Document 2qw57rvVZpNE89no5med3Ynb6

s.v C. V.fc6 ) D. V. 303, 315, 317,, CG 4 r*&** Vii < DATE ) COPE RT-539-D PKG ___ ------- ... (LOT NUMBER) PROCESSES' APPROVED BY < )"R"T-"5 39-'D' <-N ) X UK 10!%, EST. WT * , r.,, LBS. TYPED BY: JMH - JOB 40RT539DMN STANDARD HRS.___________ TIME M PREPARATION NOTES: SUPERVISOR NOTE: DO NOT USE V-303 FOR NAPHTHANlLFwHiN ' CAMPAIGNING DALAMARS YC-39-A, YC-40-A, YT-839-P, YT-840-P, YT-858-D, AND YT-868-D. '' srssssracs EQUIP | MISC | 1I J i ftST NAF'HTHANIL RED DARK: I NOTE: N24C (4NITR0-2 AMINOANISOLE HYDRO| CHLORIDE) IS AN EXPERIMENTAL CARCINOGEN. | ALTHOUGH MONITORING VERIFIES WE ARE WELL' S JJff I N-CODE I ACCT LBS I -LBS ----------- j-------- -- -- I I I I I I BELOW THE RECOMMENDED EXPOSURE LEVEL. IT IS ! | ESSENTIAL THAT YOU ADHERE STRICTLY TO* THE I J SAFETY RULES WHEN HANDLING N24C. THIS IN- I i CLUDES RUBBER GLOVES, LONG SLEEVES, SAFETY 1 | GLASSES, RESPIRATOR'AND WASH UP AFTERWARDS. I I SEE YOUR SUPERVISOR IF YOU HAVE QUESTIONS, I I t 1 1 OBTAIN 4-NITRO-2-AMINOANISOLE HYDROCHLORIDE I I 24-C.D1 J | FOR STEP 6 ' IJ I I 2 j OBTAIN METANITROANILIBE OF B-HYDROXY ' I I I I | -NAPHTHOIC ACID FOR STEP 31. I 151-C 1 [ 3 I CLEAN, DRESS, CLOSE 24* CLARIF PRESS- r\ f J I ..i -15 FRAMES I DV 1 4 (398 G) WATER INTO V-_3l ^2^_^_ 2 T 5 KRUN IN HYDROCHLORIC ACID FROM V-324 il ` M___2_____, J3j &3>.% i 6 J^DtfMP IN FROM Si' LOT . 4=100% %' I ' (^ffNlTRO-2- Js?SLy-- J13X-- i KAMINOANISOLE ___ _____________________ _ i HYDROCHLORIDE_______________J_______________ I 7 j WEIOM--QN POSTAL tAB#^ STIR 15 MIN TO WET KMU TO (71OG) AT 28-32 DEG F IxSfPHON IN SODIUM NITRITE IN 4-8 MIN. M_____>#, . TiR 5 MIN 8 RECORD:. CR__.^r__(+ )KI_JjrL_( + > I J NOTE: (1) IF CR-,KI- ADD 20$= "AS IS" IN- I CREMENTS. HYDROCHLORIC ACID ASSUME 32% J RECORD: CR______ ( + > KI^_.___ _< + > I (2) IF CR+,KI-, ADD t4= "AS IS" INCREMENTS I SODIUM NITRITE ASSUME 33% IRECORD: CR_______(+) KI_______<+) fHsTIR 30 MIN AT 28-32 DEG F MAINTAINING +CR 1 +KI FOR SI 7 ' RECORD TIME START MISC M2 3I RRY IN 40 GAL WATER IN DRUM & PRECOAT iLARIF PRESS WITH J 5 I 777--A | I ` I V 302 OR M 3 5* (60G) WATER INTO V-_dl2t:___ * 1 314 114 I^FOOR IN SODIUM HYDROJODE^ ASSUME 50% I * 4 * 115 J^FOUR .IN ACETIC ACID 8 STIR 3 MIN ASSUME 70% |-; /79 J Isw I I HENT I ' } PAGE 2 OF 3 CG 40 CODE RT-539-D <N) 4 Ii6 L'tfECORDt PHJu'S_<6.5-7.5> & IF NECESSARY CQNT. I I / ACETIC ACID ASSUME 70% I -T ADJ. TO PH 6.5-7*5 RECORD PH_:TL I ' SODIUM HYDROXIDE ASSUME 50% USE | N-COD^lFiECT LBS | | LBS - --1---- -- |j --------,iIg^--^TMm .j 30-D |^ I 7-D I DV 5 -5 ^: ^ 117 WHEN S11 STIR COMPLETE, TEST DV & RECORD: | CC.-3L._<+> KI_:3feL_<+> TEMP_______ _28--32#F NOTE: (1) IF CR-,KI-,ADD 20* `AS IS* INCRE I ' I MENTS HYDROCHLORIC ACID ASSUME 32% I I RECORD; CR____ < + > KI___(*+) <2) IF CR+, KI-, ADD 10* *AS IS1 INCREMENTS I SODIUM NITRfTE ASSUME 33% i RECORD : CR____ _( + > t8 KfeGH SULFAMIC ACID IN RUBBER BUCKET AND I J<tfeSM INTO DV M* i^friR 5 MIN & RECORD: KI.L.jtl---<-) 20 L-TF NECESSARY, ADJ TO -KI > RECORD:^-- MP DICALITE FILTER AID IN & STIR 15 MIN. ON. V-32JL AGITATOR ADD ICE, THEN T OFF AGITATOR UMP DV THRU CLARIF PRESS INTO DV USED- IN |^S23^MAINTAINING TEMP AT 28-32#F. RECORD: l^rfMg, STARTV/A TOTAL MIN H6---___ -- |>mN S23 CLARIF COMPLETE, WASH-DV <S4) .. " . K^WrNES, PUMP & PRESS FOR 20.MIN OR TO A P-R TEST ON A SMPL OF TOTAL PRESS EFFLUENT, M*HIHEVER COMES FIRST, COLLECT WASHINGS IN UgS23> .125 L^STTR 5 MIN & RECORD: TEMP__<28-32 F) |IF NECESSARY ADJ TO 28-32 DEG F AND 'ihru l^feORD _^221,,____ DEG F 126 L^r ECORD : VATJEf--" AND HOLD FOR S45 .. i ' s I ^ "^T-- 1^ | i__' ----- 1I, \7 I I 1, 10^ \6t& I I 57--A I___ _ I I 260,,-^3 6j INSTALL V-240 TEMP CHART & SET AGITATOR AT I PM ' I T RUN IN 20* (1988G) WATER ' I KRJ^N 23* (457 G) WATER INTO V-330 ` I ^SLURRY IN 20G WATER AND POUR IN TRISULPHOILI |*<OAP D 4 J^DUMP- IN META NITRQANILIDE OF B-HYDRQXY ' LM^PHTHOic ACID FROM S2 LOT KAND STIR 10 MIN. TO WET Jiksjkzz.-'l 39-A j 51 -C /<? w tise 6-r#/cx/ WEIGH SODIUM HYDROXIDE IN BUGGIE & HOLD S35 ASSUME 50% i WEIGH ACETIC ACID IN RUBBERLINED DRUM AND I OLD FOR S39 M___.#___ I | NOTE: Tl )DO NOT PROCEED.WITH BATCH <S*S 35 THRU 50) UNTIL S26 CLARIFICATION COMPLETE <2> WHEN S26 COMPLETE PROCEED WITH BALANCE OF BATCH WITH NO DELAYS TO PREVENT N-151-C SOL1N HYDROLYSIS REStJLJJNk IN BLUE TINE. # <i mi i mi i i 11 w, MfUll .* Mr* Vi* % MM a f%\/ II 3,Z I - 1 I '39*' | II II II II II a .1 7-D 1 1 30-D I & \ I I |<sw* DUP050061157 iltI __. .2^. EQUIP IT I " MENT I L PAGE 3 OF 3 USE CG 40 CODE RT-539-D <N> I LBS "20 4?piSEN S23 COMPLETE* POUR: IN N-7-D FROM S32 'kjj&ZD 2/26/82 :* N-CODE Ta Ec t I LBS I3^ujfit TO 155-1.62*1? AFAP RECORD: MIN_^t7__ I 3,2*T STIR 5 MIN TO DISSOLVE FOR S38. RECORD: j V SOLUTION COLOR_f_^ :<DARK BROWN) TTme.j Mpk Si I I CLARITY____^^^J^^ri^(MUST BE CLEAR) . I ' I NOTE: IF SOLUTION NOT DARK BROUN 6 CLEAR, I ' vj HEAT m-*e5-i 92*F AFAR AND RECORD: K I CQLBft^ L < DARK BROWN) : fe^r!ir__-<MUST BE CLEAR) . I ~----- - I -- 26 I WHEN S37 COMPLETE WITH V-26 AGITATOR OFF, | 10 l!" J<TMMEDIATELY RUN N-33 INTO V-26 AFAP | \3/C\ IMMEDIATELY TURN CJN V-26 AGITATOR & SIPHON | I jJiW-N-30-D FROM S33 IN 5-8 MIN, ^ | |4*TSTIR 5 MIN ONLY fc RECORD PHJLI*J_< 11.0-12.0) I 141 | IF NECESSARY, ADl), TO PH 11.0-12.0 | II SODIUM HYDROXIDE ASSUME 50X I ^H?ECORD PH____ ACETIC ACID ASSUME 70% 1-42 | RUN IN V-302 OR V-314> FROM S16` 1. I | 7-D 3,0-D i .1 HEAT TO 148-152*F IN 15-20 MIN AND RECORD: I ,_*F AND REC_m- #F I 4HEN S44 COMPLETE, IMMEDIATELY COUPLE DV I UNDERSURFACE IN 65-70 MIN. MAINTAIN CV AT ^ 48-152fF. RECORD STARTJViJ?.TOTAL .HI*L.j L* STIR 5 MIN 6 RECORD: DIAZO_M^__<- OR +) . BASE_7j$ilMUST BE + PH__^XlC4.5-5.> rj'"'v I4PTSTIR 15 MIN 6 DISCONNECT TRANSFER LINE AT I CV RECORD: START_,/l 4e I!s 1_- I<SPl WHEN S47 STIR COMPLETE, TEST CV AND I | RECORD: DJAZO^J2C. MUST BE - . I I BASEJ^A5~<MUST BE +) FOR BOTH HEALTH AND I I SAFETY REASONS, IF RT-539-D FINISHES WITH t I I + DIAZO, WHEN IT DRIED, IT CAN PRESENT A I THREAT OF FIRE OR EXPLOSION ON GRINDING IN | FINISHING AREA. SEE YOUR SUPERVISOR IF . | ^>PtfERE ARE ANY QUESTIONS. 14^1 IF S48 DIAZO IS + AND BASE IS ALSO + SIFT |< I IN 204 N-3-A, SODIUM CARBONATE, 6 STIR TO - DIAZO. WATCH FOAM.' RECORD: DIAZO____ __________MUST BE * BASE_______ ________ MUST BE + PH________ - ... --JeA. 8-5.2) TOTAL MIN SINCE S4Tl^a!L____ 3-A FLOOD TO 82* <8126 G) AND STOP AGITATOR 4. >. / VAT S4 <39SG) S8_<71QG) V-303 V-315 V-317 16* 12* 12*; 29* 21/ V-322 V-323 12* 12* 21* 21* W- zi. t/t-Y * DUP050061158 Co7>: A^SM- Xe 7 iSSfe * "270 s h p p -1, 1 A 3?^-: igggfe 1I3S3SS- * -. ?-- ra*-. * CS-SSST;.. 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