Document 2joQJx2X3kpgQEa9OMO0xjb86
%. . H
*
S. V.
c.v
CG i 3
CODE RT-698-D FKG___ ,
G2J62;
( DATE )
(LOT NUMBER)
A7S8
e s t . wT.'aae** l b s .
PREPARATION NOTES:____
DATE PRINTED: 5/12^2. D. V. 902,904
PROCESSES < )RT-698-D (M)
APPROVED BY EWK2/25/82
TYPED BY: KLW s t a n d a r d h r s ._____
t i me m
NON-BLEEDING
EQUIP MENT I
NAME: WATCHUNG RED B
USE N-CODE ACCT LBS LBS
PREP 1
I RECORD - P3L,,_BATCHES SINCE SPARKLER LAST
CLEANED. AFTER 4 BATCHES,.CLEAN, DRESS
SPARKLER & PRECOAT WITH i 5* DICALITE
FILTER AID
T OBTAIN FOR S11 2-CHLORO-4-AMINOTOLUENE-5-
r L-SULFONIC ACID
.
\JT\ 5BTAIN FOR S41 3-HYDR0XY-2-NAPHTH0IC ACID
INSTALL DV & CV RECORDER & CONTROLLER CHART
NOTE: RUN 15' WATER INTO V-904. PUMP WATER
FROM V-904 THRU DISTRIBUTOR. IF WATER DOES
t NDT COME OUT OF ALL DISTRIBUTOR HOLES WITH
I FULL FORCE, NOTIFY SUPERVISOR .
777-A
740-C 82-C
932
I^T RUN 20* (415G) WATERINTO V-932 & HEAT-TO
I 80-100 DEG F
ADD IN 8-9 MINDRESINATE X
rriR 5 MIN & RECORD:
(9.5-10.5)
'STIR 20 MIN OR LONGER TO DISSOLVE FOR S44
H ffrAX
NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF.
AREA UNDER V-922
922
RUN 3B* (782G) WATER INTO V-922
-'3 WEIGH SODIUM HYDROXIDE IN V-926 & RUN IN
M JA_______ TURN ON AGITATOR & STEAM i, DUMP IN FROM S2
2-CHL0R0 4-AMI NOTOLUENE
LOT (M 0%
-JJA7-
_________ _________
7. ___
i 5-SULFONIC ACID _________ _____ ____________
DUMP IN ACTIVATED CARBON
LH3 1 DUMP IN FILTER AID |>4^fyEAT TO 212-214 DEG F WATCH FOAM!!!!
25 10
I I^TRECORD : BY,,-afc___< + > IF NECESSARY ADJ TO
\ l>BY SODIUM HYDROXIDE
ASSUME 5%
!J>"T STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF
I | STEAM. WATCH FOAM. RECORD: SPARKLER PRES-
I INSURE ______ PSI IF NOT ZERO NOTIFY SUPVR. \yr | CIRCULATE 15 .MIN OR LONGER THRU SPARKLER
i I UNTIL SOL1N IS CLEAR. MAINTAIN AT 190-195 F I I FOR SI 9. RECORD: STARTAL MIN_1?I i | CLARITY_________HT__iJ?:5~_ F tf REC fQ$- F
7-D I 22 740-C I 1127
I I 113-B |
777-A I
25 10
7-D i, I
JUL281S82
N32887
DUP050464592
EQUIP | MENT 1
1 USE j N-CODE 1 ACCT
PAGE 2 OF 3 CG 32 CODE RT-698-D <M> ! LBS I
i LBS
^CVI'UMx RUN 2* (58G) WATER INTO V-904/CV WHEN'S17 COMPLETE, PUMP IN V-922 THRU SPARKLER. MAINTAIN V-922 AT 190-195 DEG F
RECORD: START__/iJ?.i/3i^\T0TAL MIN__fi___
1 I 1
1
1 1 !
!
1 1 !
i
902
"5 '
1203 RUN. 54 * (1407G) WATER INTO V-902
v+arn DUMP IN CALCIUM HYDROXIDE & STIR TO SMOOTH f f SLURRY | 2X WEIGH SODIUM HYDROXIDE IN V-926 & RUN IN AND HOLD IFOR S41
11 1 530 1 i!
! _3L25j
542-D 7-D
1 I |
i !
MISC 6
L25T MEASURE
UNITS IN V-928 FOR S35
1
HYDROCHLORIC ACID
M__/
\2Jr* WEIGH SODIUM NITRITE IN PT FOR S38
.
! Mud \//-Qni
! 28-D |
725-A |
53
166
544 367
922 WHEN SI 9 COMPLETE., STOP PUMP & INSERT V-9I 7 )T PLUG
IN 15' (309G) WATER & HEAT-TO 190-195
?CULATE 15 MIN THRU SPARKLER PUMP V-922 THRU SPARKLER INTO V-904/CV
922 9
RUN IN 9* (177G) WATER INTO V-922 AND HEAT \ 1 TO 190-195 F* CIRCULATE 15 MIN THRU SPARKLRi
904/CVlZffjr PUMP V-922 THRU SPARKLER INTO V-904/CV 110 1Iv35*r0[ WWlHEN MTY BLOW OUT SPARKLER INTO V-904/CV 1ljj4,^T-?'0UR IN IGEPAL CO-630
l2>T HEAT TO 165-170 DEG F FOR S34
1
lI
I
} 47 I 979--D i 47
!
CV -11
I | NOTE: IF N-740-C SOL`N'WAS PUMPED DIRECTLY I | FROM SPARKLER TO CV, OMIT STEPS 33 & 34*. 1313 | RUN* IN 1 - L95G>, UAJER INTO Vr^___ ____ , i S^ C0PLp^1%~4<f*?4
I f THRU-UNDERSUtf.ACE DISTRIBUTOR INTO CV AF4 12-^S M|NK>T|A>N1!A 11^65^70
H lREEuRD: STMT___,,'r^l_ WrAr^MI RUN IN HYDROCHLORIC ACID N-28-D FROM S23
1 '
1
eIN 12-15 MIN
i
|36^fjSTIR 15 MIN AT i65-170 DEG F*
SX3301
ADJ TO 48* (4536G) AT 32-38 DEG F
r J^-RECORD: TEMP_^J$i__ F, VOLUME
,J
138| RUN IN SODIUM. NITRITE N-725-A FROM S2.4
M
I - L^AFAP. (5-1 MIN) & RINSE IN PT
* I
X3#"T STIR 30 MIN AT 32-38 DTEIMGEF SMTARINTT_A4Ij^:fNG, _ /
t +DR, +KI FOR S40 RECORD: NOTEt I CRL_1__( + ) KI_^___( + > AS IS" INCREMENTS
I <11, IF CR-, KI- ADD- 20#
-l HYDROCHLORIC ACID
ASSUME 32%
L.RECORDl CR______< + > KI_____IS_ *C+I)NCREMENTS
I,
--...^
i2yflF CR+, KI- ADD 20* "AS
DIUM NITRITE
., '
RECORD: CR< + > KI_.( + ) ` ASSUME
33%
DUMP IN FROM S3 & STIR 10 MIN LOT 3-HYDR0XY-2-NAPHTH0IC ACID- ^.7<k.<sL--
I JUtMk I___ &L11
I:l I. .1
\3/oo
I 28--D |
I
725-A 82-C
,1. i 1021
i' , i
DUP050464593
DATE PRINTED: 5/12/82
EQUIP MENT
E 3 OF 3 CG 32 CODE-RT-698-D <M> I DUMP IN AMMONIUM CHLORIDE
USE LBS
221
N-CODE 165-A
ACCT LBS
221
--------------------------------------------------------- ---------------
!4S*'| IMMEDIATELY AFTER S41 COMPLETE', WITH V-902
AGITATOR ON PUMP V-92 THRU UNDERSURFACE
DISTRIBUTOR INTO CV.IN 18-22 MIN. LET TEMP.
RISE^REELY.
~
3RD: START.V^j&L.TOTAL /SIN
___
STIR 15 MIN & RECORD: PH__UJ,V__(9.-9.8)
TEMP _AJ3L- DEG F <40-5 DEG F) AND IF" PH IS BELOW 9.0 ADJ TO PH 9.0-9.B
SODIUM HYDROXIDE
ASSUME 50%
& RECORD PHJZl */. DIAZO,,i-srL<-) ASSUME 32% BWPKafet+) HYDROCHLORIC ACID
|4u KT^ESM EJECT V-932 FROM S8 INTO CV
|r POUR IN I OCTANOL
HEAT TO 173-175 DEG F IN 55-65 MIN AND
RECORD: HTDEG F & RECDEG F '
3
7-D 28-D
1&
588-A
3
902 \7 \ DUgING S46 HEATING, RUN I' <268G) WATER
14 ! MiffO V-902 tr| TURN ON AGITATOR & STEAM & DUMP IN BARIUM I !JGHtlORIDE HEAT TO 155-160 DEG F G STIR TO DISSOLVE
259
16-B 259
CV 15&^T^JHEN S46 COMPLETE, STRIKE V-902 AT, 155-160F
15 I | THRU UNDERSURFACE DISTRIBUTOR INTO CV IN
I | 2-3 MIN
.
..
I L^RECSRD: START_Zs L_TOTAL MIN__ftfc__
IS^n HEAT CV TO 193-195 DEG F IN i-15 MIN.
152 I SJJ-R 6 MIN AT 193-195 F. RECORD START^^S
~"6f TR 2 MIN S52 STIR RECORD PH51ftf_<8.8-9.3)
IF NECESSARY, ADJ TO PH 8.8-9.3 ASSUME 50%
^ND RECORD: PH______ ___
ASSUME 32%
WHEN S52 STIR COMPLETE, FLOOD TO 180-19*
(+/-18000G) AND STOP AGITATOR
7-D 28-D
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY THRU PRESSING, DUMP IN I OCTANOL, STIR 5 MIN 6 STOP AGITATOR. RESUME PRESSING.
i
588-A
10
FIN
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OP TP
DUP050464594
N32887.01
DUP050464595
N32887.02
DUP050464596
N32887.03
DUP050464597