Document 2j16V3EbgpoLqb2nVdEv1Y6VL

Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 R I RI EE OR AM A IS A Date: December 31, 1992 Customer Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 29, 1992 VISTA Product: 5305 Railcar No Order No ACFX 41162 0019422-001 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.537 0.00 9.8 1.9 0.483 0.72 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E V Bagwe Laboratory Supervisor VAB.0001202490 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: /Z -/ t Time Logged In: 2-3 zhlShip Date: I FtAX LCAR ANALYSTS Product: Logged In By:_ Order No: Car No.: W/4Z- Silo(s) Customer: Turnup Mm Jtd I Compartment A Sample From Bottom I Moisture ,/r BL I Contamination BR Bulk Density 1 BD w/antistat * S+o Viscosity RVCM .403 CA Bottom .// j 7 .^Tjr . 7-2/ ./S( CB Bottom 2L sr .CJS . 7/7 .0d( B Bottom . / .rs^ - 7ZZ. .025 Tappi Test Contamination Composite Screen Analysis .06 or less A Mesh 40 60 80 Weight % Q.o*> 0+ p .el * 2^ f.i .07-----------.15 .20----------- .60 100 /r// J> 120 j+.t 140 |/4L 200 */f Pan A1 Avg. Microns: 1+0. i % Glassies: <./ Po Color L: + +.H a .i>Z b A7& Static Flow: a /7.< Technician VAB.0001202491 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: December 29, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 22, 1992 VISIAProduct: 5225 Railcar No.: VIPX 45787 Order No.: 0016429-007 Property Test Method Specification Analvsis Moisture, % ABR-1A 0.3 Max. 0.28 Inherent Viscosity ABR-10 0.48-0.54 0.49 Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. NDS 5.0 Max. 0.0 19.2 2.7 Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, PPM ABGC-26 8.5 Max. 1.564 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 6m tU Amy E. BagweTT Laboratory Supervisor VAB.0001202492 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date:___ Product: 5225 Car No.: */s?2 ? Time Logged In: 1*7 >Q Logged In By: /n .7 Silo(s) Ship Date mHts Order No: l(e> 42$ -667 .1Customer Compartment A Sample From Moisture Bottom - BL Contamination BR /-b Bulk Density ,S~& BD w/antistat Viscosity RVCM ftoo CA b Bottom ^ .cS /Z // Mn CB Bottom 23 f ? .5Z>+ .^52-4 B Bottom !& 7 n .Sf(* * /tT^ Screen Analysis Mesh 40 Weight % o.o 60 e.S! 80 t** &.(e 100 4>.& !3.<* iZ" (3.** PSX 140 &%/ 200 % w lassies:1 __ Avg. Mici jns: (S!. Pan 9.7 a cr * Color L: ^.^7 cL t.7 Static Flow: ,7.i Technician: VAB.0001202493 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: December 17, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 15, 1992 Product: 5305 Hear No.: VIPX 45719 Order No.: 0019422-000 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.12 0.540 0.00 9.5 3.4 0.010 0.72 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202494 * Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: to- Time Logged In Ship Date:. FI A ILCAR Product: 4SWCar No.: Logged In By: Silof s): Order No: Ooft4oLJL-Doa Customer: Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM .010 CA Bottom /4 l4 ,7a a .OS'! CB Bottom 3S (q>o .nMi B Bottom G>o .7a a- Tappi Test Contamination Composite .06 or less .07-----------.15 .20----------- .60 Screen Analysis Mesh Weight x 40 VO D.z> 60 80 100 120 140 200 Pan 0-53 Hh(* /S./Lo /// 2 21 /bY //- / 7 3i. y ?o 3V Avg. Microns: / % Glassies: 9 Color L: b Static Flow: Technician: mmrnmmmmmmim rntmmm VAB.0001202495 i* k Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERT I R I C A T EE OR ANALYSTS Date: /^//sr/^2- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner VIS1A Product: 5325 Lot No. : Order No. : > ProDerty ................ 4 Moisture, % Test Method ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorptioni ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 SDecification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analysis & py______________ OSll 0-0 <7.1 ... AS rise 6-ZL- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amfx^itSU ILaboratJory Snpervisor/Lead VAB.0001202496 RES I is B A G B L E N D I O'! s i i fM $1 o V 202497 mqm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: /2-| Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: IzJBl'i'Z' VISIAProduct: 5265 Lot No. Order No. 00/76 4-5>"00/ Trailer No r- 6 / 3T Property Moisture, X Bulk Density, gm/cc Test Method ABR-1A ABR-2A SDecifloation 0.30 Max. 0.520 Min. Analysis 6. lb i O.'&f' Particle Size Distribution X On 40 Mesh X On 200 Mesh ABR-3 0.1 Max. *NDS 6.0 /s.S X On Pan 5.0 Max. /. ^ Specification is 30 .OX Max. for the 200 Mesh plus Pan. Res1dua1 VCM, ppm ABGC-26 8.5 Max. D.Q6> Inherent Viscosity ABR-10 0.63 - 0.70 0 * fofa Polyvinyl Chloride, Virgin Resin, Not Reprocessed. VAB.0001202498 4 Q 2 W PQ O < CQ w os i nwn VMM VAB.0001202499 Mlup imn mrnmmm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 & CERTIRICA E OR ANA SIS Date: lzi\b(^ Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: izjeft2, VISIA Product: 5265 Lot No Order No Trailer No 0SCX>3 00/7&4^-^ Property Test Method Specification Analysis Moisture, % ABR-1A 0.30 Max. Bulk Density, gm/cc ABR-2A 0.520 Min. Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. 13.8 A.o Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. a.)B8 Inherent Viscosity ABR-10 0.63 - 0.70 0 &>*? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead VAB.0001202500 V VAB.0001202501 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIRIGAT E OR ANALYSTS Date: December 3, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 1, 1992 Product: 5325 Lot No.: 05045 Order No.: 00017073-001 Trailer No.: T-7956 ProDerty Test Method Moisture, % ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorption ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 SDecification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analysis 0.30 0.510 0.0 7.0 2.0 142.5 25.9 0.109 0.81 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. aboratory Supervisor/Lead VAB.0001202502 h <n 1* \fS INn> Q RE S i BAG B LE N D pmmn mmmmmmmmmmmm 0001E02503 X Vista Polymen Highway 25 Aberdeen, Mississippi 39730-0091 A Division of Post Office Box 9 1 Phone (601) 369-8111 Vista Chemical Company CERTIFICATE OR ANALYSIS Date: December 3, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 1, 1992 Product: 5325 Lot No.: 05016 Order No.: 00017073-001 Trailer No.: T-7956 Property Test Method Moisture, % ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorption ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analysis 0.22 0.504 0.0 9.0 3.1 140.0 25.5 0.096 0.80 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202504 R E S IN BAG BLEND t s j r* Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen,, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSTS b Date: December 3, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 1, 1992 Product: 5325 Lot No.: 04975 Order No.: 00017073-001 Trailer No.: T-7956 Property Test Method Moisture, % ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorption ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analvsis 0.21 0.510 0.0 4.8 1 .8 148.1 27.3 0.077 0.81 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. aboratory Supervisor/Lead VAB.0001202506 mm mmmmmmmmmmm mm v mm VMM mW wmmmmm i PMHfl a Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIEICATE OR ANALYSIS Date: December 3, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: December 1, 1992 Product: 5325 Lot No.: 04912 Order No.: 00017073-001 Trailer No.: T-7956 Property Moisture, % Test Method1 ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution % On 40 Mesh ABR-3 % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorption ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analvsis 0.13 0.486 0.0 6.4 1 .2 144.3 25.9 0.737 0.81 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202508 o^1 l Ia u3 m -o 2 aa O) O O a (0 CO c > 01 & a. >\ rnrnmm mmrnmmmmmmm Hji'PMii* mm A $001202509 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601} 369-8111 CERT"XEICATE OR ANALYSTS ft Date: November 30, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: November 25, 1992 Product: 5305 Railcar No.: ACFX 41163 Order No.: 0018345-001 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analysis 0.16 0.539 0.00 6.2 1 .4 0.139 0.72 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor mmrnmmmmm VAB.0001202510 P Vista Polymers Highway 25 la+ (V+'5`SZ!> A Aberdeen, MS 39730 ANALYSIS Load Date: / /- -*? Product: Time Logged In: JD. Logged In By Ship Date: Order No: Car No.: r Silo(s): < 79-&T'? JhCustomer: iAJLWIAJLa A* *1 Compartment A CA CB B Sample From Bottom Bottom Bottom Bottom Moisture BL Contamination BR Bulk Density BD w/antistat .S2- .// 4 / JC t. .siL, . JS f / ' Viscosity . 72-z- .mi .123 RVCM .23 b Vo! _____________________^ Tappi Test Contamination Composite .06 or less '/ .07 - ---- .15 Screen Analysis .DSC .20----------- . 60 Mesh Weight % 40 >`>0 0,6 60 2 .to -ft z 80 ALit 100 /z.sy 2*:i 120 /J.lo 140 /S.1 200 S. JO Pan Avg . Microns: ft./. 1 % Glassies: </^s Color L: 9f. rz a - JO b Static Flow: 0 / f-Z. Technician * __________________ VAB.0001202511 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIRIGA*TE OR ANALYSIS A Date: November 23, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: November 20, 1992 VISTA Product: 5305 Railcar No.: UTCX 46421 Order No.: 0018345-002 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analys 0.11 0.536 0.00 10.5 2.2 0.154 0.73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy EYBagweT Laboratory Supervisor VAB.0001202512 Vista Polymers Highway 25 Aberdeen. MS 39730 A Load Date: /O' 2 Time Logged In: Ship Date : ll!xO Ft A. X LCAR ANALYSIS Product Car No.: #642-/ _ Logged In By: Silo( s): Itr.tlt Order No:_ 'Mki Customer NUrwJU\ Mesh Weight % 40 0* 0 0.0 60 80 100 120 140 200 Pan t/.yf />.-? Y "--1--r -- 1X07 7 Jo.l 31.3 hjo Avg. Microns: . I3t % Glassies: ^m J/----%f ---- Color L: ^^ o-tl b f * 5/ Static Flow: Technician: /w ft mmmmmw mm VAB.0001202513 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 C E R T I PICATE OR ANAL.YSI Date: K jl Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VIS1AProduct: 5395 Order No.: OOll43S'! Trailer No.: Property Moisture, * Test Method ABR-1A Specification 0.30 Max. Analvsis o. Hard Particles e 7 mins. Bulk Density, gm/cc ABR-12 ABR--2A 25 Max. 0.440 Min. i o.SH Bartender Dry Time, mins. ABR-7 5.5 Max. Particle Size Distribution % On 40 Mesh ABR-3 0.1 Max. o.o % On 200 Mesh *NDS !& & 515 On Pan 5.0 Max. Specification is 20 .0515 Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. 0.0 && Inherent Viscosity ABR-10 0.94 - 0.98 0 VAB.0001202514 / R E S IN BAG BLEND i i i nun mi inni mmm 1202515 VfSfa Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: l I- I Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VIS1A Product: 5305 Lot No.: Order No. : &o/ -Ooo Trailer No. T- 37 L Property Moisture, % Test Method ABR-1A SDecification 0.30 Max. Analysis , d8 Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. ___________________ /7-y 3.8 *Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. O'O&C* Inherent Viscosity ABR-10 0.71 - 0.76 &*75 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202516 \ PVC BULK TRAILER ANALYSIS Date Customer^ Technician FRONT Product Silo___ LfSL MOIST I CONT. Top Bottom Top I .eg I. Bottom GEL I 2. 2. I I. Trailer Number Time /J13 O Order No. 3 76? BULK DENSITY I .521 DRY TIME COLOR L= A= vise RVCM B= II L= MIDDLE 2. I. i i A= B= i END 2. A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0<Q9 Screen Analysis - Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. p Q.l Min. 60 A3<f 7.// 11,.oi g.7/ 3.9 /V.2. 22J 27& I7.V On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 l*4o 3.1 Glassy Pan Part. Remarks VAB.0001202517 Vista Polymers A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIRICATE OR ANALYSIS Date: Afcv * IZt Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: fiJcrv )Z, Product: 5305 Lot No.: Order No.: OO Trailer No.: VB1A a Property Test Method Specification Analvsis Moisture, % Bulk Density, gm/cc ABR-1A ABR-2A 0.30 Max. 0.510 Min. D,Q`l 0.6'/3 Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh 0.1 Max. *NDS tLSL % On Pan 5.0 Max. 3 *Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 0.71 0.76 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory rvisor/Lead VAB.0001202518 Date If* Customer Technician PVC BULK TRAILER ANALYSIS ______ Product S 3 QJf _____ Silo______ __________ />ui Trailer Number ___ Time 1330 Order No_________ / ~ 313 FRONT MIDDLE END Particle Size Distribution: Screen Analysis________ U2._____ Min Mesh Size 40 60 Gross Wt. _________ ________ Tare_________ __________ Net Wt. O~O0 0J H on Mesh 0*0 * f Screen Analysis Min. P Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 _________ ________ _________ ________ On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 J.V6 t.1 7.7* /S.? /6.1J 32.0 13.& 726 Z7. / J4. tC On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 Glassy Pan Part. J.1 Glassy Pan Part. Remarks VAB.0001202519 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIRICATE OR ANALYSIS Date: /fjlbfazs Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ///iz/*?^ Product: 5265 Lot No. : 0"504-0 Order No. : QO!C,oQir-d>/ Trailer No. : T" 84$4 ProDertv Moisture, % Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.30 Max. 0.520 Min. Analvsis O. lb D. 536 Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan 0.1 Max. *NDS 5.0 Max. n-4 2.4 Specification is 30 .OX Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. o.oro Inherent Viscosity ABR-10 0.63 - 0.70 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. VAB.0001202520 R E S IN BAG BLEND VAR0001202521 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 -k ft Cft--z K i I OAT EE OR ANAI_Y Date til it, Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: tf/t OBBaaa: a- VIS1A Product: 5265 Lot No 0504(0 Order No.: OOlboS^-OO/ Trailer No &4S4 Property Moisture, x Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.30 Max. 0.520 Min. Analvsis 0.24 D.54f> Particle Size Distribution ABR-3 x On 40 Mesh X On 200 Mesh X On Pan 0.1 Max. *NDS 5.0 Max. Lo /o-7 . o *Specification is 30.OX Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. D0(p) Inherent Viscosity ABR-10 0.63 - 0.70 o .IcL Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora VAB.0001202522 R E S IN BAG BLEND & 5,Coo 1 I I MMP mm* mmmmmmmmmmmmmm ***mmmmHmm* wmmmm VAB.00012&2523 mm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h CERTIEIGATE OE ANALYSTS Date: N&V* /lf Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Atoo. H. VISTA Product: 5305 Lot No.: Order No. : QOI>*30"O6/ T ra i 1 e r No. : TF Property Moisture, % Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.30 Max. 0.510 Min. Analysis 0.O3 4.575 Particle Size Distribution % On 40 Mesh ABR-3 0.1 Max. OO % On 200 Mesh *NDS % On Pan 5.0 Max. Specification is 30 .OX Max. for the 200 Mesh plusi Pan. Residual VCM, ppm ABGC-26 8.5 Max. o.o4( Inherent Viscosity ABR-10 0 -*j 1 o o> 0-73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor rvisor/Lead VAB.0001202524 Date. IHI-7SL Customer Technicia PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number. Time <7?30 -IOfO Order No. Particle Size Distribution: Screen AnalysisMin Mesh Size 40 Gross Wt, Tare Net Wt. % on Mesh a to 0^0 Screen Analysis 60 art e. Min. Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 1 On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 Glassy Pan Part. .16 (SST 3^-f? {430 /4Cm 11? On Rotap ishaker 49i gms. Resin plus 1.0 gms. Carb ' 80 100 120 140 200 Pan Glassy Part. . VAB.0001202525 *a Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C ER I X E OR ANA SIS Date: Moo. 10,1*1*12- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Alov- l&i VISTA Product: 5305 Lot No.: Order No.: Q6 I&4-3Q 'COO Trai ler No. : 7"--333 Property Test Method SDecification Analysis Moisture, % ABR-1A 0.30 Max. O.D(o Bulk Density, gm/cc ABR-2A 0.510 Min. Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. b. 0 % On 200 Mesh *NDS !B - U % On Pan 5.0 Max. Specification is 30 .0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 0.71 - 0.76 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. sor/Lead VAB.0001202526 PVC BULK TRAILER ANALYSIS A Date //A Customer Technician FRONT Product Silo --" MOIST Top Bottom CONT. Top Bottom SI I. GEL I 2. 2. I I. I Trailer Number Time Order Nn. 0O/f) ^30 BULK DENSITY I DRY TIME I tI L wCOLOR = Q.lk B . /?/ L vise RVCM o/ MIDDLE 2 END A= B= I. I I I L = A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt % on Mesh 0-0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 6J* fa# Itf- fm.f- 30& Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 BL Glassy Pan Part. Remarks VAB.0001202527 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 R X RIC ANALYSIS Date: Alay . Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Nero. VIS1A Product: 5325 Lot No. &50K0 Order No. oonoi 3 -mo Trailer No. T-77V/ ProDerty Test Method Moisture, % ABR-1A Bulk Density, gm/cc ABR-2A Particle Size Distribution ABR-3 % On 40 Mesh % On 200 Mesh % On Pan Average Microns Cold Plasticizer Absorption ABR-16 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 SDecification 0.30 Max. 0.480 Min. 0.1 Max. NDS 5.0 Max. 140 - 160 No Spec. 8.5 Max. 0.78 - 0.84 Analvsis o.an /).5o4 00 ef. 0 3-1 /fa.o ^5:51 0- 0^6? d'8o Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor uT rvisor/Lead VAB.0001202528 - t R E S IN BAG BLEND Pf wmmmmt * MV 02529 Vkta Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: November 11, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: November 9, 1992 Product: 5305 Railcar No.: VIPX 45841 Order No.: 0018345-000 Prooertv Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvs 0.17 0.532 0.00 10.8 2.4 0.588 0.74 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. u y E**' Bagwell Laboratory Supervisor VAB.0001202530 Vista Polymers Highway 25 Aberdeen, MS 39730 FtA X LCAR Load Date: Time Logged In: Ship Date 02 oo Product: Logged In By: Order No: 0 0 Car No . : ^ Silo(s): 1)6 & Customer: O ASO Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM 14a Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 O .O O*0 06 60 // CA Bottom CB Bottom B Bottom .S3<- 53 l 736 .Ool .07 -oi . 15 .n4d 20 . 60 80 tf. (Z, JL 100 tf.P 7 d 120 1*73 3*o 140 /A/7 200 '<// Pan A /? Avg. Microns: 1'3%'Lp % Glassies: U2i Color L: Technician: a b /^ Static Flow: /*.T '3'd> \ I N VAB.0001202531 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601J 369-8111 CERTX FIOATE OF ANALY Date: November 11, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention L. G. Haefner Ship Date: November 10, 1992 Product: 5225 Railcar No.: VIPX 45275 Order No.: 0016429-003 Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. 0.28 Inherent Viscosity ABR-10 0.48 - 0.54 0.49 Particle Size Distribution % On 40 Mesh ABR-3 01 Max. 0.0 % On 200 Mesh NDS 24.5 % On Pan 5.0 Max. 4.2 Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, PPM ABGC-26 8.5 Max. 1.098 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202532 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date:_ Time Logged In: / SToo Ship Date: Hft0 Product: Car No.:_ 4-Z 27 j Logged In By: Silo(s): UC Order No: /If 4^0 0 3" Customer : nWrvUis\ too /yjri- Compartment A Sample From Bottom Moisture .of BL Contamination BR I?-- Bulk Density BD w/antistat Viscosity RVCM .4^0 70>o CA Bottom 3 f<e \ \ .503 bc4$ CB Bottom .28 n r Bf Bottom . Js 5 .S62 .Hb /oci Screen Analysis Mesh 40 Weight % <D-> 60 Q.t % Glassies /Color 'L : 91.5Z, a 100 /! $ 120 //.9f *3,9 140 200 /SikS /2.2S 3/3 *f-s Pan 2/c> Avg. Mi b 2.94' Static Flow: / Techn lcian: A * VAB.0001202533 Vida Polymars A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: November 11, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: November 9, 1992 Product: 5305 Railcar No.: UTCX 46395 Order No.: 0018345-003 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvs 0.11 0.535 0.00 10.3 4.3 0.055 0.73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Bagw Laboratory Supervisor VAB.0001202534 Vista Polymers Highway 25 Aberdeen. MS 39730 Load Date: Time Logged In: Ship Date ,jihjsl' RAILCAR ANALYSI urof Product Logged In By: Order No: DO Car No.: /yp Silo(s) Customer: L 7/ L 4L Compartment A Sample From Bottom Moisture BL Contamination BR ,ol m Bulk Density BD w/antistat Viscosity RVCM ,121 CA Bottom .if 'vm-. V>` ` r |! 'T .fjy '121 CB Bottom t* A A B Bottom A1 1 is 37 , 75o Tappi Contamination Composite Screen Analysis Mesh Weight % 40 C? a Qc o .06 or less 60 Zi 80 .07 .15 .20 .60 100 s 3 o-7 120 140 m 2 a./ 200 Al2 /o-s Pan J.n Avg. Microns: Color L: (v .6 ( aA b % Glassies: Static Flow: <9 /?.s? Technician: V- VAB.0001202535 Vista Polymers Highway 25 Aberdeen. MS 39730 A RAILCAR ANALYSIS Load Date: Time Logged In Ship Date: Produc Logged In By Order No: Car No.: Silo(s): Customer: COMPARTMENT A CA CB Moisture % Contamination / / / Bulk Density Color "L" Color "a" Color *'b" Static Flow / / / B / / Viscosity RVCM Screen L ysis Mesh eight 40 d> 60 80 100 120 140 200 Pan srsi MM /%s' % <3.0 w .. ll.Ce eight 497 % ao js? tz- (7. S' 27U MO Weight % oe? 0.7* !-*--9ifVf-- Z.c !3.% Z0L> 19^ 133 P-7 Weight % Technician: VAB.0001202536 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OR ANALYSIS Date: A/oo . / /f Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 VISTA Product: 5265 Lot No. : 0^0 Lf-fa Attention: L. G. Haefner Ship Date: /\Jov* Order No. : Trailer No.: aaae Property Moisture, % Test Method ABR-1A Specification 0.30 Max. Analysis n- Bulk Density, gm/cc ABR-2A 0.520 Min. Particle Size Distribution % On 40 Mesh % On 200 Mesh * On Pan ABR-3 0.1 Max. *NDS 5.0 Max. 0-0 /o'? J? 6 Specification is 30.0% Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. 0 *Qb/ Inherent Viscosity ABR-10 0.63 - 0.70 OjJffa Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supe rvisor/Lead VAB.0001202537 * ) m R E S IN BAG BLEND &5.0OO v Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Cnfczr Kr"> IFI CA AIM A SIS Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 V1S1A Product: 5305 Lot No. : 0*50*1% Attention: L. G. Haefner Ship Date: JU4J4JUL mBsmemEBm Order No.: Ob Trailer No.: 060 Property Moisture, 515 Test Method ABR-1A Specification 0.30 Max. Analysis o./4 Bulk Density, gm/cc Particle Size Distribution % On 40 Mesh % On 200 Mesh ABR-2A ABR-3 0.510 Min. 0.1 Max. *NDS .. 0, 6.0 515 On Pan 5.0 Max. Specification is 30.0515 Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. a.o9>2> Inherent Viscosity ABR-10 0.71 - 0.76 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory^-eupervi sor/Lead * VAB.0001202539 o 2 w PQ O < CQ oo W oS VAB.0001202340 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A C EE re X F7 I CAT EE OR ANALYSIS Date: Not)' &. Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: hfov. 2. Wz. VTS1A Product: 5265 Lot No. : OSO*/0 Order No.: DO ff 'Oo O Trailer No.: 7- Property Moisture, % Bulk Density, gm/cc Test Method ABR-1A ABR-2A Specification 0.30 Max. 0.520 Min. Analysis O.IL 0-53P> Particle Size Distribution % On 40 Mesh % On 200 Mesh % On Pan ABR-3 0.1 Max. *NDS 5.0 Max. oo //V Si.4 Specification is 30.OX Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max Q.O^O Inherent Viscosity ABR-10 0.63 - 0.70 o.6>7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory rvisor/Lead VAB.0001202541 R E S IN BAG BLEND VAB.0001202542 I Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A 9 IO Customer: Premier Polymers 3001 Watterson T rail P. O. Box 99571 vJef f ersontown , KY 40299 Attention: L. 6. Haefner Ship Date: i n > VSIAProduct: 5305 Lot No Order No Trailer No &0/75&7-O t>2~. Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A W3R-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis * I ^____ -.s-q i 200 mesh & *4 K5 7E- Pan 3- I Polyvinyl Chloride, Virgin Resin, Not Reprocessed. VVlgjP../ Laboratory Supervisor/Lead VAB.0001202543 PVC BULK TRAILER ANALYSIS Date. Customer *4 /C/ Product Silo___ SJoS Technician / FRONT MOIST Top Bottom I J.V. 2. CONT. Top Bottom I1 IS GEL 1 2. i I l. Trailer Number rime___09 Order BULK DENSITY I. DRY TIME COLOR . 5<SJ A = 0.2 B= I I. L = MIDDLE 2. A= B= i i i i L= END A= B A vise RVCM 0 Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare n P Net Wt. on Mesh Screen Analysis 40 0.0 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Remarks____ siMin On Rotap baker. 491gms. Resin (lus 1.0 gm s. Carb 60 80 100 120 140 200 Glassy Pan Part. t-7 Min. 60 7-t-7 /r-W IH-IO /#0 2-- /. /<? /V- 7 3o. o On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 100 120 140 200 (.oL 1 Glassy Pan Part. mmmmmmmrn w mmmm. p * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: October 23, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: October 22, 1992 VIS1A Product: 5305 Railcar No.: ACFX 41162 Order No.: 0017572-000 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.15 0.533 0.00 9.4 2.4 0.029 0.73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202545 Vista Polymers Highway 25 Load Date: ? Time Logged In: Ship Date: RAILCAR Product: Logged In By: Order No: Aberdeen, MS 39730 A Car No.: 4UL Silo(s) n ? Customer: O^ASLA Compartment Sample From Moisture Contamination A Bottom d CA Bottom /jr CB Bottom J3 B Bottom ,// Bulk Density BD w/antistat Viscosity RVCM ns4 mi Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 DiOO 0.0 60 Q.Q 7 o.( .i*n . n$(* .IIS' ,S3 7 .J5Z .D/U, 80 4,7/ Vi 100 //.o3 22.\ 120 IkAL 33.2, 140 11.70 33.4 200 iUr M- Pan 1.2 2 3.4 Avg. Microns: 12a. 2^ % Glassies , Color L: P9-47 a 0 2 b J* 6> / Static Flow: 0/ Technician VAB.0001202546 1 Vista Polymers Highway 25 Aberdeen. MS 39730 ILCAR ANALYSIS okkgrale: por NW\ A Load Date: Time Logged In Ship Date: Product: Logged In By: Order No: Car No Silo(s): Customer: COMPARTMENT Moisture % A CA Contamination / / Bulk Density Color "L" Color "a" Color "b" Static Flow Viscosity IQJB. / Bottom IflJP / RVCM # Screen Analysis Mesh Weight % 40 60 80 100 03 3-7 C. l 7A CB * / B j* / // Top Bottom Top Bsiiaa 120 140 /fcJ7 /3-^( JX2 ZM-- 200 If S Pan / n Z.3 Weight %p 0j? o <Z 9-1 /// 9-3 //Sf (/.OP /*Y $*A Weight % >0 &0 m .. .o tf-n IX [e>-i0 / Weight %P >D ,O0 & ./a 13 nician: /rt- f /J-7J- S3>- I6.L 47 9-SS^ J-ff-T o -n-T- 3.2__ VAB.0001202547 w Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF Date: 2/ 0<>f. Customer: Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 2 f 0c^&. VISIA Product: 5305 Lot No Order No Trailer No OO 17 43 " 00 7'-3~U Property Moisture, 7. Bulk Density, gm/cc H Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh __ <Ll ABGC-26 ABR--10 Analysis .to . srz(. 200 mesh /2. 0 Pan /7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ratory rv VAB.0001202548 PVC BULK TRAILER ANALYSIS Pate /Q~2Product S~__________ Trailer Number Customer r f&tole _______ Silo l Time /f3 0 Technician/^4___________________ _______________________ Order No. 7"~ A Particle Size Distribution: Screen Analysis______Z.Q.Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. % on Mesh o S, st /o> f f. i 7 /9.3 if. 9 /2.7f . tfOZ* /z.o .V /. 7 Screen Analysis -----------------------Min. On Rotap shaker 49 gms. Resin plus t .0 gms. Carb Mesh Size Gross Wt. Pan 40 60 80 100 120 140 200 _________ _________ _________ _________ _________ _________ Glassy Part. Tare Net Wt. __________ __________ __________ 1 _________ _________ ________ "" _________ ' ------ - _________ ' ................... _________ ........ _________ - _ % on Mesh _________ _________ Remarks VAB.0001202549 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601} 369-8111 I IA C&fobc*- 22, \FtZ. r: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Q&fcblLY' \C\, ANALYSIS VIS1A Produc t: Lot Na.iQ5o3& Ord No. : 0O{l438 -00b Trailer No . : 7' Z&O&Cs Propertv Moisture, 7, Hard Particles @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min. Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-12 ABR-2A ABR-7 ABR-3 40 mesh 0-0 ABGC-26 ABR-10 Analvsis o.n / ~.D 200 mesh OOZ! Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. y Sup meMMSPMNMMMI VAB.0001202550 1, AHH* IN R E S IN BAG BLEND I I mm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-61 1 1 CERTIFICATE OF ANALYSIS Date: October 14, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: October 12, 1992 Product: 5305 Railcar No.: VIPX 45782 Order No.: 0017192-000 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvs 0.11 0.537 0.00 7.6 3.4 0.061 0.73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. aj Laboratory Supervisor wmmmmmmmmmmmmmmm VAB.0001202552 mmm Vista Polymers Highway 25 Aberdeen, MS 39730 A RAX LCAR ANALYS X S Load Date: P730Time Logged In: Product: Logged In By: Ship Date: tO J Order No: i in 1111 nmmaen Car No.: Silo(s) Customer: Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density o 7 I'D qo BD w/antistat CA Bottom o2 \J_ / C* S3'7 CB Bottom / B Bottom \<o i? RVCM .00> I M Tappi Test Contamination Composite Screen Analysis Mesh Weight %P 40 o.o 0.0 06 or less .07 .15 .20 . 60 60 _, // 3 80 s-bi -LL 3 _ 100 /ZJ3 aW 120 U-Jd 3a-? 140 /O.o PD-I 200 Pan 7-t --3==-----yf-- Avg. Microns: ... // 2^ % Glasslies: Color L: ? F a osy b a. n Static Flow: & / 7- Technician MRMf pi VAB.0001202553 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I F I CATE OF Aberdeen, Mississippi 39730-009) Phone (601)369-81)1 Date; />///32- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention; L. G. Haefner Ship Date; Product; 5265 Lot No. ; 0<o02-1 Order No. : 00 J Trailer No.: 7^-2 ProDertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh D0 ABGC-26 ABR-10 Analvsis D-l% <9.SV7 200 mesh 15.7 0 o4S 0 - (j> (0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Of Pan 3,0 rvisor/Lead mmmmmmm VAB.0001202554 mm cn Sr cor> P9 R E S IN BAG BLEND d cH i i c* Is rt # o00* vno\ rr--o # 5: r* rt o vo e>i I mrnmmmmmm MNP vmiNMPip Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h xI Date: (Qjf Customer: Premier Polymers 3001 Watterson T rai 1 P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: `flz'i Hz* ^ [\J N'S I S VISIA Product: Lot No.: Order No. : )OlCO0S^Or)O Trailer No /- 2/33 Procertv Moisture, V. Hard Particles> @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min. Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-12 ABR-2A ABR-7 ABR--3 40 mesh o.o ABGC-26 ABR-10 Ana1vsis O.ett 3 0.S1C 200 mesh >.OZO *.11 Pan 3-3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed visor/Lead VAB.0001202556 mmmm /V * Vjsta Polymers A Division of Vista Chemical Company I Highway 25 Post Office Box 91 X C2& Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA V <=; T c; /# SlMjl. Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date f/a/ VIS1AProduct: 5305 Lot No.: 0^Q2Jf Order No.: DOlb30&~6O Trailer No J Propertv Moisture, 7. Bulk Dens ity, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR- 1A ABR- 2A ABR- 3 40 mesh 0-0 ABGC -26 ABR- io Analvsis 0-t 0-534 200 mesh 0 Oooi 0 72- Pan / Po1yviny1 Chloride, Virgin Resin, Not Reprocessed Labo ry Suriervisor/Lead ii ii mmm MUR mmm w p> VAB.0001202558 R E S IN BAG BLEND I III n Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANALYSIS Date: September 22, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 17, 1992 Product: 5305 Lot No.: 0<4On Order No.: 0016082-000 Trailer No.: T-8396 Property Moisture, % Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh n.o ABGC-26 ABR-10 Analysis 0. ID 200 mesh (o. / Q. c37 5 Pan / Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labo il/ ory ^upervisor/Lead VAB.0001202560 ~o a u3 o Q CD O a <0 0) c > a A 02561 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 OIERT IFI Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 AM A l_ VS X S Date: September 22, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 s Attention: L. G. Haefner Ship Date: September 17, 1992 Product: 5305 Lot No. : Dtfi&OS Order No.: 0016082-000 Trailer No.: T-8396 Property Moisture, % Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 ABR-10 Analysis o.s~4o 200 mesh !(.> 6-070 0.72- Pan /A Polyvinyl Chloride, Virgin Resin, Not Reprocessed. d?_____ Laboratory S uperv isor/Lead VAB.0001202562 c a. % mmum mm i 14 ..... .... .... -- --..... i . 02563 m Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIEXCATE OR Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANALYSIS & Date: September 22, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 17, 1992 VISIAProduct: 5305 Lot No. : Q'oOZT- Order No.: 0016082-000 Trailer No.: T-8396 ProDerty Moisture, % Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh r>.o ABGC-26 ABR-10 Analysis D.&o 200 mesh /4.Z. O.Oo3 o.nz- Pan 3.& Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202564 R E S IN BAG BLEND mum w Vista Polymers A Division of Visto Chemical Company C EE R Highwoy 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 ANALYST S Date: September 22, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 17, 1992 VISTAProduct: 5305 Lot No. : 050/& Order No.: 0016082-000 Trailer No.: T-8396 Property Moisture, % Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh D.Q ABGC-26 ABR-10 Analysis 0> 0.5o 200 mesh n-3 0.00/ D.nz Pan /.a Polyvinyl Chloride, Virgin Resin, Not Reprocessed. atf Laboratory Supervisor/Lead VAB.0001202566 R E S IN BAG BLEND I^ W mm 02567 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI E I C OR Aberdeen Mississippi 39730-0091 Phone (601) 369-8111 ANALYSTS Date September 22, 1992 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 17, 1992 VISIAProduct: 5305 Lot No.: Order No.: 0016082-000 Trailer No.: T-8396 Property Moisture, % Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh D.6 ABGC-26 ABR-10 Analysis o. M 200 mesh t4.4 a o .7z. Pan <3.6' Polyvinyl Chloride, Virgin Resin, Not Reprocessed. iOJ rvisor/Lead VAB.0001202568 t) I ft I 1 kfi s- r4 vs 1\ iO R E S IN BAG BLEND o o o o! I \ *: lOTPHti mmm mtmrnmmm ^7 s N ^0 * xpl N \J &o I sjC 1 *v* ! ^ va% , * % *O * % Ik 8 4 to 1 o 3- fO o *4 -* N 02569 rnmmm iff f *' Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS I Date: l/nhz. n Customter: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: tfjtSfa'Z' VIS1AProduct: 5265 Order No.: OOi^Sl I O'OO 0 Trailer No.: T^'O>$'70> Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-IO Ana1vsis o.tL o 200 mesh A7-2- Q.0i 0. (j>{* Pan g. Z Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora rvisor/Lead VAB.0001202570 Q III *z. w CQ III CO w c< \ mmjmmrm mmm Ift* * m'll T 12G2571 * m Hamm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 C El F9 T X F=~ I CATE OF ANALYSIS A Date: * Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. 6. Haefner Ship Date: <^/J Product: 5305 Lot No.: Order No.: > O/S Trailer No.: *7Z. yS / -- Oo/ Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Ana 1ysis ./( S3.S' 200 mesh ./<// .73 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead # VAB.0001202572 Date tA -IX Customer $ /e/ Technician PVC BULK TRAILER ANALYSIS vh Silo Li 7 Trailer Number Time // /6 3i( A Order No. oc>i<rn3^~co( Particle Size Distribution: Screen Analysis(_^Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh O,,O *>, o Screen Analysis 80 100 120 140 200 ___ Min. On Rotap shaker 7,fA A3e> /-CC 4.L 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Gross Wt. _________ _____ Tare _________ ______ Net Wt. _________ ______ % on Mesh _________ ______ Glassy Pan Part. .79 2.c> Glassy Pan Part. Remarks i Star 207A Revised 1/12/87 VAB.0001202573 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369*8111 CERTIFICATE OF ANALYS X S A Date: f/iofal. Customer: Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: fa-v Product: 5305 Lot No.: fJf Order No.: QO!*5H 3 Trailer No.: 7-38/ OOA Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 6* 0 ABGC-26 ABR--10 Ana 1vsis O -02- D. 5 200 mesh */ 0s 2Z/ ^.72- Pan JU Polyvinyl Chloride, Virgin Resin, Not Reprocessed. VAB.0001202574 mm Date Customer Technician l-Ss s PVC BULK TRAILER ANALYSIS Product Silo___ &Rg_ Trailer Number Time //* f O Order No. ^0/^757-64 6 A Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare Net Wt 46 on Mesh Screen Analysis 40 S>*Q <> O Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. '?<> 9.32 /.r 3>. ( I I.oJ </ P. I Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks _____________________________________________ Star 207A Revised 1/12/87 . r* ,^L .......... *<-. V 'M V x- ' " " VAB.0001202575 ------------------ -------------------------------- ----------------------------" ~ - -- ------ -- Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 A X i c=:<Qi ./ t- Date :4 9l(6h> Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship *Date ikl*Z* Product: VISIA Lot No. : Order No. : QQ ft5r70^i-00& Trailer No.: *7"- Property Moisture, 7. Test Method ABR- 1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR- 2B Barbender Dry Time, min. ABR- 07 Particle Size Dist. ABR-3 40 mesh O.D Residual VCM, ppm ABGC:-26 Inherent Viscosity ABR- 10 Analysis .0-9-4 .3. . o.S44o 4.1 200 mesh t^.o 0-0t0 0.17 Pan 3.3 upervisor/Lead VAB.0001202576 *V 1202577 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I F7 I CATE O Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA vs i s A Date : Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ^fa}*? VIS1AProduct: 5305 Lot No. : QSOil Order No Trailer No 7^433 3 Property Moisture, 7. Bulk Dens i ty , gm/cc Partic 1e Size Dist. Residual VCM, ppm Inheren t Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh o.o ABGC-26 ABR-10 Analvsis 0.3.3__ 0-SZD 200 mesh /3.o Doaj o. 73 Pan Po1yviny1 Chloride, Virgin Resin, Not Reprocessed &- al Laboratory Supervisor/Lead VAB.0001202578 R E S IN BAG BLEND rt v" I5 % V vOQ 1 Oq V1 tSI v3lL^> MI * *3 cOl * ou *1 "1 M I S 1 oMra I1 MCO I1; " mm/m 1202579 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF J Aberdeen, Mississippi 39730 Phone (601) 369-6111 ^N^I_V'SIS A Date: Customer: - Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 9// Hz- Product: 5265 Lot No. : Order No. : Trailer No.: 3-37> Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh Q.O ABGC-26 ABR-10 Analvsis DIO O. 553 200 mesh g,7 Q.QA8 0 hb Pan J?.o Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora ervisor/Lead VAB.0001202580 I f I R ESIN BAG BLEND cro wmmm <mmimmmim HP 01202581 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS A Date: September 4, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 3, 1992 Product: 5305 Railcar No.: PLCX 42644 Order No.: 0015653-000 Property Moisture, % Bulk Density Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 ABGC-26 ABR-10 Analvsis 0.06 0.528 0.00 8.0 2.9 0.062 0.74 Polyvinyl Chloride, Virgin Resin, Not Reprocessed m Amy E. "Bagwell Laboratory Supervisor VAB.0001202582 Vista Polymers Highway 25 Lfls-f dtfK&r. Aberdeen, MS 39730 Load Date Time Logged In: Ship Date:_ W?2- Product: Logged In By Order No: Car No.: Silo(s) Customer: <V\ TA / Compartment A Sample From Bottom Moisture .(=> BL Contamination BR Y Bulk Density .S3 1 BD w/antistat Viscosity RVCM .0^ CA Bottom ,*T jr r' Ok 2- CB Bottom ,o^ JL C si? .736 -04^ B Bottom j s~~ .72-1 . Q(r>(^ Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight 4.0 % <P .06 or less K 60 _&./? ,3 80 7-y^ .07----------.15 .20---------- .60 \ 100 2^7 120 r$`Q<f 3 140 y.y? 1X-z> 200 8-o Pan y.*c. 2-7 Avg. M icrons: % Glassies: / Color L: tf4?- a b M 2- Static Flow: O / 7*7 Technician: VAB.0001202583 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OR ANALYSTS a 'i# Date: 4- Customer: September 10, 1992 Premier Polymers 3001 Watterson P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: September 4, 1992 Product: 5415 Railcar No: ACFX 41179 Order No.: 0014572-001 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analys 0.12 0.498 4.9 0.00 5.1 1.9 0.094 1.02 Laboratory Supervisor (601) 369-3624 VAB.0001202584 Vista Polymers Highway 25 Aberdeen, MS 39730 railcar ANALYSIS A Screen Analysis Mesh Weight %f 40 t> 60 /.93 3-1 200 <371 J> 0 (s> Drytime: Flow: Avg. Microns: t Color L: JjPoJy a 0-Q?^ /.S& METS: Technician: _JU,T 9'#!+' Pan VAB.0001202585 T ittfWP Vista Polymers Highway 25 A Aberdeen, MS 39730 RVC RAILCAR ANALYSIS Load Date: Time Logged In: /030 Product Logged In By: Ship Date: Order Ho: Car No. : "4! 17*? Silo(e) : 6>9oJp?/ Customer: Compartment A Sample From Bottom Top Moisture % BL Contamination BR ~g>7 /a S~L g J Bulk Density 5 Hard Particle 7 s / Viscosity RVCM t .ool CA Bottom Top JL lh H3 M9? *7 2f Screen Analysis Mesh 40 60 80 100 120 140 200 Weight % pI &.0 e& . l*Sb . 3'\ /4.22- n So. ii J. 73 /S-3 7-S' S-1 Drytime: Ml- Static Flow: & /S.S Avg . Microns: Pan X bf Color L: je>Q.fO a b JLH METS: ^*7% 9 / l3./o% Technician: M VAB.0001202586 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 9l CEERT X I Ci^TEE QF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 M *=* L_ Y S I S A Dates B/ Customer; Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 3/z<th Z" Product: 5305 Lot No.: <D5>/7 Order No.: OO 1*0 Z3>*7" 0C> C> Trailer No.: / -- Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 0 O ABGC-26 ABR-10 Analysis .53 200 mesh ft.Q .OCl .75 Pan 2.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead VAB.0001202587 m/mmm M * R E S IN BAG BLEND Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 V'S I S A Date: g\ZOf^ Customer: Premier Polymers 3001 Watterson Trail P. O. Box Jeffersontown, KY 40299 Attention: l_,, G. Haefner Ship Date: VISIAProduct: 5325 Lot No Order No Trailer No (H^o 0O/I5O >- oa 0 - 1^) 7 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR--iA ABR-2A ABR--3 40 mesh _&dQ. ABGC-26 ABR--10 ABR-16 Ana lysis .il I52<r 200 mesh 4-4 ISIS 05B .9)0 49> Pan t-2 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. mm mmmmmmmmmmmmmmmmrnm VAB.0001202589 H4p A V) j % R E S 1* HAG B LE N D o (N 0 |^ fS OO 8 % o * o % mm mmmm* a^jROnJl 7.07.590 T Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS A Date: Custoraer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G- Ship Date: Produc t Lot No Order No Trailer No Ooi 13o i - oo o T- 73/7 Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR--3 40 mesh <9.0 Ana 1vsis .17 .576 200 mesh L.2 ABGC-26 ABR-IO ABR--16 .070 $o Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead VAB.0001202591 R E S IN BAG BLEND i Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. 6. Haefner Ship Date: Product: 5465 Lot No. : 0500 / Order No. : Q& Trailer No.: T"-- 00C Property Test Method Moisture} % ABR-1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min ABR-07 Particle Size Dist. ABR-3 40 mesh Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 Analysis SA I 5" o 200 mesh OO! A// Pan jn. Labor VAB.0001202593  I I R E S IN BAG BLEND MR M Ri mm 02594 H Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSTS A Date: August 20, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: August 14, 1992 Product: 5415 Railcar No: VIPX 45820 Order No.: 0014572-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM \ Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.24 0.511 4.9 0.00 5.3 1.8 0.006 1 .03 at Laboratory Supervisor (601) 369-3624 VAB.0001202595 Vieta Polymers Highway 25 A Aberdeen, MS 3973q RVC RAILCAR ANALYSIS Load Date: _ V * / ? Time Logged In: Ship Date: 44 ^ Product: Logged In By: Order No: ) Car No.: jrXJko /VI Silo(s) ^ Customer: Compartment A Sample From Bottom Top Moisture % BL Contamination BR Bulk Density J9 -a 9 3 11 5 Hard Particle 7 Viscosity <3 Co RVCM ,DOQ> CA Bottom Top .2/ fS /3 CB Bottom Top .zz. J2 a so 9 B Bottom Top 3 7 S*9 to Screen Analysis Mesh 40 Weight Q<0 O % o.e> 60 Drytime : d 80 100 120 140 200 Pan !S.L*- !U? 10,0D 2. (S' J/.3 32.1 .0.3 /J e.</Static Flow: o_l Avg. Microns* IW.Z Color L: a 0*0 3 b /.3Z. METS: faoo ,IX?.< % Technician: v 3*3- VAB.0001202596 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A CERTIFICATE CD F=~ ANALYSIS Date: Qjf/MzL Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: )jfOfo2- VIS1A Product: *i53ciS' Lot No Order No. : Q> l Trailer No-: C> - O O ) Property Test Method Moisture, 7. ABR-1A Hard Particles. @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR--3 40 mesh o.o Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 Analvsis o./o 2. OSoS 200 mesh /S>.0 0. /S o.n Pan 6J Laborat rvisor/Lead VAB.0001202597 R E S IN BAG BLEND Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: Qjfof^'Z' Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. 6. Haefner Ship VISIAProduct: 5305 Lot No.: Order No . : Q Trailer No. : fcofatf- O Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 0-0 ABGC-26 ABR--10 Analysis n .53& 200 mesh __ & .oil .75 Pan 7-fe Polyvinyl Chloride, Virgin Resin, Not Reprocessed. abora aj sor/Lead VAB.0001202599 R E S IN BAG BLEND Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ^f\J^L_V'S I S A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KV 40299 Attention: L. G. Haefner Ship Date: /^`Z^ VISTAProduct: 5305 Lot No. : CfoOQQ> Order No. : >01*4 Trailer No. : O Propertv Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Test Method ABR-1A ABR-2A ABR-3 40 mesh Ana 1vsis ____ 200 mesh Pan Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 . 315 ,7a Polyvinyl Chloride, Virgin Resin, Not Reprocessed. wmmmmm mimm mmm pwmmmmm VAB.0001202601 rr 0) Ua vS> R E S IN BAG BLEND i III w-* I U o I oo 0 01 i mm mmmmm mum Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTI R I CAT EE O R ANALYSIS A Date: August 5, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: August 4, 1992 Product: 5415 Railcar No: ACFX 41164 Order No.: 0013479-001 Property Moisture, % Bulk Density n Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.12 0.508 4.9 0.00 4.5 1.5 0.005 1 .04 Laboratory Supervisor (601) 369-3624 VAB.0001202603 Vista Polymers Highway 25 A Aberdeen, MS 39730 E>VC RAILCAR ANALYSIS Load :Bate 7 -J/- Time Logged In: / f6 6 : Sfah Ship Bate Product: 5415 Car No . 4/1C Logged In By: Sllo(e) : Order No oof Customer C ?/ Compartment A Sample From Bottom Top Moisture % BL Contamination BR Bulk Bensity .// 3 21 5 Hard Particle 7 Viscosity -f l RVCM CA Bottom Top ./Z. t4 J 4 .fo9 CB Bottom Top SO 2- 9* JS / &Z B Bottom Top .of it . S'/a Screen Analysis Mesh 40 Weight % 0.0 60 /.4J 3.3 80 Zo.33 VO.L 100 J4-, U 21.* 120 7,*r' _ZdA7 140 S-.L 200 -2,23 Drytime: 1 Static Flow: 3 / 3.0 Avg. Microns: Color L: METS: a .o3 b /, r/ /UL.I % Pan , 74^" AS Technician: VAB.0001202604 Vista Polymers A Diviwon of Vista Chemical Company CCEIRT I F7 X Highway 25 Post Office Box 91 OF7 Aberdeen, Mississippi 39730 Phone (601) 369-8111 ISJ *=* l_ Y S I S Date: Customer: Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: " VIS1A Lot No.: 05OO^> Order No . : f-dOO Trailer No.: hO Z-* Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 00 ABGC-26 ABR-iO Ana 1vsis n .6&4 200 mesh i 0/3, .(*4 Pan JU Polyvinyl Chloride, Virgin Resin, Not Reprocessed. sor/Lead VAB.0001202605 nl t o Q R ESIN BAG BLEND tr I! bo i I3 I w- V) 0 Oi v/1 O v 1o 1^ rmmmm mm 1202606 V. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 & Customer: Premier Polymers 3001 Wattersan Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Shi p Product: 0375 Lot No 0*4^1 ^ Order No.: OOiS^H I-Q0 t> Trailer No . : ~T " $ Propertv Moisture, V. Hard Particles @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-12 ABR-2A ABR-7 ABR--3 40 mesh 0*0 ABGC-26 ABR-10 Analvsis * 4 .5T7 4.b 200 mesh #3 Q<51C? Pan 2.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ory rvisor VAB.0001202607 * I Q 2 W J CQ O < CQ CO U od (T CO 1 tT~ O VAB.OOOl 02608 * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 TX X Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 vs x s A 7/ hz- Customer Premier Polymers 3001 Natterson T rai 1 P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L- G. Haefner Ship Date: j'-} ft'l. VBIA Product: 5325 Lot No. o4Mo Order No.: T rai1er No.: 7^ 5^^ 7 f Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 ABR-16 Analysis .i4 200 mesh 4.4 /5?> ,05& QO at Pan !.& Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory )<ui rvisor/Lead VAB.0001202609 RES1.. jiAG BLEND sjd^l/ZD o I % ~l CM to Jr$S * V$ c*i <9kO |' o 1 o\ co f V mm fMUPPMPHVM 001202610 Vista Polymer* ADjvinonof Vista Charmed Company Highway 25 Rost Office Box 91 CERTIFICATE OF I Aberdeen, Mississippi 39730 Phone (601) 369-8111 ^Ni^L_YSIS L A Date: 7 /zo/?> Customer: Premier Polymers 3001 Matterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G- Haefner Ship Date: *7}li#jT-* Product: 5265 Lot No. : 0^^^f Order No.: OO J<&/?'0 O d Trailer No.: ~T^-Q/l3 Property Moisture, X Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis , in 200 mesh <?Q.O .035 , bb Pan iiO Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora tU,_____ sor/Lead VAB.0001202611 RES 1 . 6 AG B LE N D < V * ` Ml WI VAB.0001202612 4 PHW Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X IT I CATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A Date: July 17, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. 6. Haefner Ship Date: July 14, 1992 Railcar No: VIPX 45875 Order No.: 0013479-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR- 1A ABR- 2A ABR- 7 ABR- 3 ABGC -26 ABR- 10 Analysis 0.24 0.506 4.8 0.00 5.2 1.9 0.012 1.02 Laboratory Supervisor (601) 369-3624 VAB.0001202613 Vista Polymers Highway 25 A Aberdeen. MS 39730 RAILCAR ANALYSIS Load Date : J2-- Product Time Logged In ffjo Logged In By: Ship Date :lllb7* Order No: Car No.:. OL21 SilO(6) ustomer: 7-r- Compartment A Sample From Bottom Top Moisture % BL Contarnination BR Bulk Density /7 S7 /o /> 5 Hard Particle 7 I -ys Viscosity RVCM to!*! Dt CA Bottom Top CB Bottom Top /4- LS. .<*209*- J3 / 12 10 /O B Bottom Top 7_ l$ Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight P.lt LC*Q A. % jfcfc 7,0 Drytime: 4& Static Flow: 0 L Color L: a a. so b Avg. Microns ms *j METS: tfn&y L IZi-t /o/ Technician: VAB.0001202614 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERT I X OF ANALYS I S A Date: Customer: Premier Polymers 3001 Ulatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 7/8/^Z- Product: 5325 Lot No. : Order No. : OOI~OCO Trailer No . : *7^- 5&7^\ Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR--3 40 mesh oo Analysis .86 -6lL 200 mesh ABGC-26 ABR-10 ABR-16 3o Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. mmrnmm mmmm mmmmmmmmmmmmrn VAB.0001202615 R E S I. BAG BLEND VAB.0001202616 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CER I I Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA Is A 7: !<oh Customer: Premier Polymers 3001 Watterson T rai 1 P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 7 Product: 5325 Lot No. : Order No - : C>C>t2L T railer No . : VIS1A "00 ( Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0. 6 Analysis - IS 5/(s> 200 mesh 5~- 6 ABGC--26 ABR-10 ABR-16 .075 .60 Pan <3-5. + Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor visor/Lead VAB.0001202617 IRES . BAG B LE N D 001202618 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X F7* I OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 IS Date; Customer: Premier Polymers 3001 Ulatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention; L. G. Haefner Ship VIS1AProduct; 5305 Lot No.: Order No. : Qq /32 >3 ~OOf Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0o ABGC-26 ABR-10 Ana 1vsis IQ 511 200 mesh 4-6 .75 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora isor/Lead 4 VAB.0001202619 * PVC BULK TRAILER ANALYSIS Date Customer Technician FRONT MIDDLE Product Silo___ Cfi2+6g4- Trailer Number Time loss' Order No. 0O15LZ3-AQ/ MOIST I2 BtMiom \uo CONT. Top Bottom GEL i 2. 2. BULK DENSITY i .57/ I I II DRY TIME COLOR L^.3 A B -l$S L= vise RVCM %z 0 A= i. i i B= L= END A= B= Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 6. OO 0.0 t Screen Analysis V Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus i.o gims. Carta 60 80 100 120 140 200 Glassy Pan Part. 6 5* //.So tSK" (0.00 /S.} w 3L& Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carta 60 80 100 120 140 200 _L?3 as Glassy Pan Part. Remarks mw V-AB.0001202620 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601J 359-8111 X I CA ANA V S X s A * *?hh Date 2- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: jf P VBIA Product: 5305 Lot No.: Order No*: DOlZGQ&'OdO T rai1er No.: 7^7Z75~ Property Moisture, */. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh o. O ABGC-26 ABR-10 Analysis .54 > 200 mesh /^3 ^' o44 m- Pan 3. Z- Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor rvisor/Lead VAB.0001202621 mmm VMMPMKM r* oN >'/'s o\ O Ov \ Q W VS o< CQ lB CO U \ o <3j C5--I vri Oi V i s ) vS Of *0 'VO \d 'i r\ T ^0 *5 V <& i"Y X3 O* So> 28S I 2 tCS V\r V]Rihv"[ `VVl^N Qya 1 o\ r^ *? I o^l p- <xJ O s* II VO< VAB.0001202622 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C El FR "T I P X C A T El O P A N AI__ V' S I S A h7/7 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date = limbi' VISIA Product: 5325 Lot No. : Order No . : O 0 i I 2- 5" OC 8 Trai1er No T'Z&Ol Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR--3 40 mesh 0 O ABGC-26 ABR-10 ABR-16 Analysis 'Ll . 5lO 200 mesh 4.> !<& .077 SI.3 Pan Aft Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202623 oos'/g AB. 001202624 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE O Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYS X S & Date: 7/7/W Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Lot No. : 044^1 Order No. : OOI 1573 ~ 2>CO * Trailer No. : T7 2&Ol3^ Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 ABR-16 Ana 1ysis * 200 mesh 3.0 /58 .0/2. 77 4.4 Pan /S Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead VAB.0001202625 R E S IN BAG LEND PRMVMi m mmtf mm WH-- VV Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 h CERTIFICATE OF ANALYS X S Date: 7 - *2-- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KV 40299 Attention: L. G. Haefner Ship Date: ~7 "" ^ VEIA Product: 5305 Lot No. Order No Trailer No >&/* Z &J- 3g2. O Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh O. O ABGC-26 ABR-10 Anal vsis 200 mesh 7-*7 .0ShL 75 Pan Jt. ? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead Net Wt. % on Mesh _________ _________ Remarks / VAB.0001202627 PVC BULK TRAILER ANALYSIS h Date 2 Customer B 9 .2 Technician /H r ft* Product Silo___ A MOIST CONT. I2 i. Bottom | Top i Bottom GEL l FRONT 2. 2. I. I I Trailer Number Time / y^-O S2 Order No. BULK DENSITY I *5// DRY TIME l II COLOR L A = > B = Mif L= vise RVCM S'J MIDDLE I END 4*44 i A B= i L= A= B- Particle Size Distribution: Screen AnalysisMin Mesh Size 40 Gross Wt. Tare P f Net Wt. 4k on Mesh 0.0 (DO Screen Analysis 60 i Min. Mesh Size Gross Wt. Tare Net Wt. 4k on Mesh 40 60 4 On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 Pan Glassy Part. i3-n is. 7' %6>/Z> 3.9S /./? MS 7-1 P.c/ On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb y Pan 80 100 A2Q 140 200 Glassy Part. 7 y Remarks VAB.0001202628 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h IS Date: Custonier: Premier Polymers 3001 UJatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ^(l {4`Z*' vm Product: 5305 Lot No.: Order No. \ QO~00& Trailer No. : 7^\5"77 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM , ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0-0 ABGC-26 ABR-10 Analvsis .5'Z4 200 mesh 0.0 Ml ,73 Pan 3.j Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Supervisor/Lead Remarks VAB.0001202629 PVC BULK TRAILER ANALYSIS r>a<p 7- / - 7 Customer pfe*>l&r Technician Af^ Product Silo___ iff MOIST CON T. Bottom f Tup Bottom GEL I i l. Trailer Number Time Order No. -777 BULK DENSITY I DRY TIME I COLOR L =-91.47 vise RVCM FRONT i 2. a = .S3 b = *2 fU I II L= MIDDLE 2. ENDPH M | 1. F1 i II m A= B= LA= B= Particle Size Distribution Screen Analysis It Mesh Size 40 Gross Wt Tare ? Net Wt. H on Mesh 0* A w l. Screen Analysis I 4' Mesh Size Wt Tare Net Wt % on Mesh 40 Remarks Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. !L> 7.4 c 13.10 J r. 4J 3 /4. 7 S/.0 ZZ ..L XX 7.0 s, / Min 60 shaker 49 gms. Resin plus 1.0 gms. Carb Pan 80 100 120 140 200 Glassy Part. VAB.0001202630 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSTS A Date: June 29, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 26, 1992 Product: 5225 Railcar No.: PLCX 43753 Order No.: 0011491-002 ProDertv Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.14 0.50 0.00 4.9 1.9 0.351 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe Laboratory Supervisor VAB.0001202631 Vista Polymers Highway 25 Aberdeen, MS 39730 jirc. RAX L.CAR Load Date: Product: Car No.: Time Logged In:__ ey/sT Logged In By: Silo(s) : Ship Date:. Order No : OOll'tfi-OO*" Customer S0 /Y o sr? Compartment Sample From Bottom Moisture ut BL Contamination BR 5 Bulk Density BD w/antistat SZf Viscosity RVCM 5o4- Bottom 03 - / .9i0Z .351 IW Bottom /o S /6 i war Bottom /f S2J J&l dll Screen Analysis Mesh 40 Weight % 60 80 100 120 140 200 Pan 211 /(*/ 50U 03. D h>5 & % Glassies Avg. Microns: /d Color 'L: &a b ?.?? Static Flow: Technician: d/ 4 VAB.0001202632 > Vista Polymers Highway 25 Aberdeen, MS 39730 h RAILCAR ANALYSIS L 9ZLoad Date: -//- Product: Time Logged Logged In By: Ship Date: Order No: Car No.: Silo(s) Customer: Compartment # Sample From A Bottom Moisture BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM L CkJ Bottom CB Bottom e IS Bf Bottom > : L Screen Analysis Mesh 40 Weight ________ % 60 ________ 80 ________ 100 ________ 120 ________ 140 ________ 200 ________ Pan % Glassies Avg. Microns: Color -L: __________ a _______ b _______ Static Flow: ______/ Technician: VAB.0001202633 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF & M ^ L_ V S I S & Date ?Zs Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G- Haefner Ship Date: VKD\ Product: 5325 Lot No Order No 64-^74 60/244- Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR--3 40 mesh Analvsis ,Z2- 200 mesh $3 Pan J?V ABGC-26 ABR-10 ABR--16 . 6>S? . 2V 7,? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001202634 A Q I to PQ O < to :2 w to Q* 4 ni w* 001202635 f Vista Polymers A Division of Vista Chemical Company CERT X F~ I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h OF ANALYSIS Date: b/i^/iA Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5305 Lot No.: Order No . : Trailer No.: Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-iA ABR-2A ABR--3 40 mesh 0*0 ABGC-26 ABR-10 Analysis ______ tS3<> 200 mesh .Z(*3 , Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Pan * a\ Labora tor y Supervisor/Lead VAB.0001202636 Date -/. 92- Customer pf*v>if+r Technician PVC BULK TRAILER ANALYSIS Product Silo___ CS 7 Trailer Number Time //?> Order No. g)/a? ftU ~OoQ A Particle Size Distribution: Screen Analysis /> Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 Q.oO 0.0 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus t .0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. _ *zt ,c t.l7 >4- I c,4 9.1*' U.3 zf.s 29,4 M.3 3.33 C. 7 /.at Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202637 Vista Polymers A Derision of Vista Chemical Company Highiway 2l5 Post Office Box 91 FfcTXFICATE OE Aberdeen, Mississippi 39730 Phone (601) 369-6111 fl Date: June 24, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 22, 1992 VISIAProduct: 5225 Railcar No.: ACFX 41147 Order No.: 0011491-001 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.11 0.51 0.00 9.0 3.8 .226 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H. D. Lucas Laboratory Supervisor PMMP mm VAB.0001202638 "hi*1 Ml* Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged Ship Date: ^ RAILCAR ANALYSIS Product Car No. ftcFX Logged In By: S?7. Silo ( s ): C) Order No: po //4q/( , Customer /$?/#< 3 . /vp Compartment Sample From Bottom Bottom Bottom Bottom Moisture BL Contamination BR Bulk Density BD w/antistat .// IS C7* .0 ? \i .S"> /> .CC9 Viscosity RVCM SOC, .2ZL IE! 5b! ' Ut> Screen Analysis Mesh 40 Weight A * po % 0,0 60 . LO LZ. 80 l.sf 100 njo z+.t. 120 12.712<r.t. 140 t- is' M.7 200 f, 0 % Glassies: t*? Avg. Microns: F Color L: 77.// a /.r7 b 2.U Static Flow: a , Pan /. 92- Technician: * VAB.0001202639 t i Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date:. -/f- ? 2- Product: Time Logged In Logged In By: Ship Date: Order No: Car No.: 4^//^7 Silo{s): Customer: Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM ^ca) Bottom CB Bottom i B' Bottom Screen Analysis Mesh 40 Weight ________ % 60 80 _________ ________ 100 ________ 120 ________ 140 ________ 200 ________ Pan % Glassies: Avg. Microns: Color 'L: __________ a _______ b _______ Static Flow: _____ / Technician: VAB.0001202640 I % Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: June 24, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 22, 1992 VISIAProduct: 5415 Railcar No: ACFX 53140 Order No.: 0012535-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.15 0.509 4.9 0.00 6.1 1.7 0.009 1.00 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001202641 mm I Viata Polymers J Highway 25 Aberdeen, MS 39730 RAILCAH ANALYSIS flCFX. Load Date: <> V? a. Product: Car No. Time Logged Ship Date:. b/2 /&O0 Logged In By: Order No: /?? Silo(s): Customer: Screen Analysis Mesh Weight %P 40 Or.G> 0 60 Jl inDrytime: 80 /f'rf 33. o 100 /7-V7 3y. 6 120 / / 3 / <23 A 140 4L11 200 Static Flow: 0 / g Q> Avg. Microns Pan -Ss LI /s8. / Color L: METS a O O 2- b /-/J7 z USA % Technician /h / fA VAB.0001202642 V?sta Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI F ICATE OF Aberdeen, Mississippi 39730 Phone (601) 369-6111 ANALYSIS A Date: June 23, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontowni KY 40299 Attention: L. G. Haefner Ship Date: June 18, 1992 VISTAProduct: 5225 % Railcar No.: UTCX 46455 Order No.: 0011491-000 Property Moisture, X Inherent Viscosity Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.15 0.50 0.00 6.4 2.3 2.563 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202643 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILOAR ANALYSIS Load Date: Product: Time Logged In: O^S3^ Logged In By: Ship Date Order No: Car No. : 4^ Silo( s ) : &&Q Customer A Compartment Sample From Bottom Moisture BL Contamination BR Bulk Density tQ r BD w/antistat Viscosity RVCM /4P- ZSl,3 Screen Analysis Mesh 40 60 Weight % 0*00 0.1 .3Z.L Bottom J3 3 g Bottom 3 Bottom dC * 4w 2 j>r3 80 lit /f.c 100 i4.n ,29* 120 !3.1o 27. t. 140 7, 3 /r./ 200 j. Pan /.J42.J % Glassies: <./ 9, Avg. Microns: !&JZ0 Color L: ***** a l.*3 b Z Static Flow: -Q.__ / *-* Technician: % VAB.0001202644 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I R" i g^tee: of analys X s Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jef f erson town , KY 40299 Attention: L. G. Haefner Ship Date: blt&fa-' Product: 5305 Lot No . : Order No.: OO/ZS^-666 Trailer No. :-57&tA Property Moisture, X Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A i* ABR-3 40 mesh 6-0 ABGC-26 ABR-10 Analysis 200 mesh Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory tif ervisor/Lead VAB.0001202645 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 OEJRTX FI CATE OF Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: /ZZ-/q Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: (o\il |<i VISIAProduct: 5465 Lot No . : faia Order No Trailer No. OOlZ-l O4!^ -OOO Property Test Method Moisture, % ABR-1A Hard Particles @ 7 min ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR-3 40 mesh 6. O Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Analysis i 200 mesh a .0t> //! Pan isor/Lead mm m VAB.0001202646 I a 2 W I pq O < CO C/3 W OS TI'O iI 0sO m VAB.0001202647 mmmmm mmmmm VAB.0001202648 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phono (601) 369-8111 CERTIFICATE O R" ANAL YS I S N : ip)zz.4? Customer: Premier Polymers 3001 Watterson T rai 1 P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: C,Jz-l |<?2. VISIAProduct: 5325 Lot No. : D^f73 Order No . : Q 0lZ4cfl-OOO Trailer No /-&7Q8 Property Moisture, V. Bulk Density, gm/cc rticle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh D-O ABGC-26 ABR-10 ABR-16 Ana 1vsis __ - Iffi 200 mesh nz MS' .044 Si Pan Lf> Polyvinyl Chloride, Virgin Resin, Not Reprocessed. VAB.0001202649 R E S IN BAG ii i Q 2 PQ nSI AB.0001202650 Vista Polymers A Division of Vista Chemical Company Highway 25 Posf Office Box 91 i Aberdeen, Mississippi 39730 Phone (601) 369-8111 vs i s Date: h/S-S-hz. Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jefiersontown, KY 40299 Attention: L. G. Haefner Shi p (sjnh^ Product: 5265 Lot No .'.Qlftffof Order No. : OO&lZLb-ODQ) Trailer No . : ~T~ (a\b `Z* Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis ./y .536 200 mesh .020 MS' Pan .3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. % VAB.0001202651 r S W ,1 Vista Mymari A Division of Vista Chemical Company Highway 25 Past Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730 Phone (601) 369*8111 M & L_ V S X S A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ifilt&h?' , VIS1AProduct: 5265 \ /IOTA Lot No.: (y-rihZL Order No.: 0012-45C -60 o Trailer No. : ~T~-~ *1705* Property Moisture, V, Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 6.0 ABGC-26 ABR-10 Ana 1vsis .it 200 mesh .-f.f .057 . Pan ? 5 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory ^iiO ervisor/Lead pnppMMMfiPMin mmm MMRPHM VAB.0001202653 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 \n A IX Date: &>/ZZ-fo Customer Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: V' S I s Product: VBIA Lot No OMtn m Order No.: 0 & 1~O0Z> Trai1er No.: Propertv Test Method Moisture, X ABR-1A Hard Particles @ 7 min ABR-12 Bulk Density, gm/cc ABR--2B Barbender Dry Time, min ABR-07 Particle Size Dist. ABR-3 40 mesh O.Q Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Analysis .20 J 43 200 mesh Cl .orl Pan 1.3 borj^t Supervisor /Lead _____ pages Page ... , o f Regulars or Begs V OJ \ mm rnmmymmmmmm *i f .f)001202655 t - * +. 01 0Q AC <L V ?\ UMlM ?| CD 3 O ' *1 Ml* PMMVRPP 3 f VaM)001202656 *. .1 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen,, Mississippi 39730 Phone (601) 369-8111 A Date: June 19, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 15, 1992 VKIAProduct: 5225 Railcar No.: UTCX 46465 Order No.: 0009535-004 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.30 0.49 0.00 11.1 3.6 1.952 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy BV Bagwell Laboratory Supervisor VAB.0001202657 Vista Polymers \ Highway 25 Aberdeen, MS 39730 A RAX LCAR Load Date: (s? "72- Product: Time Logged In: /J1 & * Logged In By Ship Date s Order No: SXS Car No . : 4 Silo( s ): >o&f :PlCustomer /Va ma^T Compartment Sample From f\) Bottom Moisture BL Contamination BR 13 Bulk Density .srz- BD w/antistat Viscosity RVCM ,4f H.p. G fkOb Screen Analysis Mesh Weight % 40 6-0 60 O.Oto O.l C ct) Bottom ,3* it tt.&>( 80 100 ( Bottom .o% ? .5*f Bottom <1 1 17 .sr^ <`5o'2-- 1.9SZ 120 140 200 Pan fo.U ILA 3-W X Glassies: Avg. Microns: tHo.z. Color L: a J/ b Static Flow: / *2 2^ Technician: /Aft d/h/% % VAB.0001202658 / Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: June 19, 1992 Customer: Premier Polymers 3001 Watterson P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 15, 1992 yisiAProduct: 5415 Railcar No: PTLX 422 Order No.: 0012220-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.12 0.505 4.8 0.00 4.2 1.4 0.023 1.02 aJ Laboratory Supervisor (601) 369-3624 VAB.0001202659 A 4n/O' Vista PolvmerB Highway 25 Aberdeen, MS 3973q PVC RAILCAR ANALYSIS Load Date: -A Product: Car No . : ^ea^ 7 Time Logged In: <D /<>& Logged In By: Silo(6): Ship Date Order No: /90D& Customer: Mesh Weight % 40 0.0 Q 0*0 60 U.X ------ -------- Mp------ 80 M<) Up.? 100 120 lY-t>2 7-</7 a?.I /to 140 IP? U? VP 200 M 3.? Drytime S.v Static Flow 0 / 1* Avg. Microns: Par ii Co lor L: hffjvy .17 b Technician: METS to z //Sf-"7 y/fStI VAB.0001202660 Vista Polvmers Highway 25 A Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date Time Logged In: Ship Date Product: Logged In By: Order No: Car No.: siio(e Customer: /i/o /W -e Compartment Sample From Moisture % Contamination Bottom Top Bottom Top , o3 Bottom Bulk Density Hard Particle Bottom Top i jT IS 1 RVCM Screen Analysis Mesh Weight %P 40 &.D 60 2. 80 231^7 100 ^LK 120 C>/1 / 3- / 140 2-^1^ 200 2./o -$L2= Pan Drytime: JL Static Flow: tP Avg. Microns: ^ Color L: /ft?, ft, a #'0? b /,/d METS: //Z7.I % Technician: -fd /tr' VAB.0001202661 fMMMMPP Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner VIS1AProduct: 5305 Lot No-: Order No.: GO 1~ & && Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-IA ABR-2A ABR-3 40 mesh 0.O ABGC-26 ABR-10 Analvsis .AO . b3Z- 200 mesh ibs ,057 05 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Pan 4s Labor a rvisor/Lead VAB.0001202662 I 1ti\ CJ> VAB.0001202663 ft Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CC EE F? ~T I I CATE OF IM ft L_ Y S X S A Date Customer: Premier Polymers 3001 kJatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5305 Lot No.: 001Order No. : Trailer No.: "T-*' Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR 3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis 200 mesh ST .oc,z ,71 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. '60/ Pan t ervi VAB.0001202664 Q Z w Q < m I i\iiii w as \iii( mm* V w w 1 0001202665 MW Villa Polymers A Division of Villa Chemical Company X Highway 25 foist Office Box 91 I CA Aberdeen, Mississippi 39730 Phone (601) 369-8111 analvsX s :Date //llZh Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date : (elllttfls VBIAProduct: 5265 Lot No . : 0*4^5*7 Order No.: OOfZ573'MO Trailer No. : "7C Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A I ABR-3 40 mesh D.O ABGC-26 ABR-10 Analysis . 10 .545 200 mesh 4.b oe>o Pan /.7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora visor/Lead VAB.0001202666 Vata Polymers A Division of Vata Chemical Company Highway 25 Post Office Box 91 CERT I R* I CATE OF Aberdeen, Mississippi 39730 Phone (601) 369-8111 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Ujtt k 2^ " 5"5 VISIA Lot No.: Order No . : QQ f ZZ /0 ~0CO Trailer No.: ~7~<^*7$T/ Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh o.o ABGC-2& ABR-10 Analvsis ./<f 200 mesh ' 46 .osi Pan AS Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead VAB.0001202668 ** * I R E S IN BAG .E N D HPPliPMI 11 ....... ............ "*.... \mmmmmrnmmmmmmmmmammm Vista Polymers A Division of Vuta Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF 4 Aberdeen, Mississippi 39730 Phono (601) 369-8111 ANALYSIS A Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: blltfa'l' VIS1AProduct: 5265 \ /ipTA Order No. : OOl'Z'3*7S~6QO Trailer No.: ~7^5'70S~ Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh o.o ABGC--26 ABR-10 Ana 1vsis ./3 ,5Zl 200 mesh /,o.4 ,oz\ . or Pan /. z, Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor pervisor/Lead H VAB.0001202670 Oo' i a * I V u t3j g Q CL oO) 0) a CO w c > *e a 01 0n 30 ac a CL A VAB.000M)2671 tm424M Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERT I F I CATE OF ANALVS X S A Date Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VISTA Product: 5305 Lot No. Order No.: Qo 122. i(o ~OOO Trailer No.: T""^03 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis .06 .52^ 200 mesh .n*> Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. llabora . if.-- i VAB.0001202672 Dale Customer fr<M r PVC BULK TRAILER ANALYSIS Product Silo _ Trailer Number T&ss Time }3~ffl& Order No. 0O/2S/& -oo Panicle Size Distribution: Screen AnalysisMin Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh a o*7 0.0 Screen Analysis 60 at Min. Mesh Size 40 60 Gross Wt. Tare Net Wt. 9b on Mesh On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 80 100 120 140 200 9 70 fsyo f76Cp lS_ 3si l&b 27.+- XLt /<*.+- &>rC? On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 Glassy Pan Part. /.20? Glassy Pan Part. Remarks HHI wmmmmmmmrnmmmm VAB.0001202673 m vt=' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OE ANALYSIS Date: June 11, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 8, 1992 Product: 5225 Railcar No.: VIPX 45856 Order No.: 0009535-003 Property Moisture, % Inherent Viscosity Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.25 0.50 0.00 10.3 2.8 1.564 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202674 Vista Polymers Highway 25 Aberdeen, MS 39730 FtAX LCAR ANALYSIS Load Date Product: Time Logged In : Q/Q Logged In By: Ship Date: _jyg Order No: Car No Silo(s) s 80 : (mrwJL^. Customer 7U TttJUL Compartment G Sample From Bottom Moisture */.<>___ BL Contamination BR 3 Bulk Density BD w/antistat Viscosity RVCM .Zdi CA Bottom . CB Bottom B Bottom A Screen Analysis Mesh Weight 40 Qc % 60 J, , 80 nsr iS.L, 100 12. VC J4.7 120 13.1 f 140 tf2- n.s 200 5~M U>,b Pan 1.96 3J % Glassies: X-- J y*_______ Avg. Microns: Color L: ^7'ff a hXj__ b {tftf Static Flow: ^ _/Xl Technician: VAB.0001202675 T Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In:. Ship Date: F2, A X LCAR ANALYSTS ?z Produgt: Logged In By: Order No: Car No.: Silo(s) Customer: Compartment Sample From Moisture Contamination Bulk Density om Bottom Bottom Bottom o. ZSJ Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight X .0 D.O .2 ctf //, /<yf /a. i S3. 3 29- 7 /t.oo S AJ /y S3 o /<?-3 3-2 % Glassies: / &o j Avg. Microns: / Color L: 97~lt> a f-t>r b /?? Static Flow: 0jjzj Technician: \ VAB.0001202676 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X R" I OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: Lot No.: Order No.: OOtLl^"000 T rai1er / Propertv Moisture, X Hard Particles @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-iA ABR-12 ABR-2A ABR-7 ABR--3 40 mesh 0D ABGC-26 ABR-10 Ana 1vsis 5".0 200 mesh /S~,/ d3o Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead VAB.0001202677 R E S IN BAG BLEND y m* Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I I C2 /A T E O F7 ^IVI^LV'S I S A Date: (p Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5325 Lot No. : L- Order No.: QO11 Trailer No.: / ^ &7Q>3 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR--3 40 mesh 0.0 ABGC-26 ABR-10 ABR--16 Ana 1vsis .2lo 200 mesh h* I_____ l^&.D ____ -cnt M 3L.2. Pan J?- 0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora a/ visor/Lead VAB.0001202679 PMIMK A a o < CQ Z CO Cd Hi mwii immim VAB.0001202680 Wf Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X F* X O AT E Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSX S A Date: June 8, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: June 1, 1992 Product: 5415 Railcar No: PLWX 44269 Order No.: 0011540-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.23 0.521 5.0 0.00 4.7 1.6 0.030 1.02 Laboratory Supervisor (601) 369-3624 VAB.0001202681 Vista Polymers Highway 25 Aberdeen, MS 39730 IP VO JR A X LCAR AN AL, YS I S Load Date: 72 Product: Time Logged In: 0 Y6-& Logged In By: ft(pShip Date: Order No: No. : Silo(s): Customer kja ?%*** Compartment A Sample From Bottom Top Moisture % 23 BL Contamination BR _4_ 3 3 Bulk Density <!? e?f 5 Hard Particle 7 2. /ML w Viscosity RVCM 1.0 l& .020 CA Bottom Top CB Bottom Top 2/ .;?3 33 zs 77 - 2. <5?* Sl% B Bottom Top . aa- 3 3 5^7 Screen Analysis Mesh Weight % 40 >. 0.0 60 Iff 80 mt <76,9 100 t&z ZorO 120 140 7. 200 *- -------------------------- fr7 Pan Drytime: Static Flow : * Avg. Microns* /27. Color L: Technician: METS: b / iis;z> % "rnmmmmmm VAB.0001202682 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship L- 7-?L Product: 5415 Lot No. Order No. T railer Property Moisture, V. Test Method ABR-1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR-3 40 mesh b.c>o Residual VCM, ppm ABGC-26 Inherent Viseosi ty ABR-10 Analvsis .// .S't'? 4.7 200 mesh f - .014* Lot Pan t.t Supervi MUM mmtmmmrnmmm VAB.0001202683 mm Dale Customer Technician B ^- FRONT MIDDLE END PVC BULK TRAILER ANALYSIS A Product Silo___ -6?/ Trailer Number 7~'?7 Time g 3 o Order No. BULK DENSITY .S> ? DRY TIME I COLOR L= A = D- / vise <> RVCM B= / 2-7 I L= A= B= i L- A= B= Particle Size Distribution: Screen Analysis /*> ...... Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Glassy Pan Part. Tare Net Wt. ( % on Mesh o 6 ,o Screen Analysis Mesh Size Gross Wt. 40 3S? n.u /`/.(S' f.Jf saQ- am 3S~.3 15-3 u.r 1,0 r.i Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 (L3JT 13-- Glassy Pan Part. Tare Net Wt. % on Mesh Remarks VAB.0001202684 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F=" X CATE OF & N ^ L_ V S I S A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner A Ship Date : ^/?2- VKIAProduct: 5305 .-.okzs Lot No Order No @0 I0O& Trailer No.: Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR"3 40 mesh 0.0 ABGC-26 A8R--10 Ana1vsis . /a , 5z0 200 mesh 4-3 .0*10 .75 Pan 2.4 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. r VAB.0001202685 * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F7 X C2 ^ T EE OF ANALYSIS A Date Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: (pjdh^ VISIAProduct: 5305 Lot No. : Outfit? Order No. : 0t K^MO-Cdd Trailer No. : "T^-S"/ Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh n.o ABGC-26 ABR-10 Analvsis , // .532 200 mesh t,-l , O/ZL . 72- Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. r/Lead VAB.0001202687 Q O < OQ W Od \ I I i f A 4 VAB.OC 31202688 mmm Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ^ l_ V S X S A3 Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5305 Lot No-: Ctitfio Order No.: Qq f Trailer No.: *7?SV Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 6 >0 ABGC-26 ABR-10 Analysis *!6 ,52t> 200 mesh C>-0 * 72^ Pan .Q Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead VAB.0001202689 R E S IN BAG bLEN D / 3 ,5 6 0 .0001202690 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 FtT I F I OATE OF ANALYS X S A Date: May 22, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: May 18, 1992 Product: 5225 Railcar No.: PLCX 43709 Order No.: 0009535-001 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.15 0.51 0.00 12.3 31 1.467 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe IS]/ Laboratory Supervisor VAB.0001202691 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged In: : -Sfl* Ship Date Product: Logged In By: Order No: Car No *+3 7o9 Silo(s) : : Pa*Iaj>.-- Customer Compartment Sample From Moisture Bottom Contamination Bulk Density BD w/antistat Viscosity RVCM Bottom Bottom .S77 Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight p.oo .12. S'. 2* /O.Zl' 14-11 //.70 4./7 /.s% % > Z. X/./ 2f. 23. /2-3 J: t % Glassies: Color L: f7* ft a /. b Avg. Microns: Static Flow: jp / 7.7 Technician VAB.0001202692 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 A Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: May 22, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: May 18, 1992 Product: 5225 Railcar No.: ACFX 41155 Order No.: 0009535-000 Property Moisture, % Inherent Viscosity Particle Size, X on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.13 0.50 0.00 14.9 3.8 o.wy Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E^yBagwe Laboratory Supervisor VAB.0001202693 V %<0 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYS 31 S Load Date: Product: Time Logged In: /3<3^* Logged In By: :_EM Ship Date Order No: : 4HS5 Car No Silo(s) Customer : P/?/hfAf Compartment Sample From Bottom Bottom Moisture BL Contamination BR Bulk Density (2 r r /*v /? 12. LL 25 21 .m BD w/antistat , /i $n /s .oT7? Viscosity RVCM .01* DO. . 134 Bottom // 3 is i Oi .49Z* Bottom */o i <r .S7f .'5U Oil Screen Analysis Mesh Weight 40 Q-00 X 60 m 2- 80 100 120 140 200 Pan //.K" 7.*Lr 1.1* 21.1 21.1 zZ.7 /y,9 3,8 X Glassies: <-i % Avx, Microns: /31*3 Color L: 1 f- ?* a /* 7 (r b Static Flow: o/7.? Technician: /pt I VAB.0001202694 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: S^l I 9 Z_ Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KV 40299 Attention: L- G. Haefner Ship Date: f Product: 5225 Lot No.: 04-^od Order No. : OCOty&CsC> -- OOO Trai 1 er No . : HT- Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 6.0 ABGC-26 ABR-10 Analysis ,5%f 200 mesh OS /. 7^/ / 5/ Pan /. & Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor dJ visor/Lead VAB.0001202695 <N /\) ST* V) \ ia "o3O *5 2 Q CL o* o OL <0 (/> c > 0 Oft a c*n CD 3 a> Oeft o e a. 001202696 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-6111 CERT X R" I CATE OF" ANALYSIS A Date: MAu 2-- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ty iq, VB1A Product: 5305 Lot No. Order No.: OOIlSL/^000 Trailer No. : Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh o<o ABGC-26 ABR-10 Ana 1vsis 200 mesh /o-o .D&f ,723 Pan P. 9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory S rvisor/Lead VAB.0001202697 m+m PVC BULK TRAILER ANALYSIS A Date Customer Pre**: Product STS Oik Silo___ L%<( Technician mm MOIST Top Bottom CON'T. Booom GEL 1 .<m * t*4 I FRONT 2. 2. l I. I Trailer Number. Time /03Q Order No. 0CD / BULK DENSITY I DRY TIME I COLOR L= V 3? A= B = /.43 L= vise RVCM MIDDLE 2. END i. 1 i 1 2- 1 * _________ 1_________ 1 m 1 I A- B= LA= B= Particle Size Distribution: Screen Analysis io Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 t.po 0*O Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .o4 J Min. 60 4.o /. ii.it >>4 n.tt i,if r.oo 41.S- 21.1 10-0 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 s.4t fit Glassy Pan Part. Remarks VAB.0001202698 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 A I I CA ! tr/iDfop. Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date : 5/ XS VISIA Product: Lot No.: rd No.: DQlD^5Q'D0O Trailer No. : 7"" +ZD Propertv Moisture, V, Hard Particles* @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min. Particle Size Di st. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-12 ABR-2A ABR-7 ABR-3 40 mesh 6-0 ABGC-26 ABR-10 Analysis . t4 1 S.D 200 mesh n.e> Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory upgrvisor VAB.0001202699 mm R E S IN BAG BLEND o o< \ 7 Cr-* \ mmmmrnf m A 4 *o 202700 Vista Polymers A Division of Vkta Chemical Company I Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 X cz ^ OF ANALYSIS A =Date S'/zo Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship *Date S/rtfa VIS1AProduct: 5265 Lot No. : Order No.: COO3-3~OOO Trailer No.: 'T-'CC> Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh D-D ABGC-26 ABR-10 Analvsis ,14 200 mesh /s:3 .077 . (ot? Pan 3. S' Polyvinyl Chloride, Virgin Resin, Nat Reprocessed. labora isor/Lead VAB.0001202701 I Ml Uij cS ri\ o-i A *1 Jl Q 2 w o) D o < 3 2 CO Cl) oc vJ 'IP o 1 ^ Kl 1 c^J 1 ^ id| v4> si II id 1 1 acj|| ^ 81 ^^ 1^ *^1 11 ^ t1I 0 o o| I nw mmmm* m A VAB.OOi 1202702 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: ^/ZO Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: tp/Itffa'Zs Product: VISIA Lot No.: ,, Order No.: 0C> l(05& 'OOO Trailer No.: /-"<?#33 Property Test Method Moisture, 7. ABR-1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min ABR-07 Particle Size Dist. ABR-3 40 mesh o-o Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Analysis . lU> ^me A `SOL 200 mesh A3 Pan /. 3 J./Z^ rvisor/Lead VAB.0001202703 A w Ml I Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CEERT I F7 I Cf^TEE QF ANALYSIS A Date: 5l2I))q~3L Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VISIA Product: 5305 Lot No. : Order No . : 001105^000 Trailer No. : T'*'^>033 Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-iA ABR-2A ABR--3 40 mesh - 0 ` CL ABGC-26 ABR-10 Analysis 57/ 200 mesh 43 J&l . 7a Pan JP.P) Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor mmmm PHU VAB.0001202705 R E S IN BAG BLEND * C.1 25 u | 1 M (O I I 1 aCQ mA I1 w 4 [J 1 [} I o <K R; & o io CnT V VAB.0001202706 mm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTI F X OAT E OF ANALYSIS A Date: May 13, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: May 12, 1992 VISTAProduct: 5225 Railcar No Order No UTCX 46584 0009535-002 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.15 0.51 0.00 11.3 2.5 1.129 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor V ....... mmrnmmm VAB.0001202707 t Vista Polymers Highway 25 Load Date: r- y- r- Time Logged In: Ship Date RAXLCAR Product Logged In By: Order No: Aberdeen, MS 39730 A Car No.: U-fc. f-t rtf Silo(s): Customer: Compartment Sample From Bottom ______ Bottom Moisture ,/.r BL Contamination BR Bulk Density 1 7 . S~f 2-- BD w/antistat ,/-2.4f*0 Viscosity RVCM <576 /./? Bottom .// S7f ,*5X7 Bottom ./* <? </ .sr/ .5# Screen Analysis Mesh 40 Weight % 0.0 60 . 00 80 ..4Jk. f.9 100 19.14 X/.1 120 AT.?7 J/./ 140 /t.C.7 23.3 200 //.3 Pan /. *4 -?.5~ % Glassies: Color L: 97So a /-</ b Avg. Microns: /37.T" Static Flow: a / <&o Technician: 4 VAB.0001202708 Visks Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE O F7 ANA L_ V'S I S A Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Shi p VIS1AProduct: 5325 Lot No.: 6>4<]50 Order No.: T rai1er Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh &0O Analysis ,/*> 200 mesh 2.8 ABGC-26 ABR-10 ABR-16 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora tory rvisor/Lead VAB.0001202709 * * A / 4 70 m 03 2 03 > O tw 55 O m t VAB&OO1202710 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A 4 Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention; L. G. Haefner Ship VISIA Product: 5305 Lot No Order No.: QO /073"OOf Trailer No.: Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A A8R-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analysis ,Q4 ,5/2 200 mesh /g?.44 .07f 73 Pan 3.9> Polyvinyl Chloride, Virgin Resin, Not Reprocessed. j at isor/Lead VAB.0001202711 HWOMIMP PVC BULK TRAILER ANALYSIS A Date r-c-fL Customer Premier0 Technician Product Silo___ 671 MOIST Too Bottom l. .ot ** CON'T I2L Bottom i GEL l FRONT 2. 2. I. i Trailer Number 7-1S4 Time oiv r Order No eniDna3'ao] BULK DENSITY DRY TIME II , 1 2- COLOR L = 19Uo A == .Jj Il B= L= RVCM MIDDLE 2. I END i 2. A= B= i i L- A= B= Particle Size Distribution: Screen Analysis _____LO- Min Mash Size Gross Wt. Tara Nat Wt. H on Mesh Screen Analysis 40 0.0 60 .of Min. Mesh Size 40 60 Gross Wt. Tara Nat Wt. % on Mash On Aotap shaker. 49 gins. Resin plus 1.0 gms. Carb 80 100 120 140 200 7.11 H.tZ- if. to ii.S7 .A, it to 2/. Z \ Si.7 ZZ, 7 On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 too 120 140 200 Glassy Pan Part. s.r Glassy Pan Part. Remarks VAB.0001202712 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730 Phone (601) 369-8111 l_ V' S I S A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KV 40299 Attention: L. G. Haefner Ship Date: s'/thz. Order No.: 000tf$5^-000 Trailer No.: Propertv Moisture, */. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh o.c> ABGC-26 ABR--10 Analvsis . It . 53 200 mesh .1$1 .73 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead VAB.0001202713 Date Customer Technician ffem M& PVC BULK TRAILER ANALYSIS Product ST3 HISilo___ Trailer Number 7^J/^ Time J030 Order No Coctf&S*? -mu Particle Size Distribution: Screen Analysis_______ _________ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. H on Mesh 6.60 c.o *>? *- A. & *7.1 .*70* f, Hi 3.4F Screen Analysis Mesh Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Tare Net Wt. 4b on Mesh Remarks AB.0001-202714 Vista Polymers A Division of Vista Chemical Company cert i f=- i Highway 25 Post Office Box 91 OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 XS Date: `5'js'l^'Z^ Customers Premier Polymers 3001 UJatterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: f. VIS1A Product: 5305 Lot No. Order No.: 0O / O 1153^D OO Trailer No.: ' j - Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 0.0 ABGC-26 ABR-10 Analysis 06 200 mesh /Q.% ,625 .73 Pan J?- 7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora VAB.0001202715 Date Customer Technician pfemfe PVC BULK TRAILER ANALYSIS A Product Silo___ kSl Trailer Number. Time Order No. 00/0*7^S-g>tg) FRONT i MIDDLE 1 END I. i. I L= A= B= L= A B- 02\S Particle Size Distribution: Screen Analysts Jo Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 (KOO Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 1 * | A i 1 j -J Min. M.lt, tun*0 zz-z. mt rN to.zc s. 21J /A f On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. -2-7 Glassy Pan Part. Remarks ^ARmni?02716 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F I CATE CD R" *=irM^L_V'S I S Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5415 Lot No. : Order No.: Trailer No.: /-" VKI\ Property Moisture, V. Test Method ABR- 1A Hard Particles @ 7 min. ABR- 12 Bulk Density, gm/cc ABR- 2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR- 3 40 mesh DO Residual VCM, ppm ABGC -26 Inherent Viscosity ABR- 10 Analvsis _ J. 4 4i $ 200 mesh _S.b__ .Dot / Pan -L$- at Su visor/Lead VAB.0001202717 11 I SI 1I I 1I r i \i h IA M i u T3> O Q i i D0 oc "D C4> O E CO a) m 012027* 18 2454 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 certificate of Aberdeen, Mississippi 39730 Phone (601) 369-8111 analysIs Date: fT/^5 Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VISIAProduct: 5265 Lot No. : Order No. : ^'OC> Trai1er No. : / Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analysis )4 . T5o 200 mesh .m , kb Pan 3.6 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. SvJUJ sor/Lead VAB.0001202719 <-U rc >l\ <r| <i ,! Q zr\ W tj O < 3 CO w a: cO VA V WPVWMP cr co $r :3- o W 02720 m Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adendeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF & N l_ V S I S Date: 5'/5'/`?Z- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: ^/| Produc t Lot No.: 04-434- Order No.: 0 ocQQ&St-06(0 Trailer No Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Analvsis .04 .53! 200 mesh 15. i .o4& .loL Pan 4. Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ory S sor/Le ad VAB.0001202721 Tm m Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C2 EE F? ~T I R' I CATE OF ANALYS X S Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Product: Soto Lot No.: o44ie> Order No.: 000^057-000 Trailer No Propertv Moisture, 7. Hard Particles @ 7 min. Bulk Density, gm/cc Barbender Dry Time, min Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-12 ABR-2A ABR-7 ABR-3 40 mesh 0.0 ABGC-2h ABR-IO Analysis -3-(p 200 mesh 10-6, 0/Q Pan /9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor rvisor/Lead mmmmmmpKrn wmmmmmmmm imp mm VAB.0001202723 D cl o> o 0 a (0 CO c > 9 a GO O cc Cmft CL \ vM0001202724 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Customer: Premier Polymers 3001 UJatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: VlSlA Lot No Order No. : 0OC$Q5*l"O0C? Trailer No.: Proper tv Test Method Moisture, 7. ABR-1A Hard Particles < 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR--3 40 mesh D.C> Residual VCM, ppm ABGC-26 Inherent Viscosity ABR--10 Analysis .ft I .&>! 4.4 200 mesh .0LI A// Pan IS VAB.0001202725 A eT> C r>> -2 CD 3 V VA]: 001202726 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT IF I C2*^~rE OE Aberdeen, Mississippi 39730 Phone (601) 369-8111 IS A Date Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Produc t: Lot No.: Order No.: DO / CCXoD ' DOQ Trailer No.: /- ^ ^(a (o Propertv Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR --3 40 mesh 0.0 ABGC-26 ABR-10 Ana lysis . !Z .53Z. 200 mesh //& .o/4 .72 Pan <f. I Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora r/Lead VAB.0001202727 *4 ' 01202728 t Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF IS Date: tff'ZO Customer: Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. tShip Date = 4h(*h VIS1A Product: 5325 t No. : 0^/-^ ft-l Lo Order No. : OUOH'OO&t ~OU / Trailer No Propertv Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 ABR-16 Ana 1ysis . // 200 mesh 5^5" 14-7 .9/ ^L-C> Pan /.5~ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. mmm T mu VAB.0001202729 3%no O -O a2 Q a. U) o CoO oCO oIA oin om 4) CO a30> T> Cv r> e CO 3 e cr~ VAB.O 202730 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERT X I CJ VS I s Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VISIA Product: 5325 Lot No - : 044II Order No.: > OCtf052'~0 DI Trailer No.: / QZSQ Propertv Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh n.D ABGC-26 ABR-10 ABR-16 Ana lysis .m Am 200 mesh 6>.a 144 .rxA _*80 Pan A7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead VAB.0001202731 rl N c* a on u 3 *o a 8 cl \ c > o a> a (O CO C > m0 CL o> CD a3> * 0 QC Q. \ mmm I1 mmm A 3 VAB.Q )1202732 *|4M* ** Vista Polymers A Division of Vista Chemical Company cert- i i Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369*8111 aanalysis A Date: tf'f'ZO/tfZ' Customer: Premier Polymers 3001 Watterson Trail P. 0- Box 99571 Jetfersontown, KY 40299 Attention: L. G. Haefner Ship Date: VIS1AProduct: 5265 Lot No . : O^DS Order No. : 0OC$>>2- /- OOO Trailer No . : "7~ t>7%? Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0,0 ABGC-26 ABR-10 Analysis * /4?_______ 200 mesh q.*l .083 Pan <s Polyvinyl Chloride, Virgin Resin, Not Reprocessed. LaborZxoTy Sd(g^*visor/Lead VAB.0001202733 z' \n * Ia fVN u 3 T3 Oa O) o a> Q. CO CO c > 01 * a o o c & A VAB.0(ttJ202734 I r- Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 I I CA Date: 4li^h^ Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date 4!I 4(<? ^ f\J ^ V' EE> I S Product VIS1A Lot No. : Order No ceoQ'rti - ooo T 74 toTrailer No Property Moisture, '/. Test Method ABR-1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min ABR-07 Particle Size Dist ABR-3 40 mesh b-0 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Ana1vsis jn z 4-A 200 mesh 3A .nrt /. isu Pan 1.5 visor/Lead VAB.0001202735 <\) ) )a o 3 S "o 2 Q a. O) o (i YS) 0 a A9 0 co c > c* & o oc a<9. * A > JJP01202736 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ^ M L_ V S X S A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date VISIAProduct: 5265 Lot No. : Order No. T rai1er nnn Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh Q.O ABGC-26 ABR-10 Analysis J& .55b 200 mesh 9-5 5b Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. % VAB.0001202737 \V ` VA] 14)001202738 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE F Aberdeen, Mississippi 39730 Phone (601) 369-8111 XS Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date Product: 5305 Lot No. : 044&CI Order No.: Doo4344-00! Trailer No.: Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh . o.o ABGC-26 ABR-10 Analysis , 13 ,578 200 mesh ns 00(& S3 Pan 4s Polyvinyl Chloride, Virgin Resin, Not Reprocessed. rvisor/Lead VAB.0001202739 Qas tu a o < CQ C/5 W * t i KWH upmp wmmmm mm 01202740 mmm n-> Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 CERTXFICATE Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSX S A Date: April 10, 1992 Customer: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: April 7, 1992 Product: 5415 Railcar No: PTLX 42185 Order No.: 0008458-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR- 7 ABR-3 ABGC-26 ABR-10 Analysis 0.05 0.494 4.7 0.00 5.1 1.6 0.021 1.02 irmrf jnt <sao I Amy E. agwAl Laboratory Supervisor (601) 369-3624 VAB.0001202741 Vista Polymers Highway 25 <r Aberdeen, MS 39730 Load Date: 7 9 Time Logged In: thShip Date Z#o RAILCAR ANALYSIS PnV Product: Car No. Logged In By: /*? <71 Silo(s): & <&, g<K%-cco Customer juntos Screen Analysis Mesh 40 Weight AJ2 % 60 .30 * C? 80 /f-3f 3 (p* ^7 100 31.3 120 / 7- / 140 3 7 7-7 200 S'. / Pan 7? / c= Drytime: Static Flow: Color L: />Q-77 OJJ Avg. Microns: / -2V Technician: METS: 7 VAB.0001202742 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F~ I OF ANALYS I S i A Date: tf-fl Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L- G. Haefner Ship Date: Produc t: Lot No.: Outfit*) Order No.: Trailer No.: ~00& Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0,0 ABGC-26 ABR-10 ABR-16 Analysis ./<? .506, 200 mesh /V^. / ik6' / Pan J?-/ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. visor/Lead VAB.0001202743 1/7 H 0~ rtf i k/> la o 9 a ToJ a O) O 0) GL cu CO c > a d 3 a a VAB.(J)1202744 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 M ^ L_ Y S X S A Date: 4l^fa^ Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: VIS1AProduct: 5265 Lot No.: OWo4 Order No.: Q&C) /Z03 2- ~ Trailer No & Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC--26 ABR-10 Analysis ./o .534 200 mesh 55 Pan _Lh Polyvinyl Chloride, Virgin Resin, Not Reprocessed. llaborat rvisor/Lead VAB.0001202745 24U VABl001202746 5 Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERT I I OF ANALYSIS A\ Da te: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: Product: 5305 Lot No.: 2$ Order No.: OooQ&t4-0O& Trailer No . : *7-' {-f 11 Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Ana1ysis .on 5^l(o 200 mesh .oo4 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ervisor/Lead mmm mm n# VAB.0001202747 1( Vn V Cv \ I i CQ IN O ft < CQ UJ Cd N* Ci o\ of o*$ <S Qftfr % %ft <r> O& -*r -#* S3 ft Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERT X F7" I Ci^TEE: OF ANALYSIS A Date Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date * vfote Produc t Lot No. Order No. Trai1er No. : / " Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR 1A ABR-2A ABR--3 40 mesh 0-6 ABGC-26 ABR-10 Ana 1ysis . il .533 200 mesh .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Pan s. I Jtifl_____ Lab pervisor/Lead VAB.0001202749 O Ol o mo CL mOft 3 mOft Oft <r V Vinyl Sample Log 202750 J Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTI R I CAT* EE OR ANALYSIS Date: April 3, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: April 1, 1992 Product: 5225 Railcar No.: VIPX 45910 Order No.: 0006956-003 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.24 0.51 0.00 9.9 3.3 8.035 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe" Laboratory Supervisor VAB.0001202751 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: JT- f JZL Time Logged In: =Ship Date *ff\h RAX LCAR Product: Car No.: *4~9/0 Logged In By:_*fe2 Silo(s )i Order No: Customer: f Compartment A CA Sample From Bottom 3 T>t*f Bottom Moisture j_o * oS BL Contamination BR 2- iz Bulk Density .u BD w/antistat Viscosity RVCM 8 .as' CB B Bottom Bottom ./z .*9 . 0 . ^p/ 3 ? IML Screen Analysis Mesh 40 Weight QiQ X OcO 60 80 100 120 140 200 Pan /z.f2- rzjs~ g.ss- y.% hU *2 tu_ 2S.L psn 171 9*9 3.2 X Glassies: l(% Avg. Microns: .S Color L: a /.37 b Static Flow: & / <T*3 Technician: X- / VAB.0001202752 ) A* v Vista Polymers Highway 25 Aderdeen, Mississippi 39730*0091 A Division of Post Office Box 91 Phone (601) 369-8111 Vista Chemical Company CERTIFICATE OF ANALYSIS Date: " J~ Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: 2 2 ^ Produc t Lot No - : Order No.: 0OO H Trailer No.: ~T-si) Proper tv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 0. o ABGC-26 ABR-10 Ana lysis , 2 2, .r/6 200 mesh S.O Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. ratory Supervis ead VAB.0001202753 PVC BULK TRAILER ANALYSIS Customer Pr e rv? Technician FRONT Product Silo___ MOIST Top Bottom . i<22 2. CONT. Top Bottom I6 8 GEL \ 2. II Trailer Number Time l ^Oo Order No. BULK DENSITY I DRY TIME I I COLOR L= 100.Z3 A= 0>\ 3 b = \t}[ L= MIDDLE 2. END i i ii 2. A= B= L= A= B= A I vise RVCM F/qcO % Particle Size Distribution Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh m. 2- <S> Screen Analysis Mesh Size Gross Wt Tare Net Wt 9% on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 O* Ob o> l 'PAi \44 13-S3 14 ~)Z 37. | a*).* 9 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Psn Part. 1.8 o 3, (o Glassy Pan Part. Remarks Star 207A Revised 1 /12/87 :0001202754 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTXFICATE Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: March 18, 1992 Customer: Premier Polymers P.O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: March 13, 1992 VISIAProduct: 5225 Railcar No.: VIPX 45748 Order No.: 0006956-002 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.23 0.52 0.0 11.1 3.0 2.163 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001202755 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: % Time Logged In: 730 Ship Date Product: Logged In By: QOO^SL Car No. Silo(s): Customer: r/teMlCfU AU/niAS Compartment Sample From A CA yBottom 31* Bottom CB Bottom B Bottom Moisture BL Contamination BR M. Bulk Density o? Jl 2- .0 9 .07 P 7 BD w/antistat Viscosity RVCM J2L J_____ Z.lb* S/L / L>(pc> Screen Analysis Mesh 40 Weight % 0,0 60 o. 30 0-h 80 100 120 140 200 Pan U//,4T /-? 9.9S 23.-9 .27.2 $fit 0-- It. 9 3.t> % Glassies Avg. Microns: z 0 7.7APfColor L: ?7.fL a b 3-0 3 Static Flow: / Technician: 0 ^ I VAB.0001202756 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A xi a vs i s 3h&/<? Customer s Premier Polymers 3001 Wattersan Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship :Date 3 Ml Produc t VISIA Lot No Order No Trailer No OOa&ZlO'OOO T' BUS Propertv Moisture, 7. Test Method ABR-1A Hard Particles> @ 7 min. ABR-12 Bulk Density, gm/cc f Barbender Dry Time, min. ABR-2B ABR-07 Particle Size Dist. ABR-3 40 mesh 0-0 Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Ana1 vsis , // Z .527 200 mesh g.7 M Pan M. rvisor/Lead VAB.0001202757 o3 a9 GC O9. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERT I I CATE OF ANALYSIS A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G_ Haefner Ship Date: Product: Lot No.: Order No.: 0OO82SV -OO/ Trai1er No.: Property Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh >. O ABGC-26 ABR-10 Analysis . /& . S7Q 200 mesh /JS' Pan 'tO Polyvinyl Chloride, Virgin Resin, Not Reprocessed. tory Supervisor/Lead 4 VAB.0001202759 PVC BULK TRAILER ANALYSIS A Date__3-LZzll- Customer Pf e m/v-'T Pmrinet S~2-Z- Silo 6>n Technician MOIST CONT. Toe Bottom I Top Bottom I lo 1 GEL 1. FRONT 2 2. II Trailer Number. Time Order No. T7!*? BULK DENSITY I , T70 DRY TIME 1 COLOR L = %.r^ vise A -- /, O II B= L= RVCM A- 2. B= I II I L- END A= B* * Particle Size Distribution: Screen Analysis Mesh Size /o 40 Min On Rotsp shaker. 49 gms. Rasin plus 1.0 gms. Carta 60 so 100 120 140 200 Glassy Pan Part. Grosa Wt. Tare Net Wt. H on Mesh Ot oo 0>Q JZ^ .z OO n.e ii.vr tt.TM 2-i.r !0.<H (,'l^C 20. f A?. jT 7L.ZU . S' Screen Analysis Min. On Rotap shaker 49 gms. Resin plus Mesh Size 40 60 80 100 120 1.0 gms. Carta Pan 140 200 Glassy Part. Gross Wt. _________ _________ _________ _________ _________ _________ _________ _________ Tare Net Wt. h on Mesh _________ _________ _________ _________ _______ _________ _________ _________ _________ _________ _________ _________ _________ _________ _________ ____ _________ _________ Remarks VAB.0001202760 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERT I I CC FA "T E OF FAMFAL-V'SIS Date: Sfltefo-Z. Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship *Date 2hzh Product: 5325 VKIA Lot No Order No . : Q 00*711 *1-000 Trailer No Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR--1A ABR-2A ABR-3 40 mesh b.0 ABGC-26 ABR-10 ABR-- 16> Ana lysis 24 200 mesh 133 .21 2 L.6 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor ory S visor/Lead 4 VAB.0001202761 I 1 s : 8 3 |I -- >< 2 I 8____| 4-- 1 ^1la____ |l M " S*J ilj H- I Bulk ' G./C.C, k |jj| l O) o f i % 4 4 k Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601) 369-8111 A cert i x cc fa ~r e: of ANALVS I s Date: 3jlO>I^Z^ Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date Produc t Lot No.: Qi4''7ff Order No.: QOC) *711 Trailer No.: ~T-fe36>& Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-1A ABR-2A ABR-3 40 mesh 0,0 Ana 1ysis , 50 (a'L-l 200 mesh 5T6 ABGC-26 ABR-10 ABR-16 <Ho9> S7 z .o 4 Pan //? Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Hi____ rvisor/Lead VAB.0001202763 u mO O o. * c ft M > o3 a C CL m(am J02764 3 dSI * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369 8111 IFIC CD A l\l Ai V S X s A :M Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date 5 v3/12, VIS1AProduct: 5265 Lot No 0&03 Order no .: o/-ooo T- DIZITrai1er No. : Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh D-D ABGC--26 ABR-10 Analvsis .11 200 mesh 9.6 ____ Pan 2-2 Polyvinyl Chloride, Virgin Resin, Not Reprocessed OL rvisor/Lead VAB.0001202765 MM lA Ia o3 "O am O CL O) o o Q. (0 w c > a am*CA 30 cc C* a<3. \ A C(|l202766 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A X I CC ^ Date : 3h(*foZ- Customer: Premier Polymers 3001 Watterson Trail P. 0- Box 99571 Jeffersontown, KV 40299 Attention: L. G. Haefner Ship Date: PvJ V' S I MUK Product: Lot No often Order No. : Trailer No. : Propertv Moisture, 7. Test Method ABR-1A Hard Particles @ 7 min. ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min. ABR-07 Particle Size Dist. ABR-3 40 mesh D-D Residual VCM, ppm ABGC-26 Inherent Viscosity ABR-10 Ana 1vsis . 7.0 ____________________ 57/ 200 mesh 3.3 . 02S~ I.ISL Pan ervisor/Lead VAB.0001202767 f  -nr I * w MMMIM Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 \ A Date: March 12, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: March 11, 1992 Product: 5225 Railcar No.: ACFX 41180 Order No.: 0006956-001 Property Moisture, % Inherent Viscosity Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.19 0.52 0.00 8.6 2.1 1.973 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Laboratory Supervisor wenMnemi* Mi MM MM>M^MM i VAB.0001202769 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date F*VC RAILCAR ANALYSIS Product: 3?25 . QIlP Car No Time Logged In: Ship Date: Logged In By: Order No: - 60 i Silo(e): Customer ; l K. CtM - &Mstiee Compartment Sample From A Bottom l Moisture BL Contamination BB .If /3 Bulk Density BD w/antistat .!*(* t 7,l Viscosity RVCM /.W CA Bottom JM. ,/<r ttf ?</ .8*? CB B Bottom s J*f Bottom J7 2 / .0? Jf to / .3 73 5/S /.4*t .5/< (.4ot Tappi Test Contarnination Composite .06 or less Screen Analysis Mesh 40 60 80 Weight % 0-00 m .07 . 15 .20 .60 100 120 140 200 Pan /2S3 IV. 9Q <L7l_ /-ol o?. ( CPA: Color L: 94/f % Glassies: a A/6 b >c/ Avg. Microns: J*W.g Static Flow / 7 S Technician: VAB.0001202770 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I F7 X C2 T EE OF ANALYSIS A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L- G. h zShip Date sluh Product: 522!: Lot No A//A Order No.: C)0&~OOO Trailer No.: Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh 0.0 ABGC-26 ABR-IO Ana1vsis // 200 mesh 96 Z.kc> .57 Pan 2.6 Polyvinyl Chloride, irgin Resin, Not Rep essed. r/Lead 1 VAB.0001202771 PVC BULK TRAILER ANALYSIS A Customer Technician Co / Trailer Number. Time 0^53 O Order MOIST CON'T. I2E Bottom j Top Bottom I // I 77 GEL I BULK DENSITY I DRY TIME I COLOR l = 9tn FRONT 2 I. A= 2. B -l.?L I II I L* vise RVCM 'jt/ous MIDDLE i END A= B* l I I I L- A* 2. B Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Resin plus 1.0 gnts. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 00 0 .O 60 80 100 120 140 200 fKO 7.91 /ins t!(,(? 7.1/ o- X) IS.8 5SS 271 1.8 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 60 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. fm Glassy Pan Part. Remarks______________________________________ j1 VAR 0001707777 Vista Polymers A Division of Vista Chemical Company CERT I F7 X Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 OF ANAI__ V'S X S A Date:3 HZ* Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention L. G. Haefner Ship Date Product: Lot No.: Order No . : Q0O ~7(?03 " OO 0 Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh &>.0Q ABGC-26 ABR-10 Analvsis .04 . S.3 $ 200 mesh /Zl . 030 __ bb Pan 20 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Lab tory Supervisor/Lead VAB.0001202773 4 ' i urn VP 02774 { i< v 4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 C2 EZ R T I R" X CATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: MojuX 4 Product: 5305 Lot No.: Order No. Trailer No.: ~ 00& >^2> Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 ABR-10 Ana lysis ./ ..57 / 200 mesh /D. 9 .0/3 . 72. Pan J.S Polyvinyl Chloride, Virgin Resin, Not Reprocessed. oratory Supervisor/Lead 4 VAB.0001202775 Date Customer Technician PVC BULK TRAILER ANALYSIS Product S3 OS' Trailer Number Time V Order A Particle Size Distribution: Screen Analysts Mesh Size 40 Gross Wt Tare Net Wt H on Mesh 0.0 0,90 Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min shaker gins Carb Glassy Pan Part. 60 100 120 140 200 D. OS -&-L. Min. //.r / j/r 11A -23.3 3&J- On Rotap shaker 49 gms. Resin ptus 13 /0,9 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks VAB.0001202776 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFIGATE OF* Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANTAL,YS X S A Date: March 5, 1992 Customer: Premier Polymers 3001 Watterson P.O. Box 99571 Jeffersontown, KY 40299 Attention L. G. Haefner Ship Date March 2, 1992 Product: 5415 Railcar No: VIPX 45872 Order No.: 0007269-000 Property Moisture, % Bulk Density Brabender Dry Time, Mins Particle Size, % on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.18 0.504 4.8 0.00 5.2 1.6 0.014 1.01 Laboratory Supervisor (601) 369-3624 % VAB.0001202777 Vieta Polymers Highway 25 Aberdeen, MS 39730 A RA ILCAH ANALYSI S Load Date: a-*?''? Product: Time Logged In: e>^o o Logged In By: Ship Date: Order No: HTJoi-c co Car Ho. Silo(s): Customer: Compartment A Sample From Bottom Top Moisture % BL Contain inat ion BR Bulk Density Hard Particle Viscosity RVCM Sol I Log. Mk CA Bottom Top UL aJ .sol CB Bottom Top ./r u .sol / B Bottom Top Mi xJ Screen Analysis Mesh Weight 40 Q?0 % <0$ 60 .oa. 80 17.71 100 120 hs.^ l.w 2 n. i 140 200 Pan L4.0T 2* $$ .7/ JL / s.a . JM. Drytime: IlS Static Flow: 0 / Avg. Microns: M21 Color L: /00* ff a ao(> b /.ZI Technician: METS Is S' iU.C% VAB.0001202778 m p-'""'' r---- *t" mmmmmmwmm -J Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 A II ANA V' S3 X S Date = 2- Customer: Premier Polymers 3001 Watterson Trail P. . Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner 3= A02*Ship Date VISIA Product: 5305 Lot No Order No Trailer No qoo&cm-mo 7 Propertv Moisture, '/. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0-> ABGC-26 ABR-10 Analysis , /5 200 mesh . oof J21=l Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed visor/Lead vmmmmm T VAB.0001202779 T o N r* i si (V a i u3 mg O CL O) o a> a (0 CO c > a oc a W *24M A V Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jefiersontown, KY 40299 Attention: L. G. Haefner dfejfzShip Date: VIS1AProduct: 5265 Lot No.: Order No. : 00Cf~$*73 "0C& Trailer No. : 0L&2. Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 ABR-10 Ana 1vsis .5?4 200 mesh /Z. 7 02,4- Pan Z-3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 4 VAB.0001202781 3 oc a. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adetdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: February 24, 1992 Customer: Premier Polymers P.0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: February 18, 1992 VBIA Product: 5225 Railcar No.: GACX 73412 Order No.: 0006956-000 Property Moisture, 7. Inherent Viscosity Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10 ABR-3 ABGC-26 Analysis 0.07 0.53 k- 0.00 6.3 1.9 0.001 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. . Bagwe Laboratory Supervisor i MW wmmmmmmmmmmmmmmmmmmmmmmrrnm wmm VAB.0001202783 Viata Polymers Highway 25 Aberdeen. MS 39730 A RAILCAR ANALYSTS Load Date: Tine Logged In: 0U3Q Product: Logged In By: Ship Date:. Order No: Car No.: 73 V/2- Gey Silo(6 Uo COO Customer: lf\JLV)MJLA Compartment Sample From Bottom Moisture BL Contamination BR .O 7 Z.. Bulk Density BD w/antistat Viscosity RVCM ,LOO Bottom . o (& ? 370 ,530 .SOI Bottom ,0 3 / 3(p7 Bottom .0b 2. Tappi Test . 06 or less .07 . 15 .20 Contamination Composite % Screen Analysis .60 Mesh Weight % 40 #.><? 0.0 60 OJO 80 ni 100 /4.t>7 120 14.7? 08-S 140 8.43 70-8 200 3J7 Pan 0.90 CPA 13s~ % Glassies Z* /'/# Avg. Microns: J//9 Color L: 97.S7 a /' b Static Flow: Q / 2L. Technician : (?) ^ S'S. VAB.0001202784 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: z/z4*/<? Z- Customer: Premier Polymers 3001 Ufatterson Trail P. 0. Box 99571 Jeffersontown, KV 40299 Attention: L. G. Haefner Ship Date VISTA Product: 5305 Lot No.: Order No.: C)C&^& Trailer No. :7^- Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ob ABGC--26 ABR-10 Analysis /s~ .57T 200 mesh uq sDS& 13 Pan 3.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor /Lead VAB.0001202785 ooCM S co o M * 5 8 N Si o a. 8 8 Kr> 3 CM <N ?y 3 a si N *0 N <k o 4 O <>t ro BO O C *23* mt> C CL * Iflptl p WWi -^1 V>, rvA A- K o VAB. 000 f202786 imm W*. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adendeen, Mississippi 39730-0091 Phone (601) 369-6111 CERT X F7 X CATE OF ANAL VS I S Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date = 2~}2A\C1-2- Product: 5225 Lot No. Ajjfr Order No.: 0006>8(-~00l. Trailer No.: 3*1! Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR--3 40 mesh h.O ABGC-26 ABR-10 Analysis , /> . 200 mesh > bfab , 52- Pan IA Polyvinyl Chloride, Virgin Resin, Not Reprocessed. a Laboratory Su ml visor/Lead VAB.0001202787 l?i*h PVC BULK TRAILER ANALYSIS A Date Customer Technlcuin AJO fllTL_ FRONT Product 6 VO MOIST CONT. 12B. './0 \ m# % i Bottom I Top [// At Bottom 2. GEL t. II Trailer Number. ~7~ 37/ Time <23*0 - 2330 Order No. OOOQ>Z\Z~bC> BULK DENSITY I DRY TIME I COLOR vise RVCM a-/. 3/ B= 0 i L= O 78 MIDDLE 2. A= B= i iI I L= END A= B= Particle Size Distribution: Screen AnalysisMin On Rotap shaker. 49 gms. Rasin plus 1.0 gms. Carb Mash Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tara Nat Wt. H on Mash 060 /> /Q.4( /zSO U.23 L-to 2.2< & 72. &.Z, 20$ 3L& &t,l /2$ Screen Analysis Mash Size Gross Wt. 40 Min. On Rotao shaker 4fl aim Resin oius 1.0 ami. Carb Pan 60 80 100 120 140 200 Glassy Part. Tara Nat Wt. H on Mash Remarks VAB.0001202788 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: Customer: . 2V f * Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: fxjp. Product: 5265 Lot No. : Order No. : OOOfeftfdL*&0C) Trailer No. : /-^ Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 ABR-10 Ana1vsis .04 577 200 mesh Jo-5' - OO! (^4 Pan /. 3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. rvisor/Lead VAB.0001202789 T A o> o o 1? Q. 03 CO c > & 01 o e O3 cc o CL imvmv iffffflP m tMKMMlM a VAB.00012S2790 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A c9l<oh Date IFICA O PtU&oe, Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 VS I S Product: 5325 Lot No . VIS1A Attention: L- G. Haefner Date of Shipment: ~To i iton* Order No. Trail er No. cobifftfi' 0 *7^5^ Proper ty Moisture, V. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-^| ABR-2B ABR- 40 mesh OD ABGC-26 ABR-10 ABR-16 Analysis 200 mesh !3.Co 132S . Qlo(p L si zes Pan 3.3 L0C/3 rvisor/Lead flat ss-jlttAA QjL^&7^ sic. fklsrct. k/unA Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 IFIC O Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 VS I S Date: f'do.n, Customer Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G- Haefner Ship Date: VIS1AProduct: 5225 Lot No /Va- Order No. : 00O^>/St Trailer No Property Moisture, 7. Bulk Density, gm/cc Particle Size Dist Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 ABR-10 Analysis .07 200 mesh 1L& AF7 Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. miw supervisor /Lead VAB.0001202792 Date ^ Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ O Trailer Number. Time Order No. 0OO&> %! 9- -0<Df Particle Size Distribution: Screen Analysis ------ Mesh Size 40 Gross Wt. Tare p --------- ---- Net Wt. % on Mesh 0.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb SO 80 100 120 140 200 Glassy Pan Part. 03:- y.?/ /#-&? /i. 4? J&fo 0.0 7-2 U. </ 30 o <2<f. 2_ //, ? 2$ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 90 100 120 140 200 Glassy Part. Remarks. VAB.0001202793 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ^M#=*L_V'SIS Date: f3f Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: f'cb. 13, VBS\ Product: 5305 Lot No Order No Trailer No 0OO& ^3'Oocy (o5Z~ Propertv Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh mJl_____ ABGC-26 ABR-10 Ana1vsis svR____ 200 mesh <..2, _____.004 .72- Pan ./ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. isor m mmmm VAB.0001202794 Date -t 3 -9 Customer Technician PVC BULK TRAILER ANALYSIS Product Silo Trailer Number Time A Particle Size Distribution: Screen Analysis Min Mesh Size Gross Wt. Tare Net Wt. 46 on Mesh Screen Analysis 07- <p.o __ Min. Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 60 _________ _____ _________ ______ _________ ______ _________ _____ On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carto 100 120 140 200 S3- 7 / ZZM- - ' /*3 27? . IS- 2- /S S On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb SO 100 120 140 200 4MP Glassy Pan Part. S.Q3_________ a.f _ Glassy Pan Part. Remarks. % VAB.0001202795 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A IF I VS X S : j/t ihz Date Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Shi p Date: (d/Sifa^ VISIA Product: 5305 Lot No OfBIZ Order No Trailer No. GDOb9b'<000 7loo Property Moisture, V, Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh ABGC-26 tui ABR-10 Analysis .n .51/ 200 mesh fo-c> /DZ- .73 Pan A.l Polyvinyl Chloride, Virgin Resin, Not Reprocessed isor/Lead VAB.0001202796 * *t ............................................................................................. ........... - ........... " 1 ----------- - 11 1 1111 4J6gbnd ]M Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERT I R I C^TEE OR ANALYSIS A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G_ Haefner Ship Date: Q-!IaJ4 sk Product: 5225 Lot No Order No.: 000,&/ - OOO Trailer No-: 3'7/ Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh 0.0 ABGC-26 ABR-10 Ana 1ysis o 200 mesh 7. .oo4' .5/ Pan .! Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Of visor/Lead VAB.0001202798 pte Z-/Z-4L. Customer PreW Technician PVC BULK TRAILER ANALYSIS Product Trailer Number. T-J-?/ 0o A Particle Size Distribution: Screen Analysis_____ LQ.Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh Screen Analysis 40 o*o o 0. 0 60 80 too 120 140 200 .01 .2 Min. 7. 7</ /?,f / ts.ot Art 3. it / J1C 2 7. L 29*9 /?'/ On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 60 80 100 120 140 200 Tare Net Wt. % on Mesh Glassy Pan Part. Ao9 2>.i ____ ____ Glassy Pan Part. Remarks VAB.0001202799 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 CERT I F I CATE OF ANAI__V'S I S February 14, 1992 Customer: / Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY ' 40299 Attention L. S. Haefner Ship Date February 10, 1992 Product Railcar No GACX 73408 Order No. 0006811-000 Property Moisture, 7. Bulk Density Brabender Dry Time, Mins Particle Size, 7. on 40 Mesh 200 Mesh Pan Residual VCM, PPM Inherent Viscosity Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABGC-26 ABR-10 Analysis 0.08 0.507 5.0 0.00 4.2 1.5 0.024 1.02 my t. pagwell Laboratory Supervi sor (601) 369-3624 * VAB.0001202800 Viata Polymers Highway 25 A Aberdeeni MS 39730 RAILCAR ANALYSIS Load Date: -f-9z Product: Time Logged In: /<ft3o Logged In By Ship Date: 2\\ bk^ Order No: Car W. = 73 Sllo(e) : - 660 Customer: 6-&0 ^7/ AloTXshiL-' Compartment A Sample From Bottom Top Moisture % 7 BL Contamination BR 3 Bulk Density 7 Hard Particle 5 X' / Viscosity RVCM l.Dtb ,01^ CA Bottom Top oL sr .Sole CB Bottom Top .o$ tj>/Pv B Bottom Top 3 Screen Analysis Mesh Weight % 40 cf: && 0*Q 60 o.gfj U_ 80 m 100 120 12 140 200 4hZ Drytime: Static Flow: t L Avg. Microns Color L: 1*1.06 a Q.oS b 113 : METS %<4- z i2oA & Pan 0.73 us Technician: tmrnm--mrnimmmm VAB.0001202801 I mt M Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 11 CERT I E I CATE O F7 ANALYSIS A Date: (lo/4Z- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: <P// o ha. Product: 5305 A) jLot No.: Order No.: 00OC?*&>/-OOf Trai1er No.: Property Moisture, 7. Bulk Density, grn/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-H ABR-2B ABR--3 40 mesh ABGC-26 ABR--10 Ana 1ysis . /o_____ .572- 200 mesh Lb .00/ .7X Pan A3 Labor VAB.0001202802 Date Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ S?o i Trailer Number. Time /4/i Order No. T A / Particle Size Distribution: Screen Analysis lo Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis 40 b.a* 0.0 Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. ... t.Cf <L f,Z /J. S'/ 2-7. 2 40 tr.t J.SZ, 4.6 . CJ A3 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001202803 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE O Fr ANALYSIS A Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. S. Haefner Date of Shipment Produc t: Lot No.: Order No.: DOO/olSU-dOC. Trailer No Propertv Moisture, '/. Test Method ABR - //f Hard Particles @ 7 min. ABR-12 Bu1k Density, gm/cc ABR-2B Barbender Dry Time, min. ABR--07 Analvsis '0*5 4 .4w 4..7 Particle Size Dist . ABR-3 40 mesh 0.0 200 mesh 77 Pan Z-i> Residual VCM, ppm Inherent Viscosity ABGC-26 ABR--lO Not more than 8.5 PPM This material was produced to yield an inherent viscosity in the range of_ an , Labora VAB.0001202804 \ \ (N [A In \a o 3 m2 Q CL O) o a> Q. co 05 c mm* > 1 l om CL VC CL ..................... ** MmniHvmMMi* ** .k A <20 I Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A TFIC ANALYSIS Date : g!to h'Q- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Hag'fner Date of Shipment: Product: VISIA Lot No. : 04P,Z<O Order No.: ooa&^-ooo Trailer No Proper tv Moisture, */. Test Method ABR-//} Hard Particles @ 7 min. ABR-12 Analysis Bulk Density, gm/cc ABR-2B Barbender Dry Time, min ABR-07 Particle Size Dist. ABR 40 mesh 0.0 200 mesh tt.O Pan S' Residual VCM, ppm ABGC--26 Not more than 8.5 PPM Inherent Viscosity ABR--10 This material was produced to yield an Minheren t viscosit the raannagte o f an M in / / labora Superfv i so r / Lead VAB.0001202806 t -A ia o T33 9 O OL O) O 0) CL CO w c Ol CL 3 3 OC CL i\ fWHPHHIt i VAB.QOO12028Q.7 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIFICATE OF ANALYSIS Produc t: S%>:T Customer: Attention: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY L. G. Haefner 40299 Date of Shipment *&/?7/ Trailer No. : S77A Lot No.: Order Mo.: OCObT&f-ooo Property Test Method Moisture, X ABR-1A Bulk Density ABR-2B Brabender Dry Time, Mins ABR--7 Particle Size, X on ABR-3 40 Mesh 200 Mesh Pan Residual V/CM, PPM ABGC-26 Inherent Viscosity ABR-10B Ana lysis J_0 ,0tj_ !J3 ai Labor VAB.0001202808 rr> cC Vista Polymers A Division of Vista Chemical Compony Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: zl4fa Z- Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G- Haefner Ship Date: VIS1A Product: 5305 Lot No.: Ajffir Order No.: 0oo^4-^l-oo6 Trailer No.: Property Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-1A ABR-2A ABR-3 40 mesh D.o ABGC-26 ABR-10 Analysis .os sie> 200 mesh 2.6 .OSS' .73 Pan /4 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. % VAB.0001202810 J Customer PVC BULK TRAILER ANALYSIS A Panicle Size Distribution: Screen Analysis 40 Tare Net Wt % on Mesh 0X0 0~O& Screen Analysis Mesh Size Gross Wt Tare Net Wt h on Mesh 40 Min On Rotsp shaker. 49 gms. Resin pius 1.0 gms. Carb 60 80 100 120 140 200 /.o /P 32*2 /r.z. v.<P MS 4J7 J2.S5 /7S7 &J 1. S 2.5.1 3LO 2o.9 to Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carto 60 60 100 120 140 200 Glassy Pan Pari. o.to /.6> Glassy Pan Part. Remarks MM m *I VAB.0001202811 r* Vista Polymers A Division of Vista Chemical Company High 25 Post ce Box 91 Aderdeen, Mississippi 39730*0091 Phone (601} 369-8111 A CER I I O *=rvi^ vs i s Date: PtbruuGUru 3( Customer: Premier Polymers 3001 Ulatterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G Haefner Ship Date: {'tjDOUUU 5/ VIS1AProduct: 5305 Lot No Order No Trailer No Mjpr <3m -060 Propertv Moisture, V. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-2B ABR-2B ABR-3 40 mesh D. O ABGC-26 ABR-10 Ana1ysis .02~ -57(0 200 mesh 7c5- & ,76 Pan (/> i($ sor/Lead f VAB.0001202812 Date Customer Technicia PVC BULK TRAILER ANALYSIS Product Trailer Number 7/ Time Order sin Oeoswz-odd A Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh Q.OO G-0P Screen Analysis ^a 0.0 Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 0.65 192- /43/ /S'. 72 //-Z5 S22 0,1 7-2 20 6> 3f . 2 23-5 /l.6 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 0.2 /&J3 SV 60 80 100 120 140 200 Glassy Pan Part. AS2. 2b f/,, O Glassy Pan Part. Remarks 7 4^/07 WWHMPMNWMfWWM* T Mi tWUfWf VAB.0001202813 Vista Polymers A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-6111 A CERTIFICATE OF ANALYSIS Date: //z 3/fp- Customer: Attention Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY L. G. Harfner 40299 . ijz/ho. Date of Shipment Product: 5265 : 7SZ7 Trailer No Lot No : QH&fl Order No.: VISTA ooo Property Moisture, */ Inherent Viscosity Particle Size, '/. on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10B ABR-3 ABGC-26 Analysis 0.0 4S /A .60! lsor/Lead VAB.0001202814 I u 51 O CL. CD O * 3 b a cc a. > 02815 Vista Polymers A Division of Vista Chemical Company IFIC Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601J 369-8111 A N ^ V' S T S \ A Date: i/nfa'i' Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: lilt* fat- VISTAProduct: 5305 Lot No Order No Trailer No C00577S-000 8Z47 Property Moisture, */. Bulk Density, gm/cc rticle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-2B ABR-2B ABR-3 40 mesh 0-0 ABGC-26 ABR-10 Ana 1ysis db 200 mesh g.o oo! 75 Pan /7 Laborat Supe or/ VAB.0001202816 3o cc amn. T> C % whmm *m MM r*\ 5*> Ml mw VAB.OtDS1202817 ' -ii PMHDilN W Vista Polymers A Division of Vista Chemical Company I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A ANAL. YS X S Da te Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: / /ft, h ^ Product: 5305 Lot No.: 0425*1' Order No.: Trailer No.: ^^ Propertv Moisture, */. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-2B ABR-2B ABR-3 40 mesh D-D ABGC-26 ABR-10 Analysis ,5Z1 200 mesh .00/ >73 Pan / VAB.0001202818 0m1 CO 03> cc <O0l a xri jO JE CD => vpn l -O VAB.OO1 I'm ** 2M Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 CERTIFICATE OF ANALYSIS A Date: / j f'l Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Harfner Date of Shipment: / //(/?/^2- Produc t: 5345 Lot No.: 040/3 Order No.: 0005173 - 000 Trai1er No.: Propertv Moisture, V. Test Method ABR-2B Hard Particles @ 7 min ABR-12 Bulk Density, gm/cc ABR-2B Barbender Dry Time, min ABR-07 Particle Size Dist. ABR- 40 mesh 0-0 Analvsis .440 4& 200 mesh Pan Residual VCM, ppm Inherent Viscosity ABGC-26 ABR-10 Not more than 8-5 PPM This material was produc ed to yield an inheren t viscositv .in the ran of an VAB.0001202820 \ wmimv wmmmmmmmmmmmmmmimmmn i p>^--ww ........... ... Visto Polymers A Division of Vista Chemical Company c:e:f?t x Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 x cate of analys i s A Date: Customer: Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Date of Shipment Ja^. i3. Product: 5325 VISIA Lot No. : Order No.: 0004469-006 Trailer No.: Proper ty Moisture, V. Bulk Density, qm/cc + Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-2B ABR-2B ABR-3 4C) mesh 0.0 ABGC-26 ABR-10 ABR-16 Ana Ivsis .401 200 mesh ?-/ / 4-2.1 , 0SL> .>! Pan _jA 25:7 Labora to dJ Supervisor/Lead VAB.0001202822 s * o VAB.0001202823 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Ix Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 a a VS I s A Date: Customer Premier Polymers 3001 Watterson Trail P. 0. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Date of Shipment: ihfaz. Product: 5325 VISIA Lot No 04057 Order No.: <0002-9/8 -0C> /Trai1er No T- iso, Proper ty Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Average Microns Residual VCM, ppm Inherent Viscosity Cold Plasticizer Absorption (CPA) Test Method ABR-2B ABR-2B ABR-3 40 mesh f).0 ABGC-26 ABR-1O ABR-16 Ana 1ysis .09 200 mesh 4# l49.o '05! ,0Z Pan LS r%' Super ill or/Lead VAB.0001202824 VAB.0001202825 \n \ i. Q CL VAB.0001202826 AJtawA4 34M Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: ihfa'i* Product: 5265 VIS1A Customer: Attention: Premier Polymers 3001 Watterson P.0. Box 99571 Jeffersontown, KY L. G. Harfner 40299 Date of Shipment: ibh'L Trailer No. Lot No. Order No. coo zxcti' -oo2- Property Moisture, V. Inherent Viscosity Particle Size, V, on 40 Mesh 200 Mesh Pan Residual VCM, PPM Test Method ABR-1A ABR-10B ABR-3 ABGC-26 Analysis .n . bU> 0-0 2 l* l .DO! sor/Lead VAB.0001202827 r CK ) S') ( I a u 3 o 2 O CL *Ni PBM -I 'I M* IN 4 II il A L^ O) o a> o <A CO 0) c > a pQ<X&lP o 2 oc a. ?! E co 2:> 3 VAB.Oflm202828 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: kJo^L Z, Customer: Premier Polymers 3001 Watterson Trail P. O. Box 99571 Jeffersontown, KY 40299 Attention: L. G. Haefner Ship Date: JjQm. 7, mz- Product: 5305 Lot No.: Aftfir Order No.: 0065034-001 Trailer No.: Proper ty Moisture, 7. Bulk Density, gm/cc Particle Size Dist. Residual VCM, ppm Inherent Viscosity Test Method ABR-2B ABR-2B ABR-3 40 mesh 6-00 ABGC-26 ABR-IO Analvsis / -ji_______ 546 200 mesh oot .15 Pan --------r /A 'Laboratory r/Lead VAB.0001202829 PVC BULK TRAILER ANALYSIS Date 7.-9 f Customer Technician Product Silo^_ FRONT MOIST CONT. Top Bottom I Top Bottom II GEL I. s~ 2. 2. Trailer Number O Order No. BULK DENSITY I. DRY TIME I COLOR I MIDDLE END i ii A= , B= i. i i i L - A B= k vise RVCM Particle Size Distribution: Screen Analysis Mesh Size Gross Wt Tare Net Wt. % on Mesh Screen Analysis 40 60 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. t>fiS Y-2Z /I.SV /l.tL /A IX 4 M~t 3S'. 7 ati 23- Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 6-12. LA Glassy Pan Part. 7"1 Remarks Star 207A Revised 1/12/87 VAB.0001202830