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2. Air Pollution from Brake Lining Asbestos
The samples of airborne wear debris from the dynamometer tests of a
Pinto disc brake continues being examined for asbestos by Technical Services
Department using a new sample preparation technique. The procedure used to
prepare the membrane filters for electron microscope examination is one developed
in the laboratory of Dr. I'. J. Selikoff, et al, at the Ht. Sinai School of Medicine
in New York. In this procedure, the filter sample is oxidized in a low temperature,
activated oxygen asber, dispersed in a dilute polymer solution on a glass slide by
mechanical mashing, mounted in a film of the polymer on copper EM grids, and
carbon shadowed. By examining the samples at more than 37/000 magnification, the
number and size of the asbestos fibers are determined; this information is used to
determine total mass of asbestos present. The m* ethod has the advantage of ellmin-
atlng the obscuring effect of other wear debris present. It has the disadvantage
that the original asbestos fiber bundle size distribution is destroyed and only
total mass of asbestos may be determined, since fiber bundles are broken down into
individual fibrils during sample preparation.
The examination of the samples is not yet completed and appropriate
quantitative reference samples have not yet been prepared and counted - thus,
obtaining an estimate of actual asbestos content requires, at this time, a reliance
on Mt. Sinai laboratory experience to estimate asbestos losses from the samples
during sample preparation. However, a preliminary estimate based on the incomplete
data available to date indicates that asbestos fiber probably comprises less than
0.02$ of the airborne wear dust, or less than 0.01% of the lining worn away.
3. Support to Divisions
A. Material Evaluation
Dynamometer tests were performed at the request of Brake Engineering
Department to characterize 15 candidate disc brake lining materials and 4 different
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