SAMPLE OF THE PRODUCT IN THE DELIVERY TRUCK. THE NITROMETHANE DELIVERY TRUCK SAMPLE IS ANALYZED IN THE TE II LAB.Refer to the TE II Laboratory Analytical Procedures Manual. The sample point is usually located near the rear of the truck on the top of the carrier tank. 4. RECEIVE AND PRINT OUT THE RESULTS FROM THE MAIN LAB'S ANALYSIS BY FAX OVER THE COMPUTER. VERIFY THAT THE MAIN LAB'S REPORT AND THE CERTIFICATE OF ANALYSIS ARE IN AGREEMENT (BOTH VERIFY THE CONTENTS OF THE TRUCK AND THAT THE MATERIAL IS WITHIN THE SPEC LIMITS). STAPLE THE LAB REPORT AND THE CERTIFICATE OF ANALYSIS TOGETHER AND HAVE THE LEAD OPERATOR COMPARE THE TWO. BOTH THE LEAD OPERATOR AND AUXILIARY OPERATOR INITIALIZE THE TOP SHEET AFTER VERIFICATION AND TURN BOTH REPORTS IN TO SUPERVISION. (IN CASE THE FAX BOARD ON THE COMPUTER IS OUT OF SERVICE, WRITE THE FULL CONTENTS OF THE MAIN LAB'S RESULTS ON THE CERTIFICATE OF ANALYSIS AND INITIALIZE). 5. IF THE MAIN LAB'S ANALYSIS AND THE CERTIFICATE OF ANALYSIS DO NOT AGREE, AS DEFINED ABOVE, THEN DO NOT UNLOAD THE TRUCK. NOTIFY THE LEAD OPERATOR FOR FURTHER INSTRUCTIONS. 6. ONCE THE TRUCK HAS BEEN CLEARED, NOTIFY THE LEAD OPERATOR SO THAT HE CAN UNLOCK THE PUMP SUCTION. SPOT THE TRUCK AT THE NITROMETHANE UNLOADING PUMP. CHECK THE VAREC ON THE NITROMETHANE TANK TO PREVENT OVERFILLING. Notify your immediate supervisor if the tank level is 11 feet or above before unloading. | SL 006404 CONFIDENTIAL: Subject to Protective Order of 14th Judicial District Court Do. 91-1145 7. DOUBLE CHECK THE SUCTION AND THE RECIRCULATION VALVES ON THE NITROMETHANE TANK WHICH ALSO TIES INTO THE UNLOADING LINES OF THE NITROMETHANE TANK, MAKE SURE THAT THE VALVES TO THE NITTROMETHANE TANK ARE CLOSED TO PREVENT CROSS CONTAMINATION. Do not assume that the person before you closed all the valves!!! 8. CONNECT THE GROUND CABLE TO THE TRUCK. 9. CONNECT THE UNLOADING HOSE TO THE NITROMETHANE UNLOADING LINE LEADING INTO'THE TANK. (The driver will connect the other end of the hose to his truck.) The truck should arrive with receptive fittings for our connections. 10. USE N2 TO UNLOAD THE NRE TRUCK. DO NOT USE THE UNLOADING PUMP. MAKE SURE THAT ALL KELLY FITTINGS ARE REPLACED WITH N2 FITTINGS. NO AIR TO N2 ADAPTORS ARE ACCEPTED!!! (The truck driver will connect the other end of the N2 hose to the truck and regulate the pressure.) 11. THE TRUCK IS NOW READY TO BE UNLOADED. OPEN THE SUCTION VALVE AT THE NITROMETHANE TANK. ALSO OPEN ANY BLOCK VALVES THAT MAY BE IN THE NITROMETHANE SUCTION LINE LEADING TO THE TANK. MAKE SURE THAT THERE ARE NO LEAKS. 12. CHECK THE VAREC ON THE NITROMETHANE TANK TO MAKE SURE THAT THE LEVEL IS COMING UP. WATCH THE TANK LEVEL CLOSELY TO PREVENT OVERFILLING OF THE TANK. 13. STAY BY THE TRUCK THE ENTIRE TIME THAT IT IS BEING UNLOADED IN CASE OF A LEAK, ETC. Ik. AFTER THE TRUCK IS EMPTY, TURN OFF THE N2. THE DRIVER WILL CLOSE THE N2 VALVE AT THE TRUCK. BE SURE TO BLEED THE N2 HOSE BEFORE DISCONNECTING. 15. THE TRUCK DRIVER WILL THEN BLEED OFF EXCESS N2 PRESSURE FROM HIS TRUCK INTO THE LINE. WHEN THE N2 REACHES THE DESIRED PRESSURE IN THE TRUCK, CLOSE THE BLOCK VALVE NEAREST TO THE UNLOADING HOSE. THE DRIVER WILL CLOSE THE VALVE ON HIS TRUCK. BE SURE TO BLEED THE HOSE OFF AT THE BLEED VALVE BEFORE DISCONNECTING. 16. DISCONNECT THE GROUND CABLE FROM THE TRUCK. 17. CLOSE ALL VALVES TO THE TANK AND CHECK THE VAREC LEVEL OF NRE TANK, AND LOCK THE PUMP SUCTION. 18. AFTER THE UNLOADING PROCESS IS COMPLETE, GET THE LEAD OPERATOR TO SIGN THE TRUCK DRIVER'S PAPER WORK. INSTRUCT THE TRUCK DRIVER TO RETURN TO THE SCALES. SPI LL/RELEASE POTENTIAL 1 . MAKE SURE THAT ALL BLEEDS ARE CLOSED AND PLUGGED. 2 . MAKE SURE THAT ALL LINES TO THE TANK ARE CLOSED. 3. WATCH TANK LEVELS TO PREVENT OVERFILLING. CONFIDENTIAL: SL 006405 cnhi^ct to Protective Order otSM Judicial District Court . Mo. 91-1145