Document 2Rvban6vDwv0mgdZy96b7qGDL
GENERATOR'S WASTE MATERIAL PROFILE SHEET
PLEASE PRINT IN INK OR TYPE (Bit*. 12-piteft).
SUBMITTED TO WASTE TECH SERVICES
DATE:
.Tune-. 16- 1989-
WTS 005.3_____________ Waste Profile Sheaf Code
A. GENERAL INFORMATION 1 Generator Name: ?FC lndusty,1^- Ioc3. Facility AM**: P - B* lUU
Lake Charles. LA (Colombia Southern Road)
6. Technical Contact:
7. Title:
. .
2. 4.
Generator Generator
USEPA ID: State ID: _
LAD 008086506
Tame
5. Zip Code: 70602 8. Phone: (
B. MAIL WASTE TECH SERVICES 2. Company Name: ________________ 4 Address: _______________________ _
INVOICES TO 1. 0 Generating Facility (A, above), or
____________ ____________________________3. Phone: (
)
S. Zip Code:
C. i NAME OF WASTE _________ Trench Clean-out______________________________________ ________ 2. PROCESS GENERATING WASTE Chlorinated hydrocarbon production, WTU
3 Is this waste a Dioxin listed waste as defined in 40 CFR 261.31 <e.g,, F020, F021. F022. F023, F026. F027, or F028)? Yes S No If yes. DO NOT COMPLETE this form.
D. PHYSICAL CHARACTERISTICS OF WASTE
2. Does the waste have a 3. Physical State @ 70* F:
strong incidental odor?
G Solid 3 Sorro-Soiid
No 03 Yes If known. G Liquid G Powder
rtMcnh*- Acrid
Other:
4. Layers: G Multilayered 0 Bi-layered G Single Phased
5. Specific Gravity:
Range: 1.20- 1.25
6. Free Liquids:
Yes G No
Volume: m-sn
%
7 pH D<2 G > 2-4 O 4-7 0 7 7-10 Q 10- <12,5 Q > 12.5 H Range
_________ NA
8. Liquid Flash Point: < 73F 73-99*F CHI 100-139"F 140-199F > 200#F None Closed Cup OopenCup
E. CHEMICAL COMPOSITION
Chloroethane6 Trichloromethane 1,2-Dichloroethane Tetrachloromethane
Trir h 1nrnpfhpnp 1 1 9-Trirhlnrnpthanp 1,1,1fi-Tprrachlnroethane 1 r 1 r 2 . 2-Tfptrahloroethans Tpf.rarhl nrosthene Ppntar.h] nroethane Hpvarhlnroethane H e x a r h 1orobutadiene D-v-^-dich loro benzene
MIN. - MAX.
73706. --2 : 07715
8.5 %
0" 11 %
4 TJ7T79
% %
0.07 - 0.11 %
3- 5 %
0.5 - 1.25 %
1.5 - 3.5 %
1.7 - 2.1 %
1.5 - 3.0 %
2.5 - 4.0 %
10 13 TT5--------- TOT"
%
U n k n o w n chlorinated hydroc arbW*a1-4 7% % Indicate if this waste contains any of the following:
NONE or LESS THAN or ACTUAL
PCB's
C3 < 50 ppm
42 Ppm
Cyanides
< 50 ppm ________ ppm
Phenotics Q
D < 50 ppm ________ ppm
Sulfides
<
50ppm
ppm
F. METALS Indicate if this waste contains any of
the following:
i. Geptox/tclp or 2. G Total
METAL
LESS THAN or ACTUAL.
(Parts Per Mllll n)
Arsenic
G< 5 Q< 500 UNK
Barium
Q< ioo
u nk
Cadmium
< 1 < ioo UNK
Chromium
G< 5
IJNK
Lead
G< 5 < 500 UNK
Mercury
G< 0.2 Q< 20 UNK
Selenium
Q< 1 G< ioo UNK
Silver
G< 5
UNK
Chromium-Hex < 5 Q< 500 UNK
Copper
< 5
UNK
Nickel
a< 5 < 134 UNK
Thallium Zinc
< 5 G< 130 UNK
< 5
UNK
n<
H< <
hl. uzbyi
:-7 n
ASTE ANALYSIS E. ORT .vironmentai Laboratory :FG Industries, Inc.. Lane '.'naries, La.
Nation or Sample: ample '.'oliector:
Still line trench cleanout at Per Tri. (WTS-005.4 i
Eeing drummed at Per In.
W. H. Cooper
:ample Method/Dev ice:
Random graD - dipper
Date /'Time or Sampling :
8-10-90
11:35 am
Date All Analyses Completed: 8-31-90
Report Submitted Ev: Date:
Garv Pre.jean 9-11-90
ANALYSIS RESULT:
Test Parameters I anitabi1itv 'orrosivity
() N/A Reac 11v i tv
<S) N/A
TCLP Toxicity
(mg/L)
N/A
S/A Eil inch/yr
As
Ba Cd Cr Pb
HsL
Se
Standard 140 F 2-12.5 0.250 max
.. ............
5.0 max 100.0 max 1.0 max 5.0 max 5.0 max 0.2 max 1.0 max 5.0 max
ND 2.20 0.09
ND 0.66
ND . 0.04
0.05
Lab Log Sample \~o 137 3 1
' ther Parameters 1if needed ) ' ' ! N/A
.D, none detected
CHLORINATED HYDROCARBONS ( ppm
Ihloroethene Chloroethane
( VC ) l EC i
PCBs i
i
Dicnlormethane
(MeC12 )
!Heat
1
1.1-Dichloroethene
( YDC )
0.31 Value
i
1,1-Dichloroethane
( DCE )
I.2-Dichloroethene
(c is/trans)
Chlorine
Trichiorometha^
(CHC13 )
0.11
1.2-Dichloroethane
( EDC )
0.98 Water
1.1.1-Trichioroethane
( MC )
Tetrachlorometl^pe
(CC14 )
0.26 Densitv
Trichloroethene
(Triehlor) 19.20
1.1.2-Trichloroethane
( TCE )
10.10 Ash
Tetrachlorethene
(Perchlor) 133.00
1.1.1.2-Tetrachloroethane (unsvm)
Sodium
1.1.2,2-letrachioroethane ' s vm )
Pentachloroethane
Penta)
para-Dichiorobenzene Hexacnloroethane Hexacnlorobutadiene Unknown C1HC
lp-DCB) !HEXA) (HCBD)
i
i
t f t
l
I
|
i
ppm) ;
i
BTY/lbl |
%|
wt%
-
a/ml
wt%
Tv t, %
Total C1HC
ppm )
863.90
--SL 02160
Disposal Method
Incineration V s t e Tech
Profile No
MS - 005 . 1
:'7ST PROCEDURE
-AE LOO 0 >.
\
ARAMETER
METHOD USED
: - n 11 a b i 111 v
^ C A
'orrosivity ' PH J
-''N/A
'orrosivity 1 incn/vr) ^.\/A
'
Penskv-Martens Closed Cup Tester ASTM Stanaara D-93-79
SW-846 Method 0040 pH measurement
Setaflash (losea Cup Tester ..STM Stanaard D-J278-78
National Association of Corrosion Engineers Stanaard TM-01-69
Other (Specify);
"<
Other
!
1 Spec i t'y ) 1
Other (Specity )
Keactivity
wf</ 1
`Jne
lit': irnat i\ e answer will classify
reactive )
1 . Normally unstable without detonating? Reacts violently with water?
.1 . Forms potentiallv explosive mixture with water/ 1. Cyanide or sulfide bearing waste which ran generate toxic
gases, vaDor or times under pH conditions netween 1 ana 12.5 ?
5. Capable of detonation or explosive reaction if subjectea *. o strong initiating source or if heated under confinement'.'
6. Readily capable of detonation or explosive decomposition or reaction at standard temperature and pressure?
7. Forbidden Class A, or Class B explosive as defined in 49CFR 173.51, 173.53, and/or 173.887
SW 846
SW 846
SW 846
Parameter
Method Parameter Method Parameter Method
EP Toxicity
.
SW-8 4 6
As
6010
Ag
6010
PC B
LD-25T1
Method ISIS
Ba
6010
C1HC
5030
U1HC
LD-2 5 6 2A
l/Y/A
Cd
6010
Sodium 3050.6010 Heat \alue1LD-2562B
j:r
6010
..pH
904 5
'.hiorine
LD-2 5 6 2 D
:clp*
Pb 6010
Water
LD-2 5 66
/.? He 7 4 7 0
7-v s n
ID-2 5 61
1 Se
6010
i1
*To\ieity Characteristic Leaching Procedure
[aBORATORY IDENTIFICATION Laborato rv: PPG Lake Charles Anaivstls): W. Hebert
American Labs
Test Parameters Anaivzed and Date
CiHC
8-15-90
TCLP metais. volatiles. -:emi-v olat l les H-31-'-
ti
: c :
Si 2l607
From : American Laboratories and Research Services, Inc.
P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320
Date: August 31, 1990
To: Mr. W. H. Cooper PPG industries Chemicals Division p.o. Box 1000 lake Charles, LA 70602
The following analytical.results have been obtained for the indicated sample which was submitted to this laboratory:
Sample I.D. AA04599
Sample location: PPGMW
Lab log 1373
Collected by: W H COOPER
Collection date: 08/10/90 Time: 11:35
Laboratory submittal date: 08/16/90 Time: 20:00
Received by: RLH
Validated by: RLH
Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 08/20/90 Time started: 17:25
Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 08/27/90 Time started: 13:45
Parameter: TCLP Volatile Organics Method reference: EPA 624 Result: see appended report Date started: 08/23/90 Time started: 14:31
Date finished: 08/21/90 Analyst: MJF
Date finished: 08/31/90 Analyst: JSC
Date finished: 08/23/90 Analyst: BB
SL 021608
Mr. W. H. Cooper Page: 2 August 31, 1990
Sample I.D. AA045j9 (continued)
Parameter: TCLP Semi-Volatiles Method reference: EPA 625 Result: see appended report Date started: 08/31/90 Time started: 02:42
Date finished: 08/31/90 Analyst: BB
lL- /373 Data for TCLP Metals mg/L
Component Name
Arsenic, TCLP Barium, TCLP Cadmium, TCLP chromium, TCLP Lead, TCLP Mercury, TCLP Selenium, TCLP silver, TCLP
Concentration
Not Det 2.2 . 09
Not Det . 66
Not Det . 040 .05
Component MDL
.005 .1 .01 .03 . 04 . 005 .005 . 03
Data for TCLP Volatile Organics ug/L
Component Name
Benzene Carbon Tetrachloride Chlorobenzene chloroform 1,2-Dichloroethane 1,1-Dichloroethene Methyl Ethyl Ketone Tetrachloroethene Trichloroethene vinyl chloride Pyridine
Concentration
Not Det 54 74 77
130 67
Not Det 40000 2300
Not Det Not Det
Component MDL
10 10 10 10 10 10 10 10 10 10 100
SL 2l609
Mr. w. H. Cooper Page: 2 August 31, 1990
Sample I.D. AA04o99 (continued)
Data for TCLP Semi-Volatiles ug/L
Component Name
1.4-Dichlorobenzene Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4-Dinitrotoluene Hexachlorobenzene cresols, total 2,4,6-Trichlorophenol 2.4.5-Trichlorophenol Pentachlorophenol 2.4-D 2.4.5-TP (Silvex) chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene
Comments: Reference Lab Report No. R1385.
Concentration
34 24 Not Det 40 Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
10 10 10 10 10 10 10 10 50 50 100 10 10 2 1 1 1 10 20
If there are any questions regarding this data, please call.
SL 2l6lo