Document 2Ryav49D99axXDLoOdakd4QOb
PFOA and Associated Salts
Environmental Fate and Transport Title
Technical Report Sum m ary - Assessm ent of the Bioaccum ulative Properties o f Ammonium Perfluorooctanate: Static (fish test)
Laboratory or Author
3M Env. Lab
Completion T y p e Date Robust summary, technical report, ' critique by J. Giesy
5/31/95 (M SU )
Ecotoxicity Elements Title
96-hour acute static toxicity to fathead minnow ;_FC-143
Laboratory or Author
3M Env. Lab
Completion T y p e Date
6/29/74 R obust sum m ary,
copy of data sheet
96-hour acute static toxicity to fathead m innow - F C -26
3M Env. Lab
11/10/74
Robust summary, copy of data sheet.
96-hour acute static toxicity to bluegill sunfish - F C -143
3M Env. Lab
4/8/78
Robust summary, copy of data sheet
96-hour acute static toxicity to bluegill sunfish - F C -143
3M Env. Lab
Two reports : "The Effects o f Continuous Aqueous
Exposure to 7 8 .0 3 on Hatchability o f Eggs and Growth
and survival o f Frv o f Fathead Minnow fPim eohales
Drom elasV and "Sum m ary o f Histopathological
Exam inations o f Fathead M innow (Pim eDhales Dromelas) EG & G Bionomics,
Exposed to 7 8 .0 3 for 30 Days".
W areham , MA
Technical R eport Sum m ary - Aquatic Toxicity Testing: FC-
143 (Lot-37) L.R. 56 2 5 S
3M Env. Lab
Toxicity to activated sludge - F C -143 Technical Report Sum m ary - M ulti-Phase Exposure/Recovery Algal Assay Test method (F C -143)
48-h o u r acute static toxicity to D a p h n ia m a g n a - F C -143 (3 studies on diet) Chronic Toxicitv o f Fluorochemicals to DaDhnia m aana (W ater F lea) - F C -143, and statistical analysis of data provided b y A S c I Corp., Duluth, M N
3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab
5 /2 7 /7 8
June 1978 and Sept.
1978
5/8/80
6/4/80
11/16/81 5/5/82, 5/6/82, 6/2/82
8 /3 1 /1 9 8 4 , 8 /1 0 /9 8
Robust summary, copy of data sheet
Robust summary, copies o f two final reports. Robust summary, technical report Robust summary, copies of data sheets Robust summary, technical report Robust summary, copies of data sheets Robust summary, { sum m ary report, ; letter report
96-hour acute static toxicity to fathead minnow - FX-1001
3M Env. Lab
2 /2 /8 5
Robust summary, copy of data sheet.
003732 I *
PFOA and Associated Salts
i
Ecotoxicity Elements Title
Activated sludge respiration inhibition (O E C D 2 0 9 ) - F C 126
Microtox test - FC -126
48-hour acute static toxicity to D a p h n ia m a g n a - F C -1 2 6
96-hour acute static toxicity to fathead m innow - F C -1 2 6 A ctivated sludge respiration inhibition (O E C D 2 0 9 ) - F X 1003
Microtox test - F X -1003 Static Acute Toxicity o f F X -1 0 0 3 to the Fathead Minnow, P im ephales prom elas Static A cute Toxicity of F X -1 0 0 3 to the Daphnid, D a p h n ia m agna Growth and Reproduction Toxicity Test with N 2803-3 and the Freshw ater Alga, S elen astru m capricornutum Acute Toxicity o f N 2 8 0 3-3 to the Fathead Minnow, P im ephales prom elas Acute Toxicity o f N 2 8 0 3-3 to the Daphnid, D a p h n ia m agna
Microtox test - FC -143
Microtox test - F C -1 18
Microtox test - F C -1015-X
Laboratory or Author
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab E nviro S ystem s, Hampton, New
H am p shire E nviro S ystem s, Hampton, New
H am p shire T .R . Wilbury Laboratories, Inc, Marblehead, MA T .R . Wilbury Laboratories, Inc, Marblehead, MA T .R . Wilbury Laboratories, Inc, Marblehead, MA
3M Env. Lab
3M Env. Lab
3M Env. Lab
Completion T y p e Date
Robust sum m ary,:'
copy of data
!
4/20/87 sheets.
'1
Robust summary, 1
copy of data
4/29/87 sheets.
Robust summary,
copy of data
4/30/87 sheets.
Robust summary,
copy of data
5/1/87 sheets.
Robust summary,
copies o f data
2/16/90 sheets
Robust summary,
copies of data
3/7/90 sheets
Robust summary, :
final report,
3 /1 5 /9 0 protocol
Robust summary,
final report,
4 /9 /9 0 protocol
1/24/96
Robust summary, final report
1/24/96
Robust summary, final report
3/7/96 4 /2 4 /9 6 4 /2 4 /9 6 4 /2 4 /9 6
Robust summary, final report Robust summary, copies of data sheets Robust summary, copies o f data sheets Robust summary, copies of data sheets
C03733j
<
PFOA and Associated Salts
Ecotoxicity Elements Title
Activated Sludge Respiration Inhibition T est - F C -1 0 1 5 -X Acute Toxicity of F C -1 0 1 5 to the Fathead Minnow, P im ephales p rom elas Growth and Reproduction Toxicity Test with F C -1015 and the Freshw ater Alga, S elen astru m capricornutum
Acute Toxicity o f F C -1015 to the Daphnd, D aph n ia m ag n a
Laboratory or Author
3M Env. Lab T .R . Wilbury Laboratories, Inc, Marblehead, MA T .R . Wilbury Laboratories, Inc, Marblehead, MA T.R . Wilbury Laboratories, Inc, Marblehead, MA
i<
Completion T y p e Date Robust summary, copies of data
4/25/96 sheets
5 /1 5 /9 6
Robust summary, final report
5 /1 5 /9 6
Robust summary, final report
5 /1 5 /9 6
Robust summary, final report
Summary Reports
Title Technical Report Sum m ary - Final Com prehensive Report: FC 143
Laboratory or Author 3M Env. Lab
Completion Date
3 /2 3 /7 9
Type
Robust summary, technical report
! <i 4
( '{
003734
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i
ACUTE TOXICITY TO FISH
TEST SUBSTANCE
Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC116, FC-126, FC-169, orFC-143. (Octanoic acid, pentadecafluoro, ammonium salt, CAS # 3825-26-1)
Remarks: The 3M product lot number was 83. The test sample is FC-143. It's purity was not sufficiently characterized, though current information indicates it is a mixture of 96.5 -1 0 0 % test substance and 0 - 3.5% C, C7, and C9 perfluoro analogue compounds.
METHOD:
Method: Not noted.
Type: Static acute
GLP: No
Year completed: 1977
Species: Pimephales promelas
Supplier: Not noted.
Analytical monitoring: Temperature, pH and DO
Exposure period: 96-hours
Statistical methods: Graphed LC50
Test fish age: Not noted.
Length and weight:
Average length = 2 inches
Average weight = 1.6 g
Pretreatment: Not noted.
Test conditions:
Dilution water: Carbon-filtered City of St. Paul, MN water.
Dilution water chemistry:
Temperature: Not noted.
Dissolved Oxygen: Not noted
pH: Not noted.
Stock and test solution preparation: Not noted.
Concentrations dosing rate: Once
Stability of the test chemical solutions: Not noted
Exposure vessels: Not noted.
Number of replicates: one
Number offish per replicate: Not noted.
Loading rate: Not noted.
Number of concentrations: five plus a blank control
Water chemistry during the study:
Dissolved oxygen range (24 - 96 hours):
4.7 - 5.7 mg/L (control exposure)
4.0 - 4.9 mg/L (50 mg/L exposure)
pH range (24 - 96 hours):
003735
7.0 - 7.1 (control exposure) 6.4 - 6.5 (50 mg/L exposure)** Test temperature (24 - 96 hours): 70 - 72F
RESULTS
Nominal concentrations: Bk control, 10, 20, 30, 40, and 50 mg/L Element value: 96-hour LC50 = 70 mg/L (C.l. not calculated)
Element value based on nominal concentrations
CONCLUSIONS
The test sample 96-hour LC50 for fathead minnow was extrapolated to be 70 mg/L.
Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY
______
Reliability: Klimisch ranking 3. There is insufficient documentation of the methodology. The LC50 was extrapolated from an insufficient number of data points. The general health and age of the fish are not noted. Sample purity was not properly characterized and it lacks analytical confirmation of test substance concentrations.
REFERENCES
This study was conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request number 2340.
OTHER
Last changed: 5/24/00
003736
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