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PLAINTIFF'S EXHIBIT -,-- /;"Sa-58i * i ^ i, _ ^ Transactions of tnc TESTH MMAL HHifteMil\.l rTi5.N -- -' -*-*>**- -' 'I the agr-^ffl!!^^t;%u!5,|g3i^sg ..i-*wiijt&WMgBBBSm eomiHim iDomiiL : ;bygimists Jt `.at c Hilijjllijjlljillilllljill;: - 29 - . MPOHT OP THE COBIITTEE OH THRESHOLD LIMITS _ DR. L. T. PAIRBALL (D. S. Public Health Service)] It is obviously difficult, where a large number of substances is involved, to review the maximum allowable concentration values in detail at an annual nesting. Fbr that reason, provision was nade early in the organisation of the American Conference of Governmental In dustrial Hygienists for a Committee on Threshold Limits to study this question and to report to the'Conference at its annual meeting. The composition of this Com mittee is not fixed but is changed by annual appointment and the threshold limit values are similarly maintained in a fluid state by annual revision. For a number 'of years the Cosmittee has subjected these values to oereful scrutiny and attempted to bring them into olose conformance with practice. ^ ^ " ` During the present year, it was folt that the eonoept of maximum allowable values had now reached a stage where more extensive participation of the members of the Conference in the formuletion of these values based upon personal experience in the field would be of deoided assistance. This year, therefore, your Committee has for the first time, I believe, made a direct attempt to obtain a statement from each member of the Conference with roferenoe to tho annuel threshold limit values end the response from the individual members has been most generous and helpful. ' ' * * ` " ,,. ' / tji nf pose of the nnnti i*mH-inn nf threshold limit values,it hos been the pur ** wini>. inih) m pn* hand protect the individ- ual~worV"n- "d on the other would impose no impossible burden on the manufac turer. This balance is difficult to achieve but con be attained by just such a series of adjustments as is provided for in the Constitution of the Conference, i There is no industrial poison so potent, so virulent, that it eannot be manufac- j tured safely under carefully controlled conditions. The manufacture and wide- j spread use of such a substanoe as lead tetraethyl and the preparation of extremely l poisonous war gases are good illustrations of this. In faot, the chemical manu facturing industry in general has been able to maintain a high standard of safe industrial practice by the installation of suitable eontrol measures for the pro tection or its workers. There is no reason why such safe industrial control measures cannot bo extended to industry in general wherever industrial poisons occur. ' ** - r . * .* , 4 * ** * ' In addition to the eonmonts of tho members of tho Conference, a few criti- ' cisms from other sources have reached ust oonoerning tho 1947 values. Those may ' be briefly summarised as follows> ' ~ 1. Concerning the membership at large, criticism has taken the form that (a) values were arrived at by consulting tho membership at large, and (b) that the members were not consulted. 2. The publication of the values in the Industrial Hygiene N ewsletter made - it appear that the values were those of the U. S. i>ublic Health Service. TJhether ' "this was wishful thinking or not, the source of the 1947 values was dearly in ' dieated at tho time of publication. ------ ---.. ... .. . ... - ' ' ' ` :----r ** ' .3. Criticism has olso taken the form that the values given wero not arrived *v. or based upon scientific evidence. The latter has particularly interested . ... .- ..., . . .. . : .20 .: ; - im-- . '!'/ ^ lv?0v; .. .. - ' - ,,V -7 . * - 2C0 ' ` . your present Cosnittee. No specif ie "scientific evidence" has so far been pre sented for our consideration along w . with this criticism* .' ***** ^ While it will doubtless be very advantageous to have what slight be called ; permanent or standard maximum allowable eonomtration values, it must be borne in mind that all our values at the present time are fluid and subject to annual re- i vision* They should not be adopted as fixed or legal values, but meroly as guides to assist us in defining more or less safe working conditions. It is felt that eventually definite values oan be .established which will give full and ample pro tection to the worker. *. ' ' ;. . * . ' *- . . * ,,* t The following changes have been st^de.in the values from those of the 1947 conference* ' . . Bentene has been decreased from SO to S5t ppm . . Chlorine has been decreased from 2.to 1 ppm ' .... . - Formaldehyde has been decreased from 10 to S ppm Hydrogen chloride has been .decreased from 10 to 5 ppm ' Hydrogen eyraide hrs been deereased from 20 to 10 ppm ' Hydrogen selenide has been decreased from 0.10 to 0.0S ppm Trichloroethylene has beat deereased from ISO to 100 ppm .. Iodine has been changed from .1 mg./cu.m, to 1 ppm " _ ' 2-Butnnone has-been increased from-200 to 250 ppm ' . .................'. Isbpropyl'ether has been increased.from 400 to 500 ppm' Antimony has been increased from 0.1 mg./cu.m.,to 0.5 Arsenic has been increased' from 0.1 mg./eu.m to. 0.5 . Sulfuric acid has been increased from 0.5 mg./cu.m. to 1.0 It must be borne in Blind that these values are not'indices of toxicity and are not intended to aporoach that value. Accordingly, the oosmaratlvw toricity of these compounds eannot be established on the basis of their numerical maximum allowable concentration value. "' ;; : ----- --. p^nnla imry d"T" "nd toxic substanoea-.__ Therefore., it is a figment th thlnV we can set down a precise limit below which there is complete anfety and ^mediately above which there mav be a high percentage of cases of poisoning imt those exposed. .... " wlth <n Comn<t< hn get values below which it is fair to expect reasonable protection and above whioh it is reasonable zo expect chat i?e~oan have occasional eases of^poisonina. ~ ------------- ----------------------------- - ' THRESHOLD LIMIT VALUES ADOPTED AT APRIL, 1948, MEETING OF AMERICAN CONFERENCE OF GOVERNMENTAL INDUSTRIAL HTGIBUSTS IN BOSTON, MASSACHUSETTS 4: v'. Ethyl. c - ^:-iv SUBSTANCE v Acetaldehyde Aoetio aoid Aoetio anhydride Acetone GASES AND VAPORS >. ' P.P.U. r- SUBSTANCE 200 Aorolein in- 10 Acrylonitrile rther4 6 kjnrnrm GOO -Amyl acetate P.P.U. 0.5" 20 ; 100 1 200 SUBSTANCE P.PJt. - . SUBSTANCE ' P.P.M. .iso-Amy1 alcohol - V loo Ethyl fonaatc . . - .. 100 ...Aniline . s Ethyl silicate ' 100 lArsine ' ^ 0.05 Formaldehyde ' * s Benzene (benzol) ~ - 56 Gasolene -' - 600 '`Bromine .. :i Heptane . * 500 .|1,3-Butadiene " :1,000 Hexane 500 n-Butanol so Hydrogen chloride . ." 5 2-Butanone n-Butyl acetate ___2S0 - 200 Hydrogen cyanide Hydrogen fluoride ' 10 3 Butyl oelloeolTe 200 Eydrbgen selenide 0.05 Carbon dioxide 6,000 HydPogen sulfide 20 Carbon disulfide 20 Iodine 1 Carbon monoxide Carbon tetrachloride r\ - * 100 60 Isophorone Mesityl oxide ' - 25 50 Cellosolve ' ` ;.v - 200 Methanol 200 Cellosolve acetate - - ' 100 Methyl acetate 200 Chlorine - ' " 1 Methyl bromide - 20 2-Chlorobutadiene ' 25 Mothyl butanone 10Q Chloroform 1-Chloro-l-nitropropan e Cyclohexane Cyclohexanol -' Cyclohexanone Cyolohexene - Cyclopropane (propene) o-Dichlorobenzene Diohlorodifluorone thane 1.1-Dichloroethane 1.2-Dichloroethane (ethylene dichloride) 1.2-Dichloroethylene "v Dichloroethyl ether / '^ Diehloromethane ' * ' Dichloromonofluoromethane 1.1-Dichloro-l-nitroethane -- 100 20 400 -. 100 -vlOO -400 400 SO 1,000 100 75 ' 200 - 16 600 1,000 10 Methyl cellosolve 25 : Methyl oellosolve acetate 25 Methyl chloride ' 100 Methylcyolcbexane 600 Methylcyclohexanol 100 Methylcyclohexanone 100 Methyl formate 100 - Methyl iso-butyl ketone 100 . * Monochlorobenzene Monofluorot richloromethene 75 1,000 Monon itrotolu ene 5 Naphtha (coal tar) 200 Naphtha (petroleum) 600 Nickel carbonyl - 1 Nitrobenzene 1 Hitroethane '" ` 100 Nitrogen oxides (other than N^O) 25 1.2-Dichloropropane Nitroglycerin ' 0.5 (propylene dichloride) 76 Mitromethane '" " 100 Dichlorotetrafluoroethan e 1,000 2-N itropropene 50 Dimethylaniline 5 Octane 500 Diaethylsulfate . 1 Ozone 1 Dioxene 100 Pentone - - 1,000 Ethyl acetate 400 Penton one (methyl propenone) 200 u Ethyl alcohol ' Ethyl benzene ''Ethyl bromide Ethyl chloride J ,. . A > ' '1,000 J 'i - 200 200 1,000 Phosgene Phosphine ^as ?v.v.-v. t ... . phosphorus trichloride Iso-Propanol . _-** 1 , 0.06 ' 0.5 <00 Ethylene chlorohydrin Ethylene oxide - Ethyl ether ocr 6 * 100 400 I Propyl acetate iso-Propyl ether ' feiibine .~L * : . 200 '..T- ... . ;> 500 ' 0.1 A V \ J SUBSTANCE - 32 - # GASES JWD VAPORS (eont'd.) . P.P.U. - ' : SUBSTANCE P.P.M. Stoddard solvent , lJ.^SOO . Toluene A. - - Styrene monomer - . 200 / Toluidine ' :'/ Sulfur chloride . . . Trichloroethylene Sulfur dioxide / 1,1,2,2-Tetrachloroethane .- !/*~- IQ0e * : Turpentine Vinyl chloride ." `Vf r . Tetrachloroethylen* '`"'loo. jyide - ' - .200 ' -5 100 100 500 200 SUBSTANCE TOUC DUSTS. JFUUES AMD lilSTS . Ug. per eu. m. . SUBSTANCE Mg. per eu. a. Antimony 0.5 - Mercury .. Arsenic 0.5 Pentachloronaphthalene Barium - 0.5 Pentacnlorophenol -? Cadmium Chlorodiphenyl" 0.1 Phosphorus (yellow) .. Q. . -- Phosphorus pentachloride Chromic acid and chromates as Crc^O.l Phosphorus pentasulfide Cyanide as CM Selenium, as Se Dinitrotoluene 1.5 . Sulfuric aoid Fluoride 2.5 Tellurium . . Iron oxide fume 15 Tetryl Lead "' 0.15 Triehloronaphthal ene Magnesium oxide fume 15 Trinitrotoluene Manganese . 6 Zino oxide fume . 0.1 0.5 0.5 0.1 1 1 0.1 1.0 0.1 1.5 5 1.5 15 MINERAL BUSTS SUBSTANCE M.P.P.C.P. SUBSTANCE M.P.P.C.P. Alundun . '' Asbestos Cerborundum > -- -' Dust (nuisance, no free silioa) Mica (below 5% free silica) Portland eenent ' Talc 60 5. SO 50 60 60 20 Silica: high (above 50% free Si0) medium (5 to 50% free Sityt) low (below S% free SiOg) Slate (below S% tree SiOg) . Soapstone (below S% tree SiQg) Total dust (below 6% free SiOg) 5 20 50 50 20 50 MATERIAL OR RaDIAIICN RADIATIONS Radiant fEnergy Radiant MATERIAL OR RADIATION Energy Gemma (roentgen per day) ' Radon (curies per cubic meter) 0.1 10-8 Thoron (curies per cubic moter) IQ'8 2-ray (roentgen per day) . - 0.1 ~ V - I. r ;$*<' '.-.1s t*:-- ,-*'. A*** - * ^_v.'-:ciI.TV-..u... * % *.. ' - /*/ r / / f* A- > A . '' (The report of the Conmittee on Threshold Limits was accepted.) A ' .* . M.'-