Document 2RQggR0p3wm1ZVa0egxbbvYjr
AR226-2663
53
RESEARCH
Proven Results.
AR226-2663
Analytical Report
Air Sampling Fluorochemical Report DuPont Washington Works - Air Sampling Program Round 8
Exygen Research Report No. L0001448
12. /11
Testing Laboratory
Exygen Research
.,3058 Research Drive
State College, PA 16801
Requester
Michael D Aucoin URS Corporation Barley Mill Plaza Building 27 Room 1260 Lancaster Pike and Rt 141
Wilmington, DE, 1.9805
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 1 of 7
3058 Research Drive Sfate College, PA 16801, USA
T: 800.281.3219 F: 814.272.1019
Summary
:
Seven solid media samples were received by Centre Analytical Laboratories, Inc.(dba Exygen Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes collected. Sample WWK-A-AMS6-E8 had sampler problems during collection. No results are reported for this sample.
The samples were analyzed for Perfluorooctanoic Acid;(C8 Acid) using liquid chromatography /mass spectrometry (LCMS). The method employed is entitled "Method of Analysis for the Determination of Perfluorooctanoic Acid (PPQA) in OVS Airtubes by LCMS" (James Miller,
Exygen Research, February 17, 2003).
The OVS tubes were separated into three fractions for specific fluorochemical analysis. Fraction A consisted of the filter, backing material and plastic ring. Fraction B contained the
first bed of XAD resin and the PUP backing. Fraction C contained the second bed of XAD resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C
/was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (C10 Acid)
was added as a surrogate spike to each fraction prior to extraction.
Instrument operating conditions can be found at the beginning of each analytical run. Raw instrument data is given in Appendix A. Chain-of-custody information can be found in AppendixB.
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Pae 2 of 7
Results Summary
Request #
Air Volume Sampled (L)
C8 Acid (mg/m3)
WWK-A-AMS1-E8A WWK-A-AMS1-E8B WWK-A-AMS1-E8C WWK-A-AMS1-E8 (Total)
1666
1666
1666
: < 0.00006 < 0.00006 NA
< 0.00012
WWK-A-AMS2-E8 A WWK-A-AMS2-E8 B ... WWK-A-AMS2-E8 C WWK-A-AMS2-E8 (Total) ;
1461 1461 , 1461
<0.00007 < 0.00007
NA
< 0.00014
WWK-A-AMS3-E8 A WWK-A-AMS3-E8 B WWK-A-EMS3-E8 C WWK-A-EMS3-E8 (Total)
-
WWK-A-AMS4-E8 A
WWK-A-AMS4-E8B WWK-A-AMS4-E8 C :
WWK-A-AMS4-E8 (Total)
WWK-A-AMS5-E8 A'
WWK-A-AMS5-E8 B WWK-A-AMS5-E8 C
WWK-A AMS5-E8 (Total)
1400 1400 1400
1521 1521 1521
1431 1431 1431
< 0.00007 < 0.00007
NA < 0.00014
;
< 0.00007 < 0.00007
NA < 0.00014
< 0.00007 < 0.00007
NA < 0.00014
NA - Not Analyzed. B fraction was below the quantitation limit, therefore the backup fraction does not require analysis.
1. "<" is defined as not detected at or above the reported level.
.
. 2. Sample results have not been corrected for blank results or control spike recoveries.
3. Please note the following descriptions of the OVS sample tube fractions:
Fraction
Fraction Description
Frit Extract 1st set beads extract 2nd set beads extract
(not analyzed)
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 3 of 7
'w
QC Data
LCS
Please note: One control sample was spiked with each perfluorooctanoic acid to give a final concentration of 500 ppb through the tube at a rate of 1-liter per minute for one hour (60 liters of air). The fractions were separated and analyz acceptable range for control recovery is 75-125%.
Request # Control 1
CSAcid (amount spiked - ppb)
500
CSAcid (amount recovered -
435
ppb)
C8 Acid
(percent recovery 87
Blanks
Request # WWK-A-AMSFBLK-E8 A WWK-A-AMSFBLK-E8 B
Vol. Of Air (L)
0
-
0
,
G8 Acid , (ug/fraction)
<0.10 <0.16
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 4 of 7
^jrrogates .'.'.'.. '' '''.' /'.^''.. .': ".'"'' ,..../,. ^/: . '
A surrogate spike (C10 Acid) was added to all OVS tubes to give a final concentration of 500 ppb in the extract.
Surrogate spike recoveries are given in the following table. There are no set criteria for surrogate spike
recoveries. Advisory ranges are 75-125%.
.--
: ^
Sample #
WWK-A-AMSFBLK-E8 A WWK-A-AMSFBLK-E8 B
WWK7A-AMS1-E8A WWK-A-AMS1-E8B WWK-A-AMS2-E8 A ;-' WWK-A-AMS2-E8 B WWK-A-AMS3-E8 A WWK-A-AMS3-E8 B WWK-A-AMS4-EB A WWK-A-AMS4-E8B WWK-A-AMS5-E8 A WWK-A-AMS5-E8 B
Control Spike A Control Spike B
Amount Spiked (PPb)
Amount Recovered (PPb)
500 ,
.
454
. 500 500
^318 434 .
500
-^ ^253
.
500
475
500
; 283 ;
500
. : ':.: 502 .':.
500
: 269
500 . 447
'500
-
373
500
447
500 500 500
"
.
.
-
::
. . 394
437'-.' :. 278
Percent Recovery (%)
91
64* 87 51* 95 57* - 100
'54* ; ' ,
89 75
89
79 87
56*
llK^* Surrogate recovery outside of advisory range.
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Pae 5 of 7
Calculations
Request #
WWK-A-AMSFBLK-E8 A WWK-A-AMSFBLK-E8 B
WWK-A-AMS1-E8A WWK-A-AMS1-E8B ,,WWK-A-AMS2-E8 A WWK-A-AMS2-E8B WWK-A-AMS3-E8 A WWK-A-AMS3-E8 B WWK-A-AMS4-E8 A WWK-A-AMS4-E8 B WWK-A-AMS5-E8 A WWK-A-AMS5-E8 B
Control Spike A Control Spike B
Vol. Of Air (L)
0 0
1666 1666 1461 1461 1400 1400 1521 1521 1431 1431
0.
0
CSAcid (raw-ppb)
<10 <10 <10 <10
31
<10
27
<10
53
. <10
71
<10
435
<10
CSAcid (ug/fraction)
<0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.44 <0.10
C8 Acid (mg/m3)
< 0.00006 , < 0.00006 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007 : < 0.00007 < 0.00007
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 6 of 7
Example Calculation
'
/ .'.,,".
For sample WWK-A-AMS2-E8 A C8 Acid, ; ;.-. ,-
',:
,
: =
[31ng/mlofC8Acidx(lml)x(lug/100Qng)x(lmg/1000ug)] / [(1461 L) x (1 m3 /
.. . .,-iOOOL)]', ' : ^. -.';.' ^ ;.':,;,, ; . '. '../;';,. ,.;,.' ^
< 0.00007 mg /m3
Signatures
P
'aul
^ -'
Connoll
^ _ _ y, LCMS Team
_ _ Leader
_'/ . ^
Y2//^/^^T ^ohn M. Flaherty, Vice President
Other Lab Members Contributing to Data James Miller
^|^5/<3C|
Date
4^W
Date
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Pare 7 of 7
Table 1. Login Information / Field Data
Sample ID
Exygen Lab ID
Date Received Description
WWK-A-AMSFBLK-E8 A WWK-A-AMSFBLK-E8 B WWK-A-AMSFBLK-E8 C
WWK-A-AMS1-E8A WWK-A-AMS1-E8 B WWK-A-AMS1-E8 C WWK-A-AMS2-E8 A WWK-A-AMS2-E8B WWK-A-AMS2-E8 C WWK-A-AMS3-E8 A WWK-A-AMS3-E8 B WWK-A-AMS3-E8 C WWK-A-AMS4-E8 A WWK-A AMS4-E8 B WWK-A-AMS4-E8 C WWK-A-AMS5-E8 A WWK-A-AMS5-E8 B WWK-A AMS5-E8 C
Control Spike A
Control Spike B Control Spike C
L0001448-1 L0001448-2 L0001448-3 L0001448-4 L0001448-5 L0001448-6 L0001448-7 L0001448-8 L0001448-9 L0001448-10 L0001448-11 L0001448-12 L0001448-13 L0001448-14 L0001448-15 L0001448-16 L0001448-17 L0001448-18 L0001448-19 L0001448-20 L0001448-21
12/13/03 Frit extract
12/13/03
1st set beads extract
12/13/03 2nd set beads extract
12/13/03
Frit extract
12/13/03
1st set beads extract
12/13/03 2nd set beads extract
12/13/03 Frit extract
12/13/03
1st set beads extract
12/13/03 2nd set beads extract
12/13/03 Frit extract
12/13/03 1 st set beads extract
12/13/03 2nd set beads extract
12/13/03
Frit extract
12/13/03
1 st set beads extract
12/13/03 , 2nd set beads extract
12/13/03
Frit extract
.12/13/03
12/13/03
1st set beads extract 2nd set beads extract
12/13/03
Frit extract
.
12/13/03
1st set beads extract
.
12/13/03 2nd set beads extract .
Air Volume Sampled (L)
-' ", ! ,
'.. !- ^ !.
..
0 .
o
!
o 1666 1666 1666 1461
..
'
'
.
1"
.
.
1461
1461
:
'1400
1400 .
1400
:
1521
1521
1521
' .
..1431
1431
; .
.''
1431
''.'0,
,
,
:
-0'
.' 0,
-
'
. '
.
': /
..' '
"'
vsssaasa^
m^WS^ K-;:-:%%K:5g a~|
'i^SS''"
Table 2. Chain of Custody
Sample ID
WWK-A-AMSFBLK-E8 A WWK-A-AMSFBLK-E8 B WWK-A-AMSFBLK-E8 C
WWK-A-AMS1-E8A WWK-A-AMS1-E8B WWK-A-AMS1-E8C WWK-A-AMS2-E8 A WWK-A-AMS2-E8B WWK-A-AMS2-E8 C WWK-A-AMS3-E8 A WWK-A-AMS3-E8 B WWK-A-AMS3-E8 C WWK-A-AMS4-E8 A WWK-A AMS4-E8 B WWK-A-AMS4-E8 C WWK-A-AMS5-E8 A WWK-A-AMS5-E8 B WWK-A AMS5-E8 C
Control Spike A Control Spike B Control Spike C
Date Collected
12/12/03 12/12/03 : 12/12/03 12/12/03 . 12/12/03'
12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03 12/12/03
NA NA NA
Date Received at Exygen
Date Extracted by Exygen
12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 : 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03 12/13/03
12/30/03
12/30/03
NA
12/30/03
12/30/03
NA .. 12/30/03
12/30/03
NA
12/30/03
12/30/03
NA
12/30/03
12/30/03 . NA
12/30/03
12/30/03
NA
.
. 1.2/30/03
.
.
.12/30/03 NA
.
Date Analyzed
by Exygen
12/30-12/31/03 12/30-12/31/03
NA 12/30-12/31/03 12/30-12/31/03
NA 12/30-12/31/03 12/30-12/31/03
NA 12/30-12/31/03 .12/30-12/31/03
NA 12/30-12/31/03 12/30-12/31/03
NA 12/30-12/31/03 12/30-12/31/03
NA 12/30-12/31/03 12/30-12/31/03
NA
f v ^ 3058 Research Drive
State College, PA 16801
RESEARCH
'?
^ i^y
Phone:814-272-1039 Fax:814-231-1580
Login #:
1558 .
Project: Project Storage: Company Name: Submitted By:
Status:
P0000419 ,
DuPoht de Nemours & Co, Inc. Michael D. Aucoin Unreceived
Login Type: Started: . Date Start:
Immediate Receipt of Samples
T12/15/.2.0.0.3..
.
..
Due Date;,
12/29/2003
Received Date: 12/13/2003
Received By:
AMMERMAN, MARK
Spread Sample:
Label:
Project Title/Type: Analysis of PFOA in OVS Tubes 7 ROUTINE
ExygenSD/PI: MILLER, JAMES
Login Notes:
As per Mike Aucom-sample WWK-A-AMS6-E8 is cancelled..
Conform Notes:
ConformCOC Sample: Conform COC: Conform Sample: .Conform Request:
MSA 12/15/03
True True True True
Package i^K0002039
Carton
Pac kages / Container'S .
Mail Date / Condition
Shipper/ ID
12/13/2003 1:30:47PM Packsige & Contents Uncompromised
FEDEX 8363913019500200
.' .
.,
:
'
Temp. Control/Temp.
None 23.3
Direction / Handled By
RECEIVED AMMERMAN, MARK
Container # C0021141 C0021142 C0021143 C0021144
-C0021145 C0021146 C0021147 C0021148 C0021149 C0021150 C0021151 C0021152 C0021153 C0021154 C0021155 C0021156 C0021157
C0021158 C0021159 C0021160 C0021161
Gross Weight
7.1 g
7.1 g
7.1 g
7.1 g
, 7-1 g
7.1 g
7.2 g
.7.2 g 7.2 g ;
7.2 g
7.2g
7.2 g
7.1 g
7.1 g
7.1 g
7.2g 7.2g 7.2g
7.1 g 7.1 g
7.1 g
, -
...
.
Container Type Other Other Other Other
Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfg.J-ot
Miscellaneous Item Key
None
Description
ICOC
12/15/2003 Login.rpt
^U5^)
Report Version: Dec 12 2003 11:28AM Page 1 of 4
Instance:
R0076149
R0076149
ogin
, ; '. .
Sy"?16 'P
.,
I'0001448-0001
Matrix GAS
001448-0002
GAS
1.0001448-0003
GAS
L0001448-0004
GAS
L0001448-0005
GAS
L0001448-0006
GAS
L0001448-0007
GAS
L0001448-0008
GAS
.. L0.001448-0009 , L0001448-0010
GAS GAS
:L0001448-0011
GAS
L0001448-0012
GAS
L0001448-0013
GAS
L0001448-0014
GAS
L0001448-0015 L0001448-0016 L0001448-0017
.GAS
GAS
'
GAS
L0001448-0018
GAS
L0001448-0019
GAS
L0001448-0020
GAS
L0001448-0021
GAS
^ ' ' "
:
,
: Samples
Fraction' OVS Tubes
Sample : , ; WWK-A-AMSFBLK-E8 A
OVS Tubes WWK-A-AMSFBLK-E8 B
OVSTubes
WWK-A-AMSFBLK-E8 C
OVS Tubes .WWK-A-AMS1-E8A
OVSTubes . WWK-A-AMS1-E8B ',
OVSTubes WWK-A-AMS1-E8C
OVSTubes: WWK-A-AMS2-E8 A .
OVS Tubes WWK-A-AMS2-E8 B
.
. OVS Tubes !: WWK-A-AMS2-E8 C ' OVS Tubes ; WWK-A-AMS3-E8 A
OVSTubes
OVS Tubes OVS Tubes
WWK-A-AMS3-E8 B .: WWK-A-AMS3-E8 C: , WWK-A-AMS4-E8 A
OVS Tubes
WWK-A-AMS4-E8 B ;
OVS Tubes WWK-A-AMS4-E8 C .
OVS Tubes
WWK-A-AMS5-E8 A
,
OVSTubes , WWK-A-AMS5-E8 B ,
OVSTubes WWK-A-AMS5-E8 C
OVSTubes OVSTubes OVSTubes
;. Control 1 A
Control 1 B Control 1 C
.: ,:
;;-
/
';..;
:
.-'
'.
:
;
.
Date Sampled Date Received
12/12/2003 12/13/2003
12/12/2002 12/13/2003
12/12/2002 12/13/2003
12/12/2003 12/13/2003
12/12/2003
'
12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/12/2003 12/13/2003
12/15/2003 12/13/2003
12/15/2003 12/13/2003
12/15/2003 12/13/2003
Date Due 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003 12/29/2003
12/15/2003 i Login.rpt
u 054
.
Report Version: Dec 12 2003 11:28AM Page 2 of 4
Instance:
R0076149
^
101010
001448-0001
Container ' o0021141/Other/NONE
L0001448-0002
Container C0021142/Other/NONE
LOOOl 448-0003
Container: C0021143 / Other / NONE
L0001448-0004
Container C0021144 / Other /NONE
L0001448-0005
Container C0021145/Other/NONE
L0001448-0006
'
Il^ila, "0021.1C4o6n/'tOaitnheerr/
,,. ,
NONE
'
'
. ., ...
L0001448-0007
Container C0021147 / Other / NONE
L0001448-0008
Container
C0021148 / Other / NONE
L0001448-0009
Container C0021149 / Other / NONE
L0001448-0010
Container C0021150/Other/NONE
L0001448-0011
Container C0021151 /Other/NONE
^BMO01448-0012
'
Container
12/15/2003 Login.rpt
ogin
Bottles
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
UU5^)
Report Version: Dec 12 2003 11:28AM Page 3 of 4
Instance:
R0076149
^ 4188784029901
C0021152 / Other / NONE
^.0001448-0013
Container
;0021153 /Other /NONE
L0001448-0014
Container .COQ21154 / Other / NONE
L0001448-0015
Container C0021155 / Other / NONE
L0001448-0016
Container C0021156/Other/NONE
L0001448-0017
Container C0021157/Other/NONE
, L0001448-0018
Container
4|g^ C0021158 / Other / NONE
^iBIIil I --'
.
: "
"LoOOl 448-0019
Container C0021159/Other/NONE
L0001448-0020
Container C0021160/Other/NONE
L0001448-0021
Container C0021161/Other/NONE
Method Method . Method Method Method Method Method Method Method
12/15/2003 Login.rpt
uU5o
Report Version: Dec 12 2003 11:28AM Page 4 of 4
Instance:
R0076149
^ 11628754546
CHAIN OF CUSTODY/ANALYSIS RE
RESEARCH
Exygen Research Sample Receiving 3117 Research Drive State College, PA 16801, U T: 814.231.8032 ' F: 814.231.1580 exygenresearch.com
^^^i^ai^iji^^^^S^^^B^B^^^BHHHIIiBB1^^
Client (name & address):
Project Manager (Name & E-mail Address):
ft^^.m U3^ rYhV^Ph/^n ^c^r
, . , Phone:
(^^) W^-\\06^ Fax:
,
.'
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form
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ExyLIMS#
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Collection Collection s 0 3 0
Client Sample Identification
Date
Time
0 u 2U Specify Matrix
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LAB USE ONLY
Comments
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OTHER INFORMATION
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Cooler ID # yl'Cf /--- Cooler Temp. (C) ^
Received (ay
-^A
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J ^==----------------
/ < , LAB USE. ONLY .
Date
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^h7'-i
Time
(?^:3&
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.
DuPont Washington Works Air Sampling Program
yes or no
Weather: 12/11 =
Overcast, 37 degrees, possible snow flurries.
12/12=
Overcast, 28 degrees, few flurries.
SAFER operational:
yes yes or no
Comments:
Total minutes column is the reading from the monitor counter. Pump AMS-6 stopped with 939 minutes on the counter but would restart to calibrate. Had difficulty getting pump AMS-3 to start to calibrate.
12/12/2003
Page 1 of 2
R ES EARC H
Sample ^Condition Upon Receipf Form
Protocol ff Exygen Study # Date & Time Received Condition .of Samples Temporary Storage Location
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Initials & Date Waybill #
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Comments:
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Mav 24, 2002/3
0: WORD .proLL-s^-luuiir.SiiinplfCondilionoiiRecL'ipt.duc
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