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J O N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 BILL HAGQ1AN 0XYCHEH - BAYPQRT 5761 UNDERWOOD PASADF.NA TX 77307 LABORATORY ANALYSIS REPORT REPORT DATE APR- 17. 1992 SAMPLES REC'D APR- 10* 1993 REQUEST NUMBER *M515________ PAGE NUMBER 1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED RESULTS Micrograms Front 8ack Front 032392001 ETHYLENE OXIDE Cl. 4 Cl.4 C1.0 032392002 ETHYLENE OXIDE Cl.4 Cl.4 Cl.? 032392003 SLAhfit.... ETHYLENE OXIM NONE DETECTED Milligrams PPM 32392004 ETHYLEfC OXIDE BADGES CO. 0010 CO. 02 032392005 ETHYLENE OXIDE BADGES CO.0010 CO. 02 032392005 ETHYLENE OXIDE BADGES CO.0010 CO. 02 032392007 BLANK.... ETHYLENE OXIDf : BADGES NONE DETECTED Milligrams PPM 032392010 METHYL CELLOSOLVE DIETH. GLYCOL NONQMETHYL ETHEI CELLOSOLUE CELLOSOLVE ACETATE CO.0049 CO.0039 CO.0038 CO.0032 CO. 05 CO. 04 CO. 04 CO. 03 032392011 MOHYL CELLOSOLUE DIETH. GLYCOL MONOMETHYL ETHE CELLOSOLVE CELLOSOLVE ACETATE CO. 0049 CO.0039 0.0052 CO.0032 CO. 06 CO. 04 0.07 CO. 03 PPM Back C1.0 Cl,2 COMMENTS. SAMPLE 032592001 ASSUMED TO BE SAMPLE 032592001. SAMPLE 032592042 TRANSFERRED TO REQ.# 173892 <0NLY 15 SAMPLES PER REQUEST PAGE PLEASE). P.O.# BAY-U17311. C MEANS LESS THAN Respectfully submitted, xo.', T'-y V'\ /; , J Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8935 PRINTED IN U.S A. n N3TL5LQ National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: BHL HAGEMAN PXYCHEH - BAYPOR1 5761 UNDERU00D PASADENA TX 77507 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17j 3992 SAMPLES REC'D APR. 10, 1992 REQUEST NUMBER 164516 PAGE NUMBER 1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 3239201? 032392013 032392014 032392015 METHYL CEULOSQLVE D1ETH. GLYCOL MONOTETHYL ETHEI CELLOSOLVE CELLOSOLVE ACETATE METHYL CELLOSOLVE DIETH. GLYCOL MONOMETHYL ETHEI : CELLOSOLVE cellosolve acetate METHYL CELLOSCH.VE DIETH. GLYCOL HONOMETHYL ETHEI CELIOSULVE CELLOSOLVE ACETATE METHYL CELLOSOLVE DIETH. GLYCOL MONOTETHYL ETHEI : CELLOSOLVE CELLOSOLVE ACETATE tlilligrafts CO.0049 CO.0039 CO.0038 0.0040 CO.0049 0.0073 0.014 CO.0032 CO.0049 0.0075 CO.0038 CO.0032 CO.0049 CO.0039 CO.0038 CO.0032 RESULTS PPM CO. 06 CO. 04 CO. 05 0.04 CO. 06 0.08 0.18 CO. 03 CO. 06 0.08 CO. 04 CO. 03 CO. 06 CO. 04 CO. 04 CO. 03 C MEANS LESS 1HAN Respectfully submitted, i 1 v. '' \ Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448 2 30M 1-92 OCC 8936 PRINTED IN U.S.A. IJ N0TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 T0: SyMYPORT 3761 UNDERUOOD pasadena tx 77307 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17, 3972 SAMPLES REO'D APR. 10, 1992 REQUEST NUMBER 3*4517 PAGE NUMBER ' OF REQUEST. SAfPLE NUMBER ANALYSIS REQUESTED 032392016 032392017 032392018 032392019 METHYL CELLOSOLVE 0IETH. GLYCOL MONOMETHYL ETHEI cellosolve rai.LOSO.VE ACETATE Ilfc IHYL CELLOSOLVE D1ETH. GLYCOL MONOMETHYL ETHO CRinSOlVE CEI .I Om.VE ACETATE TiETHYL CELLOSOLVE DIETH. GLYCOL MONOMETHYL ETHEI CELLOSOLVE CELLOSOLVE ACETATE METHYL CELLOSOLVE DIFTH. GLYCOL nONOMETHYL ETHEI CELLOSOLVE CELLOSOLVE ACETATE Milligrams <0.0049 <0.0039 <0.0038 <0.0032 <0.0049 <0.0039 <0.0038 <0.0032 <0.0049 <0.0039 <0.0038 <0.0032 <0.0049 CO.0039 CO.0038 <0.0032 RESULTS PPM <0.06 CO. 04 <0.04 <0.03 <0.06 <0.04 <0.04 <0.03 <0.06 <0.04 <0.04 <0.03 <0.06 <0.04 <0.05 <0.03 C MEANS LESS THAN Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8937 PRINTED IN U.S.A, N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: DLL HAGFMAN PXYCNErt - BAYP0RT 5761 UNOERUOQD PASADENA TX 77507 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17. 1992 SAMPLES REC'D APR. 10, 1992 REQUEST NUMBER 164518________ PAGE NUMBER ? OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED RESULTS 032392020 BLANK BLANK CONTAMINATED WITH ALL FOUR SOLVENTS Milligrams PPM 032492001 ETHYLENE OXIDE BADGES 0.0023 0.04 032492002 ETHYLENE OXIDE BADGES <0.0010 <0.02 032592001 BUTYL CELLOBOLVE 0.016 0.23 Hilliarams Front Back front PPil Back 032592002 BUTYL CELLOSGLVE 0.074 <0.0038 11 <0,06 032592004 BLANK.... BLANK NONE DETECTED Milligrams PPM 032592010 032592011 ilONOETHANOL AMINE <0.027 BLANK.... MONOETHANGL Al IINE <0.72 NONE DETECTED Milligrams PPM 032592020 PYRIDITE <0.0015 <0.02 OTHER SOLVENT PEAKS PRESENT 032592021 PYRIDINE <0.0015 <0.02 OTHER SOLVENT PEAKS PRESENT 032592022 PYRIDINE <0.0015 <0.02 OTHER SOLVENT PEAKS PRESENT COTENTS: NATLSCO RECOrrOiDS 100L AS MINIMUM SAILING VOLUTE FOR AMINES. < TEWS LESS THAN TIE RESULTS WERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: 75% - BUTYL CELT OSOLVE. Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8938 PRINTED INU.S.A. n NEITL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 rati HAGEMAN 0XYCHEM - BAYP0RT 5761 UNDERW0D PASADENA IX 77307 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17, 1992 SAMPLES REC'D APR, 10, 199? REQUEST NUMBER m31B PAGE NUMBER ? OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 032592023 032592024 PYRIDINE PYRIDINE RESULTS Milligrams PPM CO.0015 CO.02 OTHER SOLVENT PEAKS PRESENT CO.0015 CO.03 OTHER SOLVENT PEAKS PRESENT comments: NATLSC0 RECOMMENDS 100L AS MINIMUM SAMPLING VOLUTE FOR AMINES. < TEAMS LFSS THAN Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory /-;v ,/ ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8939 PRINTED IN U.S.A. n N0T15CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: MU. HAGFHAN CXYCHEM - BAYP0RT ST61 UNDERWOOD PASADENA TX 7/507 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17, 1992 SAMPLES REC'D APR. 10. 1992 _ REQUEST NUMBER 1M519 PAGE NUMBER -1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 032592025 PYRIDINE 032592024 PYRIDINE 032592027 BLANK.... BLAW 032592028 PYRIDINE 032592029 BLAM<.... BLANK 032592030 032592031 032592032 032592033 032592034 ACETONE ACETONE acetone ACETONE ACETONE RESULTS Milligrams PPM <0.0015 <0.02 OTtCR SOLVENT PEWS PRESENT <0.0015 <0.02 OTHER SOLVENT PEWS PRESENT CONTAMINATED OTHER SOLVENT PEAKS PRESENT Milligrams Front Back Front <0.0019 <0.0019 <0.04 OTHER SOLVENT PEAKS PRESENT CONTAMINATED OTFER SOLVENT PEAKS PRESENT Milligrams PPM 0.020 <1.0 0.0064 <1.0 0.062 <1.0 0.0086 <1.0 <0.0024 <1.0 PPM Back <0.04 < MEANS LESS THAN THE RESULTS HERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: BOX - PYRIDJME. Respectfully submitted, ,-y ...-t' v / /. 7 - -V/! , / f - ; A-5 /' > \ CM -.A , /: / 7/ v\- / ' / / ../ . Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8940 PRINTED IN U,S A. __ IJ N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO- BPXILYLCHHFMAGE-MBANAYPORT 5761 UNDERWOOD PASADENA TX 77307 LABORATORY ANALYSIS REPORT REPORT DATF APR. 17, 1992 SAMPLES REC'D APR. 10, 1 r& REQUEST NUMBER 16431? PrAGcE NwUuMiviBoEcRn ' OF REQUEST SAMPLE NUMBER ANALYSIS REQUESTED 032592035 032592036 032592037 ACETONE ACETONE BLANK.... BLANK 032592040 032592041 ETHYLENE OXIDE BADGES ETHYLENE OXIDE BADGES RESULTS Milligrams PPM 0.0034 C1.0 0.021 C1.0 CONTAMINATED OTHER SOLVENT PEAKS PRESENT liilligraes PPM 0.012 0.36 0.014 0.43 n C MEANS LESS THAN Respectfully submitted, y"' - "Y -, ' /: ' : -a ;V// ,Y"'' y-y / , / (( / / / 0 ,/-j . Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 occ 8941 PRINTED IN U.S.A. JQ Nausea National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 * Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: 13ILL HAGOIAN OXYCHEtt - BAYPGRT 3761 UNDERWOOD PASADENA TX 77307 LABORATORY ANALYSIS REPORT REPORT DATE APR. 17. 1992 SAMPLES REC'D APR. 10. 19V2 REQUEST NUMBER 17389? PAGE NUMBER 1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 032592042 ETHYLENE OXIDE BADGES Milligrams 0.020 RESLft TS PPM 0.57 < MEANS LESS THAN Respectfully submitted, / , / /'. / t ' / Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 0CC 8942 PRINTED IN USA. n N3TL5CQ National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 * Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO BILL HAGEMAN GXYCHEM - BAYPQRT 5761 UNDERWOOD PASADENA TX 77507 LABORATORY ANALYSIS REPORT REPORT DATE AFfi. 17, 19V? SAMPLES REC'D APR. 10, 1992 REQUEST NUMBER *6*515________ PAGE NUMBER OF REQUEST. ANALYSIS REQUESTED ACETONE BUTYL CELLOSOLVE CELLOSOLVE CELtOSOLVE ACETATE DIETH. GLYCOL MONDMETHYL ETHEI ETHYLEtC OXIDE ETHYLENE OXIDE BADGES IfclHYL CELLOSOLVE MONOETHANOL AMINE PYRIDINE METHODOLOGY OSHA METHOD 07 EQUIVALENT QSHA PETHOD 07 EQUIVALENT OSHA METHOD 53 EQUIVALENT OSHA METHOD 53 EQUIVALENT OSHA METHOD 07 EQUIVALENT OSHA METHOD 07 EQUIVALENT OSHA tCTHOD 49 EQUIVALENT OSHA METHOD 53 EQUIVALENT GAS CHROMATOGRAPHY OSHA METHOD 07 EQUIVALENT Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8943 PRINTED IN U.S.A, 13 ,1 "*1 NBTLSCa National Loss Control Service Corporation ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2468 PRINTED IN U.S.A. n ----- --r-- N3T1SQ3 '' National Loss Control Service Corporation Name Title -1/no/ Firm S'/?/?? Address 'Zr/ // ^/S/7/Bus. Tel. No. __________ environmental sciences laboratory, k-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2486 ANALYSIS REQUEST No. 164516 NC 82-fl 25M 2-91 PRINTED IN U.S.A. n --. j Nansen ----------------------------------------------------------------------------------------------------------------------------------------- National Loss Control Service Corporation Name Title Firm Address A?AocAsr<> . 'sr3r' 1-------77*50^ Bus, Tel. No. ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2488 ANALYSIS REQUEST No. 164517 NC 82-8 25M 2-91 PRINTED IN U.S.A. n Nausea National Loss Control Service Corporation ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2468 Name Title Firm 'ryni+A* Address z> 76 / Sfvg/d "7/Bus. Tel. No. / .------ 'zxr rrsor ANALYSIS REQUEST No. 164518 Yo'P' FIELD NUMBER SAMPLING VOLUME ANALYZE FOR- LABORATORY NO. RESULTS &*50S>} sx&no/t? 67(/9? w \/ idfte/g/'Ms'&A ________ z______________________________ rtZ&ZOTO $c4M zzfezA S$ 026990 1/ a ... 11_____ ______________________ C$//ji EE/?0 /t/ip 026991 -j-ojc/tyOO'Z. (f/0/h /*/3o79? 02699? Ox/or* kcr)/:&^v- tET$ 026993 ________ ^_________________________________________ Wz5J2GO^ /%m$z 7ZS9?CD</ >* iEf& / OfO&y/S/i5 026995 irmre^ /7/czV///f&/7p^s^sl#<. ISj/TeC 026996 ktwflsfr /%0/70-C 'fyb/&^s72Sf<<. ^3^^920// R/Mftt 026997 W*?) ; 5J2 5920 3S> (s8Ds?i r> Zy ^Q'ZO T/ AfS* V^3Z35> r,-7SCfZO'T^ $&/?! #jrer> ^Z&?37Z5 ^3^V7J l026998 1 026999 027000 027001 0?zS9<vz<s 4%A /u o/s^ (L, 027002 DATE COMPLETED ANALYTICAL METHOD: NC 82-8 25M 2-91 OCC 8947 PRINTED IN U.S.A. n N3TL5C0 National Loss Control Service Corporation Name /Z/IC Title Firm /2rt' Address ______________________ ___________ Bus. Tel. No. -p/sArrSo ____________ ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2468 ANALYSIS REQUEST No. 164519 5^ NC 82-6 25M 2-91 PRINTED IN U.S.A. 0 O O C_; 5ENDER RETAIN YELLOW COPY . - please DO NOT PULL FORM SET APART N3U5CD National Loss Control Service Corporation > O 3 J 0 O O -0- ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 * 708/540-2488 Name Address Bus. Tel. No. FIELD NUMBER JUoH'L SAMPLING VOLUME ANALYZE FOR- m fib ANALYSIS REQUEST No. 173892 9 lo LABORATORY NO. RESULTS J270lg DATE SAMPLES TAKEN DATE RECEIVED BY LABORATORY DATE COMPLETED ANALYTICAL METHOD: NC 82-8 2SM 2-91 UW5I1 COMMENTS: OCC 8949 PRINTED IN U.S.A. OxyChem, r^)M latwntfr l OXT Bayport Plant PURCHASE REQUISITI No. 01559 PURCHASE ORDER NO. bay -g f 23/f DATE: VC: VENDOR: A/j&r/^ro. / /r.s'Sr - tC / r *. -*- > /' Z CA/j- ' /S'- /S-,.. s /rfr / SS / *Vi> &/f . z/ z#---/? - too zz L fr /y/r - ? '/23% r ' *v"'' :" '' y'A AFTER flfeCEfPT OF INVOICE SHIP TO ARRIVE F,0 B POINT FREIGH1 TERMS SHIP VIA f SALES TAX ITEM / J y QUANTITY /P /c tf/Y/sS/s DESCRIPTION z/ss-/', '7/t> zf'"; Y ^ /'s '//'-//sT7 Z /'/*'Z3 d.**/''?/'=? Y/f s /' 'Y'Z / r- 5 & 7 f 7 ; -1" J/ ZL If zj F-rffss /Y/2. 7.............. *2/Sr/ Z/YsS Z~Y> Y/smYs<Z Y '// Y' '' // zj Y^YsrY ZYY>YsjsY<'5 /,^'YYs /YY ej ?Y^sr*s YY*?syr?Y?sP7sZ?<r ^Y?sY 7^ 5 //*,-/ Z/A?s YZ / / Y/ssY*YY /YY, i___________ mr-*= ,, ir, , .f T TYPE OF EXPENDITURE: EXPENSE CAPITAL O INVENTORY O OTHER /~2ACCOUNT:------ ^ Z Z Z .ZZ s AR/WORK ORDER SPECIAL INST./USE ......... .......... REOUISITIONER: EXT.NO.: - APPROVAL: '/ 3 (/ " '7 LifOVC'AATTiImONu-: rW'Sf , AUTH. LEVEL: ___ PURCHASING DEPT. APPROVAL: DATE REQUIRED:__________________________________________ OVERTIME/PREM. CHARGES APPROVED YES NO DPREMIUM FREIGHT APPROVED YES NO OCC 8950 DATE tf-ry-z // 0 (YiSS M c-g-LLu,^llf 032> 'I>A1:; WlTftl- C4&5rr0:_ QOp fjlfj CLLo5c>lvA iCA - c rzLo^bLvf /tc* OCC 8951