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Page 201-6 CHEMICAL DIVISION LAME CHARLES,LOUISIANA LACORATORY PRODUCT REPORT TRI-ETHANE SHIPMENTS 1980 AVG. JAN. 29 FEB. 32 Type 324 Color Specific Gravity * .Distillation Ranee APHA 25/25 C C 8 1.304 77 1.311 1.311 Low High 73.4 81.0 73.4 73.6 81.4 80.4 Moisture Acidity PPM 51 PPMasHC! 2 44 41 22 Soluble Chlorides PPM (0.5 (0.5 (0.5 Aluminum Scratch APHA 32 23 20 Non-Volatile Residue 0.0002 0.0003 - MAR. 29 APR. MAY 30 32 JUNE JULY 29 30 AUG. 53T 30 OCT. 29 NOV. 33 DEC. 31 1981 AVG. 6 6 7 5 55 1.308 1.308 1.305 1.305 1.312 1.306 5 56 6 1.307 1.304 1.309 1.307 6 1.308 73.8 73.1 73.4 73.3 73.4 73.4 73.5 73.1 80.9 78.1 82.3 81.1 83.5 81.8 82.1 79.0 47 48 62 65 57 66 60 49 1 1 53 21 23 (0.5 (0.5 0.2 (0.5 (0.5 (0.5 (0.5 (0.5 37 44 39 25 40 40 45 45 0.0006 0.0003 0.0006 (0.0001 0.0001 0.0004 0.0003 }.0003 73.3 73.6 73.4 82.7 83.8 81.4 44 1 (0.5 52 2 (0.5 53 2 (0.5 38 16 ! 34 0.0001 o.oftoi 0.0003 SL 013931 * Sp. Gr* specification = 1.300 - 1.320 * c rV*V & CHEMICAL DIVISION IAKE CHAItlES. LOUISIANA LABORATORY OPERATIONS REPORT '7RI-ETHANE' . ,, TTPE 3?A SIABILIZATION Wr. % VifiL v r nr. Nt Cutoni oe FILM (HE 1980 Avg i JAN 29 0.-02 0.34 0.72 0.01 0.32 0.76 FED 32 MAR 28 0.01 0.33 0.74 0.01 0.36 a 76 APR 30 0.03 0.39 0.76 MAY 32 0.01 0.37 0.72 JUNE JULY 29 30 0.01 0.35 0.71 0.01 0.34 0.72 AUG 30 0.01 0.33 0.73 SEP 31 0.01 0.34 0.74 OCT 29 0.01 0.33 0.71 NOV 33 OEC 31 1981 Avg . 0.01 0.37 0.70 0.02 0.37 0.66 0.01 0.35 0.73 Me iiivl CiiLonoronM DOL CIS I .Z-DteilLOnOtTHYLENE Tn I ciaonoc Tiivit.Nl 1 . 2-Dl CHLODOETUANE 1BL NRE U 1 TfTOE THANE _PL TLE 1 ,1 ,2 - Tn r ciilohoe thane SBL 94.79 94.93 1.40 1.39 (0.01 (0.01 (0.01 0.0 0.11 0.09 0.73 0.73 1.41 1.39 94.44 1.46 (0.01 0.0 0.11 0.74 1.48 94.52 1.45 0.01 0.0 0.09 0.76 1.50 94.18 1.56 0.01 0.0 0.08 0.81 1.51 94.36 1.43 0.01 0.0 0.14 0.74 1.54 94.81 1.45 (0.01 0.0 0.19 0.75 1.52 94.43 1.40 (0.01 0.0 0.31 0.72 1.46 94.62 1.36 0.01 (0.01 0.18 0.74 1.48 94.56 1.39 0.01 0.0 0.09 0.72 1.37 94.51 1.42 0.01 0.02 0.07 0.72 1.47 93.96 1.59 (0.01 0.18 0.75 1.44 94.10 1.20 0.01 0.02 0.46 0.62 1.20 94.45 1.43 fO.Ol 0.17 0.73 1.45 (0.01 0.67 0.03 0.0 - 0.59 (0.01 0.0 - 0.64 0.0 0.0 - 0.59 0.0 (0.01 - 0.65 0.0 0.0 - 0.62 0.0 0.01 - 0.62 0.0 0.00 -- 0.60 0.03 0.00 -- 0-61 0.09 (0.01 - 0.61 0.48 - _ 0.62 n. T6 - 0.59 0.37 __ 0.66 0.27 _ 0.62 0.12 (0.01 STABILIZING TANKS MOISTUPE PPM PH HCl Acidity ppm NO!) - VOL A T 1 L E Rt S 1 DUE " Color Speci r 1C Gpavi iv APHA Avc. Dli TtLLATIOM RADGE C Soluir F r. -- - Low III Gil rpM 40 35 6.7 0.3 6.8 1.0 (0-0001 76 0.670 - 73.6 76.6 (0.5 - SL 013932 41 6.7 3.0 - 5 1.306 43 6.7 4.0 - 6 - 73.5 81.0 (0.5 - 86 6.9 1.0 - 15 - - 56 6.7 1.8 - 6 - -- -- 51 53 6.9 6.9 2.0 2.0 (o.oooi 0.0004 5 (5 1.315 1.306 70 6.9 2.0 -- 5 - 58 6.8 3.0 - 4 - 43 45 6.7 6.8 4.0 3.0 [0.0001 67 1.309 1.305 41 6.5 7 - 52 6.8 2.5 0.0002 6 1.308 74.0 74.3 0.0 73.3 81.9 PASS - - 73.4 73.2 - 81.6 81.3 - (0.5 (0.5 -- 73.5 80.0 (0.5 Sutrjct oi 14 rntfF ' UiM--- ; ; ` J- < vt i iid ic Lal stt ' yl-Xl ---------- Jo- COUE ` Page 202- Subjcct tt* Protect USTRIES of I4t Judicial Distrie*. Court CHEMICAL DIVISION 3 Mo. LAKE CHARLES, LOUISIANA LABORATORY OPERATIONS REPORT fr) TRI-ETHANE II 1980 AVG. JAN. 29 FED. MAR. 32 29 APR. MAY 30 32 JUNE JULY 29 30 SL 013933 AUG. SEP. 30 - 31 Vv. . 29 *ov. 33 DEC. 31 1981 AVG. II 7o EDC MAKE-UP ppm 43 Ee (GC Analysis - ppm) pm 0.40 1,2-Dichlurethane Wt . % 97.15 Trichloroethylene 930 1,1,2-Trichlorethane 17542 U-Tetrachloroethane 26 h2o FURNACE FEED ppm 49 __________________________ PPn* 15.68 Fe ppm (GC Analysis - ppm) Chloroprene Chloroform 1,2-Dichloroethane Wt . Carbon Tetrachloride Trichloroethylene 1,1,2-Trichloroethane % 47 647 99.25 504 4736 142 41 42 0.30 0.13 98.27 846 15496 10 98.19 899 15987 58 50 44 6,77 7.18 38 114 99.23 0 4633 222 74 238 99.00 454 5625 291 32 0.24 98.40 298 14579 25 51 5.49 0.59 72 74 99.37 (1 1774 271 40 0.08 48 0.18 62 0.29 97.17 420 26282 33 98.19 790 17802 45 97.41 443 22315 53 56 4.18 0.61 60 13.7 1.21 70 15.9 1.99 149 11 98.96 0 2811 3134 53 159 99.43 18 3772 22 34 148 99.43 29 4150 26 58 0.16 97.16 1794 23605 8 51 18.4 2.45 95 0 98.65 0 12965 17 59 0.15 96.39 746 31977 0 66 5.0 1.86 99 0 99.24 20 6039 74 47 55 0.62 0.25 30 0.46 46 0.29 97.09 623 25591 3 97.41 491 22790 5 98.05 107 18140 0 97.65 248 24474 (1 59 10.7 3.23 62 9.9 0.68 33 9.2 1.03 45 15.2 1.29 39 17 99.34 16 5216 3 82 47 94.95 43 3337 8 13 39 99.84 32 539 93 21 14 99.79 0 1033 14 47 0.26 97.62 642 21587 20 54 10.1 1.49 64 72 91.49 51 4325 348 HEAVY STILL FEED H?0 ppm Fe ppm (GC Analysis - ppm) 1,2-Dichloroethane wt . % Trichloroethylene 1,1,2-Trichloroethane U-Tetrachlorocthane 57 3.4 97.91 5065 12177 23 70 2.5 57 1.9 98.38 4653 6931 1 97.80 5560 10107 106 42 2.6 63 1.1 62 6.1 71 1.6 98.07 1843 10601 88 97.79 1835 14216 62 98.19 3285 10377 - 97.96 4369 11088 2 54 1.4 74 1.4 69 1.7 60 4.9 43 2.6 65 3.5 97.06 13360 11898 90 96.60 7268 21700 2 98.08 6033 13629 13 98.10 3822 12397 22 98.06 526 15538 15 98.68 1153 8396 13 61 2.6 97.90 69 76 12240 38 HEAVY STILL BOTTOM Fe ppm 59 (GC Analysis - Wt. %) 1,2-Dichlorocthane 58.77 1,1,2-Trichloroethane 29.40 Heavies * 1.55 30 38 70.98 61.85 20.64 27.24 3.12 4.44 36 146 43.67 35.63 4.80 70.60 25.20 1.28 *Includos: Tetras , Penta, Ilexa and Unidentified. 63 62 60 41 87 34 48 17 44.68 40.37 42.49 44.47 12.7 15.3 42.40 43.14 12.3 32.24 50.72 2.5 36.21 47.58 15.5 28.59 51.13 19.2 61.36 46.12 30.78 41.52 7.3 9.9 <k'OKK Sub jotW T.O of Ht'u JmiiT >'. i*V bv -A 5 Mt * i ( strict *5 trrt~r Court 55 48.26 38.38 3.40 Patje 202TRI-ETHANE (veJ) II 1980 AVG. JAN. 29 FED. 32 PPG A>U3TR1E3 CHEMICAL DIVISION Lake Charles,Louisiana COHFlOWTI.^f*: Subject to rrottfotiv? {i^ r :t Court WAR. 29 APR. MAY 30 32 ru. ' JUNE JULY 29 30 AUG. 30 *h- rr-iH-- -H4-- SEP. OCT. NOV. 31 29 33 DEC. 31 1981 AVG. VINYL STRIPPER FEED H-0 ppm 59 Fe ppm 13.09 (GC Analysis - Wt. %) Vinyl Chloride 0.29 1,1-Dichloroethane 98.13 41 29 9.73 9.10 0.17 0.56 98.63 98.41 38 3.56 0.39 98.72 78 0.84 63 5.15 0.13 0.37 98.20 98.61 67 6.25 62 5.37 75-------- 87 3.76 16.2 0.42 0.32 0.35 0.38 99.06 98.45 99.56 99.34 44 17.1 65 6.9 66 5.3 60 0.42 0.23 0_.49 0.35___ 98.99 94.92 98.11 98.42 VINYL STRIPPER BOTTOMS "2______ __ Fe _ (GC Analysis-Wt. Vinyl Cliloride 1,1-Dichloroethane E2HL 51 ppm 0.22 0.05 98.40 44 45 0.26 0.06 0.02 0.03 98.83 98.89 39 0.06 0.01 99.10 47 0.95 55 0.14 56 0.23 46 0.59 0.02 0.04 0.04 0.10 98.28 98.95 99.37 99.07 61 0.23 46 0.17 0.05 0.10 99.83 99.55 54 0.07 32 49 0.07 0.06 48 0.24 0.18 0.09 0.03 0.06 99.39 97.74 97.38 98.87 DCE PRODUCT TANK H^O Fe ppm 55 ppm 0.27 (GC Analysis - Wt. %1 ___1,1-Dichloroethane.________ - 49 0.52 46 0.05 -- 45 0.04 - 57 0.78 52 0.25 -- 52 0.13 - 54 0.19 - 55 0.19 62 0.17 -- 68 0.13 - 37 59 0.19 0.10 -- 53 -- ...MC REACTOR CRUDE (GC Analysis - Wt. 1,1-Dichloroethane Methyl Chloroform 1,2-Dichloroethane 1,1,2-Tr icliloroe thane U-Tetrachloroethane S-Tetrachloroethane Pentachlorocthane Ilexachloroethane 41.71 40.07 39.82 39.88 36.02 37.37 37.49 37.73 - 12.14 5.64 3.25 1.18 0.06 12.37 5.54 3.13 1.35 0.07 12.39 5.61 3.19 1.37 0.06 12.44 5.58 3.19 1.35 0.06 -- _ _ 36.63 36.81 38.75 35.38 37.94 38.24 38.83 37.81 39.47 38.50 38.91 40.77 39.66 38.60 38.01 37.10 37.32 37.99 12.33 6.52 3.73 2.01 0.13 12.45 6.39 3.58 1.76 0.11 12.51 5.89 3.36 1.50 0.09 12.30 6.89 3.79 1.99 0.12 12.30 6.07 3.39 1.57 0.08 12.42 5.81 3.29 1.42 0.07 12.32 12.67 5.38 5.65 3.05 3.21 1 .24 1.35 0.05 0.06 12.41 5.94 3.36 1.54 0.08 OL U 1 vvvi 1 Paye 202- '10 TUI-ETHANE 'C^H) II 1980 AVG. RECYCLE STILL BOTTOMS H?0 ppm Fe ppm AF-109C ppm (GC Analysis - Wt. %) 1,1-Dichloroethane Methyl Chloroform 1,2-Dichloroethane 1,1,2-Trichloroethane U-Tetrachloroethane S-Tetrachloroethane Pentachloroethane Hexachloroethane 59 6.06 - 0.83 44.87 (0.01 30.37 13.66 8.00 2.94 0.13 JAN. 29 FEB. 32 53 5.65 - 59 3.35 - (0.01 42.06 0 30.79 14.60 8.41 3.74 0.20 (0.01 44.08 29.77 14.07 8.11 3.61 0.17 PPG ^p&USTRiES CHEMICAL DIVISION LAKE CHARLES,LOUISIANA MAR. 29 APR. MAY 30 32 JUNE JULY 29 30 49 2.55 - 54 41.34 - 53 2.31 -- 59 1.20 - 63 1.68 - CONPH?Pf'TI*l-i Subject to Protectiv" AUG. 30 ------- Htr rlH rrS------- SEP. 31 OCT. 29 NOV. 33 DEC. 31 1981 AVG. -- 6? 1.30 - 57 1.17 - 54 1,33 - 38 4.69 - 54 3.57 - 55 5.85 - (0.01 44.11 0 30.74 13.66 7.02 3.29 0.14 0.13 54.62 0 22.23 11.29 7.33 3.20 0.19 (0.01 44.53 (.01 27.56 14.67 8.30 4.25 0.26 0.01 47.88 0 26.21 13.74 7.87 3.89 0.22 0.01 45.88 0 28.36 13.71 8.03 3.62 0.19 . 0.01 45.46 (0.01 26.22 14.90 8.41 4.46 0.27 (0.01 47.61 0 26.86 13.64 7.83 3.68 0.19 0.02 49.46 0 27.32 12.59 7.33 3.12 0.14 0.07 49.18 0 27.31 12.72 7.34 3.21 0.15 (0.01 46.65 0 29.02 13.45 7.82 3.34 0.15 0.02 46.79 (0.01 27.70 13.59 7.82 3.62 0.19 MC PRODUCT STILL BOTTOMS U20 Fe AF-109C (GC Analysis - Wt. %) ppm ppm PPm 52 10.57 - Methyl Chloroform 1,2-Dichloroothane 1.1,2-Trichloroethane 1.10 - 53.16 U-Tetrachloroethane S-Tetrachloroethane Pentachloroethane Hexachloroethane 24.61 14.48 5.24 0.23 41 9.81 - 48 6.57 - 44 4.79 - 0.70 0.69 -- 52.59 25.03 14.39 6.50 0.35 52.68 25.10 14.49 6.40 0.33 0.60 54.60 24.30 14.11 5.89 0.26 51 94.32 - 42 62 UU_6J1_ 5.27 - 4.73 _ 46.24 23.45 15.33 6.71 0.54 1.19 - 53.52 26.40 14.93 7.82 0.49 0.84 - 48.89 26.26 15.10 7.57 0.46 56 11.52 - 48 1775 0.92 51.89 25.04 14.67 6.63 0.36 0.44 -- 48.55 26.92 15.22 7.89 0.46 37 2.11 - 53 38 12.65 4.94 _- 2.41 - 49.94 25.31 14.58 6.85 0.35 2.63 51.72 24.29 14.18 6.16 0.33 2.04 53.60 23.95 14.00 5.82 0.28 46 9.32 0.96 _ 52.35 24.82 14.28 6.37 0.32 47 14.56 - 1.51 51.38 25.07 14.61 6.72 0.38 MC PRODUCT STILL REFLUX II^O ppm 51 - - - - --- --- - -- 63 63 Fe ppm 4.52 - - - - _-- - - -- - - (GC Analysis - Wt. %) Vinyl.idene Chloride 0.07 - - (0.01 - -- _- - -- 0.02 0.01 1,1 Dichloroethane (0.01 - - 2.21 - --_ --- - -- 0.01 1.11 Methyl Chloroform 97.12 - - 97.68 - --- _- - -- 98.35 98.02 1,1,2-Trichloroethane (0.01 - - - _ - _ - - - - (0.01 (0.01 SL 013935 Page 209-1 PPG ll^BSTRIES CHEMICAL DIVISION LAKE CHARLES* LOUISIANA TRI-ETHANE R II OPERATIONS CONFIDENTIAL: Subject to Protective Order of I4tl Judicial District Court No. 91-1145 GENERAL 1980 Productions T/r MC (Records) MC (Area) 248.7 233.1 Tri-Ethane (Records) 261.7 JAN. 29 FEB. 32 258.9 268.6 287.7 265.4 264.1 273.9 MAR. 29 APR. 30 202.5 217.3 226.7 14.5 14.5 0 WAV 32 JUNE JULY 29 30 AUG. 30 283.5 286.5 290.3 345.4 356.7 367.6 247.5 263.8 245.9 265.3 258.3 280.6 SEP. 31 OCT. 29 336.3 388.5 345.6 401.0 356.2 408.9 NOV. 33 DEC. 1981 31 AVG 231.5 236.6 232.4 315.0 262.7 321.3 268.6 337.0 276.6 Tri-Ethane Shipped T/D 265.7 258.7 195.0 265.1 218.4 300.4 238.3 307.8 159.2 417.5 366.2 208.8 339.8 272.6 Tri-Ethane Inventory Tons 6413.3 7554.E 10093.8 8971.7 2262.9 1923.1 5655.6 4159.9 7777.8 5854.5 7079.9 7849.9 7753.3 6411.4 VC to VC I HCL to VC I TCE-Tetra to VDCM * T/D 69.9 T/D 40.6 T/D 61.2 129.5 76.2 67.2 196.3 86.0 76.1 150.9 87.8 67.9 33.7 19.4 70.9 86.4 50.1 56.8 86.2 50.3 17.9 64.3 37.5 43.6 21.9 12.8 60.8 15.3 8.9 63.9 3.4 2.0 58.3 0.0 0.0 21.3 0.0 0.0 47.7 65.7 35.9 54.4 EDC Make-up VC-HCL to DCE Rx. T/D 451.1 't/D 320.4 Make-up HCL to DCE Rx. T/D 2.1 Total Cl Consumed t/D 229.2 DCE to MC Rx. T/D 289.8 Hvys. Still Btm.Trans.* T/D 38.0 TCE I to W.R. * 1/D TCE-Tetra to Per/Tri T/D 47.9 HCl Vent Condensate % T/D 10.3 HCl to HCl System T/D 121.0 Aux. HCl to DCE Rx. T/D 0.5 Aux. VC to DCE Rx. T/D (0.01 548.1 304.9 2.4 239.8 301.3 46.2 54.1 23.5 1.6 127.9 0.0 0.0 563.6 300.9 1.7 240.9 310.5 36.9 47.3 34.8 13.3 122.1 0.0 0.0 491.8 234.8 1.9 196.1 237.0 24.3 14.9 67.2 13.5 113.3 0.0 0.0 113.8 35.4 0.4 10.2 17.0 11.2 0.3 -55.6 6.5 10.3 0.0 0.0 505.7 333.7 0.4 268.9 331.7 26.3 23.9 83.0 3.0 133.0 0.0 0.0 549.7 390.8 0.6 324.9 404.2 34.3 0.9 126.4 3.6 177.9 0.0 0.0 424.5 301.9 0.8 222.0 289.6 28.9 3.2 95.4 7.2 109.8 0.0 0.0 395.1 314.4 L.6 231.9 308.6 37.1 3.6 78.2 12.9 115.9 0.0 0.0 452.6 389.5 1.2 316.7 393.5 31.1 0.0 129.4 17.7 163.4 0.0 0.0 509.5 473.2 1.2 366.8 454.5 24.4 0.0 143.0 13.9 188.1 0.0 0.0 281.0 262.3 0.4 213.3 270.9 25.7 25.6 84.3 12.2 107.5 0.0 0.0 392.4 435.7 367.7 309.1 1.2 1.2 293.0 243.7 368.6 307.3 18.6 2H78 14.4 16.1 U9.3 81.6 11.9 9.8 150.6 126.7 0.0 0.0 0.0 0.0 SL 013936 I ________________________________ * Cl2/C only @ C12/C only to OHC II Page 209-2 GENERAL Man Hours/T MC Prod. Production Salaried 1980 AVG. JAN. 29 FEB. 32 PPG MUSTRIES CHEMICAL DIVISION LAKE CHARLES,LOUlSIANA TRI-ETHANE IX OPERATIONS MAR. 29 * APR. 30 MAY 32 JUNE 29 JULY 30 C'.'MFlUF.NTt Ah: Subject oL L<tb t p,-ot ct i *1 r''"r io ''* 1 IMi'triict Court *> 1- l in 5 AUG. SEP. 30 31 OCT. 29 NOV. 33 DEC. 31 1981 AVG. 0.182 0.280 0.130 - - - -- _ -_ - -- 0.205 0.190 0.138 0.147 - _ -- -- -- - - 0.143 Man Hours/T Tri-Ethane Shipped Bulk 0.048 - - -- -- _ Drum Salaried 1.493 -- - --- -- _ -- _ --- -- - -_ _- --- -- - -- - Steam (140# Basis) #/T MC Power KWH/T MC Natural Gas MSCF/T MC Well Water MGAL/T MC AIBN #/T MC Ferric Chloride #/T MC 5652 162.6 4.3 0.8 2.10 2.81 5776 110.1 4.5 0.5 4.65 2.74 5742 114.2 4.6 0.4 4.08 4.6 6331 132.7 5.1 0.8 2.45 4.4 46943 5379 1774.0 96.2 22.1 4.0 13.3 0.1 22.1 2.76 8.1 7.2 4665 84.6 3.8 0.0 1.99 5.5 5152 122.5 3.8 0.0 2.36 5.00 5001 107.2 3.0 0.0 2.64 3.82 4367 129.6 2.8 0.0 1.41 3.04 4378 75.6 2.9 0.0 2.96 3.36 Nitrogen T/T MC 0.13 0.10 0.08 0.09 3.05 0.14 0.11 0.15 0.16 0.11 0.12 YIELDS Unit Pdn. Basis + Trans. Cl9 97.7 C 95.1 Record Pdn. Basis + Trans. cl? 96.8 C 93.9 100.6 100.2 99.5 99.4 100.6 98.1 99.4 95.0 99.4 98.1 100.3 97.4 100.8 95.9 99.3 95.0 99.5 96.5 99.1 96.0 98.8 99.7 96.5 98.5 97.6 99.9 95.0 98.7 98.2 96.3 98.0 96.0 98.7 98.7 95.9 96.6 97.5 97.3 94.4 94.8 OciL Unn! w*^nv7/ 4731 135.4 2.6 0.0 3.49 304 5206 85.8 2.5 0.1 5.89 1.53 5157 108.5 3.6 0.2 3.15 4.11 0.31 0.15 0.14 98.8 98.2 98.1 95.4 97.8 99.1 96.8 96.7 99.2 97.4 98.6 96.7 Unit was down most of the month. (Values not included in 1981 AVG.) Page 209-3 PROCESS CONDITIONS 1980 AVG. Furnace_Data Conversion % ___HaturalGas___________ SCFH Feed Flow #1 Pass GPM #2 Pass GPM Inlet Pressure #1 Pass Psig #2 Pass Psig Outlet Temp. #1 Pass F #2 Pass op Outlet Pressure #1 Pass Psig #2 Pass Bridgewall Temp. Psig op 46373 61 61 220 223 927 908 155 153 1216 JAN. 29 FEB. 32 49526' 50356 64 63 63 63 216 219 218 222 939 936 959 960 152 153 1223 156 157 1222 CHEMICAL DIVISION LAKE CHARLES,LOUISIANA TRI-ETHANE II OPERATIONS MAR. 29 APR. MAY 30 32 JUNE JULY 29 30 JSiihi'v*- to I'rot of I4ti* Judicial ; :;i.l Court #o. 91.-1145 AUG. SEP. 3D 31 OCT. 29 NOV. 33 DEC. 31 1981 AVG. 52586 39048 46632 51691 47400 33963 39657 46512 40326 34951 34387" 65 52 59 65 57 48 51 56 51 45 56 65 51 59 64 57 44 51 56 52 45 56 228 233 206 206 216 217 242 244 236 240 193 200 226 232 246 251 216 223 203 216 221 225 966 964 158 161 1274 937 936 151 152 1129 918 910 156 155 1183 950 950 ' 137 179 1179 905 891 P 142 1219 851 768 148 151 1123 951 855 170 176 1158 957 857 930 896 888 818 178 178 1194 162 173 1228 159 169 1108 929 895 144 162 1187 VC-HCL STILL Liquid Feed Flow Vapor Feed Flow Vapor Outlet Temp. Bottom Temp. Top Pressure HEAVIES STILL GPM SCFH op op Psig 77 264715 109 363 138 63 60 76 69 346924 366034 325236 55550 107 107 105 108 363 363 363 359 136 136 136 139 79 82 64 49 274900 315967 285419 159800 112 121 124 117 362 370 367 353 138 149 146 145 79 183965 112 374 154 54 71 94 271510 203356 138755 111 114 118 373 372 381 152 150 162 70 243951 113 366 145 Feed Flow Vapor Outlet Temp. Bottom Temp. DCE REACTOR VC-HC1 Feed Make-up HC1 Feed Aux. HC1 Feed VC Feed Temp. (Middle) Vent Flow Top Pressure GPM 68 F 202 op 252 74 200 254 76 200 258 77 201 268 58 199 248 68 203 256 77 207 267 59 200 255 SCFH 222220 191576 191791 179472 114225 237200 265021 233014 SCFH 2037 2050 1493 1868 1359 642 - 1232 SCFH 901 0 0 00 0 0 40693 GPM 0 0 0 0 0 0 0 0 "F 140 136 138 138 138 140 140 138 SCFH 3164 2100 1952 1413 1505 1336 1110 2636 Psig 44 44 44 44 43 41 34 32 52 197 251 217700 1490 14588 0 137 3136 36 58 197 259 66 197 262 258110 1024 7 0 140 3149 38 31234J 1077 0 0 141 3307 39 64 196 246 52 196 254 66 199 257 271728 218075 547 1042 00 00 140 141 2744 1437 38 36 224188 1257 4607 0 139 2152 39 t SL 013938 Page 209-4 CHEMICAL DIVISION LAKE CHARGES,LOUISIANA ____________________ TRI-ETHANE ^ II OPERATIONS PROCESS CONDITIONS 1980 AVG. JAN. 29 FEB. MAR 32 29 APR 30 DCE DOPP KETTLE Vapor Temp Pressure F Psia DCE FLASHER ENT. COL. Vapor Outlet Temp. F 214 13 160 183 8 155 198 7 154 195 176 _6______ 4 150 144 VINYL STRIPPER Feed Flow GPM Vapor Outlet Temp. F Bottom Temp. F Top Pressure Psig 62 210 252 63 54 211 257 65 56 215 253 65 53 217 252 65 39 214 251 65 MC REACTOR DCE Feed Flow Cl?. Feed Flow Bottom Temp HC1 Vent Flow System Pressure DCE RECYCLE STILL GPM SCFH F SCFH Psig 47 44 41 113244 111137 102045 228 213 224 113539 86731 63184 91 91 91 38 98354 224 0 91 15 55305 222 79250 85 Feed Flow Vapor Outlet Temp. Bottom Temp. Vent Pressure GPM F F Psig 110 171 267 15 94 171 271 15 91 171 266 15 87 171 266 15 82 172 272 15 MAY 32 JUNE JULY 29 30 AUG. SEP. 30 31 OCT. 29 NOV. 33 DEC. 31 1981 AVG. 199 11 190 12 185 12 195 13 187 9 190 9 213 13 214 9 194 9 159 161 160 163 159 161 168 163 158 65 206 250 65 73 213 251 65 63 209 251 65 59 211 247 62 67 208 250 65 80 198 250 65 78 207 251 65 62 202 252 65 62 209 251 65 50 116220 228 163714 90 56 45 30 34 49 51 41 142753 11549S 106279 134595 159510 151576 128629 221 226 231 228 225 230 229 148443 116991 104021 139242 158862 154871 127427 90 90 92 92 92 90 91 41 118492 225 111895 90 111 170 264 15 124 172 266 15 108 169 264 15 103 171 263 15 128 170 265 15 150 170 2fi7 15 141 171 266 15 113 170 267 15 111 171 266 15 TCE-TETRA BY-PRODUCT Flow GPM 17 16 16 14 9 17 21 16 16 21 25 22 20 18 MC PRODUCT Flow to Stabilizing Tanks GPM 40 HIGH PRESSURE CONDENSER Outlet Temp. F 37 33 31 38 29 30 14 40 25 58 39 42 42 -- SL 013939 35 32 43 49 * 47- 44 ot 41 39 0 35 c *NFlOl h JCCT- fr l'T< Aici* . Ho. 9 Dlttt 40 40 36 32 *r ;urt 39