Document 2q9R77EqQ7EdGO8ZVEQYwpRYg

F, H. BEADLES (23) DIRECTOR OF PRODUCTION WILMINGTON F&F C. W. THEOBALD DIRECTOR RESEARCH DIVISION WILMINGTON F&F K. F. BROWNING (2) CONSUMER PRODUCTS SALES MARKETING & PRODUCTS MGR. WILMINGTON F&F C.C; J,, Wo Nestor, Wilm. F&F Go To Vaala, " " P. I, Poindexter " " L. So Baker, " R. B. Davis, " " D. L. Herndon, '* " J. O. Graves, " " Go I. Mulholland, Flint 0. Ho Bullitt, Jr., Lab. Po J. Graham, Exp, Sta. File: 3320 Marshall Laboratory April 25, 1967 MARSHALL DEVELOPMENT LABORATORY SUPPLEMENTARY RELEASE LETTER #1997-C REPLACEMENT OF SULFATE Ti02 WITH CHLORIDE Ti02 IN 603-LINE ALKYD HOUSE PAINTS No Approval Action Required The attached covers the conversion of 603-Line Alkyd House Paints to the use of chloride process TiO^j W-185, "Ti-Pure*1' R-902 Hi Gloss. At the same time H-454, 10% solution of phenyl mercury oleate is replaced by G-796, 100% phenyl mercury propionate, at equal mercury content in another simplification towards obsoletion of H-454. MARSHALL DEVELOPMENT LABORATORY E. OYLER JE0:hfm Attach. Registered Du Pont Trademark APPROVED APPROVED DATE_ DATE MARSHALL DEVELOPMENT LABORATORY SUPPLEMENTARY RELEASE LETTER #1997 B REPLACEMENT OF SULFATE Ti02 WITH CHLORIDE Ti02 Product or Line Number 603-Line Alkyd House Paints Related Release Letter No. 1997-A No Approval Sulfate Chloride Replaced Replacement Replacement Change in Procedure Mill Cost Stability Data Available W-28 W-123 Equal Wt. X* None * Months 12&18 W-43 W-129 Equal Vol. Increase c/gal.Adequate X W-50 X W-131 Equal Decrease*5. 5q/gal.Inadequate Hiding X* Tints Only W-124 W-185 X New Standards Issued. Yes ______No X Estimated Annual Consumption Change. Chloride Increase 283,000 Based on 1966 Production Sulfate Decrease 297,200 Active Formulating Practice Revised. Date Formulating Practice to be Written. Yes No Initial -Chloride Ti02 Formula Date. *Nos. 40 and 42 Whites use W-185 at equal weight to increase hiding about 5-8%. Tints use W-185 to equal tinting strength, abou,t 5% reduction, to effect slight cost savings. ifgpp N42507.01 DUP030022278 Properties Thoroughly Evaluated Shelf stability Chalk resistance Tint retention Appearance retention Cleanliness retention Whiteness (whites) R. L. #1997-C Compared to Std. "^ Variation* X X X X X X ^Better cleanliness and less yellowing result in improved appearance and an apparent if not actual improved tinting retention. Whites are less yellow initially and during exposure. Compared to Std. Properties - High Spot Evaluation Equal Variation Production limited to laboratory batches of whites and several tints. Pre-alignment considered to be unnecessary. List Critical Tests required for alignment beyond control testing None DUP030022279