Document 2JMkrOY04B6RqM7ZLdRrBnop6

Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CER IFIC F Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 YS X s A January 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 20, 1992 VIS1A Product: 53B5 Railcar No.: VIPX 45827 Order No.: 0005127--009 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.13 Bulk Density, GM/CC ABR-2A 510 Min 0.554 Brabender Dry Time, Mins ABR-7 6.0 Max 4.8 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 13.3 Pan 10.0 Max 2.6 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 7 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.142 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E IS fiagwe Laboratory Supervisor (601) 369-3624 VAB.0001200576 Vista Polymers Highway 25 Aberdeen, MS 39730 F*VC RAILCAR ANALYSIS Load Date: / /7*-? Time Logged Ship Date:f *2^ Product: Car No.: Logged In By: /If/ Od&oWI'OQI Silo(s) Customer: A Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density .ft A3 BD after Fluff ,27 Hard Particle 7 II 57 Viscosity RVCM 40 Mesh/Glassies C> CA Bottom . J3 /9 .^3 o CB Bottom . JO J8 B Bottom / 0 Screen Analysis Mesh 40 Weight CAP % 0,0 60 /3 .2 80 (f < 0 C0 it.) 100 LLte 120 LfslS 2f,2 140 11. 200 kM jj.j Pan / tf Drytime: 4-J Static Flow: > / r.t Avg. Microns: Color L: )7 a 22 b H-O.b Technician: VAB.0001200577 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I I c:^ Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYS X S A January 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 21, 1992 VISIA Product: 5385 Railcar No.: ACFX 41167 Order No.: 0005932-001 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.02 Bulk Density, GM/CC ABR-2A 510 Min 0.576 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.8 Pan 10.0 Max. 2.1 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 7 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.161 Inherent Viscosity ABR-10 .90 to .95 0.95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. gw Labora tory Supervisor (601) 369-3624 VMM I MM VAB.0001200578 w Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date ai RAILCAR ANALYSIS Product: 5385 <111UCar Ho kiteTime Logged In: (D taOO Logged In By: Ship Date:__/ Order No: Silo(s) :. Customer A/O ^8)fcf Compartment A Sample From Bottom Moisture % BL Contamination BR lo Bulk Density BD after Fluff Hard Particle 7 5 77 Viscosity M. RVCM tlGl 40 Mesh/Glassies CA Bottom (6 It Bottom o . o Bottom . /O & Screen Analysis Mesh Weight % 40 A *> 0.0 60 0.3Si 0.&> 80 l&o 100 SV.o 120 !&tL 140 JM. 200 (6.& Pan 103 Drytime: Static Flow: 0 ///& Avg. Microns: Color L SM a b A <3/ Technician: TW4P IMMMi mmmrnmm mmmmmmmmmmmmmmmmmmmrnm VAB.0001200579 r Vista Polymers A Division of Vista Chemicoi Company IX Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 V'S X S A Date: January 24, 1992 Customer GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 16, 1992 VISIA Product: 5385 Railcar No.: GACX 73309 Order No.: 0005932-000 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. .14 Bulk Density, GM/CC ABR-2A 510 Min. Brabender Dry Time, Mins ABR-7 6.0 Max 4.8 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.0 200 Mesh NDS 15.8 Pan 10.0 Max. 3.7 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 15 Vinyl Chloride Monomer ABGC-26 8.5 Max Inherent Viscosity ABR-10 .90 to .95 .93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Laboratory rvisor (601) 369-3624 VAB.0001200580 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: /-/"?2 Time Logged I Ship Date: l 1 fc> Product: Car Ho.: Logged In By: Silo(s): Order Ho: 000&}^Z^'&C& Customer sU z> Compartment A CA Sample From Moisture % Bottom BL Contamination BR r t& Bulk Density BD after Fluff ................................................................................ Bottom /</ jr u ,52?o Hard Particle 7 5 ' Viscosity ,430. RVCM /433 40 Mesh/Glassies 0 cJ> CB Bottom 1 ./</ ? cP B Bottom , / 2- j / .ssy O Screen Analysis Mesh 40 Weight %? 0,0 60 .0<f /- 80 / 100 120 D 153 140 (13 200 Pan /y? /*~2 3.7 Drytime: 11.:. Static Flow: O / *T'V Avg. Microns: Color L: /0 0,7,0 a Technician: t' mmm mm VAB.0001200581 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERT I I C#=lTE VS I S January 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0- Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 23, 1992 VKIA Product: 5385 Railcar No.: PLWX 44461 Order No.: 0005932-021 Property Test Method Specification Analysis Volatiles, X ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min 0.557 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, X on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 15.5 Pan 10.0 Max. 2.8 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.085 Inherent Viscosity ABR-10 90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Bagwe11 Laboratory Supervisor (601) 369-3624 VAB.0001200582 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date Time Logged In: Ship Date: RAILCAR ANALYSIS Product: o Logged In By: Order No: Car No.: Silo(s) Customer: M uhujt Compartment Sample From Bottom Moisture % BL Contamination BR sOlr ?* 9 Bulk Density BD after Fluff Hard Particle 7 5 .31 ( tl Viscosity RVCM 40 Mesh/Glassies 0 Screen Analysis Mesh 40 60 Weight *r c> Drytime: o.t 3.0 *3 Bottom r .S3S~ Bottom .0( S .J>7? ,S71> Bottom * oSK 9 .jsrr^ .33 7 C? O <z> 80 100 120 140 200 Pan I 0-99 tSJ_ST /O ?*?</ f>o V.i> /7? 9.0 /8-3 St?o SU` /?? IS, /0*_Z. <8-2 3.r? Static Flow: & / /J-& Avg. Microns: /3 ft O Color L: a ?&*/ b A Jo Technician: (nr -rg. VAB.0001200583 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Ii V'S i s January 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 24, 1992 VEIA Product: 5385 Railcar No.: VIPX 45910 Order No.: 0005127--011 Property Volatiles, V, Test Method ABR-1A Specification Analysis 0.30 Max. 0.10 Bulk Density, GM/CC ABR-2A 510 Min 0.574 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.5 Particle Size, % on ABR-3 40 Mesh O.1 Max. 0.00 200 Mesh NDS 8.2 Pan 10.0 Max. 2.1 40 Mesh Glassies (By Compartment) ABR-6 5 Max. Avg. 0 A CA CB B Glassies average of 5 for railcar; O 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.062 Inherent Viscosity ABR-10 90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Esr Bagwell Laboratory Supervisor fAOl1 369-3624 I VAB.0001200584 4 Vista PolymerB Highway 25 Aberdeen, MS 39730 Load Date: /r3JLSJ^ Product: Tine Logged In: >1&f{9 Ship Date: Logged In By: /9f Order No: QO0*5~~0f^ Car No.: Silo(s): zz .& Customer: <UUL&HP /Wo Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff .sit Hard Particle 7 5 Viscosity RVCM ,Hz 40 Mesh/Glassies > CA Bottom O CB Bottom ZL D B Bottom ,/D szL O Screen Analysis Mesh 40 Weight >.Q'C> % 'C) 60 80 100 120 140 200 Pan JL& Mllffl fUh M,3t C/J2- JjxT c2> / Cur* Drytime: Static Flow: 4? / // 7 : /r/f Avg. Microns Color L: M/o a b Technician: VAB.0001200585 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 IFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 vs i s A January 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 27, 1992 VIS1A Products 5385 Railcar No.: GACX 73412 Order No.: 0005127-012 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max 0.16 Bulk Density, GM/CC ABR-2A .510 Min. 0.577 Brabender Dry Time, Mins ABR-7 6.0 Max. 4. B Particle Size, V. on ABR-3 40 Mesh 0.1 Max 0.00 200 Mesh NDS 7.1 Pan 10.0 Max 1.8 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 1 0 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.083 Inherent Viscosity ABR--10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.v>Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200586 > Vista Polymers Highway 25 Aberdeen. MS 39730 A Load Date: Time Logged In: haShip Date: \ RAILCAR ANALYSIS Product: 5385 Car Ho. : ___________ Logged In By: Order No: ObO^f^'P/3- SlloCsVj vyi--^ Customer : CCAAJutoxP Compartment Sample From Moisture % Contamination Bottom Bottom , /X Bottom . /3 Bottom Bulk Density BD after Fluff , r 7U Hard Particle 7 5 Viscosity RVCM jfea 40 Mesh/Glassies Screen Analysis Mesh 40 Weight % 4'a <? o*o 2.0. 60 /,r r-? 7 42. U 23*o tt.s- 80 a. a 2 7. 2* 100 M>i7 2t.S~ 120 //.It 22,3 9.3 140 s: 7t //. c s,r 200 9 Pan , 7Z /.<P Drytime: .f Static Flow: 0 / r.f _ Avg. Microns: . / ho* i& Color L: ? 7- 7 4 a .02, b _ iif Technician: VAB.0001200587 T Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I X CATE O Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANALYSIS A January 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 28 VIS1A Product: 53B5 Railcar No.: ACFX 41148 Order No.: 0005932-003 Property Test Method Specific a tion Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.17 Bulk Density, 6M/CC ABR-2A .510 Min. 0.577 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 6.4 Pan 10.0 Max. 1.6 40 Mesh Glassies (By Compartment) ABR--6 5 Max. Avg. 1 A CA CB B Glassies average of 5 for railcar; 1 1 1 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR--12 25 Max. 2 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.166 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.^Bagwell Laboratory Supervisor (601) 369-3624 m Mpmipi PHOT VAB.0001200588 m mm Vista Polymers Highway 25 Aberdeen. MS S9730 A RAILCAR ANALYST> Load Date: Time Logged In: (2< ft Ship Date: 1 Product: Logged In By: Order No: Car No.: Silo(s) : ?7C?, (&17&SS Customer y"/ Compartment A Sample From Bottom Moisture % BL Contamination BR y Bulk Density ,T77 BD after Fluff Hard Particle 7 5 Viscosity if z ce . ,*2-3 RVCM 40 Mesh/Glassies ' Screen Analysis CPM. If'C'ir 6.0 Mesh 40 Weight % P'OO 0,0 /,? 60 .ti /. r CA Bottom .// CB Bottom 3 s' .7<f B Bottom ,/7 / 1 / 80 /* -*7 * za.p 100 2.t* 6 /?.? 120 /a.7* 21.4 /c.9 140 S'. 7 f 4. //,4 0 .T2 200 A7 Pan .7? Drytime: s.c Static Flow: _ c / t.l _ Avg. Microns: US.I Color L: a o<S . b _ /.^r Technician: T'fc VAB.0001200589 Visla Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369*81 1 1 A CERT X I CATE A N A VS I s Date: February 4, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: January 29, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46472 Order No.: 0005127-013 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min 0.585 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, V. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 8.6 Pan 10.0 Max. 1.6 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.068 Inherent Viscosity ABR-10 90 to . 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. `Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200590 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: h 2*7' f2~ Time Logged In: //** Ship Date Product: Logged In By: Order No: Car Ho. Silo(6) -.CXJ7Z Customer V# MeMt-- Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff Hard Particle 7 5 Viscosity RVCM 40 Mesh/Glassies 0 CA Bottom /Z- o CB Bottom .63 /S B Bottom *3 2/ S7& &b o. Screen Analysis Mesh Weight % 40 6. 0*0 60 o. & (3 80 foijSb 100 {<ZSJ 120 140 6*3? (&J7 200 tjr3o Pan o.& fjZc> Drytime: ihi Static Flow: / Avg. Microns: Color L: a A 07 b I-&I Technician: VAB.0001200591 Vista Polymers A Division of Chemical Company Highway 25 Post Office Box 91 IFICATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 YS X s A Date: Customer February 6, 1992 GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 3, 1992 VJS1A Product: 5385 Railcar No.: GACX 73393 Order No.: 0006603-000 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.03 Bulk Density, GM/CC ABR-2A 510 Min 0.550 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 4.4 Pan 10.0 Max 1.2 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 O O 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 12 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.085 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell Laboratory Supervi (601) 369-3624 VAB.0001200592 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date Time Logged In: Ship Date: Product: Car No.: Logged In By: Silo(s): Order No: QC&(okO&rQC& Customer Compartment Sample From A Bottom Moisture % BL Contamination . BR Bulk Density .o'l' x $ BD after Fluff Hard Particle 7m 5 Viscosity l RVCM JtD .ot^ 40 Mesh/Glassies ______ Screen Analysis Mesh Weight %r 40 *.o 60 /. J7 a.? CA Bottom * _J <( CB Bottom . >2_ H /o -5V/ B Bottom .03 ~r * 0 a0 80 /f-O't' 32-0 100 )&<p ZZ-\ 120 ?-Yt /7^ 140 Mo? SI 200 J2-/9 <f Pan -&y /2_ Drytime: Static !Flow: O //OS' Avg. Microns: / 73.9 Color L: /**' ? a "-9Z- b 2-i.c> Technician: VAB.0001200593 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 IFICATE O Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 ANA N'S I S A V February 11, 1992 Customer GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 5, 1992 VIS1A Product: 5385 Railcar No.: ACFX 41165 Order No.: 0006483-000 Propertv Test Method Specification Analysis Volatiles, X ABR-1A 0.30 Max. 0.03 Bulk Density, GM/CC ABR-2A 510 Min. 0.550 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max 0.00 200 Mesh NDS 4.4 Pan 10.0 Max. 1.2 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles. 7 Mins. ABR-12 25 Max. 12 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.085 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.(/Bagwell Laboratory Supervi (601) 369-3624 VAB.0001200594 %* r* Vista Polymera Highway 25 Aberdeen, MS 39730 A Load :Date <P- 5 Time Logged In:. Ship Date: RAILCAR ANALYSIS Product: 5385 Logged In By: Order No: Car Ho.: Silo(s Customer: Compartment Sample From Moisture % Bottom Bottom 5h------------------------------ BL Contamination BR > Bulk Density A37 3^ 2 BD after Fluff Hard Particle 7 * 5 jS/Z /iy .55# ,59/ Viscosity ,7/S RVCM 40 Mesh/Glassies jg. Screen Analysis Mesh 40 60 80 100 Weight 0.0 O U.37 /Z7/ % 6 * t) 3JI. 7 ^9/ Bottom .SS7 120 140 /97 Bottom oA , 5/2-' ,<S/V 200 J.S~! Pan /2- Drytime: Static Flow: Q.--L f.? Avg. Microns: Color L: ab Technician: 9^ VAB.0001200595 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 IFIC e: o Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A N ft vs i s A Date: February 11, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 7, 1992 VIS1A Product: 5385 Railcar No.; VIPX 45794 Order No.: 0006483-001 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min. 0 566 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.1 rticle Size, V. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.9 Pan 10.0 Max 2.2 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.016 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy EV^ Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200596 Viata Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged Ship Date: RAILCAR ANALYSTS P roduct: Logged In By: Order No Car Ho.: IT 7 Silo(s): Customer: /o z* Compartment A Sample From Bottom Moisture % BL Contamination BR O Cp Bulk Density BD after Fluff Hard Particle 7 n 5 // r3 Viscosity RVCM 40 Mesh/Glassies .01(0 o CA Bottom Z S&L o CB Bottom <=>1 i .jsn/ o B Bottom o Screen Analysis Mesh 40 Weight % OSO 0*0 60 .Drytime: S' ! 80 100 /7>7 ^?JT^ 120 4M Static Flow: & / 140 Lki 200 ^4 Pan ),)D ZL< Avg. Microns: -MM. Color L: Z&O*'?? a 0 b Technician: sHt7~ -h /t' VAB.0001200597 Vista Polymers A Division of Vista Chemical Company I I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601) 369-8111 a ANA VS I s A v. February 14, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship' Date: February 10, 1992 VISIA Product: 5385 Railcar No.: ACFX 41136 Order No.: 0006483-002 Propertv Test Method Specification Ana1vsis Volatiles, 7. ABR-1A 0.30 Max. 0.07 Bulk Density, GM/CC ABR--2A .510 Min. 0.575 Brabender Dry Time, Mins ABR--7 6.0 Max. 5.0 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 11.4 Pan 10.0 Max 2.7 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 0 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 13 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.056 Inherent Viscosity ABR--lO .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. `'Bag we 11 Laboratory Supervisor (601) 369-3624 VAB.0001200598 * Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date: Product 5385 Logged In By Order No: T Car No.: Silo(s): .& Customer T~|Q Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density 07 2? 3/_ BD after Fluff Hard Particle 7 32 5 Viscosity RVCM 40 Mesh/Glassies 0 CA Bottom 03 CB Bottom 03 L /? B Bottom 03 Screen Analysis Mesh 40 Weight % 0.0 60 c.C# 80 tv* 100 120 u Drytime: Static Flow / Color L: 929 a 6JS7 b 140 200 Avg. Microns Pan (.35 82- Cs> Technician: VAB.0001200599 Vista Pdlymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ifi OF A N A vs i s A February 14, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 12, 1992 VIS1A Product: 5385 Railcar No.: PLWX 44461 Order No.: 0006483-003 Property Test Method Specification Analysis Volatiles, V. ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min. 0.581 Brabender Dry Time, Mins ABR-7 6.0 Max 5.0 Particle Size, V. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 4.8 Pan 10.0 Max. 1.4 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) A CA CB B Glassies average of 5 for railcar; 10 max. in a single compartment. 0 00 0 Hard Particles, 7 Mins ABR-12 25 Max. 6 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.015 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.^Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200600 Vista Polymera Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date Time Logged In: Ship Date: /^/1`2^2^ Product: 5385 Logged In By: CjSl Order No: T: Car No Silo(e) : (?7i. Li 7 Customer Oujtrrp Compartment A Sample From Bottom Moisture % ,O BL Contamination BR 3 Bulk Density BD after Fluff Hard Particle 7 5 a Viscosity fej RVCM ,0l< 40 Mesh/Glassies 12 CA Bottom .></ -? .S7S D CB Bottom ? <9 B Bottom .S79 Screen Analysis Mesh 40 Weight 3*00 % 60 4je. 80 20-9^ 100 11.99 2*1.0 120 /S.3 140 3.9i> 7.9 200 2.29 Pan 0. 72. Drytime: 5.e> Static Flow: o t9.f Avg. Microns: J79.3 Color L a ,0L b 3<13 : Technician C& VAB.0001200601 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 l I CATE O Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 V*A V'S I s February 19, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention Plant Chemist Ship Date: February 17, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45839 Order No.: 0006483--005 Property Volatiles, V. Test Method ABR-1A Specification Analysis 0.30 Max. 0.12 Bulk Density, GM/CC ABR-2A 510 Min. 0.576 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max 0.00 200 Mesh NDS 7.0 Pan 40 Mesh Glassies (By Compartment) ABR-6 10.0 Max. 1.8 5 Max. Avg. 0 A | CA CB B Glassies average of 5 for railcar; O 0 0 0 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 2 Vinyl Chloride Monomer ABGC--26 8.5 Max 0.736 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001200602 rr i Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date :J2L Time Logged Ship Date: L3 Product: Logged In By: Order No: Car Ho.: Silo(s): Customer: fYVjXtQ Compartment Sample From Bottom Moisture % Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Particle 7 si Viscosity RVCM 40 Mesh/Glassies J71 SIL S% Screen Analysis Mesh Height 40 ChQ<^ % OrO 60 80 100 i.n Ml ML 120 lo.fr a/,y 140 S-Q ILA 200 Ml ?,o Pan Drytime: Hi5 UZJ1Static Flow: 0 / /Q4 Avg. Microns: Color L: Up o</ b Technician: Ih, VAB.0001200603 Vista Polymers A Division of Vista Chemical Company XI Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601J 369-8111 AIM A vs x s A February 19, 1992 Customer s GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 14, 1992 Product: 5385 VK1A Railcar No.: ACFX 41180 Order No.: 0006483--004 Property Test Method Specific a tion Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.04 Bulk Density, GM/CC ABR-2A .510 Min. 0.55 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 8.1 Pan 10.0 Max. 3.1 40 Mesh Glassies ABR-6 5 Max. Avg.^ 0 u<r (By Compartment) A CB B Glassies average of 5 for railc 10 max. in a single compartment 0020 Hard Particles, 7 Mins ABR-12 25 Max. 9 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.001 Inherent Viscosity ABR-IO .90 to .95 0.91 Polyvinyl Resin, Not Reprocessed. AAmmyy Eb.. Bfctaaagwweelt--' Laboratory rvisor (601) 369-3624 VAB.0001200604 Vista Polymers Highway 25 Aberdeen, MS 39730 A f Load Date: 2,^/0 - f 2^ Product Car No.: #//tO Time Logged In Ship Date : /ioo Logged In By: MAL S11o(b1: Order No: Q@C6>i$3~0(y4' Customer: (>7&.~?7 hio -- Compartment 1 A Sample From Bottom Moisture % BL Contamination ___ BR oH' $ Bulk Density BD after Fluff svCp Hard Particle 7 5 7fi.fi Viscosity i RVCM 40 Mesh/Glassies . *}> / DO 1 CA Bottom .| t CB Bottom i-- 4?> /0 B Bottom , 0 3-- (( Screen Analysis Mesh Weight % 40 Q. && o-o 60 & 200 Pan Zl *37 Drytime: Static Flow: Color L: !__ a rb Z-^7 / Microns: Technician: * VAB.0001200605 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Ofn<ce Box 91 Adrdeen, Mississippi 39730-0091 Phone (601) 369-8111 l ICATE OF ANALVSXS A Date: February 24, 1992 Customers GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 19, 1992 VBIA Produc t s 5385 Railcar No.: VIPX 45910 Order No.: 0006483--006 PrBPirJte V/olatiles, V. Test Method ABR-1A 0.30 Max. Bulk Density, GM/CC ABR-2A .510 Min. Brabender Dry Time, Mins ABR-7 6.0 Max Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 200 Mesh NDS Pan 10.0 Max 40 Mesh Glassies ABR-6 5 Max. Avg (By Compartment) Glassies average of 5 for railcari 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. Vinyl Chloride Monomer AB6C-26 8.5 Max Inherent Viscosity ABR-IO .90 to .95 Polyvinyl Chloride, Virgin Reein * -Not: Reprocessed. 0.08 0.562 5.0 0.00 12.4 3.0 0 3 0.012 0.94 Laboratory Supervisor * (601) 369-3624 VAB.0001200606 Vista Polymers Highway 25 A Aberdeeni MS 39730 Load Date 2 ~'/t ~ 9 2~ Time Logged In 02x> o Ship Date: Product 5385 Logged In By Order Ho: Car Ho.: 4S9/o Silo(s): fjl7? : <U-CArcp Customer tic TrfGtoL- Compartment A Sample From Bottom Moisture % o4- BL Contamination BR Bulk Density [S LS BD after Fluff Hard Particle 7 m. 5 303. Viscosity RVCM 40 Mesh/Glassies P CA Bottom og W 6%0 0 CB Bottom 0*h tt 0 B Bottom O Screen Analysis Mesh Weight % 40 Cj 0Q a6 Drytime: 60 /JL 80 100 J2& 120 140 Z4Z 200 /g-f Pan m 3 Static Flow: ^ ^ Avg. Microns: /4fe-3 Color L a oot b JJ3 Technician: VAB.0001200607 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: 2*// Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: f*b. 2o, IWz. Produc t Lot No Trailer No.: 4@o32.~7 Order No. : QOO7Z76, ~OOO Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR--7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Ana lysis S.l 0.1 Max. 0.0 NDS 10.0 Max. 5 Max . 25 Max. llSL ZJL D 6 8.5 Max. .90 to .95 Not more than 8.5 PPM .43 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200608 Regulars or Bags Psgs of psgss o-ni^ a Vinyl Sample Log Date Product ^AB.0001200609 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 Xi f- ^ rsj ^ i V's x s A Date: February 26, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 21, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46573 Order No.: 0006483-007 Property Test Method Specification Analysis Volatiles, X ABR-1A 0.30 Max. 0.19 Bulk Density, GM/CC ABR-2A .510 Min 0.578 Brabender Dry Time, Mins ABR-7 6.0 Max 5.0 Particle Size, 7. on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.4 Pan 10.0 Max. 1.3 40 Mesh Glassies ABR-6 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. 5 Max. Avg. 1 A CA 1 CB 1 B L _l2 2 Hard Particles, 7 Mins. ABR-12 25 Max * 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.045 Inherent Viscosity ABR-10 .90 to .95 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Laboratory Supervisor (601) 369-3624 VAB.0001200610 Viata Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Load Date; Time Logged In: J.330 Product Logged In By: Ship Date Order No Car No.: <4l*S 1S~ Silo(s): Customer Compartment A Sample From Bottom Moisture % BL Contamination ___ BR .if z jr Bulk Density .Sf! BD after Fluff Hard Particle^ CA 4 Bottom /? i L .<7Z CB Bottom J.4. 2 / .sfz B Bottom ./ I 3 ,S7(e Viscosity \ RVCM 40 Mesh/Glassies o z o zo Screen Analysis Mesh Weight % 40 0'QO 00 .. 60 i.ri ?> 80 32- 3 100 /V.77 Z9,S~ 120 140 9. 77 i9 /M 9. 200 a, 12. _ Pan 0.(p(p /.3 SJ)Drytime: Static Flow: Avff. Microns: 19Color L: 100. a"- \x h / Technician: VAB.0001200611 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 iI e: of Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 IS A Date s February 26, 1992 Customer : GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 24, 1992 VISTA Product* 5385 Railcar No.: UTCX 46497 Order No.: 0006483--008 Property Test Method Specification Analysis Volatiles, 7. ABR-1A 0.30 Max. 0.06 Bulk Density, 6M/CC ABR-2A .510 Min. 0.558 Brabender Dry Time, Mins ABR-7 6.0 Ma x 4.9 Particle Size, V. on ABR-3 40 Mesh 0.1 Ma x. 0.00 200 Mesh NDS 8.4 Pan 10.0 Max. 1.9 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) CA G1 of 5 for railcar; 10 max. in a single compartment. 1 Hard Particles, 7 Mins. ABR-12 25 Max. 5 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.076 Inherent Viscosity ABR-IO 90 to . 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E .i/tjagw Laboratory rvisor (AOt) 3A9-3A24 VAB.0001200612 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Load Date: Time Logged In: QlQo Ship Date m /WO /yn&thdL Compartment A Sample From Bottom Moisture % BL Contamination ... BR 3 (, Bulk Density .7/ BD after Fluff Hard Particle 7 % 5 Viscosity * RVCM ,435 040 Mesh/Glassies Product: Logged In By: bGC&H'irOO Car No.: #4 9 7 S1lo(s): / t ?? (Xt^uCJ^yO V- f -- CA Bottom a .2- CB Bottom . o(f> 3 S B Bottom , .C^ a 7 .37 00 Screen Analysis Mesh Welffht 40 % 0.0 60 80 100 .3/ . J.*W. *J2. 2*>.9 Jo. 3 120 P. 33 140 {JO 13. L 200 V. 10 Pan .?r /*9 Drytime: Static Flow: _ __///2* Avff. Microns: Color L: loo.ay a -"./Z b %'!(/ Technician: VAB.0001200613 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: March 2, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 27, 1992 VIS1A Product 5385 Railcar No VIPX 45719 Order No 0007361-000 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max* 0.04 Bulk Density, GM/CC ABR-2A .510 Min. 0.569 Brabender Dry Time, Mins. ABR-7 60 Max. 4.8 Particle Size, X on ABR-3 40 Mesh 01 Max. 0.00 200 Mesh NDS 9.2 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 2 (By Compartment) Glassies average of 5 for rail 10 max. in a single compartment Hard Particles, 7 Mins ABR-12 25 Max. 6 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.095 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. "15a Laboratory Supervi (601) 369-3624 VAB.0001200614 Vista Polymers Highway 2 & Aberdeen, MS 39730 A HAILCAH ANALYSIS Load Date: 3-*^/ *7^- Product: Time Logged In: Logged In By: Ship Date:. Order No: Car Ho . qsV1? Silof s) : ^ ^i('?7r L fcP Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff Hard Particle 5 7 O f /l yw MM (p Viscosity RVCM 40 Mesh/Glassies > CA Bottom 2. \t> O CB Bottom .o / 7 V sSo B Bottom j <r S7 7 3 Screen Analysis Mesh Weight % 40 <S>,, > g>, o 60 * 6s>% 80 -/ 100 120 JoS 3C?-M <22-3 140 42 7> 200 Pan /A Drytime: Static Flow: O / * Avg. Microns: /57%$ Color L: /0O- a ~0'<>7 b f-9f Technician: * f 4-*ft Tm VAB.0001200615 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: March 2, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus. MS 39701 Attention: Plant Chemist Ship Date: February 26, 1992 VKIA Product: 5385 Railcar No.: UTCX 46570 Order No.: 0006483-009 Property Test Method Specif ism Volatiles, % ABR-1A 0.30 Max. Bulk Density, GM/CC ABR-2A .510 Min. Brabender Dry Time, Mins ABR-7 6.0 Max. Particle Size, X on ABR- 3 40 Mesh 0.1 Max. 200 Mesh NDS Pan 10.0 Max. 40 Mesh Glassies ABR-6 5 Max. Avg. (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max. Vinyl Chloride Monomer ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 0.20 0.573 4.9 0.00 7.9 1.9 0 5 0.088 0.94 Amy E. Bagwe Laboratory Supervi (601) 369-3624 VAB.0001200616 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: 2 ' ^r~ ^ Time Logged In />><g Ship Date: Product Car Ho.: tivr>'d Logged In By: /*f <3 Sllo(s): <j 77 trr Order No: -- / Customer: Compartment Sample From Bottom Moisture % .2o BL Contamination BR Bulk Density BD after Fluff Ski Hard Particle 7 * 5 Viscosity RVCM Ml .o&> 40 Mesh/Glaseies O Bottom . ft 2- Bottom r P* 3 JXL OO Bottom j 3 l o Screen Analysis Mesh Weight % 40 0,0 60 % MU 80 100 /y.y* }3>to 2fS 22k 120 A>37 140 i[M 200 311 7.1 Pan dk Ml Drytime: Ml Static Flow Color L: A>0< a V ,M Avg. Microns b /Jr Technician: 12) M *nJ- VAB.0001200617 A Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: March 5, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: February 29, 1992 VBIA Product: 5385 Railcar No.: PLCX 43053 Order No.: 0007361-001 Property Test Method Specification Volatiles, % ABR-1A 0.30 Max. Bulk Density, GM/CC ABR-2A .510 Min. Brabender Dry Time, Mins. ABR-7 6.0 Max. Particle Size, X on ABR-3 40 Mesh 0.1 Max. 200 Mesh NDS Pan 10.0 Max. 40 Mesh Glassies ABR-6 5 Max Avg. (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR--12 2 5 Max. Vinyl Chloride Monomer ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 0.17 0.573 4.9 0.00 12.4 3.2 2 3 0.196 0.94 Amy E. ^Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200618 * * Vista Polymers Highway 25 Aberdeen, MS 39730 A Time Logged Ship Date: 04,0 Product: 43Q SJ Logged In By: to Order OOP 12& 1160 Customer: Compartment A Sample From Bottom Moisture % BL Contamination ___ BR Bulk Density BD after Fluff ,~?3 Hard Particle 5 7 It 3 HA Viscosity RVCM ,%n 40 Mesh/Glassies 6 Screen Analysis h Mesh 40 Weight X 0.0 60 -Z / 1 CA Bottom 1 / ^ 1 CB Bottom , /ST 3 L . r 71 . B Bottom ,/< , T* 7J - 1 1 1i l. / 80 /^-7 100 U.30 ?Z-U 120 /o.n 140 7. JV /A7 200 A?.* Pan A r* a Drytime: Static Flow: . _,f_ / Co Avg. Microns: . 1SS.1 Color L: /0>'. a OL b Technician: M* rhT t VAB.0001200619 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 OERTTEICATE OE Aderdeep, Mississippi 39730-0091 Phone (601) 369-6111 ANALYSIS A Date: March 5, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 2, 1992 VISTA Product 5385 Railcar No. VIPX 45839 Order No. 0007891-000 Property Test Method Specification Analysis Volatilesi X ABR-1A 0.30 Max. 0.13 Bulk Densityt GM/CC ABR-2A .510 Min. 0.583 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Particle Size, X on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 6.9 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 2 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 10 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.117 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.~ Bagwe 1 Laboratory Supervi (601) 369-3624 VAB.0001200620 * Vieta Polymers Highway 25 A# RAILCAR ANALYSIS Load Date: . 3 ~ I Product: Car No. Time Logged In: 1.7QO Logged In By: m T S11o(b) : 60!& (o77-Ccfi Ship Date: Order No: / -006 Customer : (a&*6b\TO m Compartment A Sample From Bottom Moisture % BL Contamination BR tb Bulk Density .rtf BD after Fluff Hard Particle 5 30 7 tO Viscosity .460 RVCM Ml 40 Mesh/Glassies Screen Analysis Mesh 40 Weight % A. Q0 0,0 60 /.3f z.y CA Bottom /? Cf<? 80 li.Olf 3i. / 100 12-47 24.1 CB Bottom *!o 6? to B Bottom ,! 2- r7? / 120 1.7j /?. & 140 4.9i /o.o 200 I. 44 6.1 Pan , it- At Drytime: Static Flow: 0 / 9,0 Avg. Microns: Color L: 91,1.3- a .40 b 2-W Technician: At& VAB.0001200621 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X FI CATE OF* Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYS X S A Date: March 5, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 3, 1992 VISIA Product: 5385 Railcar No.: ACFX 41137 Order No.: 0007891-001 Property Volatiles, % Test Method ABR-1A Specification Analysis 0.30 Max. 0.12 Bulk Density, GM/CC ABR-2A 510 Min. 0.588 Brabender Dry Time, Mins. ABR-7 60 Max. 4.8 Particle Size, X on 40 Mesh ABR-3 0.1 Max 0.00 200 Mesh NDS 6.4 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 1 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max. 11 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0. 208 Inherent Viscosity ABR-10 .90 to .95 0. 92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. 'Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200622 Vista Polymers Highway 25 Aberdeen. MS 39730 #>< A RAILCAR ANALYSIS Load Date: ? Product: Time Logged In Ship Date: 0JTJO Logged In By: Order No: 00(5 Car No.: 4// 3 7 s tlo (e): _12+A2Z Customer: Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM AVkL 40 Mesh/Glassies Screen Analysis Mesh Weight % 40 d, && AO 60 80 fXSo 100 120 140 200 tk e M.Drytime: Static Flow: ^6 Avg. Microns: Color L a o,o7 b 17* Pan a jo a 3 Technician: VAB.0001200623 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSTS A Date: March 9, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 5, 1992 VISIA Product: 5385 Railcar No.: ACFX 41136 Order No.: 0008026-001 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.04 Bulk Density, GM/CC ABR-2A .510 Min. 0.582 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, X on 40 Mesh ABR-3 0.1 Max. 0.00 200 Mesh NDS 6.5 Pan 10.0 Max. 2.1 40 Mesh Glassies ABR-6 5 Max. Avg. 2 (By Compartment) Glassies average of 5 for rail 10 max. in a single compartment Hard Particles, 7 Mins. ABR-12 25 Max. 5 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.118 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200624 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: J-Z- 7 Z. Time Logged Ship Date: RAILCAR Product: ANALYSIS Car No. Acfx W/JO Logged In By: Sllolsl: C7- &S L O Customer: I4utnr Compartment A Sample From Moisture % Bottom - &3 BL Contamination BR Bulk Density 3 29 BD after Fluff Hard Particle 5 7 /3 J //? Viscosity M RVCM dil 40 Mesh/Glassies 2~ CA Bottom 21 Mk CB Bottom /8 . T B Bottom .otb Z Screen Analysis Mesh Weight % 40 >, or? ao Drytime: 60 80 100 120 140 200 Pan 32.7 /.*S~ -XL- 9/Static Flow: o L Avg. Microns: emt Color L: a b J37 Technician: VAB.0001200625 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: March 9, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus. MS 39701 Attention: Plant Chemist Ship Date: March 6, 1992 VISIA Product: 5385 Railcar No.: ACFX 41174 Order No.: 0008026-002 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max* 0.14 Bulk Density, GM/CC ABR-2A .510 Min. 0.584 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Particle Size, X on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 7.0 Pan 10.0 Max. 1.9 40 Mesh Glassies ABR-6 5 Max. Avg. 1 (By Compartment) Glassies average of 5 for rail 10 max. in a single compartment Hard Particles, 7 Mins ABR-12 2 5 Max. 3 Vinyl Chloride Monomer ABGC-26 85 Max. 0.084 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200626 Vista Polymers Highway 25 Aberdeeni MS 39730 A RAILCAR ANALYST AcfjK Load Date: Product: Time Logged In J2.O0 Logged In By: Ship Date: _______ Order No (o->>2^ Car No. Silo(e): Customer Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density . /3 /2 BD after Fluff Hard Particle Viscosity 5 7 tS 3 RVCM ,o& 40 Mesh/Glassies / Screen Analysis Mesh 40 Weight X Ol CtO 60 A Zc z.4 CA Bottom ,o1 A5T XU' CB Bottom JZ. <S& X9( B Bottom .IP /z xi i' _2______ O _2_____ 80 if. 347 100 rt.Wt 2. r.* 120 /7, J 140 200 j. Co Zo Pan JLI /.? Drytime: Static Flow: 0 / l<7 Avg. Microns: Color L: /0Q* 2/ a . o<? b ^ 71" JL *'% Technician: Mr'ffc VAB.0001200627 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSTS Date: March 10, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 9, 1992 VIS1A Product: 5385 Railcar No.: ACFX 41163 Order No.: 0008026-003 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.04 Bulk Density, GM/CC ABR-2A .510 Min. 0.582 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 7.5 Pan 10.0 Max. 1.7 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.004 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200628 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: 3 Time Logged Ship Date:_^J> RAILCAR ANALYSIS /Q-CFX f& Product: Car Ho. > O Logged In By: /W - Sllo(s): Order Ho: OtQDf\0'F<*-&2> Customer: Af Compartment A Sample From Bottom Moisture % BL Contamination BH Bulk Density oV 7 BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies c? CA Bottom CB Bottom o mr 8 $ .<2?/ c? C B Bottom .O Screen Analysis Mesh We ight % p 40 P c) OO 60 ? - 80 /2.J3 7 100 /*?d^'C, 120 / Ir(p3 <2^.0 140 11 * C& 200 3 if 7^ Pan *Y [ 7 Drytime: JLL Static Flow: O / /O-O Avg. Microns: /S7-7 Color L: a o-o < b Technician: ^tt VAB.0001200629 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X F1 X CATE OIT Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSTS A Date: March 12, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 11, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45913 Order No.: 0008026-004 Property Test Method Spec!fication Analysis Volatiles, X ABR-1A 0.30 Max. 0.19 Bulk Density, GM/CC ABR-2A .510 Min. 0.573 Brabender Dry Time, Mins* ABR-7 6.0 Max. 5.0 Particle Size, X on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.7 Pan 10.0 Max. 1.7 40 Mesh Glassies ABR-6 5 Max. Avg 1 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment* Hard Particles, 7 Mins ABR-12 2 5 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max 0.089 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001200630 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged Ship Date FVC RAILCAR ANALYSTS Product: Car No.: Logged In By: Silo(s): 060X024,- bofi Customer: > A Compartment A Sample From Bottom Moisture % BL Contamination BR J? 3 5 Bulk Density BD after Fluff .sso Hard Particle 5 /> 7* CA Bottom ./ D .S7S CB Bottom B Bottom z Screen Analysis Mesh 40 Weight % 0 tO 60 4.77 _Jj. 80 100 Jf ss MJL %n_ Si.X 120 IM. !7.S 140 4.4S 200 OM. S.7 s-o Static Flow: 0 //&.< Avg. Microns: Pan LIl z. Color L: /&0ol 7 a 03 b Technician: A VAB.0001200631 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CER I R IGATE OR ANA SIS A Date March 16, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 13, 1992 VIS1A Product*. 5385 Railcar No.: GACX 73380 Order No.: 0008026-005 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.06 Bulk Density, GM/CC ABR-2A .510 Min. 0.579 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 12.4 Pan 10.0 Max. 2.6 40 Mesh Glassies ABR-6 5 Max. Avg 1 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.191 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagw Laboratory Supervisor VAB.0001200632 f-- Vista Polymers Highway 25 Aberdeen, MB 39730 A Load Date: Time Logged In Ship Date: RAILCAR ANALYSTS Product: Logged In By: Order No: %blh-C>> <, Car No.: Silo(s): (plkctf.tss Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR /3 Bulk Density .S(oie BD after Fluff Hard Particle 5 7 Viscosity 1 Th RVCM dm 40 Mesh/Qlassies CA Bottom &8(o 0 CB Bottom IS 0 B Bottom o(& iz <2. Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % & OP ao >3 Co <o-o>l /.-3b l2dt Drytime: M Static Flow: a / Avg. Microns: /4^7 Color L: fa 3? a b J-W Technician: VAB.0001200633 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 3 Phone (601)369-8111 CERTI EICATE OF ANALYS X S A\ Date: March 18, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 16, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46570 Order No.: 0008026-006 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.15 Bulk Density, GM/CC ABR-2A .510 Min. 0.575 Brabender Dry Time, Mins. Particle Size, % on ABR-7 ABR-3 6.0 Max. 5.0 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.3 Pan 10.0 Max. 1.6 40 Mesh Glassies ABR-6 5 Max. Avg 2 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 7 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.144 Inherent Viscosity ABR-10 .90 to .95 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe1 Laboratory Supervi MRP VAB.0001200634 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Time Logged Ship Date: 3 - /5"-9 Product: Car No.: Logged In By: /M < / Silo(e): Order No: 8ozt,-C)06> Customer: 77 Compartment A Sample From Bottom Moisture % .13 BL Contamination BR /S^ Bulk Density BD after Fluff sn Hard Particle 5 7 Viscosity RVCM * 7 --fC^------------, .458 itf- 40 Mesh/Glassies / CA Bottom .i/ /3 ,n i Z CB Bottom ,/L S Z B Bottom *jr Sr .p VS" ,S72- / Screen Analysis Mesh Weight 40 *.00 60 80 /Ml 100 14.1* 120 t.SC 140 % fi.fi L 77.6 2/.JT 17.4 /. r 200 2.66 s: j Pan .Xo A Drytime: Static Flow: l / i*X Avg. Microns: n% I* Color L: jQO* ^9 a ,0V b A7f Technician: yb T-> VAB.0001200635 Vista Polymers A Division of Vista Chemical Company CERT I F7 X Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 F ANALYSIS Date '-SJ2-3 fa2^ Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: d// 9 / Z' Product: 5385 Lot No.: Trailer No.: 11 Order No.: OGC$)(0`Z&>~OO> Propertv Test Method Volatiles, '/. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification O.30 Max. .510 Min. 6.0 Max. Ana1ysis 0.1 Max. NDS 10.0 Max. bL 5. S' /, (o 5 Max . 25 Max. cz_ 5" 8.5 Max. .90 to .95 Not more than 8.5 PPM .*5 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. lit Laborat'ory pervisor/Lead (601) 369-3624 VAB.0001200636 Regulars or Bags & </$<7> * 7%?/2 bfe^ y Vinyl Sample Log Data s - as-92. KIlmtH* 34M % % * 2 &Aju# ir -0001200637 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CER X R I C A EE OR Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSTS * Date: March 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 19, 1992 VIS1A Product: 5385 RaiTear No UTCX 46592 Order No 0008026-007 Property Test Method Specification Analvsis Volatiles, % ABR-1A 0.30 Max. 0.08 Bulk Density, GM/CC ABR-2A .510 Min. 0.575 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 8.3 Pan 10.0 Max. 2.1 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 9 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.016 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E 7 Bagwe11 Laboratory Supervisor (601) 369-3624 mm VAB.0001200638 m H 4, Vista Polymers Highway 25 Aberdeen, MB 39730 A RAILCAR ANALYSIS Load Date: f2- Time Logged In OZoo Ship Date: Ml Product: Car No.: ,^ Logged In By: At 44 Order No: $0SL(> "Oo 7 siio(e )-._2^2Z^A Customer ..atA\.Cjcmo Compartment Sample From & Bottom Moisture % ,oB BL Contamination BR Bulk Density .S7SL BD after Fluff Hard Particle 5 ~3i 7 Viscosity RVCM 'bib 040 Mesh/Glassies ~s> Bottom QG 3 S7S & Screen Analysis Mesh Weight % 40 QJ> *>d0 60 .0 IS as 80 //// 22Z, 100 SLZ Drytime: i<g_ Static Flow: Color L !*& a C) Bottom /2 3it-T2- eb Bottom oS 3 7 c> 0 120 //.Sb 140 /2.G 200 4lK 13 Pan /OS 2.J /M3 Avg. Microns: 3^ b LCs&-- Technician VAB.0001200639 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 C EE re I R I CAT EE OR Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 ANALYSTS A Date: March 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 20, 1992 VISTA Product: 5385 Rai1 car No VIPX 45891 Order No 0008026-008 ProDerty Test Method SDecification Analysis Volatiles, % ABR-1A 0.30 Max. 0.16 Bulk Density, GM/CC ABR-2A .510 Min. 0.570 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Particle Size, % on ABR--3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 8.9 Pan 10.0 Max. 2.1 40 Mesh Glassies ABR-6 5 Max. Avg. 1 (By Compartment) Glassies average of 5 for railcar 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.045 Inherent Viscosity ABR-10 .90 to .95 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy ETC Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200640 # ^A i Vista Polymers Highway 25 Aberdeeny MS 39730 A Load Date: 3 ^ / 7- ? 2-- Product: Car No.: &rp?/ Time Logged In: 62* o Logged In By: Ship Date: ^hOrder Ho: --OQ% Silo(B) :__J Customer /?o r Compartment & 3- 2-0-9 ra S Sample From Bottom Moisture % * BL Contamination BR lie. 2 7 Bulk Density BD after Fluff ._5<P/ ) Hard Particle 5 12 7 31 Viscosity Bottom ./S' I 9 Bottom .a 2 f Bottom ./G 2 RVCM 40 Mesh/Glassies 0 / &L Screen Analysis Mesh Weight % 40 D,QO 0.0 60 Q.O1/ ft 80 2/ nr 100 /X</7 120 /<9-9& 2tU 140 7. of' /./ 200 Pan - M1 ?9 Drytime: ^0 Static Flow: 0 /C2*^ Avg. Microns:/vff ^ Color L: a b / t>9 Technician: VAB.0001200641 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C EE R X R X O A R ANALYSIS A Date: March 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 23, 1992 VISIA Product: 5385 Railcar No.: VIPX 45841 Order No.: 0008026-009 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.13 Bulk Density, GM/CC ABR-2A .510 Min. 0.576 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.3 Pan 10.0 Max. 2.3 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 6 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.099 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. agwe Laboratory Supervisor (601) 369-3624 VAB.0001200642 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date Time Logged In Ship Date: Product: Logged In By: t Order No: N 7*4* Compartment Sample From r z-22-vz s ( A) /ca) Bottom Bottom Moisture % BL Contamination ..... BR A2l Bulk Density BD after Fluff +f3 5 sz. JSCfH. Hard Particle 5 7 Viscosity RVCM .otf 40 Mesh/Glassies O o Car No.: gS3Y/ Silo(s): Customer: ac Bottom og J*k.,, , SS(c Bottom 9 ,s> jrgj u && Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight 0. 00 > 3> Jf.&Z % 0.0 t.'h $0.1 Drytime: Jg, 2kStatic Flow: ^ / Avg. Microns: /S"OJZ Color L: [ot,.07ff~ a rs/SL b l'(J7 Technician: VAB.0001200643 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: March 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0* Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 26, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45896 Order No.: 0008026-010 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.08 Bulk Density, GM/CC ABR--2A .510 Min. 0.589 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.8 Pan 10.0 Max. 1.4 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 6 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.107 Inherent Viscosity ABR-10 .90 to .95 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe Laboratory Supervi (601) 369-3624 VAB.0001200644 Vista Polymers Highway 25 Aberdeen, MS 39730 1 A RAILCAR ANALYSIS Load Date: Product: Car No. : *4^% % Time Logged In: Ot>30 Logged In By: to Silo(s): (pSS~ Ship =Date 2>{V*H Order No: frolM-D / O Customer: Compartment Sample From CD Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff .of jrisk7epcS a. S^3 Hard Particle 5 7 Viscosity RVCM 40 Mesh/Qlassies /&2_ Bottom <> J S'?/ Bottom .0 C 4 S'lA B Bottom *6 J J ie> , nt Screen Analysis Mesh 40 Weight % <Sa A& 60 80 oj2 30 100 IS'U JU 120 A O, Drytime: s:o Static Flow: & 140 ? 200 *??/ ft Pan JfLL UL Avg. Microns: Color L: /Oo.^l a b / Technician: ZLl -/ ft tf- VAB.0001200645, V X Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601)369-8111 CERTIFICATE OF ANALYST A Date: March 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 27, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46413 Order No.: 0008026-011 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.02 Bulk Density, GM/CC ABR-2A .510 Min. 0.576 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.8 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max. 6 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.121 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. at Amy E. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200646 Viata Polymers Highway 25 Aberdeen. MS 39730 A RAILCAR ANALYSIS Load Date 3-27-92- Product: Time Logged In: Logged In By: Ship Date: Order No: 4L4I3 Silo(e) :_W_Z7 Customer: &/4CQ#P /ISJ Compartment Sample From w mSBCpmi Bottom Moisture % BL Contamination BR .o Bulk Density BD after Fluff Hard Particle 5 ~ip 7 Viscosity RVCM 40 Mesh/Glassies .463 A2A 0 Bottom o 7 o Screen Analysis Mesh 40 Weight %P &O 60 8! \.L 80 33. ? 100 M3g a-C y Bottom . Of B Bottom *?7 c> 120 9. 140 -77 %e. 200 7-7 f 5,8 Pan ff t-s Drytime: .9 Static Flow: O / /0-3 Avg. Microns: Color L: /W* a -0-/Z- b / $2 Technician: /yi<~T VAB.0001200647 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A' Date: March 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: March 30, 1992 VIS1A Product: 5385 Railcar No.: ACFX 53666 Order No.: 0008026-012 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min. 0.588 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.6 Pan 10.0 Max. 1.2 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 13 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0. 092 Inherent Viscosity ABR-10 .90 to .95 0. 92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Q^W Amy E. Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200648 m Vista Polymers Highway 25 Aberdeen, MS 39730 A RAXLCAR ANALYSTS Load Date: ^ Time Logged In: 2S{ tro Ship Date: Product: Logged In By: Car No.: LU Silo(B): Customer: Compartment Sample From Moisture % Contamination Bottom Bottom .os Bulk Density BD after Fluff Hard Particle .388 Viscosity RVCM -4/8 40 Mesh/Glassies Screen Analysis Mesh Weight % 40 0.00 0,0 Drytime: 60 80 100 120 140 200 Pan aw Hr*H> >-.78 *.>t LSI Static Flow: ^ / %8 Avg. Microns: l(o%^ Color L: a b /ff Technician VAB.0001200649 V" Vista Polymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: April 20, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 16, 1992 Product: VISTA Railcar No.: ACFX 41168 Order No,: 0009830-000 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.04 Bulk Density, GM/CC ABR-2A 510 Min. 0.581 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.1 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 7.7 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 1 (By Compartment) A Glassies average of 5 for railcar; i 1 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 10 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0. 153 Inherent Viscosity ABR-10 .90 to .95 0, 93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E V Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200650 Vista Polymers Highway 25 Aberdeen. MS 39730 A PV C RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date: Product: Logged In By: Order No: Car No.: -//& 8 siio(s) I'&HS Customer Screen Analysis Mesh 40 Weight % -&LP 60 80 100 3o d2 7.6 120 Drytime: L Static Flow: & / Color L: / <90- J a ?b 140 /A A 200 3.8? 77 Pan 7/ 1.1 Avg. Microns Technician: /)A Sf VAB.0001200651 Vista Polymen A Division of Vista Chemical Company Highway 25 Poet Office Box 91 CERTI FICATE OF* Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: April 23, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 21, 1992 VISIAProduct: 5385 Railcar No.: GACX 73386 Order No.: 0009830-001 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.19 Bulk Density, GM/CC ABR-2A .510 Min. 0.578 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 7.6 Pan 10.0 Max. 1.9 40 Mesh Glassies ABR-6 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. ^7| 15 Max. Avg. CA | CB 0 B o 0 l0 0 Hard Particles, 7 Mins. ABR-12 25 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.048 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 'SknlW ........ mi if* if Amy E. ^Bagwell--J Laboratory Supervisor (601) 369-3624 VAB.0001200652 I 4 Vista Polymers Highway 25 Aberdeen, MS 39730 * RAILCAR ANALYSTS Load Date Product: Time Logged In: >&&& Logged Ship Date:_ Order No: * 'DO! Car No.: 733g (s Customer: Compartment Sample From Moisture % Contamination Bottom Bottom .is Bottom jsl Bottom Bulk Density BD after Fluff Hard Particle .72 .set Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 Weight 0.6 0 % 0.0 Drytime: 60 80 100 120 140 200 Pan O.SL /2-Vf iH.Slr If.49 Mi // 3.9. i -24- /.9 Static Flow: 0 /9.7 Avg. Microns: Color L: /00-'<f a o.// b Technician VAB.0001200653 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adendeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: April 27, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 23, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45791 Order No.: 0009830-002 Property Test Method Specification Analysis Volatiles, X ABR-1A 0.30 Max. 0.12 Bulk Density, GM/CC ABR-2A .510 Min. 0.591 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 7,7 Pan 10.0 Max. 2.0 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 2 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.154 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. dt Amy E.^Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200654 Vista Polymers Highway 25 A Aberdeen, MS 39730 Jr* A ILCAR ANALYSIS Load Date:. 4-/9-9Z Product: Time Logged Ship Date:_ Logged In By: 4t3oOrder No: 00 Car So.: ^79/ Silo(6): Customer a/o TrteM Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density b3 /O aT BD after Fluff Hard Particle 5 7 Viscosity RVCM dlk 40 Mesh/Glassies CA Bottom os iz CB Bottom .OS' /z 10 B Bottom ML /o Screen Analysis Mesh 40 60 80 100 120 140 200 Weight ^2 UZJ& IfMS % do tk(& 20l . 9.7 Drytime: 5T& Static Flow: d LS.f Color L: dM b Avg. Microns Pan Technician: VAB.0001200655 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: April 27, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 24, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45897 Order No.: 0010192-000 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max* 0.17 Bulk Density, GM/CC ABR-- 2A .510 Min. 0.585 Brabender Dry Time, Mins. ABR-7 6.0 Max 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 4.4 Pan 10.0 Max. 1.5 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.139 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. BagwelJr Laboratory Supervisor (601) 369-3624 VAB.0001200656 Vista Polymers Highway 25 A Aberdeen, MS 3S730 Load Date: Time Logged In: Ship Date -JkbA- RAILCAR ANALYSIS Product: Car No.: Logged In By: Silof a 1 : Order No: / 01 T Z** 0OD Customer : OtD Compartment A Sample From Bottom Moisture % * oQ BL Contamination BR 5 Bulk Density sii BD after Fluff p Hard Particle 5 7 /y Viscosity RVCM .m 40 Mesh/Glassies Screen Analysis Mesh Weight 40 0.Q& % 60 CA Bottom .(S' % ? tSl h CB Bottom (e> ,sw B Bottom ,n 3 ML oo 80 100 120 140 200 Pan n.?f 7 3.4/ Af2l 0. 7* J&l Drytime: Static Flow: 0 / $ (o Avg. Microns: //// Color L: /PO'^ff a 0.02 b AiZ Technician VAB.0001200657 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: April 27, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 24, 1992 VB1A Product: 5385 Railcar No.: UTCX 46461 Order No.: 0010192-001 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.07 Bulk Density, GM/CC ABR-2A .510 Min. 0.570 Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 6.0 Pan 10.0 Max. 1.7 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.025 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.L/Bagwel Laboratory Supervi (601) 369-3624 VAB.0001200658 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Load Date: *7*7 Product: Time Logged In: 423 Logged In By: Ship Date:.. 4(^4 _ Order No:_ Car No. Silo(s) : =>*77, Customer Compartment Sample From Bottom Moisture % BL Contamination BR ,o 2- Bulk Density BD after Fluff .47! Hard Particle 5 7 3 Viscosity .3/0 RVCM .01^ v40 Mesh/QIassies Screen Analysis Mesh Weight % 40 OcO'Q >. O 60 33 Drytime: Bottom / of Bottom Bottom .o7 o 0o 80 100 (j.fZ- 3?.t V.f 120 iu/ 140 200 Z3i L<o ILLStatic Flow: O / Avg. Microns: Pan JZ L2- 9 Color L: /0O37 a && b Technician: Op ^<=S- VAB.0001200659 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 RTIFICATE OF ANALYSIS A Date: May 1, 1992 Customer: GENCORP POLYMER PR P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 27, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46434 Order No.: 0009830-003 Property Volatiles, X Test Method ABR-1A Specification Analysis 0.30 Max. 0.15 Bulk Density, GM/CC ABR--2A *510 Min. 0.590 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.8 Particle Size, X on ABR-3 40 Mesh 0.1 Max 0.00 200 Mesh NDS 7.5 Pan 10.0 Max. 1.8 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 2 Vinyl Chloride Monomer ABGC-26 85 Max. 0.161 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervi (601) 369-3624 VAB.0001200660 k Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date 2: Product: Car No. : 4^^ Time Logged In: /<*Q& Logged In By: /??, / Silo(s): Ship Date: 4-lm : Q%$c-6b3 Order No Customer: tie Tne-tt Compartment A Sample From Bottom Moisture % 03 BL Contamination BR fi Bulk Density BD after Fluff Hard Particle 5 7 Viscosity FVCM Air. ./fe/ 40 Mesh/Glassies 0 CA Bottom .fiL o CB Bottom /Co & B Bottom js_ 3 SZ(a Screen Analysis Mesh 40 Weight % CLO 60 f.Sb 80 !j&7 100 120 140 200 Pan Ml -U- Ml- Drytime: Static Flow: o L 7.8 Avg. Microns : MS-/ Color L: 1*-^ a e,*f b /.*/ Technician VAB.0001200661 Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 1, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus. MS 39701 Attention: Plant Chemist Ship Date: April 28, 1992 VIS1A Product: 5385 Railcar No.: PLCX 43053 Order No.: 0010192-002 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min. 0.542 Brabender Dry Time, Mins. ABR-7 6.0 Max* 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 5.3 Pan 10.0 Max. 1.6 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 1 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.064 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. al Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200662 Vista Polymers Highway 25 Aberdeen, MS 39730 PVC RAILCAR ANALYSTS Load Date y- ?r_ Product Car No.: ysos 3 Time Logged In: /so P Logged In By: ,/ Silofsl: :4lM Ship Date Order No: 101^^^002^ Customer: 76-677 fii> ___ Compartment A Sample From Bottom Moisture % * BL Contamination __ BR Bulk Density Sit BD after Fluff Hard Particle 5 7 Itfc. Viscosity y tflC? RVCM 40 Mesh/Glassies o Screen Analysis Mesh Weight 40 e.e& % 60 5 * CA Bottom 3 .S30 CB Bottom .45" .3+ B Bottom .eS * 7 .3T IT 0 c> / 80 100 120 140 200 Pan US i'Q /&J3 3 (.fa Drytime: Static Flow: ^ ,/fJa Ava. Microns: Color L a 0~l& b # Technician r MIIIMMii VAB.0001200663 rr ft Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May It 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 29, 1992 VIS1A Product: 5385 Railcar No.: PTLX 41675 Order No.: 0010192-004 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.12 Bulk Density, GM/CC ABR-2A .510 Min. 0.554 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max 0.00 200 Mesh NDS 8.9 Pan 10.0 Max. 2.2 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 2 5 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.050 Inherent Viscosity ABR-10 .90 to .95 0.91 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe11 Laboratory Supervisor (601) 369-3624 VAB.0001200664 'r Vista Polymers Highway 25 Aberdeen. MS 39730 A RAILCAR ANALYSIS Load Date: Product r Car No.: 5 Time Logged In: Ship Date: [0^ Logged In By: Silo(s) : 2- Order No: / O/tf!7sCustomer: a/p ^-- Compartment A Sample From Bottom Moisture % BL Contamination BR /o Bulk Density BD .57+ Hard Particle 5 7 8 3& Viscosity .7/0 RVCM 0-50 40 Mesh/Glassies c> CA Bottom > CB Bottom /i3. tz 5ig B Bottom / & Screen Analysis Mesh Weight % 40 O. OQ 0.0 60 fl f3 09 80 jP, 71. 100 lUHP<?3 120 fpG 140 200 Pan UL 7 Drytime: +.g Static Flow: C d!& Avg. Microns Color L: 6>(o a b Technician: m VAB.0001200665 mmm m Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFXOATE OF ANALYSIS A Date: May 6, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: April 30, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45796 Order No.: 0010192-003 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.15 Bulk Density, GM/CC ABR-2A 510 Min. 0.585 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 12.9 Pan 10.0 Max. 2.8 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins ABR-12 25 Max. 4 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.165 Inherent Viscosity ABR-10 .90 to .95 0.91 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. :S<nl UJ Amy W. Bagwe\L Laboratory Supervisor (601) 369-3624 VAB.0001200666 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: 4-29 Time Logged In: Ship Date Product: Car No.: Logged In By: /2t /diS-ooS Silo(6) Customer: &?4 -4,7? Screen Analysis Mesh 40 Weight OtO*0 % O.o Drytime: Static Flow: Technician: Microns: i- VAB.0001200667 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 6, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 1, 1992 VIS1A Product: 5385 Railcar No.: PLCX 46853 Order No.: 0010192-005 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.22 Bulk Density, GM/CC ABR-2A .510 Min. 0.570 Brabender Dry Time, Mins. ABR-7 60 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.8 Pan 10.0 Max. 2.4 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max 2 Vinyl Chloride Monomer ABGC-26 85 Max. 0.067 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200668 Vista Polymers Highway 25 Aberdeen. MS 39730 HA1LCAR ANALYSIS Load Date: 4-3o -?2 Time Logged In : <o Product: Logged In By: Ship Date: Order No: Car No.: : SSilo(8): Customer tuVtrC A Compartment Sample From Bottom Moisture % BL Contamination BR .1? 3 Bulk Density BD after Fluff ,5*1 Hard Particle 5 7 Viscosity .QtD RVCM .Ob') 40 Mesh/Glassies 0 Screen Analysis Mesh 40 Weight p-Qq % 60 .13 f.S Bottom .2.2- ? ,(?o . . 0 80 Ml 1^1 100 (\CB ) Bottom Al X ff IV B J Bottom .2( 3 ,bo ' . o 120 13, n J6.7 140 1C S' 200 1.31 Pan Uf id.s a.v Drytime: Static Flow o 9.o/ Avg. Microns: MS Color L: ^^ a b JAL Technician: VAB.0001200669 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I E I C<ATE OF- ANAL.YS I S AI Date: Customer: GENCQRP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Product: 5385 Lot No.: 0*4(t)Q\9 Trailer No. : fZ Order No. : OQI Propertv Test Method Vo 1 a t i 1 es , V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analvsis . /3 0.1 Ma x NDS 10.0 Max 5 Max . 25 Max. 8.5 Max. .90 to .9 OJ2 St. I o (o Not more than 8.5 PPM .4Z, Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora (601) 369-3624 VAB.0001200670 Regulars or Bags Pagoofpages Vinyl Sample Log X-13 Date Product Typo rx Altai*#* 1ISI VAB.0001200671 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 AI Date: May 22, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 18, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46390 Order No.: 0011213-000 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.16 Bulk Density, GM/CC ABR-2A .510 Min. 0.581 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.9 Pan 40 Mesh Glassies ABR-6 10.0 Max. 5 Max. Avg 2.9 0 (By Compartment) Glassies average of 5 for railcar; 10 max* in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max 2 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.055 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy S'. Bag Laboratory Supervi (601) 369-3624 VAB.0001200672 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: Product: Time Logged Ac30 Logged In By: Ship Date Sis Order No: /Z|3 Car No. Silo(s): Customer: /to M Compartment A Sample From Bottom Moisture % BL Contamination BR JL to G Bulk Density BD after Fluff Hard Particle 5 7 si*) ___ z a/ Viscosity * RVCM 40 Mesh/Glassies > CA Bottom a Ce CI2- O CB Bottom .A <S~ S'So O B Bottom .Jt .r/J 0 Screen Analysis Mesh 40 Weight 60 Lq A 2. 80 10.30 So% (* 100 ism 2 7. S" 120 II. *+ 2j.y 140 13. sT 200 _ /4.1 Pan /.vr~ Drytime: Static Flow: o /7,7 Avg. Microns: Color L: Joo* L2* a b 4 1A Technician VAB.0001200673 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 OF ANALYSX S A Date: May 22, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 21, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45714 Order No.: 0011213-002 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.06 Bulk Density, GM/CC ABR-2A .510 Min. 0.580 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Particle Size, X on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.6 Pan 10.0 Max. 2.8 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 2 5 Max. 1 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.030 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. / Amy /. Bag Laboratory Supervisor (601) 369-3624 VAB.0001200674 Vieta Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: Ship Date: 2- Product: m Logged In By: Order No: 1(7(3 Car No.: 4s 7/4 Silo(e): Customer : teORJLCrT Compartment A Sample From Bottom Moisture % .bL BL Contamination BR z. s Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM .0^0 i 40 Mesh/Glassies 0 Screen Analysis Mesh Weight % 40 0.0 o ** ; 60 o. Vi- $ CA Bottom i r S? 1 CB Bottom 2. 3 B Bottom > Y ,s~!l 6 oO 80 100 120 140 200 Pan /V. 32. 11.po Slzf 2i.<> /g.? Ja.C Drytime: . Static Flow: c> / Avg. Microns: /JO- 7 Color L: /fit. D& a 0-O'i- b /-<? 4 Technician: /T" ^ /Zft VAB.0001200675 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 OE1RT X FICATE OF Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 22, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46433 Order No.: 0011213-001 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.05 Bulk Density, GM/CC ABR-2A .510 Min. 0.575 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 8.2 Pan 10.0 Max. 2.3 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 3 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.088 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200676 Vista Polymers Highway 25 Aberdeenf MS 39730 Load Date: S''JL A -f Product Car No. Time Logged In: / S0 & Logged In By: /?f t Silo(e): Ship Date = 57_ Order No: /I 2V`S> ~QO / Customer: - >7 Compartment A Sample From Bottom Moisture % *03 BL Contamination 3 BR _6_____ Bulk Density BD after Fluff Hard Particle 5 7 7 3 33 Viscosity Am RVCM .on 40 Me6h/Glassies d> CA Bottom . cO__ 1 .383 o CB Bottom i .<rP f O B Bottom Y l .31/ z> Screen Analysis Mesh Weight %p 40 &o dp 60 All 4^o 80 il 100 12.13 120 /e>.4 140 C>- / (- /a-3 200 Pan d/C JLJSk 9-X a. 3 Drytime: 8 p Static Flow: O //Avg. Microns: ///- b Color L: fQ6 .13 a j{?,o b A 73 Technician: Irtt~T ^ hi VAB.0001200677 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 26, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46434 Order No.: 0011441-000 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.14 Bulk Density, GM/CC ABR-2A .510 Min. 0.579 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh Pan * NDS 10.0 Max. 9.0 2.7 40 Mesh Glassies ABR-6 5 Max. Avg. 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 1 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.040 Inherent Viscosity ABR-10 .90 to .95 0.92 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. . Bag Laboratory Supervisor (601) 369-3624 VAB.0001200678 * Vista Polymers Highway 25 Aberdeen, MS 39730 A) RA I LC AR ANALYSIS Load Date:. S-'L'O Time Logged In DU-OO Product: Logged In By: Car No. : do siiof s'): (. 77.L7L Ship Date: Order Ho: /I ''OOP Customer a/o Mer>n Compartment A CA CB Sample From Moisture % Bottom Bottom Bottom BL Contamination BR 3 3 Bulk Density 21 BD after Fluff 2 < Hard Particle 5 7 Viscosity 1 I r*t> rtuv^ CAc^v RVCM ,04 40 Mesh/Glassies iT'/z ' .4a. 3 $A4+f**- funn Screen Analysis S/^syfa. .f Mesh 40 We Ight /O. 05 % 60 80 100 120 140 A/,.22-- t>3U <w-S |A-7 B Bottom 4ft /<? 2i 5?? * .F ' 200 Pan <5Z- l3tt- %o . M____ Drytime: Static Flow: ^ / Avg. Microns: Color L: a - b /?<* VAB.0001200679 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: May 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 26, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45727 Order No.: 0011213-004 Property Test Method Specification Analysis Volatiles, X ABR-1A 0.30 Max. 0.14 Bulk Density, GM/CC ABR-2A 510 Min. 0.576 Brabender Dry Time, Mins ABR-7 6.0 Max. 4.9 Particle Size, % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.2 Pan 10.0 Max. 2.6 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 2 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.040 Inherent Viscosity ABR-10 .90 to .95 0.93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe Laboratory Supervi (601) 369-3624 VAB.0001200680 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSTS Load Date : ^ ^ Product: Time Logged In: Ship Date: vldJe Logged In By: Order No:. Car No.: 457&7 f , Silo(s): Customer: ^(Ud4hrp Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight b%oQ $St> 13 fOMj, C.2D Xo9 /,2Q llA% o.o L3. 2S,o 2U I3.if fQ'^ 3. L Drytime: *L1 IIL3.Static Flow:. o LJlJLildJ Avg. Microns: Color L: jOt>. 7X> <c>8 b /jr Technician > t- VAB.0001200681 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 27, 1992 VfSIA Product 5385 Railcar No. VIPX 45796 Order No. 0011213-005 Property Test Method Specification Analysis Volatiles, % ABR-1A 0.30 Max. 0.13 Bulk Density, GM/CC ABR-2A .510 Min. 0.576 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Particle Size , % on ABR-3 40 Mesh 0.1 Max. 0.00 200 Mesh NDS 10.8 Pan 10.0 Max. 3.2 40 Mesh Glassies ABR-6 5 Max. Avg 0 (By Compartment) Glassies average of 5 for railcar; 10 max. in a single compartment. Hard Particles, 7 Mins. ABR-12 25 Max. 2 Vinyl Chloride Monomer ABGC-26 8.5 Max. 0.171 Inherent Viscosity ABR-10 .90 to .95 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed UO Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200682 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: >'2&-'<7 Time Logged In: Ship Date:. 'LL? Product: Car No. Logged In By: Order No: ll^l 3*^6)S"" Silo(s): & Customer 4LCcnrt> Compartment A Sample From Bottom Moisture % BL Contamination BR 1 r Bulk Density .s$y BD after Fluff Hard Particle 5 S 7 3<L Viscosity W RVCM ,n\ 40 Mesh/Glassies o CA Bottom .c? 2. (p <J13 O CB Bottom C>jT j > SLl o B Bottom 6 3 fT o Screen Analysis Mesh Weight 40 Oc oO % Oc o 60 80 100 120 UAL 133$ tb.t3 l-% 21.1 2/(* 140 13.3 200 Pan s.ys /.2_ to, t 3tX. Drytime: _ S.O Static Flow: 0 / * Avfl. Microns: /S3. 1 i i ^' Color L : ar bA Technician: jk VAB.0001200683 Vista Polymers A Division of Vista Chemical Company C EE FR ~T I R* I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date; Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date Product: 5385 Lot No.: Trailer No.: 7^4^032-4? Order No. t OO t !tpj')~ OC) Propertv Test Method Volatiles, '/. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analvsis . /tT if 0.1 Max NDS 10.0 Max 5 Max . 25 Max. 8.5 Max. .90 to .9 o.o *Ll uL o V Not more than 8.5 PPM Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory (Supervisor/Lead (601) 369-3624 VAB.0001200684 Regulars or Bags Paga of pages 6 Vinyl Sample Log %'Zo - ?/ Date Product 1 VAB.0001200685 > Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 SXs A Date: June 2, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 28, 1992 VBIA Product: 5385 Railcar No.: VIPX 45864 Order No.: 0011213-007 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.14 .510 Min. 0.580 6.0 Max. 5.0 0.1 Max. 0.00 NDS 9.3 10.0 Max. 2.7 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.125 0.93 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200686 Vista Polymers Highway 25 Aberdeen. MS 39730 Load Date: Time Logged Ship Date: ]PVC RAXLCAR ANALYSTS 2- Product: 5385 Car No. _ Logged In By: Silo(s) Order No: OC*1 Customer: A Compartment A Sample From Bottom Moisture % , vl BL Contamination BR z Bulk Density sgf BD after Fluff Hard Particle 5 7 s. Viscosity RVCM . . /Z5" 40 Mesh/Glassies 0 CA Bottom 3 ,ssi O CB Bottom elU ,577 B Bottom ---#--/vf---- JL Oo Screen Analysis Mesh 40 Weight 0-ov 60 .31 % 0&-1. 80 lUl? <?.? 100 120 M0 /*.?? 22.0 140 200 6JOS Pan h3f, 2.7 Drytime: S,b Static Flow: Z IM Avg. Microns Lis'Color L : bK &> a oV' b !SW Technician: VAB.0001200687 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: June 2, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: May 28, 1992 VISIA Product: 5385 Railcar No.: PTLX 41675 Order No.: 0011213-006 Property Test Method Volatiles, X ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins* ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.16 .510 Min. 0.580 6.0 Max. 5.0 0.1 Max. 0.00 NDS 10.5 10.0 Max. 2.9 5 Max. Avg,* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compart dent Hard Particles @ 7 Mins. ABR-12 2 5 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent VisLcosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.090 0.93 Amy E.^Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200688 Vista Polymers Highway 25 Aberdeen. MS 39730 * RAILCAR ANALYSIS Load Date Time Logged In:. 01t>x> Product: Logged In By: Ship Date: Order No: I fZ-l t>'OQ(e Car No , <4t(,7r Silo(s) : ..4 7Cj Customer Compartment A Sample From Bottom Moisture % J1 BL Contamination BR 3 Bulk Density <$11 BD after Fluff Hard Particle 5 7 I J/&> Viscosity Ata RVCM Mo 40 Mesh/Glassies o CA Bottom * ( .$$3 o CB Bottom , o(*> 2 5 .$14 o B Bottom JC 3 .S 74 O Screen Analysis Mesh Weight 40 0<OQ % -&.P 60 ,13 hi 80 Ml o.3 100 13,31 Stl.S 120 UOL 140 C.&? (3.g 200 Pan S'W !.H3 fog~ IS. Drytime: Static Flow:. o L Avg. Microns Color L: W.1J a . o3 b L )S2J 0>Technician : VAB.0001200689 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369*8111 CERTIFICATE OF ANALYSIS Date: (/, Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Product: 53B5 Lot No. : OQ-Qdb Trailer No.: Order No.: ODtalC$3-'0&C) Property Test Method Volatiles, V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR--6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis 0.1 Max NDS 10.0 Max 5 Max . 25 Max. 8.5 Max. .90 to .9 o.o 57-3 . 4O Not more than 8.,5 PPM Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200690 Regulars or Bags Page of pages Vinyl Sample Log AM. Date Product Type Allnwrttf 24M 4 VAB.0001200691 * Vista Polymers A Division of Vista Chemical Company CEF Highway 25 Post Office Box 91 2 ATE OE Aberdeen, Mississippi 39730 Phone (601} 369-8111 sis A Date: June 19, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbusy MS 39701 Attention: Plant Chemist Ship Date: June 15y 1992 Product 5385 Railcar No. ACFX 41169 Order No. 0012458-000 Property Test Method Volatilesy X ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 X on 40 Mesh X on 200 Mesh X on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.14 .510 Min. 0.581 60 Max. I 5.0 0,1 Max. 0.00 NDS 13.5 10.0 Max. 4.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles # 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.047 0.93 Amy EY Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200692 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAXLCAR ANALYSTS Load Date:. 5^0 Time Logged In: noo Ship Date: Inti'S Product: Car No. : ALAiA Logged In By: Silo(e): Order No: \'LLb%~66h Customer :0 Compartment Sample From Bottom p Moisture % Jl GL Contamination BR 2 Bulk Density S7L BD after Fluff Hard Particle 5 % 7 iCt, Viscosity Av$ RVCM .oH-n 40 Mesh/Glassies 0 C3iCk Bottom 3 Bottom JAL (3 Si2 O Bottom . /1~ Z l( ,5#X Screen Analysis Mesh Weight % 40 0*0 0 o.-o 60 Ml- 80 7. t>7 m. 100 120 f.o73 ?/ 7 IS. 2 140 /o./ff 200 A 77 :Drytime 5.0 Static Flow: o /l.t Avg. Microns Color L: f a 1 /-2 b Pan /.?g V.O Technician: -5 VAB.0001200693 4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 * Date: June 22, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: June 19, 1992 VK1AProduct: 5385 Railcar No.: VIPX 45901 Order No.: 0012458-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.581 6.0 Max. 5.0 0.1 Max. 0.00 NDS 7.3 10.0 Max. 2.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles G 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.064 0.93 Amy EX Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200694 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: ^ Time Logged In: Ship Date :jWl2 RAIL, CAR ANALYST S Product: Logged In By: Order No: 1 Car No.: Silo(s): Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR ,// <r / Bulk Density BD after Fluff / S7.2. Hard Particle 5 /r 7 Z M0 Viscosity RVCM * 4 Ain 0(*4 40 Mesh/Glassies 0 Screen Analysis Mesh Weight 40 0,6 0 . % -P-C 60 .73 /r CA Bottom ,/j r CB Bottom ,at 7 J ,r77 B Bottom . /JL tz i nr ,S7 ** o OO 80 -2 O 100 /r.z* Jo.s~ 120 /hop 140 sr.ti //./ 200 Z3 Pan .If Z.0 Drytime: .T. 0 Static Flow: $ / Avc. Microns: /r?. / Color L: /OCx/f a / f b /. *r Technician: f VAB.0001200695 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERTIFICATE OE ANALYSIS Date: June 22, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: June 19, 1992 ... VKIAProduct: * Railcar No.: VXPX 45796 Order No.: 0012458-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 ]Mesh % on 200 Mesh X on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.05 .510 Min. 0.581 6.0 Max. 4.8 o oo 0.1 Max. NDS 6.6 10.0 Max. 1.8 5 Max. Avg. 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.142 0.93 ^ . f> f 1/ Amy JLt Bagwev4r' Laboratory Supervisor (601) 369-3624 % VAB.0001200696 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: < -9 Product: Car No. 4^ r7^ Time Logged In: Ship Date /&QQ Logged In By: m. Order No I "GOV" Silo(s) /l* Customer . G>Otu rt/O r?tc^4-CL f Compartment A CA Sample From Bottom Bottom Moisture % BL Contamination BR . O1/ 9 Bulk Density BD after Fluff .3> 3(=> Hard Particle 5 3 ( 7 Z =T$ C Si* Viscosity RVCM . Ik* ,/4^ 40 Mesh/Glassies V c> CB Bottom 4- (r r . JT7? o B Bottom & Screen Analysis Mesh 40 Weight %r OO 60 a-*7 80 100 120 f -3^ UA- 2,0 /&> f 2-Z-l 2&.f ?A3 140 /<> 3 200 Pan 3-2? .SJ r1 AP. Drytime (62 Static Flow: & / $ *1 Avg. Microns: //* -S- f Color L: fOO' a b ?-9<f Technician: sP{ * VAB.0001200697 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: June 23, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: June 18, 1992 ... VB1AProduct Railcar No. s PLWX 44723 Order No. : 0012458-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 .510 Min. 0.591 6.0 Max. 5.5 0.1 Max. 0.00 NDS 10.3 10.0 Max. 6.5 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 6 0.073 0.92 Amy E\ Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200698 Vista Polymers Highway 25 Aberdeen, MS 39730 A I* VC RAILCAR ANALYSIS Load Date: Product: Car No.: 4^7 aJ Time Logged In Logged In By: Sllof e ) : Ship Date: (o\[% \9U Order No:. OOlZti&'DQ / Customer: ?-&X fJo -- Compartment A CA Sample From Bottom Bottom Moisture % BL Contamination BR 11 .IS Bulk Density BD after Fluff SM Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies o CB Bottom .17 ,SS5i oO B Bottom 11 n O Screen Analysis Mesh Weight % 40 O" oO ao 60 O.&S // 80 o frSL 100 120 f(&7 U -o 140 200 Pan &to foJZ 'V Drytime: Static Flow: ^ Avg. Microns Color L:. / L*La #./A b I'M" Technician: H. VAB.0001200699 Vista Pbiymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: June 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: June 22, 1992 VIS1A Product: 5385 v m Railcar No.: VIPX 45797 Order No.: 0012458-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.08 .510 Min. 0.574 6.0 Max. 4.8 0.1 Max 0.00 NDS 10.4 10.0 Max. 2.7 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.041 0.93 ------2?---------j------------------------- H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200700 Viat:a Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Bate: / -/?- ?2~ Time Logged In: 2 3 JX Ship Date Product Car No. *s-??7 Logged In By: S j 1o(e ) : I7t,t?7 Order No: $&/~C0*7 Customer: slS z> rH Compartment A Sample From Bottom Moisture % BL Contamination BR jL $ Bulk Density BD after Fluff .-57'/ Hard Particle 5 7 i Viscosity 1 723 (fet RVCM .0*1 40 Mesh/Glassies & CA Bottom * s IX .577 l CB Bottom /* ,s&% 10 B Bottom . oS~ 7 . _S7< O Screen Analysis Mesh Weight 40 &'Q %O 60 AZ 80 /?<% 100 /.y$1 21% 120 /2- 27 2S </ 140 7-ZH I9.C, 200 Zs12- Pan AJJ Drytime: Static Flow: /O f/0'3 Avg. Microns: /%? Color L: f 00.73 0'OV b A7? Technician: /9t2 7^ VAB.0001200701 Vrsta Polymer? A Division of Vista Chemicol Compony Highway 25 Post Omce Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 OJF* ANALYSIS A Date: June 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: June 22, 1992 VISIAProduct: 5385 Railcar No.: VIPX 45838 Order No.: 0012458-005 Property Test Method Volatiles, X ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh X on 200 Mesh X on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.14 .510 Min. 0.579 6.0 Max 4.9 0.1 Max. 0.00 NDS 9.0 10.0 Max. 2.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles G 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.074 0.93 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200702 Vista Polymers Highway 25 A Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load =Date -/f-n Time Logged Ship Date: Product: Logged In By: Order No : @ Car No.: /V^TT Silo(s) : Cl C i L~)~) G>Customer : JhSL Compartment A Sample From Bottom Moisture % BL Contamination BR j* /< Bulk Density BD after Fluff . ;TS3 Hard Particle 5 /t 7 2- AtA Viscosity RVCM % 40 Mesh/Glassies 0 Screen Analysis Mesh 40 Weight 0.00 % *0 60 /jl CA Bottom ,// /J z . sio 0 80 //.// 22.2- 100 2f. f CB Bottom - /0 7 * B Bottom ./ Je . sr? oO 120 i).n 23. 4 140 iL.e /2.J 200 J.o Pan /. /& Drytime: Static Flow: /3 /y.9 Avg. Microns: /ts'.o Color L : lO d. *! a b j.if Technician: VAB.0001200703 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: 6 Product: 5385 Lot No.: Trailer No.: '*T3V7 Order No.: OOt$1ft7~G00 Propertv Test Method Vo 1 a t i 1 es , X ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassi es ABR-6 Hard Particles , 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis .oS ,S7& __& / 0.1 Max. NDS oo 7.o 10.0 Max. 5 Max . 25 Max. el / o 3 8.5 Max. Not more than 8.5 PPM .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory^Sup visor/Lead (601) 369-3624 VAB.0001200704 I PVC BULK TRAILER ANALYSIS Date C/z-s/ Product Customer Silo___ & Technician. A f AH ISO MOIST CONT. Trailer -- Order GEL BULK DENSITY Number 3?? COLOR L = Me*,z9 FRONT A - O, B = / *7 L= MIDDLE 2. I li END A= B= i L= A= B= A RVCM Particle Size Distribution; Screen Analysis to Mesh Size 40 Gross Wt Tare Net Wt. H on Mesh &6Q 6*0 Screen Analysis % t' V Mesh Size Gross Wt Tare Net Wt. % on Mesh 40 Min On Aotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 0-Tf !3. H If-dJ a: hi Li dO- (a J$d S*>*S l*>-9 2 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 60 100 120 140 200 / b(o _Q Glassy Pan Part. Remarks Visto Polymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Dates (efstffal' Product: 5385 Lot No.: 0*4431 Trailer No.: *4Qo'Z,>2> Order No.: >> {Z*? <41-660 Property Test Method Volatiles, 7. ABR-iA Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analvsis Of Ml 5/ 0.1 Max. NDS O-6 C,. f 10.0 Max. 5 Max . 25 Max. JU 0 Si 8.5 Max. .90 to .95 Not more than 8.5 PPM . f/ Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labora (601) 369-3624 VAB.0001200706 BLEND NO: >4%?/ RESIN BAG Bj-cND PRODUCT: Avg. Hicroas, 5225/5325/5415: _ VB. OOO1200707 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369 811 1 RTXFICAT OF ANALYSX S A Date: July 8, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 3, 1992 VIS1A Product: 5385 Railcar No VIPX 45885 Order No 0013275-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.576 6.0 Max. 5.1 0.1 Max. 0.00 NDS 8.3 10.0 Max. 2.1 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.105 0.93 Amy ET. Bag fell Laboratory Supervisor (601) 369-3624 VAB.0001200708 Vista Polymers Highway 25 Aberdeen, MS 39730 A FVC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date:. Product: 5385 Car /Q Logged In By: /*? Silo(6) : Order No: \^)Z'7SZ^>6& Customer: /Z4> /aZH Compartment A Sample From Bottom Moisture % BL Contamination BR ,K Bulk Density BD after Fluff . 5-72. Hard Particle 5 7 Viscosity ZJhi RVCM IQ$~ 40 Mesh/Glassies 0 Screen Analysis Mesh Weight % 40 a. oo . 0*0 60 ,?* CA Bottom M- s __ , S"7f CB Bottom ./ A - .s-?r 1,1 B Bottom n - OO <? 80 IcJo z/, P 100 /*, z?.C 120 }! Z3.t 140 L.*o /Z- z 200 4./3 Z.3 Pan /. 07 z. j Drytime: S'./ Static Flow: 0 /y.f Color L:: ff. Of a ""-// h kva. Microns: - /S4.z /*1tA ftTechnician: VAB.0001200709 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: July 10, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 8, 1992 VISIA Product: 5385 Railcar No.: VIPX 45833 Order No.: 0013315-001 Property Test Method Volatiles, % ABR--1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 .510 Min. 0.576 6.0 Max. 4.9 0.1 Max. 0.00 NDS 6.1 10.0 Max. 2.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.053 0.94 Laboratory Supervisor (601) 369-3624 VAB.0001200710 Vista Polymers Highway 25 A Aberdeen, MS 39730 TRAIL LCAR ANALYSIS Load Date: 3-*5 2~ Time Logged In Ship Date:_lZ 1 Product Car No.: Logged In By: Silo(6) Order No: /,^5/S 00/ Customer A/e "TnetfiL- Compartment A Sample From Bottom Moisture % .03 BL Contamination BR S u. Bulk Density .TS$L BD after Fluff Hard Particle 5 j_ 7 3u. Viscosity RVCM * 'D^3 40 Mesh/Glassies 0 -. CA Bottom .1^ if s ,5V<? r1 > o - CB Bottom n *5fSL / B Bottom /* 7 ,S9& A & Screen Analysis Mesh Weight % 40 ^ && . 60 A 37 23 80 /7/o <f- 100 fft**? 03.0 120 140 200 Pan jrof 1. *9-1 0e> Drytime: o ZS fLUStatic Flow: / Avg. Microns: Color L: oJ7 b L?f Technician: trrz+HA. r mrnmmmmmmmmmmm VAB.0001200711 Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: July 10, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 7, 1992 VISIA Product: 5385 Railcar No.: PLCX 43431 Order No.: 0013315-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh X on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.04 .510 Min. 0.577 6.0 Max. Lj. 0.1 Max. 0.00 NDS 5.9 10.0 Max. 1.9 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.Jl5~ 0.94 Laboratory Supervisor (601) 369-3624 W mm m wmnmmmmfmm VAB.0001200712 Vista Polyme rs Highway 25 A Aberdeen, MS 39730 FVO RAILCAR ANALYSIS Load Date 7-3 - fZ Time Logged In o&od ihi Ship Date Product: Logged In By: OOI6^1S Car No. C?#3/ Silo(6): Customer Compartment Sample From Moisture % Contamination Bottom Bottom .03 Bottom ,C>Y Bottom Bulk Density BD after Fluff Hard Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 Weight X -D Drytime: 60 A- S~3 // 80 JCJ 100 . 21.1 120 1J7 n.s' 140 200 X? Pan (.? Static Flow: > /2.? Avg. 1Microns: /&?./ Color L: a b /, fO 7t- K Technician: VAB.0001200713 1 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A Date: July 15, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 10, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45910 Order No.: 0013315-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.11 .510 Min. 0.566 6.0 Max. 4.9 0.1 Max. 0.00 NDS 8.6 10.0 Max. 3.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 2 5 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 * Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 5 0.050 \ 0.94 Laboratory Supervisor (601) 369-3624 VAB.0001200714 Vieta Polymere Highway 25 A Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date: 7-7-7 I Product Time Logged In: <Q &OG Logged In By: Ship Date: 0 Order No Car No.: 1 Silo(6): Customer: Wjq Compartment A Sample From Bottom Moisture % (/ BL Contamination BR <e Bulk Density ,5t>8 BD after Fluff Hard CA Bottom ,oJ CB Bottom 3 S~ B Bottom .qIq ? m Screen Analysis Mesh 40 Weight 0*00 % 0*Z> 60 80 100 120 V 13.of M3I 2 4. A fcfy O 140 6,yj /2, y 200 Pan V31 1_sa f.C. Drytime: Static Flow: o L llz Avg. Microns: tss.f Color I>: /&$<a jG.b CoTechnician VAB.0001200715 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: July 15, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 13, 1992 VKIA Product: 5385 Railcar No.: UTCX 46526 Order No.: 0013315-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.16 .510 Min. 0.578 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.1 10.0 Max. 3.2 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to 95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 4 0.036 0.94 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200716 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date 7 IS RAILCAR ANALYSIS Product: Car No Logged In By: Silo(s): Order No:. ISS I ^"C>o Cuetome Screen Analysis Mesh 40 Weight 0*00 % 0.0 . 60 0.13 f-s 80 12. ll 25.7. 100 N-ob 2.8'/ 120 f0(oio 2/c 140 S. 9 J/.4 200 9./ Pan / 3Z Drytime: Static Flow: O /fao Avg. Microns: Color L: a b vrt Technician: 7m iMM m VAB.0001200717 T Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 __V'S5 I S A Date: 7 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: j VISIA Product: 5385 Lot No. 04&&7 Trailer No. r- 48003/ Order No.: Q@ / 7""10OO Propertv Test Method Vo 1 a t i 1 es , 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis 0.1 Max. 0.0 NDS 10.0 Max. 5 Max . /AJL 2.1 -& 25 Max. 8.5 Max. .90 to .95 _____ Not more than 8.5 PPM . 12. Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200718 Ragutars or Bags Page of pagas o Vinyl Sample Log j HP Bulk 1 Dry icntn G./C.C.I Tima St % [ -P ,SS$L Z'.O Data Product Type 4 MlmoAtf 24M ife VAB.0001200719 > Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 X CATE OF ANALYSIS A Date: July 20, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 16, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46557 Order No.: 0013315-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 510 Min. 0.577 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.3 10.0 Max. 2.8 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 0 0.061 0.93 Lit Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200720 Vista Polymers Highway 25 A 11 Aberdeen, MS 39730 Load Date 7- /- 7-2. Time Logged In: Ship Date RAILCAR ANALYSIS Product: Car No Logged In By Order No: t? g>/svoo<^ Silo(s): Customer: AO Mjsfci Compartment r Sample From A Bottom Moisture % BL Contamination BR Bulk Density J3 t BD after Fluff Hard Particle 5 -j/y , 7 Viscosity ___ __ _ _ _ RVCM *__ * 40 Mesh/Glassies <? Screen Analysis Mesh 40 Weight % 0. o 60 rlZ~ L2, CA Bottom jf *<> r CB Bottom .n ? 1 B Bottom 22 <f /? .JTX, M0 // 80 i3-k> Z4*<f 100 l4.o7 Zt> / 120 /0* Zo.1 140 ST7 //.3 200 1.1 Pan /.?/ 2.t Drytime: Static Flow: fi /7.1 Avg. Microns: Color L: *7 b /: Technician: VAB.0001200721 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: July 20, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 17, 1992 VISIA Product: 5385 Railcar No.: UTCX 46566 Order No.: 0013315-005 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 1Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.04 .510 Min. 0.581 6.0 Max. 4.9 0.1 Max. 0.00 NDS 11.0 10.0 Max. 3.6 5 Max. Avg. * 2 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.073 0.93 Amy E. Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200722 Vista Polymers Highway 25 A Aberdeen, MS 39730 IRA I LCAR ANALYSIS Load Date Time Logged In: //J** :Ship Date 7/r? Product: Car No.: Logged In By: Silo(6 ) :_AZLA2?, t&'T' Order No: * OOS Customer: d &* fTM * Compartment * Sample From A Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff $> 571 Hard Particle 5 if 7a Viscosity AV\ RVCM .073 40 Mesh/Glassies J J CA Bottom >e>2_ 7 .5-7^ CB Bottom of / .sSl? B Bottom r 02- f e J ------- 7-- O J* Screen Analysis Mesh Weight % 40 & 60 6* C t 80 ./A. 7 2 UV 100 I3SY 11-1 120 U>. & 2Ll 140 200 Pan 1-fK H.O 3X Drytime: <^7 /-Static Flow: O/f 2- Avg. Microns: Color L: / a Q~ f b !(&( Technician: VAB.0001200723 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS A Date: July 23, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 20, 1992 Property Test Method Volatiles, % ABR--1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 VIS1A Product: 5385 Railcar No.: VIPX 45760 Order No.: 0013315-006 n Specification Analysis 0.30 Max. 0.04 510 Min. 0.582 6.0 Max. 4.9 0.1 Max. 0.00 NDS 6.7 10.0 Max. 2.1 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 5 0.072 0.93 lU Amy E. Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200724 Vista Polymers Highway 25 Aberdeen, MS 39730 ^VC RAILCAR ANALYSIS Load Date: *7 - / 7 Time Logged In: Ship Date .-3.Uq Product: Car No.: Logged In By: /y?. t Silo(s): Order No: OOC Customer: o - 7 7-#T~ Compartment A Sample From Bottom Moisture % 0 BL Contarnination 3 BR z Bulk Density .6*0 BD after Fluff Hard Particle 5 PTO 7 ^G CA Bottom // .5"?7 CB Bottom ,<5 .31 B Bottom * o3 D RVCM .R?2- 40 Mesh/Glassies O Screen Analysis Mesh Weight 40 Q.C& 60 , Qo - 34- 80 iS.7f 311 100 R 27.0 /* 7 120 140 113- ...15L 200 Pan - /a? 6-7 2./ Drytime: Static Flow: o Avg. Microns: Color L: M */( a w .07 h AJ?V Technician: VAB.0001200725 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 CERTIEICATE OR ANALYSIS Date: July 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 24, 1992 VKIA Product: 5385 Railcar No.: PLCX 43431 Order No.: 0013315-008 Property Test Method Volatiles, 515 ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 515 on 40 Mesh 515 on 200 Mesh 516 on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.581 6.0 Max. 4.9 0.1 Max. 0.00 NDS 8.2 10.0 Max. 2.4 5 Max. Avg. * 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles & 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 6 0.042 0.93 Amy tr. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200726 Vieta Polymers Highway 25 Aberdeen, MS 39730 FVC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date: Product: Logged In By Order No: 13 Car No. oot Silo(s) Customer QA-C4prG> Screen Analysis Mesh 40 Weight % 6.00 0.0 60 *4 80 / kT 27.7 100 /2. 7o z 120 //7 140 r. r/ /AO 200 rz Pan A^l 1 > ' Drytime: Static Flow: & / J7- <3 kve.. Microns: iU-1 Color L: foo. a * C3 b ACL Technician: mT VAB.0001200727 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT X EX CATE Aberdeen, Mississippi 39730*0091 Phone (601)369-8111 AIM ALi YS X S k Date: July 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 27, 1992 VISIA Product: 5385 Railcar No.: GACX 73379 Order No.: 0013922-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.13 .510 Min. 0.573 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.6 10.0 Max 2.7 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 7 0.047 0.93 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200728 Vista Polymers Highway 25 A Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date: ~7- Z3-9*~ Product: Car No. Time Logged In: Ship Date: Logged In By Order Hr,: Q>/3fZ2-^Q Customer 7J37? Compartment m Sample From A Bottom Moisture % BL Contamination BR JO 3 3 Bulk Density Sh> BD after Fluff Hard Particle 5 So 7 7to Viscosity % * ,c\lA RVCM 'Ml - 40d - Me* sh /G^la6p 6- iea6.i 0 Screen Analysis Mesh 40 Weight % Q. O 60 2.e& y-/ CA Bottom .13 V 5 A'SifZ 1 CB Bottom .12. S' - .SSI B Bottom . 03 y ^3 .7</ 1< m ------ 7-- O. f/o -- --. 1 80 100 120 140 3/.f 2S* o /7.7 /O. / 200 f.L Pan J.&L '7 . Drytime: 370 Static F low : O //Jl.O Avg. Microns: /$7./ Color L: ?fre O.Zo b 3-34 SkTechnician: VAB.0001200729 Vista Polymers A Division of Vista Chemical Company Highway 25 - Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 A Date: July 30, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 29, 1992 VISIA Product: 5385 Railcar No.: PLWX 44676 Order No.: 0014233-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 . 510 Min. 0.585 6.0 Max. 5.0 0.1 Max. 0.00 NDS 6.8 10.0 Max. 2.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 5 0.362 0.94 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200730 Vieta Polymers Highway 25 A Aberdeen, MS 3973Q PVC RAILCAR ANALYSIS Load Date:. 7 2 7' fZ- Product: Car No 1*96.7 Time Logged In: 9720 Logged In By: Silo(s): 2-- Order No: & Ol f'23'i CCO.Customer fJeTHet* Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard .>8S Viscosity RVCM Mesh/Glas ftJ5 Screen Analysis Mesh Weight 40 e> && % 60 1 80 Iff* 100 120 13kL }k>p. 140 11 200 Pan 3T+* /./z ^8 3 Drytime: Static Flow: 4 JL ?./ Avg. Microns: Color L: 1^77 o. b Technician: VAB.0001200731 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIF X CATE Aberdeen Mississippi 39730-0091 Phone (601) 369-811 1 S h Date: July 30, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 29, 1992 VIS1A Product: 5385 1 Railcar No.: VIPX 45878 Order No.: 0013922-001 Property Test Method Volatiles, % ji Bulk Density, gm/cc ABR-1A ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.07 .510 Min. 0.570 6.0 Max. 5.0 0.1 Max. 0.00 NDS 10.8 10.0 Max. 3.9 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 7 0.226 0.94 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200732 Viata Polymers Highway 25 k Aberdeen, MS 39730 iPVC RAILCAR ANALYS X S 1/w Load Date: 7-a*~9& Product: Car No Time Logged In Ship Date Logged In By: Silo(6) Order No: 00/3^22-^0/ Cuetome Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Particle S6t> Viscosity RVCM 40 Mesh/Glass , Screen Analysis Mesh Weight % 40 0,00 Qjl O 60 Si M 80 100 13.0? /J<9 2L/X ,.!21 120 <7ts- /?.</- 140 07 if.7 200 ML loS Pan J.W 3.*} Drytime: Static Flow: o Avg. Microns: JSC.2 Color L: .ot b l33y +fsTechnician: VAB.0001200733 \ Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 OF" IS A Date: jf- /-9-2- Customer: GENCORP POLYMER PRODUCTS P- 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: A -- / **2. Produc t VHA Lot No. Trailer No. Order No. d<2> t 600 Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis . r?<> 4.? 0.1 Max. O <0 NDS 10.0 Max. 5 Max. ( o 25 Max. 3 8.5 Max. .90 to .95 Not more than 8.5 PPM .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory (601) 369-3624 /Lead VAB.0001200734 Date 7-31 7 z- Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ (,11 Trailer Number. Time 223 0 Order No. <P <3 1 T~3i / 4 -- Coo A Particle Size Distribution: Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mesh Screen Analysis 40 0.00 o.o Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 . Min On Rotap shaker. 49 gms. Resin plus 1.0 gins. Carb 60 80 100 120 140 200 Glassy Pan Part. A .rr At Min. 60 > n<n M'O* 4.// 2.1/ 32.1 72.o /t y r.z- S'.? On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 80 100 120 140 200 A 07 Glassy Pan Part. 4, Remarks__ m PH mm H# mmmmmmmmmm mm VAB.OOQ1200735 wi Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF M V'S I S A I'M. Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: f VISTA Product: 5385 Lot No Trailer No I 311 Order No & o l4'394'-&o I Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 rticle Size, 7. on ABR--3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR--12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Spec i f i c a t i on 0.30 Max. .510 Min 6.0 Max Analvsis / 63 . 3"CS 0.1 Max. NDS c 10.0 Max 5 Max. 25 Max. Ll o 3 8.5 Max .90 to .95 Not more than 8.5 PPM .*3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory supervisor/Lead (601) 369-3624 VAB.0001200736 PVC BULK TRAILER ANALYSIS A Date Customer Technician Product Silo___ 53 T Trailer Number Time 112. Order si/ oI FRONT MOIST CON'T. Bunom I Top i3 Bottom s GEL 3 2. BULK DENSITY 1 DRY TIME 1 SA 1 1 11 COLOR L =/&?. = -0. o r B = i.S? L= vise RVCtfT jj MIDDLE 1. 1 1 END A= B= 1 L= A= y B= > Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 6' P Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On flotap shaker. 49 gms. Resin |}lus 1.0 c|ms. Carb 60 80 100 120 140 200 Glassy Pan Part. a.g6 (Jo Min. IH-6 1 IL.tx> It..3S' V.S/ Jr 6 3X* 0 L ,4_- 9,o 4.? On flotap shaker 49 gms. Resin plus 1.0 gms. Carfo 60 80 100 120 140 200 /.? Glassy Pan Part. Remarks VAB.UUU12U0737 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 certificate: o Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 ANALYSIS A Date: August 3, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 22, 1992 SES^BS3BB1BBSBS&SSa^^B^S^B^B^S^SBBS3B^^^^^BBBBBBBB^BSaBB3ESaEI^E3S9EEaBBBBS^SSSSSB^^BBBS Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 VISIA Product: 5385 Railcar No.: PLCX 46860 Order No.: 0013315-007 ^^sBaansnsatssBaneasaBantssB Specification Analysis 0.30 Max. 0.17 .510 Min. 0.588 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.7 10.0 Max. 2.5 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.204 0.94 Amy EL/Bagwel Laboratory Supervisor (601) 369-3624 VAB.0001200738 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date .A^UA Product: Car No j/aco Time Logged In: & / Logged In By : A? M Silo(e): <&? t c Ship Date: *7 f^-2Order No: 1S --QO *7 Customer: Sample From Bottom Moisture % 8L Contamination BS Bulk Density -// j / BD after Fluff Hard Particle 5 7 2~ *<Sr Viscosity M RVCM .tOLj 40 Me6h/Glassies Q. Screen Analysis Mesh Weight 40 0-0 0 % 0~O 60 .s Drytime: <?.9 Bottom Bottom ,/j f * Bottom J7_ / ,t(* / 7 0 Q 80 9.77 n.x 100 29.3 120 12.0 Static Flow 0 / * 140 - uM /&0 200 -V. *7 f.7 -i* Avg. Microns Pan 1.27 Color L: / fiQ. 7 f a 1Z- b lSi Teohnician 1*1 r IMMWi VAB.0001200739 r *4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 Date: August 3, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 30, 1992 VIS1A Product: 5385 Railcar No.: PLCX 47525 Order No.: 0014233-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.16 .510 Min. 0.575 6.0 Max. 4.9 0.1 Max. 0.00 NDS 7.0 10.0 Max. 2.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 6 0.027 0.93 Amy E. ffagwell Laboratory Supervisor (601) 369-3624 m4 VAB.0001200740 i * 4 *i0 k Vista Polymers Highway 25 Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date: 7-Z9~9Z- Product: Time Logged In oC, C>z> Logged In By: Ship Date: 7 (3D ft 7^ Order No: Car No * Silo(s): Customer:_ SU> Jj Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density ZA n (fi BD after Fluff Hard Particle 5 7 z xs Viscosity .fas RVCM J&7 40 MeSh/Glassies 0 Screen Analysis Mesh 40 Weight % 0. DO 0.0 - 60 l.4i Z.1 CA Bottom CB Bottom 9 r B Bottom Md 3 7 0 Ml a. 80 lS.? J7.Z. 100 IZ/>I 2?J 120 f.cf /&. 2- * 140 4.7^ r.t 200 J, d 7.0 Pan Z3 Drytime: Jta_ Static F low : ajJ, / Avg. Microns: no. c Color L: /DO. 7/ b Technician: VAB.0001200741 * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8 111 A Date: August 3, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: July 31, 1992 VISIA Product: 5385 Railcar No.: GACX 73398 Order No.: 0013922-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.580 6.0 Max. 5.0 0 * 1 Max. 0.00 NDS 7.0 10.0 Max. 2.1 5 Max. Avg.* 3 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 5 0.036 0.92 Amy K-/ Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200742 Vista Polymers Highway 25 Aberdeen, MS 3973Q r>VO RAILCAR ANALYSIS Load Date: *7-29-72- Time Logged In: 4330 Ship Date % / Product: Logged In Bv: Car No 3312 S i lo (s) : & 7. 17 Customer: jzjss/ Compartment Sample From A Bottom CA Bottom Moisture % BL Contamination BR Bulk Density -// 13 BD after Fluff Hard Particle 5 CQ 7 JT7X f y ,r7f , $C> Viscosity RVCM A 1 t 40 Mest h/Glassies a r r Vr * 0 __ o Screen Analysis Mesh 40 Weight >*0 0 % 0. O 60 A 37 Z. 7 80 /f.6o 37-2- 100 zci CB Bottom ./T" $ -3 CSo . 524- B Bottom ./o f1------. S-?6, /o 1 120 140 200 Pan 3Cb /c. t AS 7.0 2../ Drytime: co Static Flow: * / 7/4 Avg. Microns: 170.4 Color L: f 0 0*71 a o b f.74 Technician: VAB.0001200743 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 czEF?~r ifi cz^te: of ^n^l-ysis A Customer GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: "sO* Product Lot No. Trailer No Order No o O / 'tfSLj-dO Property Test Method Volatiles, X ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size, */. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis . 63 0.1 Max. NDS 10.0 Max. 5 Max . 0.00 7/ SKo O 25 Max. 0.5 Max. .90 to .95 Not more than B.5 PPM .$5 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Super!isor/Lead (601) 369-3624 VAB.0001200744 > Date Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ &7(s+Wf Trailer Number __ Time Jm Order No. A Particle Size Distribution: Screen Analysis---------------------------Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare Net Wt. 0.00 to9~ Ifrt Iffle f-?/ S(s. % on Mesh ggg 2*5 m* t* 5.1 i Screen Analysis _____ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. 40 ______ Pan 60 80 100 120 140 200 Glassy Part. Tare ______ Net Wt. ______ % on Mesh ______ Remarks mm T VAD.0001206745 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-6111 is A Date: l Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: <- / " Prooertv Test Method Volatiles, V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. n Particle Size, V. on ABR-7 ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 VISTAProduct: 53B5 Lot No Trailer No Order No &o /43!4~*ol S Dec i f i c a t i on 0.30 Max. .510 Min. 6.0 Max. Analysis .o7 0.1 Max. NDS 10.0 Max. 5 Max . c-.i _______________________________________________________ a 25 Max. j ______________________________ ____________________________________________________________________ 8.5 Max. .90 to .95 Not more than 8.5 PPM .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory (601) 369-3624 isor/Lead VAB.0001200746 Date Customer Technician ?L PVC BULK TRAILER ANALYSIS Product SJfS Silo__ (oil Trailer Number. __ Time /(P Order No. Ml A Particle Size Distribution: Screerf Analysis !o Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh &t0 ao Screen Analysis Mesh Size Gross Wt Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. om /4.3? a 31.3 1-Si Mf ui o2i>.6 AJL Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001200747 Vista Polymers A Division of Vista Chemical Company Highway 25 Pbst Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-6111 CERT I F" I CATE OF ANALYSIS Date: % - 2 " 2__ Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: $ ^ Z-2_ Product: 5385 Lot No.: Trailer No.: Order No.: l Propertv Test Method Vo 1 a t i 1 es , '/. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR--12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Specification 0.30 Max. .510 Min. 6.0 Ma x. Analysis .s?j 0.1 Max. NDS C. o 7-?- 10.0 Max. <3-- 5 Max . e> 25 Max. 8.5 Max. .90 to .95 Not more than 8.5 PPM 93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. h Labora tory rvi (601) 369-3624 VAB.0001200748 Date a -T-L Customer Technician. /nr<nCu PVC BULK TRAILER ANALYSIS Product S'3 if Silo___ (? Trailer Number. Time // Order No. A St/ o uJ Particle Size Distribution: Screen Analysts Mesh Size 40 Gross Wt. Tare Net Wt. O* O % on Mesh Q.t>___ Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Hlesh 40 Min On Rotap sitaker. 49 gms. Resin (>lus 1.0 gms. Carb 60 80 100 120 140 200 o.7? // Min. /ySI IS'.IX ?-y? 3*.2 b A 3J r 7-A On Rotap shaker 49 gins. Resin plus 1.0 gms. Carb 60 t 80 100 120 140 200 Glassy Pan Part. heff Glassy Pan Part. Remarks VAB.0001200749 mw Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 XS A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: /p. //. 4 > Product: 5385 Lot No.: Trailer No.: / - J Order No.: 00 Propertv Test Method Volatiles, '/. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, X on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR--12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis ___13 , rtf sr.o 0.1 Max NDS 10.0 Max 5 Max . 25 Max. 8.5 Max. .90 to .9 O. 0 LA Not more than 8.5 PPM Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) /Lead VAB.0001200750 Date tO'1-9 Z- GCustomer Technician 4 A^ PVC BULK TRAILER ANALYSIS Products srjir iSilo 74 Trailer Number Time ^2-^ Order No. Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt 0* Q0 % on Mesh Screen Analysis t Mesh Size Gross Wt Tare Net Wt H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. tl Min. 60 fX.ii ai ill. LJt On Rotap shaker 49 gms. Resin plus 1.0 gms. Carta Ll Pan 80 100 120 140 200 Glassy Part. Remarks Star 207A Revised 1/12/87 VAB.0001200751 Vista Polymers A Division of Chemical Company Highway 25 Post Office Box 91 I Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYS X S Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attentions Plant Chemist Ship Date: Pro Volatiles V. Bulk Density, GM/CC Brabender Dry Time, Min Particle Biz e, 7- on Test Method abr-ia ABR-2A ABR-7 ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies Hard Particles, 7 Mins Vinyl Chloride Monomer ABR-6 ABR-12 ABGC-26 Product Lot No Trailer No. Order No. Specification 0.30 Max. .510 Min 6.0 Max 0.1 Max NDS 10.0 Max 5 Max . 25 Max 0.5 Max I nherent Viscosity ABR-10 .90 to .95 Not Reprocessed iny1 Chloride, Virgin Resin, Polyviny VISIA 7 38 / C>0, </S3P-O S~ Anal .S77 O Not more than 8.5 PPM ,93 (601) VAB.0001200752 Date Customer Technician 7.- -f PVC BULK TRAILER ANALYSIS Product Silo___ 6 71 Trailer Number. 3Pf Time / 0O/4^4'~oq<1 A Particle Size Distribution Screen Analysis / Mesh Size 40 Min On Rotap shaker. 49 gms. Resin plus Y .0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. Tare r? Net Wt. H on Mesh (P.C> .<?'f JD.O<f .03 3-t*<4 (.!(=> oO___ -L3- 3?^r 39 ? a. IBiL 3 Screen Analysis Mesh Size Gross Wt. Tare 40 - Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 1 Glassy Part. Net Wt. % on Mesh Remarks VAB.0001200753 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ^Ni^L-YSIS A Date: Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Produc t: Lot No :/!///? Trailer No.: /Order No- Property Test Method Vo 1 a t i 1 es, */. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis 4 0.1 Max NDS 10.0 Max 5 Max . 25 Max. 8.5 Max. .90 to .9 0b 11 3.o 0 & Not more than 8.5 PPM 93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200754 PVC BULK TRAILER ANALYSIS A Date. ? Customer (jkt*Q>rfV Technician Product Silo___ Trailer Number _ Time ft IL&L Order mm MOIST Top Bottom lt031 CONT. Top Bottom 12wtXjf1Jf i i * GEL l 6k BULK DENSITY I DRY TIME l COLOR L y07i vise RVCM FRONT 2. i. 2.W: 2 i i i. * `8.0. ,,./.63\.f3 L= MIDDLE 2. I. I I i END A= B= L= A= B= o Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh a <*> 6.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 g ms. Carb 60 80 100 120 140 200 Glassy Pan Part. 0 lo (T. & %'*8 ^y<r fSf /Ojf- 4.7 S.o Min. On Rotap shaker 49 gms. Resin plus 1.0 gins. Garb 60 80 100 120 140 200 Pan Glassy Part. Remarks____ VAB.0001200755 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 N ^ l_ Y S I S A Date: 0/^/^Z- Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Produc t: Lot No.: Trailer No. : "T*- 50/ Order No.: 001~0O / Property Test Method Volatiles, V, ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis . ot~ 1 0.1 Max. NDS 10.0 Max. o o g.S- 2.5" 5 Max . 25 Max. a 3 8.5 Max. .90 to .95 Not more than 8.5 PPM .fJL Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Ifaborat (601) 369-3624 VAB.0001200756 Customer Technician PVC BULK TRAILER ANALYSIS Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. tt on Mesh 000 .0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Min On Rotap shiiker. 49 gms. Resin pilus 1.0 grns. Carb 60 80 100 120 140 200 Glassy Pan Part. 1^60 Min. ISTtf /4&> 1.&1 JM7 +*7 U 1 On Rotap shaker 49 gms. Resin plus 1.0 gins. Carb Pan 60 80 100 120 140 200 Glassy Part. - Remarks VAB.0001200757 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 I I CATE O Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA VS I s A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Qll&fal*' Product: 53B5 Lot No.: Trailer No.: T-3&3 06Order No. s oo / Propertv Test Method Volatiles, V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analvsis .ne> 0.1 Max. 0-0 NDS 10.0 Max. 5 Max . 25 Max. 2.2- o a. 8.5 Max. .90 to .95 Not more than 8.5 PPM .15 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200758 PVC BULK TRAILER ANALYSIS A Date___ L Customer Technician FRONT Product s;j_i Trailer Number. Silo___ Time Order No 0 7JO OO/M ^-0 0! MOIST Top Bottom I. ,0% 2. CON'T. Top Bottom I GEL BULK DENSITY i it I 2.0* 2. DRY TIME I .0 COLOR L= a - .07 mm vise RVCM l ii - Aft* i L= MIDDLE i END , A= B= i. I I I L = A= B= Particle Size Distribution: Screen Analysis_______/ 0_______ Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. _________ _________ _________ ___________ ___________ ___________ ___________ ___________ _________ Tare Net wTft1.* % on Mesh _________ _______________________ _____ I,, *.0 w u-- Jt Z^Q-- 2iT.o r' T ZT.t _______ /a 6* a/t4 ________ ___________ ___________ _________ ^A**--^-- f*m wr /*Jt> PI/ J.2. Screen AnalyM sis . Mesh Size Gross Wt. 40 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Tare Net Wt. _ H on Mesh Remarks Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I F7 I C2 <=* Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 fsj I_Y S I S A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Product: 5385 Lot No.: -- Trailer No.: I' 3*7*7 Order No. : 001^*4^^000 Property Test Method Volatiles, V, ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR--6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis .0& 0.1 Max. 0-0 NDS 10.0 Max. 5 Max . 25 Max. o 3 8.5 Max. .90 to .9^ Not more than 8.5 PPM .?3 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200760 Date Customer Technician PVC BULK TRAILER ANALYSIS Product Trailer Number f-377 A Particle Size Distribution: Screen Analysis _Min Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0.00 0.c> Screen Analysis Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 On Rotap shaker. 49 gms. Resin plus 1.0 gms. Garb 60 80 100 120 140 200 Glassy Pan Part. l*o /figs' tots' *-* P.o 3sU DJt<7 /g,o tot f.AS r.'S*- s?j Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 60 100 120 140 200 Glassy Part. Remarks__ VAD.0001209761 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT IEI Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS Date: August 20, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: August 19, 1992 visnA Product: 5385 Railcar No.: GACX 73380 Order No.: 0014809-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.05 .510 Min. 0.580 6.0 Max. 5.0 0.1 Max. 0.0 NDS 8.0 10.0 Max. 2.7 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.050 0.93 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200762 Vista Polymers Highway 25 Aberdeen, MS 3973Q PVC RAILCAR ANALYSIS Load Date: Ship Date: %[n Product: _ Logged In By: Order No: M 0 l - 0 O 6 Car No. Silo(6) Cl11 fz t nmp Screen Analysis Mesh 40 Weiuht & % 0*0 60 Drytime: S.6 80 /U3 100 A3.72 $/4~ 120 IS 7 n.s- 140 /to .+ 200 <4,00 Pan t.6 Z1 Static Flow : .o/f.4 Avg. Microns: /&s? Color L: Technician: VAB.0001200763 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CER X RIGA EE OR AM A XS A Date: August 26, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: August 21, 1992 VISIA Product: 5385 Railcar No.: VIPX 45308 Order No.: 0014809-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.09 .510 Min. 0.581 6.0 Max. 5.0 0.1 Max. 0.00 NDS 7.0 10.0 Max. 2.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. /c% lii Amy Bagwedj) Laboratory Supervisor (601) 369-3624 2 0.081 0.93 VAB.0001200764 Vista Polymers Highway 25 r A Aberdeen| MS 39730 L'VC RAILCAR ANALYSIS Load Date:_____f ` o `9 Product: Car No Time Logged In: Ship Date:. 1TP <fD Logged In By: &U1 Siio(s) :_AZ.i?7 Order No:. 14? 0*7 -O o/ Customer: Screen Analysis Mesh Weight 40 9.00 % 0-0 60 0.94 1.9 80 l4.z9 D.$> Lr 100 is.&s 30. / 120 f.xx If.9 140 s.tff 200 3S2~ 7.6 Pan hn Q.3 Drytime: S.o Static Flow: 0 /&S Avg. Microns: /Us Color L: ab Technician: VAB.0001200765 i Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 C EE F? T I R I C AT EE OR AMALYSIS Date: August 26, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: August 24, 1992 VISIA Product: 5385 Railcar No.: VIPX 45275 Order No.: 0014809-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Anal vsis 0.30 Max. 0.17 .510 Min. 0.587 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.0 10.0 Max. 3.2 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.041 0.93 Amy E. Bagwe Laboratory Supervisor (601) 369-3624 mmm # VAB.0001200766 r*-- Vista Polymers Highway 25 A Aberdeen, MS 39730 RVC RAILCAR ANALYSIS :Load Date: 9-Z.I-9Z- Product: Time Logged / Ship Date: ijzt Logged In By: Order No: l4$Cfh GO 2- Car No.: 2,'TS' m. GeuCustomer: tbrnmi__ Compartment Sample From Moisture % Contamination A Bottom .oS CA Bottom >19- CB Bottom B Bottom (7 Bulk Density .S2&. BD after Fluff Hard Particle 5 7 Viscosity Z H*-' RVCM >C4l^ 40 Mesh/Glassies O 592 o / & Screen Analysis Mesh Weight % 40 o. to A0 60 80 100 120 140 200 Pan (3.70 17.13 A f.sg [S' <27+ gy /9J flA JA J.oDrytime: Static Flow: ^ Avg. Microns: /~?3 Color L 1*1.33 6.6+ b m Technician: VAB.0001200767 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: S' ?2- Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: j9- a 9z Produc t Lot No. Trailer No. : / --->0 / Order No.: Oft Propertv Test Method Volatiles, V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, X on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis S,D 0.1 Max. 0.0 NDS 10.0 Max. 9l-8 5 Max . 0 25 Max. 8.5 Max. Not more than 8.5 PPM .90 to .95 .73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. A Laboratory Supervisor/Lead (601) 369-3624 VAB.0001200768 DfltP Customer jACq TWhnirinn ^ PVC BULK TRAILER ANALYSIS Trailer Number Silo Time A W fW Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0*60 Screen Analysis Mesh Size Gross Wt. Tare Net Wt. H on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gims. Carb 60 80 100 120 140 200 Glassy Pan Part. e.a /0.49 rt-99 n.3L; 4-89 /./ 0.9 39.9 33.3 /33 9.r Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. * Remarks t Star 207A Revised 1/12/87 VAB.0001200769 Vista Polymers A Division of Vista Chemical Company CER Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 I RX E OR ANA SX3 Date: August 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: August 26, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46517 Order No.: 0014809-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.580 6.0 Max. 4.8 0.1 Max. 0.00 NDS 8.0 10.0 Max. 2.4 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.033 0.93 uU Amy E y Bagwel Laboratory Supervisor (601) 369-3624 VAB.0001200770 Vista Poly Highway 25 A Aberdeen, MS 39730 1PVC RAILCAR ANALYSIS Load Date: <P-2 6.-92. Product: Time Logged In oGOo Logged In By: %[Ue> Ship Date: Order No: 00A Car No. : Silo(6): fliiRt.ftmpr * ,M Compartment A Sample From Bottom Moisture % ./2- BL Contamination BR a A BuIk Density BD after Fluff . rtf/ Hard Particle 5 7 y Viscosity RVCM <b*& 4D Mesh/Glassies %* o Screen Analysis Mesh 40 Weight O.eO _ % co 60 A/2- CA Bottom ./r 4 / . :T<fo 0 80 ]+. /3 100 )4. $0 2/. P CB Bottom cP I B Bottom JZ 9 3 . rfo 7 /0 o 120 J%7 140 r.tf // V 200 #.oo f.> Pan Drytiroe: `4/ 7. rStatic F low: o / Avg. 1Microns: IkJS-- Color L : /Qo> n a -- 1 b AEI Technician: _ S'd ITA VAB.0001200771 Date y Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number Time /O/i-Q Order No. -$// A Particle Size Distribution Screen Analysis Mesh Size Gross Wt Tare ? Net Wt % on Mesh Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 0*0 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. .9*1 4 /<*37 a <3? /jjfo /o _ Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. M 4 Remarks Star 207A m fc ^ b e?H Revised 1/12/87 8' > ^ 1 fc. -W- 4- ** DM VAB-0001200772 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 k Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Product: 5305 Lot No.: Trailer No.: 7~'3&) Order No.: 0 &/3" O D H Property Test Method Volatiles, V. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Ma x. Analysis o5~ S&5 . y.7 0.1 Ma x. 0.0 NDS 10.0 Max. 5 Max . ID? sn.8 3 25 Max. I 8.5 Max. Not more than 8.5 PPM .90 to .95 /Vb Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-3624 9 f rnmmmmmm VAB.0001200773 9 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 G EE R T I R X CAT EE OR ANALYS I S Date: September 2, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: August 31, 1992 VISIA Product: 5385 Railcar No.: VIPX 45797 Order No.: 0014809-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 .510 Min. 0.588 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.1 10.0 Max. 2.6 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles 0 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.130 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200774 Vista Polymers Highway 25 A Aberdeen, MS 3973Q PVC RAILCAR ANALYSIS Load Date : tm30 lbTime Logged In: 6f90 Ship Date: Product: Car No r??7 Logged In By:_ 1*4*0*1-006 Silo(s): Cu6tome tiO ___ Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Particle .05# Viscosity RVCM Mesh/Glass Avl Screen Analysis Mesh Weight % 40 0 do 0-0 Drytime: 60 */f 43 80 100 jCr_o9~ /p. 70 2Z.0 120 1*7/ 140 MS 200 Pan tL Z.(e Static Flow: a L Avg. Microns: lU Color L /*/-/ b Ilk Technician: VAB.0001200775 ' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTX E X Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANAL.YSI S Date: September 4, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: September 1, 1992 VISIA Product: 5385 Railcar No.: UTCX 46409 Order No.: 0014809-005 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 .510 Min. 0.587 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.5 10.0 Max. 2.7 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles a 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 .90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.042 0.92 Amy E. Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200776 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: 1-t -it. Time Logged In: Ship Date: eji RAILCAR ANALYSIS Product: Logged In By: l^Ho^-oos Car No. : Silo(6) Customer: m____ Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density .525? BD after Fluff Hard Viscosity RVCM Mesh/Glassies ** Screen Analysis Mesh 40 Weight % A0 60 Ml 24- 80 100 /fgg 217 2b. I 120 ft.9 Drytime: jfi Static Flow: 140 200 Pan // 7 9.5 2.7 Avg. Microns: Color L: a b / Technician: VAB.0001200777 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A September 28, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: September 25, 1992 VIS1A Product: 5385 Railcar No.: ACFX 41139 Order No.: 00164878-000 Property Volatiles, % Bulk Density, gm/cc Brabender Dry Time, Mins. Particle Size Distribution % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABR-6 Specification Analvsi 0.30 Max. 0.05 .510 Min. 0.567 6.0 Max. 5.2 0.1 Max. 0.00 NDS 8.8 10.0 Max. 2.6 5 Max Avg. * o (By Compartment) *Average of 5 per railcar? 10 max. in a single compartment. A 0 CA CB B 000 Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.050 0.92 Laboratory Supervisor (601) 369-3624 VAB.0001200778 SA Vieta Polymora Highway 25 Aberdeen, MS 3973Q 3? VC IRA X LCAR ANALYSIS Load Date:. <9. /{> Time Logged In: Ship Date: Product: Car No.: V//3? QO Logged In By: 7 Silo(s) : Order No: 00 MCustomer: </D&4ULo>t'P Compartment Sample From Moisture % Contamination Bottom Bottom <aS Bottom ,o5 Bottom Bulk Density BD after Fluff Hard si/ Viscosity . c!'io RVCM rOSO 40 Mesh/Glassies ,lz% Screen Analysis Mesh Weight 40 fyao X 60 80 100 0.75 //.bo /3.S? /5 23-2 2?A 120 //.3? 23. 3 140 0 SO /3-0 200 7-7o Pan If 2.(e Drytime: Static Flow: o L Avg. Microns Color L: /X>47 D-lO b / 77- Technician: VAB.0001200779 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI F= X Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANALYS XS A Date: September 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: September 28, 1992 VISIA Product: 5385 Railcar No.: VIPX 45308 Order No.: 0016478-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.577 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.6 10.0 Max. 2.5 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles Q 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.170 0.94 Laboratory Supervisor (601) 369-3624 VAB.0001200780 Viata Polymers Highway 25 A Aberdeen, MS 3973q PVC RAILCAR ANALYSIS \JiPi Load Date - Product: Car No.: jrj'oS Time Logged In 0 S~ox> Logged In By: /Iff SiloCs) : ?*&> - Ship Date: \z% h Order No: 0016> 4Tg-oo / Customer: Screen Analysis Mesh 40 60 Weight % a *0 _ _ if! 0*0 / ^ 80 It. If 100 /4U2- -2 9.2. 120 n.it 23.1* 140 l* X?.7 200 *79 f.C Pan /.a 7 Drytime: *1 Static Flow: * //./ Avg. Microns: }SJ.i Color L: f1.& a -' b S.I? Technician: VAB.0001200781 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 C ERT XEIGAT E OR ANALYSTS A Date: October 1, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: September 30, 1992 VISIA Product: 5385 Railcar No.: ACFX 55814 Order No.: 0016478-002 ProDertv Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analvsis 0.30 Max. 0.18 .510 Min. 0.593 6.0 Max. 5.0 0.1 Max. 0.00 NDS 9.4 10.0 Max. 2.4 5 Max. Avg. 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles a 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.034 0.93 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200782 Viata Polymers 1AJ> D Highway 25 m A Aberdeen, MS 3973Q !)PVC RA X LG AR ANALYSI S Load Date: f-^tO-92. Product: Time Logged In: Logged In By: Ship Date: Order No: f Car No.: S8/y /7l . i Silo(s) : Cuetome Compartment Sample From Moisture % Bottom Contamination Bulk Density BD after Fluff Hard Bottom LB // .S?z Bottom IB $ - Bottom IS T7 /_3 ,S*fS Viscosity RVCM Meish/Glass * * a * / - * * ... Screen Analysis Me6h Weight X 40 0 OX) 60 >.'7 Mt- Drytime: 5> 80 ffl 100 f3.ro 120 /5/g 140 /f=< o* 200 3_ Pan m Static Flow: o L Avg. Microns: IgU Color L: b f.S7 Technician: VAB.0001200783 Vislo Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 C E R I R I CA Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 R ANALYSIS A Date: October 7, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: October 2, 1992 VBIA Product: 5385 Railcar No.: ACFX 41136 Order No.: 0016478-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analvsis 0.30 Max. 0.10 .510 Min. 0.575 6.0 Max. 4.8 0.1 Max. 0.00 NDS 8.9 10.0 Max. 2.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.050 0.93 Amy E." Bagwe1 Laboratory Supervisor (601) 369-3624 VAB.0001200784 Vieta Polymers Highway 26 Aberdeen, MS 3973q A RAILCAR ANALYSIS Load Date: ^ - Time Logged In: </>p Ship Date: /oh /<? Product: Logged In By Car No. Z Silo{6 ) : oner: SO ZEkg Compartment Sample From I Moisture % Bottom , /? m [Contamination BR 1 Bulk Density BD after Fluff ,_g77 Hard Particle 5 7 To" -27^ Viscosity 1 _________________________________________________________________________________________________________________________________________________ RVCM * _______________________ -an 40 MeSh/Glassies 1i * i * 4m # * V . 0 Bottom /O Bottom r/o Bottom Screen Analysis Mesh 40 Weight x 0.0 60 80 100 120 140 200 Pan , L0 //V-2- W-Cv f(3& L.sy ftgr A/4 (,1. Si.1? 2% a. MS )3't 2.3 Drytime: /MStatic Flow: 0 Avg. Microns: Color L: \OO.SS a '2*1 b l.*7S Technician: ~T" VAB.0001200785 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: October 8, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: October 6, 1992 VISIA Product: 5385 Railcar No.: Pt^jC 42996 Order No.: 0016478-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 .510 Min. 0.582 6.0 Max. 5.1 0.1 Max. 0.00 NDS 8.4 10.0 Max. 2.1 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.028 0.93 Offerny pfxwi Amy Es. BBaaggWwee7!ll1' Laboratory Supervisor (601) 369-3624 VAB.0001200786 Vista Polymers Highway 25 A Aberdeen, MS 3973Q Load Date: _ Ship Date: TRAIL LCAR ANALYSIS dT3Q Product: Logged In By: Order No Car No.: Silo(6): Custome Screen Analysis Mesh 40 60 Weight 0*00 .K % 0.0 . .47 80 IZAU 2r,7 100 14.1? Zf.3 120 10. Lo 140 i./f 200 4>20 Pan JZ.i Drytime: x/. Static Flow: o />. 7 Avg. Microns: tst.l Color L: 100.it a * 24* b /;m Technician: +TC VAB.0001200787 Vista Pofymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone {601) 369-8111 l--l E F? | I E I C A "T f-- t 11-- A l\j A I-- V hi I S A Date: fof^/^2^ Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: to/^/tfZ^ Product: 5385 Lot No . : Ay ft Trailer No.: / Order No.: 00 I b " DO/ Property Test Method Vo 1 a t i 1 es , 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 SDecific ation 0.30 Max. .510 Min. 6.0 Max. Ana 1ysis o. /3 O.'S'Tl 0.1 Max. NDS 10.0 Max. o-o . (a / 7 5 Max . 25 Max. o Z- 8.5 Ma x. Not more tha 8.5 PPM .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 ii VAB.0001200788 Date /4-r - Customer Technician PVC BULK TRAILER ANALYSIS Product ik Silo___ S'Sg'C Trailer Number Time Order No. ffO/6 -'OO f A Particle Size Distribution: Screen Analysis -fe. /0 Mesh Size 40 Gross Wt. Tare Net Wt. % on Mesh 0*0 0 AO . -Hi i Screen Analysis 5 Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 Mfai On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb 60 00 100 120 140 200 Glassy Pan Part. J4/0 /r./o J.t3 s^?o S. 17 .*r A/ Jo.t- 20. t //. f 4. 4 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 A7 Glaasy Pan Part. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERT I R* X C^T'EE OF7 ^ ^ l_ Y S I S A Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: fOfS Product: 5385 Lot No.: a//a Trailer No.: / " 3*76? Order No . : OOOOO Propertv Test Method Volatiles, ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specifica tion 0.30 Max. .510 Min. 6.0 Max. Ana lysis O.H S"./ 0.1 Max. NDS 10.0 Max. h 1.1 5 Max . 25 Max. O 3 8.5 Max. Not more than 8.5 PPM .90 to .95 * Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200790 s PVC BULK TRAILER ANALYSIS Dale__/g-r- 72. Customer Technician Product, SJSS' Trailer Number. Time J04LO Order no. oalU^H 'den MOIST Bottom I CON'T. Bottom I DRY TIME i FRONT I 2. 1 2. I 3 Ti ,r77 B 2. I 2, 17 1 * TT TT [ fr |7 [7 COLOR L =/00. A = , o IS B - /| ^ 7 vise A RVCM MIDDLE I2- [7 END 11 1 -Ww * 1 1 *i 1 H 2. I > # rr 1 2. (7 m11 ae 17 1e 11 * [7 Ii A B= Particle Size Distribution: Screen Analysis-------------------------- Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Glassy Pan Part. Gross Wt. _________ _________ _________ _________ _________ _________ ___________ Tare Net Wt H on Mesh ..._____ ________________________ _________ O * 0 & Ltr /r.r& /*/g -?-7 3>. 7 XIJ _____ /f -i ________ ___________ s-./r s. z.o SO.3 t.4 Screen Analysis Mesh Size Gross Wt. __Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 100 120 140 200 Glassy Part. Tare Net Wt. 4% on Mesh Remarks Star 207A Revised 1/12/67 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 CERTIRIOATE OR ANALYSIS s A Date: October 9, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: October 8, 1992 VISIA Product: 5385 Railcar No.: VIPX 45872 Order No.: 0016478-005 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analvsis 0.30 Max. 0.13 .510 Min. 0.580 6.0 Max. 4.9 0.1 Max. 0.00 NDS 6.7 10.0 Max. 1.7 5 Max. Avg.* 0 (By Compartment) *Average of 5 per railcar; 10 max. in a single compartment. Hard Particles e 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.032 0.93 agwevO Laboratory Supervisor (601) 369-3624 VAB.0001200792 Vieta Polymers Highway 25 A Aberdeen, MS 39730 RVC RAILCAR ANALYSTS Load Date: /Q-7-9% Time Logged In: 09oO Ship Date:_ /O Product: Logged In By: (e4-7% Car No. -^r/72 Silo(s) Customer: rwvdtsJL Compartment A Sample From Bottom Moisture X BL Contamination BR 3 Bulk Density BD after Fluff Hard Particle 5 7 Viscosity dL 3 RVCM .05%- 40 Mesh/Glassies o Screen Analysis Mesh Weight 40 0,00 X 0>Q 60 Lie. CA Bottom -s ? o 80 12. (>Z- 20. D 100 is.So Jf.O CB Bottom .u 3 B Bottom JA 2 7 & <2 120 /Q.9J 21-8 140 s.sg f(A 200 Pan J,3j ,tr IJ- Drytime: Static Flow: o L %s Avg. Microns: Color L: >1? b ISA' Technician: VAB.0001200793 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 IS A Dates 2-- Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attentions Plant Chemist Ship Date: Product: 5385 Lot No.: Trailer No.: 7"-32-4 Order No.: C Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, 7. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-IO Specification 0.30 Max. .510 Min. 6.0 Max. Analysis ,/Q . r 73 S-.Q 0.1 Max. 0. 0 NDS 10.0 Max. 7.4 2.0 5 Max . a. 25 Max. 2. 8.5 Max. Not more than 8.5 PPM .90 to .95 / Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369--3624 VAB.0001200794 Date SO' 9-92- Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ t, 76,177 Trailer Number Time 2 Order No. A Particle Size Distribution: Screen Analysis----------/ ^-----------Min On Rotap shaker. 49 gins. Resin plus 1.0 gms. Carb Mesh Size 40 60 80 100 120 140 200 Gross Wt. _________ _________ ______ Tare Net Wt. H on Mesh 0.0 .t* to* II* 36.3 /2-lX* Z+C 19* H,t 2*72- 7. Screen Analysis Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Mesh Size Gross Wt. Tare Net Wt. % on Mesh 40 60 90 100 120 140 200 r Glassy Pan Part. /.*/ Glassy Pan Part. Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: October 14, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: October 12, 1992 VISTA Product: 5385 Railcar No.: ACFX 41171 Order No.: 0016478-006 Property Volatiles, % Bulk Density, gm/cc Brabender Dry Time, Mins. Particle Size Distribution % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies Test Method ABR--1A ABR-2A ABR-7 ABR-3 ABR-6 SDecification Analvsi 0.30 Max. 0.14 .510 Min. 0.574 6.0 Max. 0.0 0.1 Max. 0.00 NDS 8.5 10.0 Max. 2.2 5 Max Avg. * 0 (By Compartment) A CA CB B *Average of 5 per railcar; 10 max. in a single compartment 0 0 0 0 Hard Particles 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 3 0.064 0.93 Amy E. Laboratory Supervisor (601) 369-3624 VAB.0001200796 Vista Polymers Highway 25 Aberdeenf MS 3973Q^ ^VC RAILCAR ANALYSIS part Load Date Product: Car No.:__ *^//7/ Time Logged In: Ala* Logged In Bv: J*143 Sllo(s) :_12 Ship Date: Z&ltSL Order No: /--&0> Customer rc^> <VYrNJtfc\9-' Compartment Sample From Bottom Moisture X Bottom Bottom Bottom Contarnination Bulk Density BD after Fluff Hard Particle Viscosity 3ct RVCM ,DG>4 Mesh/Glassies ** * Screen Analysis Mesh Weight 40 too % 0.0 Drytiroe: 60 ML .1 80 U 27 22. 100 /W 3o.l 120 1LSL 140 L.llo Ml 200 Pan f.n to? g.r z.z Static Flow: %3 0L Avg. Microns: fSS,* Color L: l*.S3 'dl b !3t Technician: VAB.0001200797 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 A Date: October 15, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: October 14, 1992 VISTA Product: 5385 Railcar No.: PLCX 42777 Order No.: 0016478-007 Property Volatiles, % Bulk Density, gm/cc Brabender Dry Time, Mins. Particle Size Distribution % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABR-6 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. A 0 Soecification Analvsis 0.30 Max. 0.17 .510 Min. 0.589 6.0 Max. 5.0 0.1 Max. 0.00 NDS 9.6 10.0 Max. 2.2 5 Max. Avg * 0 1 CA CB B 000 Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 4 0.319 0.93 . Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200798 Viata Polymers Highway 25 Aberdeen, MS 3973Q A Load Date: fO-IP'fZ- RAILCAR ANALYSIS Product: Car No.: Pool Time Logged In: 2.30 0 Logged In By: SiloC 6): Ship Date: Order No: Customer: Compartment Sample From Moisture % Bottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Viscosity ,%n RVCM .314 Mesh/Glassies Screen Analysis Mesh 40 Weight % do 60 $3 80 JL 17.0 100 fSTiS 120 140 21& 200 iyg Drytime: g* Static Flow: * /fa Avg. Microns: Pan Color L: /ce.+Z b -J 0,6% /.?3 Technician: VAB.0001200799 Visto Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 CERT' I R I CATE OR Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 T 1 A' Date Customer s GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attentions Plant Chemist Ship Date: VIS1AProduct: 5385 Lot No.: Trailer No.: 0 Order No. : 001^66^-^00 Property Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis bOO 0.1 Max NDS 10.0 Max 5 Max . 25 Max. B.5 Max. .90 to . a 5. Not more than 8.5 PPM .93 Polyvinyl Chloride, Virgin Resin, Not Reprocessed (601) 369-3624 VAB.0001200800 BLEND NO: _OjtllSL.__________ RE Si BAG BLEND PRODUCT:___________ DATE: 7-J3-92*_______ Avg. Microns, 5225/5325/5415: TINE/TBSTED BY: //DC - % r mmwmm IH VAB. OOO1200801 f ht- Customer Return Receiving Report Plant __________________________________________ From ABUHKKff l_______ _____ ______ 0EMC08P POLTMEH VROWCMB Vista Chemical Company Pro Number Prepaid Collect Collect Amount VBIA No. CR 02122 Date Returned 11/2/92 Date of Report llA/92 Trailer Number *-379 Rail Car Number Condition Reason for Return Remarks Dispo Delivered To Return Authorized By Date Originally Shipped \ \ \V -A V7-17X5 Original--Supply & Transportation--Houston Copies--Receiving Plant{2) 1> II M <Wt]-: me+ M--- Received By Controller's--Houston VAB.0001200802 Regional Sales Office Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I F I CATE OF Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 VS I S A' Date: Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: /j/3/9^ Product: Lot No.: ccoTrailer No s *7^3 7? cotzis*} Order Propertv Test Method Volatiles, V. ABR-iA Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR--10 Specification 0.30 Max. .510 Min. 6.0 Ma x. Analvsis .63 0.1 Max. NDS 10.0 Max. 5 Max. /* <> o 25 Max. 8.5 Max. .90 to .95 Not more than B.5 PPM A3L Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-3624 mmm VAB.0001200803 PVC BULK TRAILER ANALYSIS Date /* 'W'fL Customer AfCPY Product Silo___ Technicia MOIST CONT. Tup | Bottom Top 1 Bottom Trailer Number Time Order No. COLOR k vise RVCM FRONT MIDDLE A 60 B= L A* END Particle Size Distribution: Screen Analysis Mesh Size Gross Wt 40 (h.cO Tare Net Wt H on Mash 0.0 i. Screen Analysis V Mesh Size Gross Wt. Tare Net Wt. h on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 tLii /g/r ar<jo %o Tfs Glassy Pan Part. o ) 30,5 10-6 jlAr? /<f-o 9-3 Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks. * 1 VAB.0001200804 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 A * * Date: November 4, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 3, 1992 VISTA Product: 5385 Railcar No.: VIPX 45804 Order No.: 0018152-000 Property Volatiles, % Bulk Density, gm/cc Brabender Dry Time, Mins. Particle Size Distribution % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABR-6 Specification Analysis 0.30 Max. 0.16 .510 Min. 0.580 6.0 Max. 5.0 0.1 Max. 0.00 to 00 to Ul NDS 10.0 Max. 5 Max. Avg. * 0 (By Compartment) Average of 5 per railcar? 10 max. in a single compartment. A 0 1CA CB B 00 Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.084 0.93 Amy jjjv Bagw Laboratory Supervisor (601) 369-3624 VAB.0001200805 Vista Polymers Highway 25 A Aberdeen, MS 3973Q RVC RAILCAR ANALYSIS \JlPiL Load Date : _//*"9^ Time Logged In: Ship Date Product: Car No Logged In By: CD l$\S2'~O0& s) 6&Jc#c, jijo m Compartment Sample From A Bottom Moisture % BL Contamination BR* Bulk Density BD after Fluff Hard Particle 5 7 s ,f2- i i Viscosity * RVCM 4 .0*4 40 i Mesh/G^la*s"sie* s* ___ <Q-___ 4a i Screen Analysis Mesh 40 60 Weight % 0,0 ,* CA Bottom ./4 6 CB Bottom . /r _7 L sn B Bottom .14 f .T77 - Q-____ s rf/ A? > ------- 80 >1.0 100 /r.3i 36, L 120 12.3+ 2*4^ 140 7- /s' s+,3 200 /:" Pan A ^2. Drytime: r.o Static Flow: 0 / F.L Avg. Microns: JS'J. T Color L: / 09. S2 a 0*0* b Technician: #43 VAB.0001200806 Virta Polymers A Division of Vista Chemical Company Highway 25 past Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: November 4, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 2, 1992 VIS1A Product: 5385 Railcar No.: VIPX 45783 Order No.: 0018058-000 Property Volatiles, % Bulk Density, gm/cc Brabender Dry Time, Mins. Particle Size Distribution % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies Test Method ABR-1A ABR-2A ABR-7 ABR-3 ABR-6 Soecification Analvsi 0.30 Max. 0.17 .510 Min. 0.572 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.3 10.0 Max. 1.9 5 Max. Avg.* 0 (By Compartment) A CA CB B Average of 5 per railcar? 10 max. in a single compartment 0 0 0 0 Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 4 0.027 0.92 Amy E. Laboratory Supervisor (601) 369-3624 VAB.0001200807 Vista Polymers Highway 25 Aberdeen, MS 3973Q ^VC IRA X LCAR ANALYS X S Load Date: Time Logged In: UShip Date: l Product: Logged In By: Order No: 001 Car No. Sllo(s): O Custome Screen Analysis Mesh 40 60 80 100 120 Weight 0,00 .2*! %7 0 /r.3i % 0O /%* So, f 140 7. /7 200 f- /3 /. 3 . Pan . 9+ At Drytime: u * Static Flow: Color L: /0O'~ a 0 / 9. 2, Awe Microns: .. . 4 - b A-ri -4 Technician VAB.0001200808 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: November 6, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 4, 1992 VB1A Product: 5385 Railcar No.: ACFX 41180 Order No.: 0018152-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Soecification Analvsis 0.30 Max. 0.18 .510 Min. 0.593 6.0 Max. 5.0 0.1 Max. 0.00 NDS 9.7 10.0 Max. 3.1 5 Max. Avg. * 0 (By Compartment) A CA CB B Average of 5 per railcar; 10 max. in a single compartment 0 0 0 0 Hard Particles 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.745 0.92 Amy E U Bagwelx"^ Laboratory Supervisor (601) 369-3624 VAB.0001200809 A Vieta Polynera Highway 25 A Aberdeen, HS 3973Q RVC RAILCAR ANALYSIS aw Losd Dsit/6 Time Logged In: Ship Date: ^2. Product: Car No.: SQ Logged In By: Silo(s): Order No: CD(%t<52-'66/ Customer: n* Compartment A Sample From Bottom Moisture % BL Contamination BR ./j 8 Bulk Density .>23 BD after Fluff Hard Particle 5 7 g a Viscosity RVCM * * 4 40 Mesh/Glassies * - *- + i ** 0 Screen Analysis Mesh 40 Weight % i.Oo 0,0 60 ,3f on CA Bottom 4 r /o .52/ CB Bottom ,/r ~7 ,S`9`/ B Bottom J7 f /z ,S?.2 ..................................... / :.A.............................. t & 80 2.13 /3 100 9sa 120 n.o 7 140 t$<0 200 *.su Pan j.a. 3. 1 Drytime: s'. 0 Static Flow: 0 / f./ Avg. Microns: ifu Color L: /oo, *3 .03 b /. 47 Technician: VAB.0001200810 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 vs x s A Date: ///^/^ Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Product: 5385 Lot No.: Trailer No.: } Order No.: $0/3333 ooo Property Test Method Volatiles, */. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins ABR-7 Particle Size, V. on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR-12 Vinyl Chloride Monomer ABGC-26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis o. // 0.S1G 0.1 Max. NDS OP 9.2. 10.0 Max. 5 Max . 25 Max. _o___ 4 8.5 Max. .90 to .95 Not more than 8.5 PPM 0.94 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200811 PVC BULK TRAILER ANALYSIS Aa Date //-Z-9Z- Customer Technician A4**t Product Silo___ C? (p FRONT MOIST Top ( Bottom I ,// CON'T. Top Bottom I. GEL iI f 2. I. I I MIDDLE 2. Trailer Number Time siro Order No. 00/$ S3 3 BULK DENSITY i .S'?L* DRY TIME i. COLOR l = ms7 B = in'* I OO o vise RVCM ClASf\i I END i ii Particle Size Distribution: Screen Analysis /A Mesh Size 40 Gross Wt. Tar1 e b Net Wt. % on Mesh 0.00 __(L jfl_.. S Screen Analysis % Mesh Size Gross Wt Tare Net Wt. H on Mesh 40 Min On Rotap shaker gins 60 80 100 120 1.0 gms. Carb 140 200 . 31 Min. t.s4 Id7 12.1.3 17.1 2f-l tfk * On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb 60 140 200 Glassy Pan Part. _Do 2.Z Glassy Pan Part. Remarks % VAB.0001200812 *9 Customer Return Receiving Report Vista Chemical Company Plant From A iBfejHPKiKII SMCOBP POLYMER PRODUCTS YORKVILLE ED. COIflHBPS. MS 39701 Delivered By Quantity X Description VISTA 5385 PVC REBUT Pro Number Prepaid Collect Collect Amount $ VEDV No. CR Date Returned Date of Report Trailer Number 5-382 Rail Car Number Condition Weight ORDER SO. 00180A<M)01 SHIPPED 11/2/92 JhAJLdu irlt -- (UuPfmouyi f\jUUiLo Reason for Return Remarks Disposition Return Authorized By Date Originally Shipped Delivered To Received By V7 17-X5 Original-Supply & Transportation--Houston 4 "J ' -J rn^^ +. turn wuaw - r + Copies--Receiving Rant(2) * '..................... Controller's--Houston " ~>F| ipunmnau--wia 1 1 11 -- VAB.000120081: * Regional Sales Office Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-6111 A Date: November 11, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 9, 1992 VISIA Product: 5385 Railcar No.: VIPX 45785 Order No.: 0018152-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 0.30 Max .510 Min 6.0 Max Analysis 0.12 0.594 5.0 0.1 Max. 0.00 NDS 10.5 10.0 Max. 2.5 5 Max. Avg.* 0 (By Compartment) A CA CB B Average of 5 per railcar? 10 max. in a single compartment 0 0 0 0 Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.044 0.93 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001200814 Vata Polymere Highway 25 A Aberdeen, MS 39730 3PVO Locid D&tc * /A 6-fSL RAILCAR Product: ANALYS X S Car No. : lJtPU> Time Logged In: &/&& npi Ship Date: Logged In By: c& S1 lo ( 6 ) : Order No: flOISiSZ-gdZ, Cu6torae r: a/P M Compartment * Sample From A Bottom Moisture % BL Contamination __ BR P J>~ IX Bulk Density BD after Fluff Si> Hard Particle 5 7 7 Viscosity RVCM .w * d .6*14 * 40 - M e s hi /C*lassie*4s * o , 4 CA Bottom _ Screen Analysis Mesh 40 Weight % 60 Qjx _A_ 80 t./6 12.2* 100 )2. 7? o?3 '5 CB Bottom y /*> ,S1(- B Bottom /i ,slx * / / # _____ o- a. P o 120 IS.U I(. 0 140 ni 200 3'PS' Id. S' Pan Mt 4.r Drytime: -S. D Static F low : * ,7-9 Avg. Microns: jjm Color L: JPP. 3(+ a 0*0 ^ b \ni Technician // VAB.0001200815 Vista Polymers A Division of Vista Chefmcat Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: November 11, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 9, 1992 VISIA Product: 5385 Railcar No.: UTCX 46416 Order No.: 0018152-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.590 60 Max. 5.0 0.1 Max. 0.00 NDS 8.6 10.0Max. 1.9 5 Max. Avg.* 0 (By Compartment) A CA CB B Average of 5 per railcar? 10 max. in a single compartment 0 0 0 0 Hard Particles @ 7 Mins. ABR--12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 10 0.535 0.92 Amy EXBagwel Laboratory (601) 369-3624 VAB.0001200816 Vista Polymers Highway 25 A Aberdeen, MS 3973q Load Date:....// ^ ^ RAILCAR ANALYSIS Product: 5385 Car No. ucv4 Time Logged In: 06/ ST. Ship Date: Logged In By: 00 1&ISZ-/)a3 Silo(s): Custome 6~?? Ur n Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density 3 U BD after Fluff Hard Particle 5 7 10 Viscosity qnf RVCM f 5$~ 40 Mesh/Glassies 0 CA Bottom * O Screen Analysis Mesh Weight % 40 0 CO ao 60 e>3(+ 80 i^ 100 /3-Q& (*> CB Bottom 3 38 B Bottom & / o 120 140 200 Pan Drytime: Static Flow: c LS4- Avg. Microns: Color L: b /Cr7 Technician: VAB.0001200817 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 IFI C O F" ANAL VS X S A Date: ////&/<^ Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: Product: 5385 Lot No. : y Trailer No . : 7 Order No. : QO /8 4^& "6CC> Propertv Test Method Volatiles, 7. ABR-1A Bulk Density, GM/CC ABR-2A Brabender Dry Time, Mins. ABR--7 Particle Size, X on ABR-3 40 Mesh 200 Mesh Pan 40 Mesh Glassies ABR-6 Hard Particles, 7 Mins. ABR--12 Vinyl Chloride Monomer ABGC--26 Inherent Viscosity ABR-10 Specification 0.30 Max. .510 Min. 6.0 Max. Analysis 0.1 Ma x. NDS 10.0 Max. 5 Max . 25 Max. -0 - r 8.5 Max. .90 to .95 Not more than B.5 PPM 0.45 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601) 369-3624 VAB.0001200818 BLEND NO: 0*HA*L RESi BAG BLEND PRODUCt: DATE: 7-/ J- Avg. Microns, 5225/5325/5415: 1 5/7 I BOLE BIN. DIY STATIC TIME/TESTED BY: //ac - COLON X 4 VAB.0001200819 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS H A Date: November 24, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 23, 1992 VISIA Product: 5385 Railcar No.: UTCX 46431 Order No.: 0018476-000 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.18 .510 Min. 0.590 6.0 Max. 4.8 0.1 Max. 0.00 NDS 9.0 10.0 Max. 2.1 5 Max. Avg.* 1 (By Compartment) ^Average of 5 per railcar; 10 max. in a single compartment Hard Particles 6 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to . Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 4 0.098 0.92 Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200820 Vieta Polymera Highway 25 A Aberdeen, MS 3973Q PVC RAX LCAR ANALYSIS Load Date:, // ~^ Time Logged In: Ship Date: liks Product: Car No.: Logged In By Order No: 1 S471>'007> Silo(6) Customer: ?6- ?7 O'YH <afrL~- Compartment A Sample From Bottom Moisture X BL Contamination BR Bulk Density `\S [S' BD after Fluff Hard Particle 5 H 7H Viscosity RVCM AM .oAb 40 Mesh/Glassies * * Screen Analysis Mesh Weight % 40 0_ --------------------- &> 60 0J7o L4- CA Bottom %J k SZ4- CB Bottom if Tv 5Tf B Bottom IA- \C .S3& / e? P 80 100 120 140 /3*f3 /3le 200 i/ /#g Pan Drytiroe: 4# Static Flow 6/ Avg. Microns: Col or L :/"'*< b Technician : VAB.0001200821 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS A Date: November 25, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 24, 1992 VISIA Product: 5385 Railcar No.: PLCX 43862 Order No.: 0018476-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.587 6.0 Max. 5.0 0.1 Max. 0.00 NDS 5.9 10.0 Max. 1.8 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles G 7 Mins. ABR-12 Vinly Chloride Monomer, ppm ABGC-26 Inherent Viscosity ABR-10 Polyvinyl Chloride, Virgin Resin, Not 25 Max. 8.5 Max. .90 to .95 5 0.102 0.93 my E YBagwe' Laboratory Supervisor (601) 369-3624 VAB.0001200822 Vieta Polymers Highway 25 A Aberdeen, MS 39733 4 E>VC RAILCAR ANALYSIS Load Date:, Time Logged In: fi/An Ship Date: u \tA Product: Car No. Logged In By: Order No: l ^74>-oo; Sllo(s): Customer:./ aj Tnct* L_ Compartment Sample From A Bottom Moisture % '1 -- BL Contamination BR /o Bulk Density J~?S BD after Fluff Hard Particle 5 /A- 7 Viscosity * .$30 RVCM * * 40 +Mq e s ha /G*la*ssie* s* (O L 1 CA Bottom * 1^ 7 w CB Bottom 'P %- // ,&8 -S i? 1- & o _________ B Bottom 8 .5U o Screen Analysis Mesh Weight % 40 a OO o^O 60 L343*7 80 JMl 100 120 lQj ff.7 140 $95 200 5T<? Pan 0.9o UL- Drytiroe: Static Flow: d /fjg Mic rons: [U&iAvg Color L ///. +# b L(t* Technician: VAB.0001200823 Vida Polymers ADivisionof Visla Chemical Company Highway 25 Post Office Bax 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: November 30, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 25, 1992 VISIA Product: 5385 Railcar No.: VIPX 45756 Order No.: 0018476-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.563 6.0 Max. 4.7 0.1 Max. 0.00 NDS 8.4 10.0 Max. 2.2 5 Max. Avg.* 0 (By Compartment) *Average of 5 per railcar; A CA CB 1 B 10 max. in a single compartment 0 0 0 0 Hard Particles 8 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 3 0.099 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200824 Vista Polymers Highway 25 Aberdeen, MS 39730 * //AE? VO RAILCAR ANALYSIS Load Date: / Product: Car No. Time Logged In: l^3& Ship Date: hhtr Logged In By: Order No: Q0)$ Silo(s): Customer: /J wet* L- Compartment * Sample From A Bottom Moisture X .0$ BL Contamination // BR 43 Bulk Density ,518 BD after Fluff Hard Particle 5 JK> 7 3/toC Viscosity RVCM -3$d. .m + [i 1 U ___________-- ________- __. _ 40 Mesh/Glassies 4V M* - a * * * 1 r -* CA Bottom 5" // ,576> H CB Bottom .15 20 .557 / B Bottom /3 5* 3<3 .S9Ctf O * -- Screen Analysis + Mesh 40 Weight 0-0 % g-Q 60 L2Z Q-l' 80 17/ H-+ 100 /7& -3/ 5 120 140 /3 n ./ ^(*.1 13-2. 200 Pan /_.2_0__ 14 2- Z Drytime: Static Flow: ^ Avg Microns Color L 164.57- a a&g^ b (.4-g Techn1cian: VAB.0001200825 Vista Polymers A Division of Vista Chemical Company Highway 25 tost Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: November 30, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: November 25, 1992 VISlA Product: 5385 Railcar No.: VIPX 45308 Order No.: 0018476-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Soecification Analvsis 0.30 Max. 0.17 .510 Min. 0.581 6.0 Max. 5.0 0.1 Max. 0.00 NDS 7.0 10.0 Max. 1.9 5 Max. Avg. * 0 (By Compartment) *Average of 5 per railcar; 10 max. in a single compartment. Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 4 0.424 0.92 Amy E. Bagweri Laboratory Supervisor (601) 369-3624 VAB.0001200826 Vista Polymers Highway 25 A\ Aberdeen, MS 3973Q Load Date Time Logged In: Ship Date: RAILCAH ANALYSIS Product: Car No.: i/iff 33<> Logged In By: Silo(s): Order No: r: Ate 7? Compartment A Sample From Bottom Moisture X BL Contamination BR a Bulk Density BD after Fluff \ CA Bottom \*7 SSS CB Bottom JO B Bottom 7 Viscosity RVCM 4Z3 40 Mesh/Glassies * * ^ & Screen Analysis Mesh Weight X 40 0,. 0,0 60 47 / > 80 //g-g 100 120 JLt& 14 0 0 200 3.4% yp Pan Li Drytiroe: Static Flow: * Avg. Microns: Color L I". 0 b Technician: MlTHib. VAB.0001200827 Vista Polymers # k A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: December 3, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. BOX 191 Columbus. MS 39701 Attention: Plant Chemist Ship Date: December 1, 1992 VIS1A Product: 5385 Railcar No.: PLWX 44410 Order No.: 0018476-004 Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 .510 Min. 0.578 6.0 Max 4.8 0.1 Max. 0.00 NDS 8.9 10.0 Max. 2.4 5 Max. Avg.* 0 (By Compartment) *Average of 5 per railcar; 10 max. in a single compartment A | CA CB B 0000 Hard Particles 8 7 Mins. ABR-12 25 Max* Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.263 0.94 Laboratory Supervisor (601) 369-3624 VAB.0001200828 4T Vista Polymers Highway 25 d- -I. ..... Aberdeen, MS 39730 A RAILCAR ANALYSTS -+ /W Load Date: fhP7^22 Product 5385 Car No.: fff/o Time Logged In: Of^ Logged In By: Silo(s): Ship Date: i Order No: Customer A)o Compartment A Sample From Bottom Moisture % .ot BL Contarnination BR 4 Bulk Density 570 BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies o CA Bottom ')ZL 11/ 5V(* (P CB Bottom .15 (O 5> B Bottom 12 -T' Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight o, 0Q 6 IS Hjs_ l&hR. fir+S *7&> L % OP oA- Drytime: M Static Flow: a Color L: a o L 18 Avg. Microns: *-l b 1.7<- Technician: H hi wmm f mm VAB.0001200829 Vista Polymers Highway 25 M rtul. I-L. .. '. ,`tl-r -'..........' *TH Aberdeen, MS 39730 A RVC RAILCAR ANALYSIS Load Date: (l~"3 Time Logged In: ^/Q e Product: 5385 Logged In By:__^ Ship Date: Order No: Car No. Silo(e): (o7(o+&?7 Customer: Compartment Sample From Moisture % Bottom ~t&P Bottom Contamination Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % Drytime: Static Flow: _____ L_____ Avg. Microns: Color L: Technician: nF VAB.0001200830 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-6111 CERTIFICATE 07 ANALYSIS A Da1:e: December 7, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. BOX 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 3, 1992 VIS1A Product: 5385 Railcar No.: ACFX 45864 Order No.: 0018476-005 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.16 .510 Min. 0.580 6.0 Max. 4.9 0.1 Max. 0.00 NDS 14.5 10.0 Max. 1.8 5 Max. Avg.* 0 (By Compartment) A CA | CB | B *Average of 5 per railcar; 10 max. in a single compartment 0 0 | 0 0 Hard Particles 7 Mins. ABR-12 Vinly Chloride Monomer, ppm ABGC-26 Inherent Viscosity ABR-10 Polyvinyl Chloride, Virgin Resin, Not 25 Max 8.5 Max. .90 to 0.143 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200831 Il Vista Polyiiers Highway 25 Aberdeen. MS 39730 A RAILCAR ANALYSIS Load Date \2^2^^ Ship Date In: 5VOO Khfc Product 5385 Car Ho. Logged In By: Silo(s) 0 D /z47L> 'Oa^' Customer 7C n# AfM. Compartment A Sample From Bottom Moisture % BL Contamination BR js.: Bulk Density .stz- BD after Fluff Hard Particle 5 7 /0 Viscosity RVCM il4b 40 Mesh/Qlassies Q Screen Analysis Mesh 40 We ight 0.CO % +0 60 J1 .4 CA Bottom di j zv? CB Bottom JJ 7 . C?o B Bottom * 4 * 71 0 0o 80 r.*r /0 .9 100 ILHk 23.7 120 /3.tL 2t. 140 200 . S" dL Pan . 12. // Drytime: 1 Static Flow: * / 7. f Avg. Microns: Color L: /*0.V a >r b /7/ /31.Z. Technician: M41 VAB.0001200832 ' Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369*8111 CERTIFICATE OF ANALYSIS A Date: December 10, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 9, 1992 VISIA Product: 5385 Railcar No.: ACFX 41162 Order No.: 0019557-000 Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.16 510 Min. 0.587 6.0 Max. 4.5 0.1 Max. 0.00 NDS 8.4 10.0 Max. 2.1 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment 0 1A 1 CA CB B 000 Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 5 0.067 0.93 Amy E. Laboratory Supervisor (601) 369-3624 VAB.0001200833 Vista Polymers Highway 2 5 Aberdeen. MS 39730 A RAILCAR ANALYSIS Load Date: Product: 5385 Car No.: i'll Ce Time Logged In: f7<%0 Logged In By: Silo(6): Ship Date:_ IOrder No: @ & ltf$^57~'O0O Customer: HoTtehtl-- Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density >6*7 UL BD after Fluff Hard Particle 5 7 Viscosity RVCM J2& Otol 40 Mesh/Glassies 0 Screen Analysis Mesh 40 Weight x oro 60 CA Bottom 14- CB Bottom ./(& 13 B Bottom /o 00 0 80 7. 4fT 100 120 . /w 140 7.30 14&2 200 *99- Pan f.*r <2.1 Drytime: 4 Flow: 0 /** Avg. Microns: /<r(A Color L: /** a 0O& b 1.7 & Technician: VAB.0001200834 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: December 16, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. BOX 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 14, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46414 Order No.: 0019557-001 Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 510 Min. 0.582 6.0 Max. 4.9 0.1 Max. 0.00 NDS 9.9 10.0 Max. 2.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar? 10 max. in a single compartment A CA CB B 0|0 0 0 Hard Particles 7 Mins. ABR--12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.093 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200835 Vista Polymers Highway 26 Aberdeen, MS 39730 A PVC RAILCAR ANALYSTS Load Date Product 5385 :JTime Logged In: Ship Date A^-0 o Logged In By: Order No: Ob iMk Car No. &1 Silo(s) OCX Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR J3 3 Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM .r>43 40 Mesh/Glassies O CA Bottom lUl A t o CB Bottom uz o B Bottom 3 <D Screen Analysis Mesh Weight % 40 Q . OO fl.o 60 .17 L7 80 mo ISM 100 u.d-% 120 W'QZ, 140 0*1 . 200 Pan g/.9y |,oQ 5/0 Drytime: 462_ Static Flow: V L Avg. Microns: Color L: ^ a \3 b hi1 Technician VAB.0001200836 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: December 17, 1992 Customer: 6ENC0RP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 16, 1992 VISIA Product: 5385 Railcar No.: ACFX 41166 Order No.: 0019557-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.04 .510 Min. 0.585 6.0 Max. 4.6 0.1 Max. 0.00 NDS 9.6 10.0 Max. 2.3 5 Max. Avg. * 0 (By Compartment) A CA CB B *Average of 5 per railcar; 10 max. in a single compartment 0 0 0 0 Hard Particles 6 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.029 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200837 Vista Polymers Highway 25 Aberdeen. MS 39730 A PVC RAILCAR ANALYSIS Load Date: Product: 5385 Time Logged In: !& Logged In By: Ship Date:. Order No: . : Uf/ C Car No Silo(s): ustomer ^0 21 Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density f r BD after Fluff Hard Particle 5 7 JO Viscosity ML RVCM ._02d 40 Mesh/Glassies 0 0 CA Bottom CB Bottom o 3 }*> 5^7 % 0 ? c> B Bottom *03 2 St l (&*> Screen Analysis Mesh 40 Weight % 0-0 60 </ b f 80 100 120 tl #07? 27> ' 70 <f 140 .o3 /JU. 200 Pan A/7 Drytime: (6 Static Flow: O / <fr 3 Avg. Microns 7 Color L: a b I.%% Technician: M't'T VAB.0001200838 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 A CERTIFICATE OF ANALYSIS Date: 12/21/92 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: 12/18/92 Product: 5385 Railcar No.: VIPX 45878 Order No.: 0019557-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.12 .510 Min. 0.579 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.3 10.0 Max. 2.4 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles G 7 Mins. ABR-12 2 5 Max. Vinly Chloride Monomer ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.266 0.93 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200839 Vista Polymers Highway 25 Aberdeen. HS 39730 A Load Date Time Logged Ship Date: PVC RAILCAR ANALYSIS Product: Logged In By: Order No: * Car No ^-TS'7^ A? ^1 Silo(s) Customer: Compartment Sample From Moisture % Contamination Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh Weight 40 0,00 % 60 80 100 120 140 200 Pan S3 8.L&- ism. IML 1.of H33 u? 17,2 1M Ml f. 3 a.</ Drytime: 0Static Flow: / ~7i3 Avg. Microns iSo. & Color L: /#?. 1$ a JJ b 1M Technician VAB.0001200840 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OE ANALYSIS Date: 12/21/92 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: 12/19/92 Product: 5385 Railcar No.: UTCX 46505 Order No.: 0019557-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max 0.18 .510 Min. 0.586 6.0 Max. 4*9 0.1 Max. 0.00 NDS 10.6 10.0 Max. 2.4 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 7 Mins. ABR-12 Vinly Chloride Monomer, ppm ABGC-26 Inherent Viscosity ABR-10 Polyvinyl Chloride, Virgin Resin, Not 25 Max 8.5 Max. 90 to cessed 0.218 0.93 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200841 o4 it 5*- , . - _ r-',f, * * iW^t?pb a -!>. i *% _.k '.(_ * * A Vista Polymers Highway 25 Aberdeen. MS 89730 PVC RAILCAR ANALYSIS C 7*JC Load Date: ~/-P Product: Car Ho. Time Logged In *fOo Logged In By: 41 Silo(s) Ship Date: Order No: Customer: /Wo Compartment Sample From Moisture % Contamination Bottom Bottom i_iV Bottom JJ. Bottom Bulk Density BD after Fluff Hard Particle 5 Viscosity RVCM .13o 40 Mesh/Glassies SV $11 SiS Screen Analysis Mesh Weight % 40 >,<Tc) 0,0 60 Lt 80 LSI 100 120 134,1 13-13 140 131 200 jU? lAsZ [0* (0 Pan Drytime: VStatic Flow: L Avg. Microns 1.73Color L: 160 iL 0 a PS b MS.# = _& Technician mum f VAB.0001200842 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERT X FICATE C Date: 12/22/92 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: 12/21/92 sis VIS1A Product: 5385 Railcar No.: VIPX 45900 Order No.: 0019963-001 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.21 .510 Min. 0.589 6.0 Max. 4.8 0.1 Max. 0.00 NDS 6.1 10.0 Max. 1.8 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 7 Mins. ABR-12 Vinly Chloride Monomer, ppm ABGC-26 Inherent Viscosity ABR-10 Polyvinyl Chloride, Virgin Resin, Not 2 5 Max. 8.5 Max. .90 to .95 1 0.258 0.93 H. D Lucas Laboratory Supervisor (601) 369-3624 VAB.0001200843 f* ". ** *1* \*3% * - _ 'f Vista Polymers IhUiis ' - k Highway 25 Aberdeen. MS 39730 *.- r * r A Load Date: f S ^ / P Time Logged In:.. Ship Date: 2- Product: 5385 Car Mo.: <4S?v Logged In By: & Silo(s)1 l*?7 Order No: 3 Customer: ^ /&P- <*?-+--r Compartment Sample From Moisture % Contain inat ion Bulk Density BD after Fluff Hard Particle 5 Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh Weight % 40 <>.> 00 60 Zcf 80 ??'? 100 2^-9 120 Mtoy >A S 140 /ft 2- 200 J Pan JLL Drytime: Static Flow & / O Avg. Microns / 63-5 Color L: ^ a ^ V7 b /'? f Technician: VAB.0001200844 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICAT Date: 12/22/92 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: 12/21/92 VIS1A Product: 5385 Railcar No UTCX 46486 Order No 0019963-000 Property Test Method Volatiles, X ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh X on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.581 6.0 Max. 5.0 0 * 1 Max. 0.00 NDS 7.0 10.0 Max. 2.0 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 0 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.031 0.92 Laboratory Supervisor (601) 369-3624 VAB.0001200845 iW-v. -.Vin.v^'ia* F b > * % r t ,r* ' 4? L *x. i ^fii >WI^J a n. Vista Polymers Highway 26 cy* Aberdeen, MS 39730 A Load Date: IM* Time Logged In Ship Date: /? RAILCAR ANALYSIS CcT^K Product: 5385 Car No. Logged In By: Silo(6) Order No: Customer: Compartment Sample From Moisture % Contamination Bottom Bottom ./r Bottom Botton Bulk Density BD after Fluff , Hard Particle 5 7L3abl. Viscosity RVCM _ 03 40 Mesh/Qlassies iTYo -71 . JTT/ Screen Analysis Mesh 40 Height % 60 80 0-&8 /f-25' 100 l 22-$ 9.9 120 /2./& &hJL 140 /*./? /If- 200 1.0 Pan 2.0 Drytime: Static Flow: o /** Avg. Microns: ftJAColor L: a dL. b t.f4 Technician: mm /tut) +J>C~ rnmmmmm VAB.0001200846 (J Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8 111 CERTIFICATE OF ANALYSIS A December 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist h Ship Date: December 28, 1992 VISIA Product: 5385 Railcar No.: PLWX 44376 Order No.: 0019557-006 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analvsis 0.30 Max. 0.16 .510 Min. 0.576 6.0 Max. 5.0 0.1 Max. 0.00 NDS 9.0 10.0 Max. 1.6 5 Max. Avg * 0 (By Compartment) A CA CB B Average of 5 per railcar? 10 max. in a single compartment 0 0 0 0 Hard Particles @ 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 2 0.011 0.93 UJL Amy E. Laboratory Supervisor (601) 369-3624 VAB.0001200847 Vista Polyners Highway 25 Aberdeen, MS 39730 A PVC RAILCAR ANALYSIS Load Date:_2 Time Logged Ship Date: Product: 5385 Car No. Logged In By: No: Silo(s) ~6 &(p Customer: Compartment A Sample From Bottom Moisture % BL Contamination ___ BR S 7 Bulk Density BD after Fluff .ST77 Hard Particle 5 7 to Viscosity RVCM flan on 40 Mesh/Glassies 0 Screen Analysis Mesh 40 Weight % 0.0 60 Drytime: 5**o CA Bottom .H j- ,S7t - CB Bottom JT * .S7Z. * B Bottom .tf S' - 0. _ _ <g. _i 80 %* 100 Z0.0 120 /2.r 140 /+. 200 f.O Static Flow: o /1.1 Avg. Microns Pan .#o /4 AS7.3 Color L: /00*JT` a Z2 b Technician: *-mm /M mma VAB.0001200848 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: December 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 28, 1992 VISIA Product: 5385 Railcar No.: VIPX 45870 Order No.: 0019557-007 Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Soecification Analysis 0.30 Max. 0.15 510 Min. 0.571 6.0 Max. 5.0 01 Max. 0.00 NDS 10.0 10.0 Max. 2.0 5 Max. Avg.* 0 (By Compartment) A CA CB B Average of 5 per railcar; 10 max. in a single compartment 0 0 0 0 Hard Particles 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR--10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed 4 0.153 0.93 op Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001200849 Vista Polymers Highway 26 Aberdeen, MS 39730 A PVC RAILCAR ANALYSIS i\I i Load Date: Product: 5385 Car No..: ^ Tine Logged In: /StOp Logged In By: Silo(s): Ship Date: Order No: QO/qs'^7-067 Custome r: tto'VAdki___ Compartment A Sample From Bottom Moisture % o9 BL Contamination BB Bulk Density BD after Fluff Hard Particle 5 7 Viscosity -tizt RVCM /53 40 Mesh/Glassies 0 CA Bottom 2>U O CB Bottom /s' 57 o B Bottom AS* / .SV ( o Screen Analysis Mesh 40 Height % Cl C) 60 a a* o_ 80 100 120 140 200 o Pan 6 O Drytime: & Static Flow: > IO.<0 Avg. Microns: (W* Color L: Ito.is a <U7 bM Technician VAB.0001200850 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTI R X OAT EE OR ANALYSIS A Date: December 29, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 22, 1992 VIS1A Product: 5385 Railcar No.: PLWX 44410 Order No.: 0019557-005 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.04 .510 Min. 0.589 6.0 Max. 4.8 0.1 Max. 0.00 NDS 7.2 10.0 Max. 2.1 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles Q 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.015 0.94 tU i Ammyy^vE.. Bagqwel 1 Laboratory Supervisor (601) 369-3624 L VAB.0001200851  -N * -- .t+v * imi Vista Polymers w. ' Highway 25 r<a n 7 * i,i, Aberdeen. MS 39730 . * .* A PVC RAILCAR ANALYSIS Load Date: /2 -/ S' 7Z^ Product: 5385 Tine Logged In: Logged In By: Ship Date: Order No:. Car Ho. Silo(s): V Customer: V /iS 3> M Compartment A Sample From Bottom Moisture % cn' BL S~ Contamination ___ BR )b Bulk Density BD after Fluff . si* Hard Particle 5 7 Viscosity ^36 RVCM <6 IS 40 Mesh/Glassies P CA Bottom .ol 3 9 yff- - \ CB Bottom , O'2- *? - B Bottom i4 4 . if? 4 e>.ii 6 Screen Analysis Mesh 40 Weight % Q*J>. Drytime: 60 Q-J7 h") 80 2 100 Ii.fi 120 mi 13,0 140 4- YC 123 200 3. (,6. Pan /. P& 2./ "V.& Static Flow & / 7'^ Avg. Microns: /53 7. Color L: /&G . a b /ill WW R' Technician: rficr! mm VAB.0001200852 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OF ANALYSIS Date: December 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 30, 1992 VISIA Product: 5385 Railcar No.: PLWX 44368 Order No.: 0019963-004 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analvsis 0.30 Max. 0.14 .510 Min. 0.579 6.0 Max. 5.0 0.1 Max. 0.00 NDS 7.6 10.0 Max. 1.4 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles 9 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.209 0.92 Amy ly SagweXV Laboratory Supervisor (601) 369-3624 VAB.0001200853 T fiff < . * r * 'F Vista Polymerg > * **. ' _ i * bj - *~6------------------- Ik Highway 26 Aberdeen, MS 39730 A Load Date: ^ -2^^ Product: 5385 Car No.: Time Logged In: t+'Zo Logged In By: Silo(e) Ship Date:. / Z(VOM 2-----OtvW Hr.; /i 90S OO </ Customer: *Ni / A* <2S( Screen Analyeie Mesh 40 Weight % o 60 f/<r 3 80 ll.z 100 _L^1 31.0 120 im.ez Z?,0 140 L.7!T 43 A" 200 7A Pan Drytime: >T.4? Static Flow: Color L: J a / Avg. Microns /S-J.s b to Technician: M VAB.0001200854 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 CERTIRXOATE OR ANALYSIS A Date: December 31, 1992 Customer: GENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 29, 1992 VIS1A Product: 5385 Railcar No.: UTCX 46491 Order No.: 0019963-002 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.15 .510 Min. 0.575 6.0 Max. 4.8 0.1 Max. 0.00 NDS 7.6 10.0 Max. 1.3 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment Hard Particles Q 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 . 90 to Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.136 0.92 Amy E. BagweTT Laboratory Supervisor (601) 369-3624 VAB.0001200855 -Ss ! , a 'r-J ,- ^ V , Vista Polymers ^ I .X -r . t Highway 25 iMh* Aberdeen, MS 39730 A PVC RAILCAR ANALYSIS 9^Load Date : |3. ag Product: 5385 Car Ho ,:JM3L 18 'is-Time Logged In:. Logged In By: Silo(e):. i?7, Lgr Ship Date: Order No: Customer: <Y^O Compartment Sample From Moisture % Contamination Bulk Density BD after Fluff Hard Particle Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % o.&O G-S'Z /i> a*4z 20,$ A bb 5.3 /3-2 7k. /.3 Drytime: <xx Static Flow: o z Avg. Microns .Color L IQ- u a 17 b 1X7 /ss, z_ : 0)4Technician VAB.0001200856 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 C E R I R ICA EE OR ANA SXs A Date: December 31, 1992 Customer: QENCORP POLYMER PRODUCTS P. 0. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 29, 1992 VIS1A Product 5385 Railcar No ACFX 41172 Order No 0019963-003 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabender Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 .510 Min. 0.578 6.0 Max. 5.0 0.1 Max. 0.00 NDS 7.5 10.0 Max. 1 .4 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 0 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max Inherent Viscosity ABR-10 .90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 2 0.054 0.93 Amy E.LBagwe10 Laboratory Supervisor (601) 369-3624 VAB.0001200857 Vista Polymers Highway 25 Aberdeeni MS 39730 A RAILCAR ANALYSTS Load Date:, '3-aq~<?i Product: M072- Car No Time Logged In: Ship Date: Logged In By: Order No:. / Sllo(B)J -663 Customer: Compartment Sample From Moisture % A Bottom CA Bottom CB Bottom B Bottom Contamination Bulk Density BD after Fluff . ZK* Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies `05f 2 Screen Analysis Mesh Weight % 40 0-QQ 60 JL <0 80 100 XI. I' .SI1 o& 120 13.-17 Mi 140 flo 200 3.70 111 Pan 0 Lit Drytime: Static Flow: ^ / &./ Avg. Microns: is's: i Color L: ioc a .n b A77 Technician: . ! * nrf VAB.0001200858 i Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 C EE R T I R I CAT" EE OR ANALYSIS Date: January 5, 1993 Customer: GENCORP POLYMER PRODUCTS P. O. Box 191 Columbus, MS 39701 Attention: Plant Chemist Ship Date: December 31, 1992 VISTA Product: 5385 Railcar No. PLCX 47546 Order No.: 0019557-008 Property Test Method Volatiles, % ABR-1A Bulk Density, gm/cc ABR-2A Brabendsr Dry Time, Mins. ABR-7 Particle Size Distribution ABR-3 % on 40 Mesh % on 200 Mesh % on Pan 40 Mesh Glassies ABR-6 Specification Analysis 0.30 Max. 0.17 .510 Min. 0.575 6.0 Max. 5.0 0.1 Max. 0.00 NDS 8.7 10.0 Max. 1.8 5 Max. Avg.* 0 (By Compartment) Average of 5 per railcar; 10 max. in a single compartment. Hard Particles 7 Mins. ABR-12 25 Max. Vinly Chloride Monomer, ppm ABGC-26 8.5 Max. Inherent Viscosity ABR-10 90 to .95 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. 3 0.071 0.93 Laboratory Supervisor (601) 369-3624 VAB.0001200859 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: Ship Date niv RAILCAR ANALYSTS Product: 5385 Logged In By: Order No: Car No. Silo( 6): 4 Customer: a &4L6frV-p Compartment A Sample From BottomI Moisture % .// BL Contamination __ BR n Bulk Density .5'7J BD after Fluff Hard Particle 5 73 Viscosity .934, RVCM ,tni 1 40 Mesh/Glas6ies 0 1 Screen Analysis Mesh Weight % 40 Q.O P 0,0 60 ,SC M 1 CA Bottom n 12, 3o .5-77 CB Bottom ./s' 29 .S 72. B Bottom ./ 3 n .sis 0 w 0 80 9,33 IhZ 100 JMk 23lL 120 12'17 3S,8 140 7Vo lJ 200 Pan .96 Drytime: .0 Static Flow: Ojti( Avg. Microns: f3 2. & Color L: /OQ-Z! a QJS' b Technician: VAB.0001200860 Wn!lWBaBi !LH11!K IP"PM I 1 jmWIti-uM rsmpE^Lnuwn WWW...... ..... i i ' H-. VAB.0001200861 Vista Polymers A Division of Vista Chemical Company ^ : jHk. Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: Customer: Gitto-Global Corporation 20 Mohawk Drive Leominster, MA 01453 Attention: Joyce Barbieri Ship Date: /////A?. FAX No. 508-534-8362 Product: 5305 Order No.: OOl&StfO-OOO Trailer No.: Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. Bulk Density, gm/cc ABR-2A 0.510 Min. D.5Z& Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. Q.Q % On 200 Mesh % On Pan *NDS 5.0 Max. J?. (0 Specification is 30.OX Max. for the 200 Mesh plus Pan. Residual VCM, ppm ABGC-26 8.5 Max. 0.003 Inherent Viscosity ABR-10 0.71 - 0.76 ^.73 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead VAB.0001200862 Half Customer Technician PVC BULK TRAILER ANALYSIS Product Silo___ Trailer Number Order No. \P0[ ftS" oco A Particle Size Distribution: Screen Analysis Mesh Size 40 Gross Wt Tare Net Wt. H on Mesh Oof 6.0 Screen Analysis Mesh Size Gross Wt. Tare Net Wt % on Mesh 40 Min On Rotap shaker. 49 gms. Resin plus 1.0 gms. Carb 60 80 100 120 140 200 Glassy Pan Part. 0. (<7rae f$33 #7# j,3 o.l t(.X !%(*> Min. On Rotap shaker 49 gms. Resin plus 1.0 gms. Carb Pan 60 80 100 120 140 200 Glassy Part. Remarks VAB.0001200863