Document 1gGvXEQD6M2vEOgmabnrKbJX5
f#" . s >'
s.v.
**-**.-'CG 32
< DATE >
C.V.f9011903
CODE RT-698-D PKG ;___ ___ Gi2J_14____
- (LOT NUMEriR)
EST. WT* * 2828* LBS.
DATE PRINTED: 5/12/82 D.V. 962.094____ _ _______
PROCESSES ( >RT~698-D <M>
APPROVED BY EWK2/25/32
TYPED BY: KLW STANDARD HRS- _________
TIMEM
PREPARATION NOTES:___________________
NON-BLEEDING
EQUIP 1 MENT I
NAME: WATCHUNG RED B
USE N-CODE ACC1 LBS LBS
PREP\ 1
1I 1
i I3 I4 1 ] I [
RECORD:______ BATCHES SINCE SPARKLER LAST i CLEANED- AFTER 4 BATCHES, CLEAN, DRESS
SPARKLER & PRECOAT WITH 15* DICALITE ILTER AID
OBTAIN FOR S11 2-CHL0R0-4-AMINGT0LUENE-5-
i SULFONIC ACID } OBTAIN FOR S41 3-MYDRGXY-2-NAPHTH0IC ACID ! INSTALL DV & CV RECORDER & CONTROLLER CHART | NOTE: RUN 15' WATER INTO V-904. PUMP WATER
| FROM V-904 THRU DISTRIBUTOR. IF WATER DOES 1 WOT COME OUT OF ALL DISTRIBUTOR HOLES WITH
| FULL FORCE, NOTIFY SUPERVISOR
777-A
740-C 92-C
932 |
RUN 20* <415G) WATER INTO V-932 4. HEAT-TO
n } J^SD-iO DEG F
i IN 8-9 MIN DRESINATE
? 4T jJWPlR 5 MIN & RECORD: PH___Z.Sl _ < 9.5-1 . 5)
i STIR 20 MIN OR LONGER TO DISSOLVE FOR S44
47
530-A
470
i NOTE:, NOTIFY PRESS ROOM BEFORE ROPING OFF
" AREA UNDER V-922
922 RUN 38* (782G) WATER INTO V-922
3 GH SODIUM HYDROXIDE IN V-926 4. RUN IN
M_/fL______JQL-J3L% | TURN ON AGITATOR 4, STEAM 4, DUMP IN FROM S2
7-D 740-C
220 1127
j
LOT *10OX
%
I. 2-CHLORD
Jd&lzr -JlSZl-- -9h .l WH
i 4-AMIN0T0LUEHE _______ _ _______ _____________
-SULFONIC ACID _________ _________ _________
tJMP IN ACTIVATED CARBON
25 113-B 25
IN FILTER AID
10 777-A 1
TO 212-214 DEG F WATCH FOAM!!!!
ii RECORD: BY,,_^__(-t-> IF NECESSARY ADJ TO
!
Y SODIUM HYDROXIDE
ASSUME 50%
*
7-D
\J( 1 STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF
| i STE&H'T WATCH FOAM. RECORD: SPARKLER PRES-
i L^tfRE __H___ PSI IF NOT'ZERO NOTIFY SUPVR. |1^T CIRCULATE 15 MIN OR LONGER THRU SPARKLER
JUL 261382
| I UNTIL SOL`H IS CLEAR- MAINTAIN AT 190-195
I ! FOR SI 9.^RECORD: STARTLia^Ji^sXjjOTAl^iLTNyL
i | CLARITY^fciSt^HTF & REC_*L_ F
DU P050464598
EQUIP
MENT
t PAGE 2 OF 3 CG 32 CODE RT-698-D (M) I
i------------------------- '---------------------------------------------------------------------------------------|.
904/CVH8 i RUN 2' <58G) WATER INTO V-904/CV
I
4 Ii9 f WHEN-SI 7 COMPLETE, PUMP IN V-922 THRU
- .1 | SPARKLER, MAINTAIN V-922 AT 190-195 TD>, EG F..
I . | RECORD: START_____TOTAL MIN
USE LBS
N-CODE
ACCT LBS
902 RUN 54' (1407G) WATER INTO V-902
5 SLURRY
t . lifND HOLD FOR S41
M.
SMOOTH. ] *530 1
# IN- i XU ^ isdLWLi
MEASURE Sfl| UNITS IN V-928 FOR S35 ^
\\ 1 HYDROCHLORIC'ACID M_____ L____ ILSji\l-lSJjx
s\r___T-ll rut**\ 1 i.Wic~ErIrGuH rSnOnDriIUimM iiNt tITdRt tITi:E t ImN dPt T cFruO?R nSo38 a(p-x -
.1 . --
.........
- -M
J
\lMP-\
l\t.L&' n\
't 542-D !
} 1 7-D i
1 28-D 1
1 725-A 1
530 166
544 367
922 7
922 9*
I
1m3s \ i
WHEN SI 9 COMPLETE, STOP PUMP 6 INSERT V-9221
FOOT PLUG
-1
RUN IN 15' (309G) WATER & HEAT TO 190-195 F|
'RCULATE 15 MIN THRU SPARKLER 1
PUMP V-922 THRU SPARKLER INTO V-904/CV
1
1 ------------------------------------------------------- ---------------------------- ~
--------------------------------------------------- :------------------------- --
RUN IN ?' (177G) WATER INTO V-922 AND HEAT 1
TO 190-195 F* CIRCULATE 15 MIN THRU SPARKLRi
r 904/CV t 40
I.
.1l
UMP V-922 THRU SPARKLER INTO V-904/CV WEN MTY BLOW OUT SPARKLER INTO V-904/CV
UR IN IGEPAL CO-630 HEAT TO 165-170 DEG F-FOR S34
1 X1
1I VX%7 |1 979-D.
47
CV 11 pR *><ft
L
NOTE: IF N-740-C SOL'N`WAS. PUMPED DIRECTLY
:OM SPARKLER TO CV, OMIT STEP| ^3 6 34,.
UN IN 1* (95C-) WATER" INTO' V-.
N SS2C0MPLE1
THRTKUN-KRSU^F'AC
< 12-1>^N0s>miilTAIN
1 v^tiECORD: STAR!____
!-35 j RUN.' IN HYDROCHLORfC
8-D FROM S23
12-1j MIN
II
15 MIN AT 165-170 DEG F.
>1
i
3*T|- AD4 TO 48* (4536G) AT 32-38 DEG F156X3301
tORD: TEMP_aLjjL-- F, VOLUME
____
I RUN IN SODIUM. NITRITE N-725-A FROM S24
AFAP <5-10 MIN) it RINSE IN PT
STIR 30 MIN AT 32-38 DEG F MAINTAINING
i +DR> +KI FOR S40 RECORD: TIME START.
I CR_J|4l .<+> KI__!fL_C + >' NOTE: I < 1) .IF CR-, KI- ADD 205 'AS IS." INCREMENTS
HYDROCHLORIC ACf :
I
RECORD: CR< KI____________ < + ) ASSUME 32% I_
(2) IF CR+, KI- ADD 205= "AS IS" INCREMENTS 1
SODIUM NITRITE
!
RECORD: CR;.__t + ) KI________ < + ) ` ASSUME 33% I
DUMP IN FROM S3 6 STIR 10 MIN LOT
I
3-HYDROXY-2-NAPHTHOIC ACID ___ l&JLA*.
i ISaJ-
'. iizzj iziii * 1 muzz
57-A
28-D 725-A
82--C
1021
DUP050464599
DATE PRINTED; 5/12/82
EQUIP i KENT < I
902
I PAGE 3 GiF 3
USE N-CDDE CG 32 C0DE.RT-698-D <M) | LBS
.]------------ ,-----------------
j DUMP IN AMMONIUM CHLORIDE
I 221 I 165-A I1
CV JJO^f'lHHEDlATELY AFTER S41' COMPLETE, WITH V-902 |
13 T 1 AGITATOR ON PUMP V-902 THRU UNDERSURFACE J
I | DISTRIBUTOR INTO CV.IN 18-22 MIN, LET TEMP.I
I RISE FREELY. .
I
i
RECORD: START__TOTAL MIN_____2_~
1
STIR 15 MIN. & RECORD; PH___4-f__(9.-9.8> J
TEMP
DEG F (40-5 DEG F> AND IF PH !
i IS BELOW 9.0 ADJ TO PH 9.0-9.8
|
| SODIUM HYDROXIDE
ASSUME 50% |_A!!h?_
| & RECORD PH_Jl 4_ DIAZO__~_<-> ASSUME 32% iJZI
J* BASE__L_<+> HYDROCHLORIC ACID
|
LS-ri STEAM EJECT V-932 FROM S8 INTOCV
i
n^T POUR IN I CCTANOL
30
*446 I HEAT TO 173-175 DEG F IN 55-65 MIN AND
i
RECORD: HTDEG F . RECDEG F
7-D 28-D
588-A
ACCT LBS
221
/ * t> 30
] DURING S46- HEATING, RUN 10* <268G> WATER
INTO V-902
'
u | itlRN ON AGITATOR & STEAM & DUMP IN BARIUM '
H J^CHLORIDE
J*fj^HEAT TO 155-160 DEG F & STIR TO DISSOLVE
I
I1 259 I i
` 16-B
WHEN S46 COMPLETE, STRIKE V-902 AT155-160F! /
THRU UNDERSURFACE DISTRIBUTOR INTO CV IN !
2-3 MIN
I
RECORD: START_A'l4lT0TAL MIN__#__
i
.HEAT CV TO 193-195 DEG F IN 10-15 KIN.
I
STIR 60 MIN AT 193-195 F. RECORD STARTiU^ff'
AFTR 20 MIN S52 STIR RECORD PH_JL2< 8.S-9.3)1
IF NECESSARY, ADJ TO PH 8.8-9.3 ASSUME 50% j___
AND RECORD: PH__nH--
ASSUME 32% |___ ^
WHEN S52 STIR COMPLETE, FLOOD TO 180-190* j
(+/-18000G) AND STOP AGITATOR
I
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY|
THRU PRESSING, DUMP IN I OCTANOL, STIR 5 !
MIN & STOP AGITATOR. RESUME PRESSING.
|
I
START
FIN
OPTR
I
_&MfJK
-3*J-_______
I
10
7-D 28-D
588-A
10
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