Document 1g2w8p67RenJ0bLGpnZwRJxMK
Caleb Brett Report of Aulysis 2005-005697-DRPK
PLAINTIFFS EXHIBIT
CAM-347
Sample ID : 2005-005697-DRPK-001 Sample Description : ID: Ouangxi #2 Ship name M.V. "Pacific Acadian September 2005
Date Sampled: j j ate jjecejve(j. 09-30-2005
Product:
Method EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc EP 04/2005:0438 talc * EP 04/2005:0438 talc * EP 04/2005:0438 talc FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph * USP28-NF23 talc monograph
Identification B
Test
Identification C
Acidity/ Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Lead
Calcium
Aluminum
Magnesium
Microbial Contamination, Aerobic Bacteria
Date Analyzed: 10-27-2005
Results Pass
Units
Pass
Pass <0.1 <0.1
0.2 <0.01
% % % %
<1 ppm 18.2 % 5.2 % 705 e fu /g <10 efu /g 0.2 %
<3 m g/kg
<1 5
<0.1 5.2 0.1
Pass Pass Pass
5.2 <0.1 <0.01 <0.001
0,2
% m g/kg
% % %
% % % % %
<0.1 % 18.3 % 705 efu /g
THE ANALYSIS RESULTS DENOTED () WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 11-03-05
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) S44-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
ITA-Ratcliff-000142
Intertek Caleb Brett Report of Analysis 2005-005697-DRPK
Sample ID : 2005-005697-DRPK-001 Sample Description : ID: Guangxi #2 Ship name M.V. "Pacific Acadian September 2005
Product:
Method * USP28-NP23 talc monograph * USP28-NF23 talc monograph
Test Microbial Contamination, Fungi
Asbestos
Date Sampled:
Date Received 09-30-2005
Date Analyzed 10-27-2005
Results <10
Absent
Units Cfil /g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
(
l Initial:
/frv .
11-03-05
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Pii: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 5
ITA-Ratcliff-000143
Intertek Caleb Brett
Report of Analysis 2006-001481-DRPK
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, TX 77536 Ph: (713) 844 3200 Fax:(713) 844-3330 Email: dptechctr@intertek.com
Client: Contact: Client Reference No:
Luzenac Ms. M ikki Auburn
Date Requested: Date received: Collected By:
03-06-2006 03-06-2006 Client
Client Sample Description ID: Guangxi #2A February 2006 MV Pos Eternity
RESULTS:
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product Solid Sam-Powder
Sample ID 2006-00148l-DRPK-001
REVIEWED
APR 1 JO20
QM:
This report lias been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative o f the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
03-31-06
Page 1 of 3 ITA-Ratcliff-000144
Intertek Caleb Brett Report of Analysis 2006-001481-DRPK
Sample ID : 2006-00148l-DRPK-001 Sample Description : ID: Guangxi #2A February 2006 MV Pos Eternity
Product: Solid Sam-Powder
Method EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM059 USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled:
Date Received: 03-06-2006
Date Analyzed: 03-15-2006
Results Pass Pass Pass Pass <0.1 0.4 0.2
<0.01 <1
Units
W t% % % % ppm
18.4 % 5.2 % 520 cfu / g
20 cfu / g
Passes Test Passes Test
0.4
%
<3 mg /k g <1 % <5 mg / kg <0.1 % 5.2 %
<0.1 % <0.1 ppm (mg / kg)
Passes Test Passes Test Passes Test Passes Test
5.2
W t%
<0.1 W t%
<0.01
W t%
REVIEWED
Initial: 03-31-06
APR I n 7 m
Intertek Caleb Brett
1114 Seaco Avenue, Deer Park TX 77536
U iV i..
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 2 of 3
ITA-Ratcliff-000145
Intertek
Caleb Brett Report of Analysis 2006-001481-DRPK
Sample ID : 2006-00148 l-DRPK-001 Sample Description : ID: Guangxi #2A February 2006 MV Pos Eternity
Product: Solid Sam-Powder
Method USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled
Date Received 03-06-2006
Date Analyzed 03-15-2006
Results <0.001 0.2 0.4 18.7 Pass 520 20
Units Wt% Wt% wt% wt%
efu / g efu / g
(.
Initial: 03-31-06
r eview ed APR 1n?006
l,
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 3
ITA-Ratcliff-000146
Intertek Caleb Brett
(
Report of Analysis 2006-004700-DRPK
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, TX 77536 Ph: (713)844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Client: Contact: Client Reference No:
Luzenac, Inc. Mikki Auburn SCHDLR: J. POSTON
Date Requested: Date received: Collected By:
06-30-2006 06-30-2006 Client
Client Sample Description
ID: Guangxi#2 June 2006 MV Hebei Arrow ID: Guangxi#2a June 2006 MV Hebei Arrow
RESULTS:
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product
Powder Powder
Sample ID
2006-004700-DRPK-001 2006-004700-DRPK-002
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative o f the samples submitted for testing. This report shall not be reproduced except in full without written approval o f the laboratory.
(
07-25-06
REVIEWED
AUG 0.88 21006
QM:_
Page 1 of 5
ITA-Ratcliff-000147
Intertek Caleb Brett Report of Analysis 2006-004700-DRPK
Sample ID : 2006-004700-DRPK-001 Sample Description : ID: Guangxi#2 June 2006 MV Hebei Arrow
Date Sampled: Date R ecejvetj; 06-30-2006
Product: Powder
Date Analyzed: 06-30-2006
Method
Test
Results
Units
EP 04/2005:0438 talc monograph Identification A
passes test
EP 04/2005:0438 talc monograph Identification B
Pass
EP 04/2005:0438 talc monograph Identification C
Pass
EP 04/2005:0438 talc monograph Acidity / Alkalinity
Pass
EP 04/2005:0438 talc monograph Water-soluble substances
<0.1 W t%
EP 04/2005:0438 talc monograph Aluminum
0.6 %
EP 04/2005:0438 talc monograph Calcium
<0.1 %
EP 04/2005:0438 talc monograph Iron
<0.01
%
EP 04/2005:0438 talc monograph Lead
<1 ppm
EP 04/2005:0438 talc monograph Magnesium
18.4 %
EP 04/2005:0438 talc monograph Loss on Ignition
5.1 %
EP 04/2005:0438 talc monograph Microbial Contamination, Aerobic Bacteria
670 cfu / g
EP 04/2005:0438 talc monograph Microbial Contamination, Fungi
30 cfil / g
FCC V talc monogr aph
Identification A
Passes Test
FCC V talc monograph
Identification B
Passes Test
FCC V talc monograph
Acid-soluble substances (as S04)
0.2 %
FCC V talc monograph
Arsenic
<3 mg /k g
FCC V talc monograph
Free alkali (as NaOH)
<1 %
FCC V talc monograph
Lead
<5 mg /k g
FCC V talc monograph
Loss on Drying
<0.1 %
FCC V talc monograph
Loss on Ignition
5.1 %
FCC V talc monograph
Soluble salts
<0.1 %
H TM 059
Lead
0.2 ppm (mg / kg)
USP28-NF23 talc monograph
Identification A
Passes Test
USP28-NF23 talc monograph
Identification B
Passes Test
USP28-NF23 talc monograph
Identification C
Passes Test
USP28-NF23 talc monograph
Acidity / Alkalinity
Passes Test
USP28-NF23 talc monograph USP28-NF23 talc monograph
Loss on Ignition Water-soluble substances
R \ / 1 t \A/ED
5.1 Wt% <o,i w t%
USP28-NF23 talc monograph
Iron
<0.01
Wt%
A U b U ODD---------------------------------------------------
QM:
tial: 07-25-06
Intertck Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, mvw.intertek-cb.com
Page 2 of 5
ITA-Ratcliff-000148
Intertek Caleb Brett Report of Analysis
( 2006-004700-DRPK
Sample ID : 2006-004700-DRPK-001 Sample Description : ID: Guangxi#2 June 2006 MV Hebei Arrow
Product: Powder
Method USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: Date Received: 06-30-2006
Date Analyzed: 06-30-2006
Results
<1
<0.1
0.4
18.6
Not Present
670
30
Units ppm W t% W t% W t%
efu/g efu / g
REVIEWED
07-25-06
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 5
ITA-Ratcliff-000149
Intertek Caleb Brett Report of Analysis 2006-004700-DRPK
Sample ID : 2006-004700-DRPK-002 Sample Description : ID: Guangxi#2a June 2006 MV Hebei Arrow
Product: Powder
Method EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph Identification C
EP 04/2005:0438 talc monograph Acidity / Alkalinity
EP 04/2005:0438 talc monograph Water-soluble substances
EP 04/2005:0438 talc monograph Aluminum
EP 04/2005:0438 talc monograph Calcium
EP 04/2005:0438 talc monograph Iron
EP 04/2005:0438 talc monograph Lead
EP 04/2005:0438 talc monograph Magnesium
EP 04/2005:0438 talc monograph Loss on Ignition
EP 04/2005:0438 talc monograph Microbial Contamination, Aerobic Bacteria
EP 04/2005:0438 talc monograph Microbial Contamination, Fungi
FCC V talc monograph
Identification A
FCC V talc monograph
Identification B
FCC V talc monograph
Acid-soluble substances (as S04)
FCC V talc monograph
Arsenic
FCC V talc monograph
Free alkali (as NaOH)
FCC V talc monograph
Lead
FCC V talc monograph
Loss on Drying
FCC V talc monograph
Loss on Ignition
FCC V talc monograph
Soluble salts
HTM 059
Lead
USP28-NF23 talc monograph
Identification A
USP28-NF23 talc monograph
Identification B
USP28-NF23 talc monograph
Identification C
USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph
Acidity / Alkalinity Loss on Ignition Water-soluble substances Iron
P \ / 1F W F D AUG 0 8 'UJb
Date Sampled: Date Recejveti : 06-30-2006
Date Analyzed: 06-30-2006
Results passes test
Units
Pass
Pass
Pass <0.1
0.5 0.2 <0.01 <1 18.1 5.1 490 30
W t% % % %
ppm % %
cfu/ g du /g
Passes Test
Passes Test 0.2 % <3 m g /k g <1 % <5 m g /k g
<0.1 % 5.1 %
<0.1 % 0.3 ppm (mg / kg)
Passes Test
Passes Test
Passes Test
Passes Test
5.i <0.1
<o.oi
W t% W t% W t%
tial: r. - n s
--
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
ITA-Ratcliff-000150
Intertek Caleb Brett Report of Analysis 2006-004700-DRPK
Sample ID : 2006-004700-DRPK-002 Sample Description : ID: Guangxi#2a June 2006 MV Hebei Arrow
Product: Powder
Method USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph USP28-NF23 talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: Date Recejvet| ; 06-30-2006
Date Analyzed: 06-30-2006
Results
<1
0.2
0.3
18.1
Not Present
490
30
Units ppm W t% W t% W t%
cfu / g cfti/g
07-25-06
REVIEWED
AUG 0 8 2006
1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 5 of 5
ITA-Ratcliff-000151
Intertek Caleb Brett
(
Report of Analysis 2006-007065-DRPK
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, TX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Client: Contact: Client Reference No:
Luzenac Mr. John Poston
Date Requested: Date received: Collected By:
09-19-2006 09-19-2006 Client
Client Sample Description
ID: GUANGXI 2A ID: GUANGXI 2
RESULTS:
SEE ATTACHED SHEETS
77 Intertek Caleb Brett
Product
Powder Powder
Sam ple ID
2006-007065-DRPK-001 2006-007065-DRPK-002
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative o f the samples submitted for testing. This report shall not be reproduced except in full without written approval o f the laboratory.
(
10-31-06
REVIEWED
JAN 2 20Q7
QM:.
Page 1 of 5
ITA-Ratcliff-000152
Intertek Caleb Brett
Report of Analysis
( 2006-007065-DRPK
Sample ID : 2006-007065-DRPK-001 Sample Description : ID: GUANGXI 2A
Product: Powder
Method EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph Identification C
EP 04/2005:0438 talc monograph Acidity / Alkalinity
EP 04/2005:0438 talc monograph Water-soluble substances
EP 04/2005:0438 talc monograph Aluminum
EP 04/2005:0438 talc monograph Calcium
EP 04/2005:0438 talc monograph Iron
EP 04/2005:0438 talc monograph Lead
EP 04/2005:0438 talc monograph Magnesium
EP 04/2005:0438 talc monograph Loss on Ignition
EP 04/2005:0438 talc monograph * Microbial Contamination, Aerobic Bacteria
EP 04/2005:0438 talc monograph * Microbial Contamination, Fungi
FCC V talc monograph
Identification A
FCC V talc monograph
Identification B
FCC V talc monograph
Acid-soluble substances (as S04)
FCC V talc monograph
Arsenic
FCC V talc monograph
Free alkali (as NaOH)
FCC V talc monograph
Lead
FCC V talc monograph
Loss on Drying
FCC V talc monograph
Loss on Ignition
FCC V talc monograph
Soluble salts
HTM_059
Lead
USP 29 - talc monograph
Identification A
USP 29 - talc monograph
Identification B
USP 29 - talc monograph
Identification C
USP 29 - talc monograph
Acidity / Alkalinity
USP 29 - talc monograph
Loss on Ignition
USP 29 - talc monograph
Water-soluble substances
USP 29 - talc monograph
Iron
Date Sampled: 09-18-2006
Date Received: 09-19-2006
Date Analyzed : 09-19-2006
Results Pass Pass Pass Pass <0.1 0.4 0.1 0.01
<0.001 19.0 4.9 730 60 Pass Pass 0.9 <3 <1 <5 <0.1 4.9 <0.1 1.4
Passes Test Passes Test Passes Test Passes Test
4.9 <0.1 0.01
Units
W t% % % % % % %
cfu / g cfu / g
% mg/kg
% mg/kg
% % % ppm (Wt)
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB B I^ p ^ C /W N O T ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES. Q P y J y V t D
c Initial; 10-31-06
Intertek Caleb Brett
JAN ib
1114 Seaco Avenue, Deer Park TX 77536
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www. intertek-cb.com Q M '
m7
ITA-Ratcliff-000153
Intertek
Caleb Brett
Report of Analysis
2006-007065-DRPK
Sample ID: 2006-007065-DRPK-001 Sample Description : ID: GUANGXI 2A
Product: Powder
Method USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
*Absence of Asbestos A
* Microbial Contamination, Aerobic Bacteria
* Microbial Contamination, Fungi
Date Sampled: 09-18-2006 Date Received: 09-19-2006
Date Analyzed: 09-19-2006
Results <0.001 0.1 0.4 18.8
Negative 730 60
Units W t% W t% w t% w t%
cfu / g cfu / g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
REVIEWED
Initial: 10-31-06
`
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 5
ITA-Ratcliff-000154
Intertek
Caleb Brett
Report of Analysis
2006-007065-DRPK
Sample ID: 2006-007065-DRPK-002 Sample Description : ID: GUANGXI 2
Product: Powder
Method EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM 059 USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph
Identification A
Test
Identification B
Identification C
A cidity/ Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
* Microbial Contamination, Aerobic Bacteria
* Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled: 09-18-2006 Date Received: 09-19-2006
Date Analyzed: 09-19-2006
Results
Pass
Units
Pass
Pass
Pass <0.1
0.4 0.1 0.01 <0.001 18.8 4.9 840 50
W t% % % % % % %
cfu / g du / g
Pass
Pass 0.8 % <3 m g / k g <1 % <5 m g / k g
<0.1 % 4.9 %
<0.1 % 1.4 ppm (Wt)
Passes Test
Passes Test
Passes Test Passes Test
4.9 <0.1 0.01
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK C A H S m W T T CSflfNOi p ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES. I l L l V I C - V V i ^ L y
Initial: ft*' '----
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
JAN 2 6 2Q07
ITA-Ratcliff-000155
- >
Intertek
Caleb Brett
Report of Analysis
2006-007065-DRPK
Sample ID: 2006-007065-DRPK-002 Sample Description : ID: GUANGXI 2
Product: Powder
Method USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
* Absence of Asbestos A
* Microbial Contamination, Aerobic Bacteria
* Microbial Contamination, Fungi
Date Sampled: 09-18-2006 Date Received: 09-19-2006
Date Analyzed: 09-19-2006
Results <0.001 0.1 0.4 18.6
Negative 840 50
Units Wt% wt% w t% wt%
cfu / g cfu / g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. 1NTERTEK. CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
r eview ed
ITA-Ratcliff-000156
Rug 03 07 0 0 : 5 8 a
ITS CRLEB B R E T T B R P K
(
(. 7 1 3 J 8 4 4 - 3 3 3 0
P.4
Intertek Caleb Brett
1114 Seaco Avenue
Deer Park, TX 77536
Ph: (713) 844 3200
Fax; (713) 844-3330 HTxtA/'hi-'tri'/Tintrxtek.com
R eport of A nalysis
2007-001041-DRPK
Client: C o n tact; Client Reference No:
Lu m m C, Inc, Mt- Totin Poston M.V. EASTERN QUEEN
Date Requested: D ate received:
C o llected By:
02-08-2007 02-08-2007
Client
Client Sample Description I'D; TYP- Ouangxi 9.A 2/4/07
RESULTS;
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product Solid Sample, Powder
Sam ple ED 2007-001041-DRPK-001
r e v ie w e d
AUG 0 3 2M7
(
03-21-07
s t 1"" * '
Page 1 of 3 ITA-Ratcliff-000157
Hug 03 07 0 8 : 5 9 a
I T S COLEB BRETT - DRPK
(7 13 J 8 4 4 -3 3 3 0
P* 5
Intertek
Report of Analysis 2007-001041-DRPK
Sample ID : 2007-001041 -DRPK-00 )
Sample Description : lD: T-):T'
2A 2/4/07
Product: Solid Sample, Powder
M ethod EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph
Identification C Acidity / Alkalinity Water-soluble substances Aluminum Calcium Iron
EP 04/2005:0438 tale monograph Lead
EP 04/2005:0438 talc monograph EP 04/2005:0438 tale monograph * EP 04/2005:0438 talc monograph
- EP 04/2005:0438 talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph
Magnesium Loss on Ignition Microbial Contamination, Aerobic Bacteria Microbial Contamination, Fungi _____ Identification A Identification B Acid-soluble substances (as S4)
FCC V talc monograph FCC V talc monograph
Arsenic Free alkali (as NaOH)
FCC V talc monograph FCC V tale monograph FCC V talc monograph
Lead Loss on Drying Loss on Ignition
FCC V talc monograph HTM 059 USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph U SP 29 - talc monograph
Soluble salts Lead Identification A Identification B Identification C Acidity / Alkalinity
USP 29 - talc monograph 1JSP 29 - talc monograph USP 29 - talc monograph
Loss on Ignition Water-soluble substances Iron
r eview ed
NR?f 7
q M `.
Date Sampled: 02-08-2007
Date Received: 02-08-2007
Date Analyzed: 02-08-2007
Results
Pass
Units
Pass Pass
Pass <0, <0,1
O.l
<0,01
Wt % % % % ppm
19.0 5.2 510 10 Pass Pass 0.3 <3
<5 <0.1
5.2 <0,1
0.2 passes Test Passes Test Passes Test Passes Test
5.2 <0.1 <0.01
% efu / g efu/g
% mg/kg
% mg / kg
%
% ppm (Wt)
Wt % W t1 Wt %
Iurcrtek Caleb Di e 1114 Seaco Avenue, Deer Park TX 77536
Fh; (713) 844-3200, Fax: (713) 844-3330, Email;dptechctr@kltcrtek.com, WWW.intertck-cb.com
Page 2 of 3
ITA-Ratcliff-000158
Hug 03 07 0 0 : 5 9 a
I T S CFILEB BRETT DRPK
(7 13 J 044 -3330
p. 6
Intertek
Report of Analysis 2007-001041-DRPK
Samplo ID : 2007-001041-DRPK-001 Sample Description : ID: TYP- Ouu^ I 2A 2/4/07
Product: Solid Sample, Powdcr
Method USP 29 - talc monograph
Lead
Test
USP 29 - talc monograph
Calcium
USP 29 - talc monograph
Aluminum
USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph USP 29 - talc monograph t USP 29 - title monograph * USP 29 - talc monograph * USP 29 - talc monograph * USP 29 - talc monograph
Magnesium Absence of Asbestos A Aerobai M icrobial Counts - Topical '1'otal Molds & Yeast - Topical Acrobal Microbial Counts - Oral T otal M olds A. Y east - Oral Microbial Contamination, Aerobic Bacteria Microbial Contamination, Fungi
Date Sampled: 02-08-2007
Date Received: 02-08-2007
Date Analyzed: 02-08-2007
Results <0,001 0-1 <0 1
18.8 Tlcgativc
510 JO 510
10 510
10
Units W t% Wt % Wt % Wt %
efu / g efu / g efu / g efu / g efu / g efu / g
REVIEWED
AUG 0 3
QM--
Initial: 03-21-07
--
lnici tck Caleb Brett 1114 Seaco Avenue, Deer Park TX 77538
ph- (713) 844-3200, Fax; (713) 844-3330, Email:dptechctt#intertek com, www.iiitcrtek-cb.wm
Page 3 of 3
ITA-Ratcliff-000159
Intertek
Report of Analysis 2007-006529-BRPK
Client: Contact: Client Reference No:
Luzenac, Inc. Mr. John Poston M.V. MYKALI
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, TX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Date Requested: Date received: Collected By:
06-04-2007 06-04-2007 Client
Client Sample Description
ID: GUANGXI 2
ID: GUANGXI 2A
(
RESULTS:
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product
Powder Powder
Sample ID 2007-006529-DRPK-002 2007-006529-DRPK-003
REVIEWED
JUL 0 2 2007
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative of the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
(
06-28-07
Page 1 of 7 ITA-Ratcliff-000160
Intertek
Report of Analysis
in 7.niiii
pk
REVIEWED
JUL 0 2 2007
Initial: 06-28-07
-----
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 2 of 7
ITA-Ratcliff-000161
Intertek
Report of Analysis
Initial: 06-28-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 7
ITA-Ratcliff-000162
In te rte k
Report of Analysis
2007-006529-0R P K
m z v itz V V tU
JUL 02 2007
Sample ID : 2007-006529-DRPK-002 Sample Description : ID: GUANGXI2
Product: Powder
Method EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph * EP 04/2005:0438 talc monograph * EP 04/2005:0438 talc monograph * FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM 059 USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
N. Date Sampled: 06-01-2007
Date Received: 06-04-2007
Date Analyzed: 06-04-2007
Results
Pass
Units
Pass Pass
Pass <0.1
0.5 0.2 <0.01 <0.001 19.1 5.4 150 10
Wt% % % % % %
%
cfu / g cfu / g
Pass
Pass
0.1 %
<3 mg /k g
<1 %
<5 m g / k g
<0.1 %
5.4 %
0.1 % 0.2 ppm (Wt)
Passes Test
Passes Test
Passes Test
Passes Test 5.4
<0.1 <0.01
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 06-28-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 4 of 7
ITA-Ratcliff-000163
Intertek
Report of Analysis 2007-006529-BRPK
r eview ed
JULO
Q M '-
H
U
Sample ID : 2007-006529-DRPK-002 Sample Description : ID: GUANGXI 2
Product: Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph 11USP 30 - talc monograph * USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 06-01-2007 Date Received: 06-04-2007
Date Analyzed: 06-04-2007
Results <0.001 0.2 0.4 19.5
Negative 150 10 150 10 150 10
Units Wt% Wt% w t% w t%
cfu / g cfu / g cfu / g cfu / g cfu / g cfu/g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 06-28-07
-
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 5 of 7
ITA-Ratcliff-000164
Intertek
Report of Analysis 2007-006529-BRPK
REVIEWED
JUL 0 2 20JJ7
QM-
Sample ID : 2007-006529-DRPK-003 Sample Description : ID: GUANGXI2A
Product: Powder
Method EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph EP 04/2005:0438 talc monograph * EP 04/2005:0438 talc monograph * EP 04/2005:0438 talc monograph * FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM 059 USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled: 06-01-2007
Date Received 06-04-2007
Date Analyzed 06-04-2007
Results
Pass
Pass
Pass
Pass
<0.1
0.4
<0.1
<0.01
<0.001
18.9
5.3
80
<10
Pass
Pass
0.2
<3
<1
<5
0.1
5.3
0.1
0.2
Passes Test
Passes Test
Passes Test
Passes Test
5.3
<0.1
<0.01
Units
W t% % % % %
% %
cfu/g cfu / g
% mg /kg
% mg /kg
% % % ppm (Wt)
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 06-28-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 6 of 7
ITA-Ratcliff-000165
Intertek
Report of Analysis 2007-006529-BRPK
REVIEWED
JUL 0 2 2007
.....
Sample BD: 2007-006529-DRPK-003 Sample Description : ID: GUANGXI2A
Product: Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph *USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 06-01-2007 Date Received: 06-04-2007
Date Analyzed: 06-04-2007
Results <0.001 <0.1 0.3 19.4
Units W t% w t% w t% w t%
Negative 80
<10 80
<10 80
<10
cfu / g cfu / g cfu/g cfu / g cfu/g cfu / g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial:
/^ L
06-28-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 7 of 7
ITA-Ratcliff-000166
Report of Analysis 2007-012958-DRPK
Client: Contact: Client Reference No:
Luzenac, Inc. Mr. John Poston
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, XX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Date Requested: Date received: Collected By:
10-15-2007 10-15-2007 Client
Client Sample Description
ID: Guangxi 2 M.V. "Wina" ID: Guangxi 2 M.V. "Wina"-1
RESULTS:
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product
Powder Powder
Sample ID
2007-012958-DRPK-001 2007-012958-DRPK-002
Re v ie w e d
NOV 0 5 2007
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative of the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
V
11-05-07
Page 1 of 5 ITA-Ratcliff-000167
P 8
Intertek
Report of Analysis 2007-012958-BRPK
Sample ED: 2007-012958-DRPK-001 Sample Description : ID: Guangxi 2 M.V. "Wina"
Product: Powder
Method EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph Identification C
EP 04/2005:0438 talc monograph Acidity / Alkalinity
EP 04/2005:0438 talc monograph Water-soluble substances
EP 04/2005:0438 talc monograph Aluminum
EP 04/2005:0438 talc monograph Calcium
EP 04/2005:0438 talc monograph Iron
EP 04/2005:0438 talc monograph Lead
EP 04/2005:0438 talc monograph Magnesium
EP 04/2005:0438 talc monograph Loss on Ignition
EP 04/2005:0438 talc monograph Microbial Contamination, Aerobic Bacteria
EP 04/2005:0438 talc monograph Microbial Contamination, Fungi
FCC V talc monograph
Identification A
FCC V talc monograph
Identification B
FCC V talc monograph
Acid-soluble substances (as S04)
FCC V talc monograph
Arsenic
FCC V talc monograph
Free alkali (as NaOH)
FCC V talc monograph
Lead
FCC V talc monograph
Loss on Drying
FCC V talc monograph
Loss on Ignition
FCC V talc monograph
Soluble salts
HTM059
Lead
USP 30 - talc monograph
Identification A
USP 30 - talc monograph
Identification B
USP 30 - talc monograph
Identification C
USP 30 - talc monograph
Acidity / Alkalinity
USP 30 - talc monograph
Loss on Ignition
USP 30 - talc monograph
Water-soluble substances
USP 30 - talc monograph
Iron
Date Sampled: 10-12-2007 Date Received: 10-15-2007
Date Analyzed: 10-15-2007
Results Pass Pass Pass Pass <0.1 0.6 0.34 0.02 4 18.2 5.4 1010 10 Pass Pass 1.3 <3 <1 <5 <0.1 5.4 <0.1 2.47
Passes Test Passes Test Passes Test Passes Test
5.4 <0.1 0.02
Units
Wt% % % %
ppm % %
cfu / g cfu/g
% mg/kg
% mg/kg
% % % ppm (Wt)
W t% W t% W t%
Initial: 11-05-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 2 of 5
ITA-Ratcliff-000168
Intertek
k__________________ j
Report of Analysis 2007-012958-DRPK
Sample ID : 2007-012958-DRPK-001 Sample Description : ID: Guangxi 2 M.V. "Wina"
Product: Powder
Method USP 30 - talc monograph
Lead
Test
USP 30 - talc monograph
Calcium
USP 30 - talc monograph
Aluminum
USP 30 - talc monograph
Magnesium
USP 30 - talc monograph
Absence of Asbestos A
USP 30 - talc monograph
Aerobal Microbial Counts - Topical
USP 30 - talc monograph
Total Molds & Yeast - Topical
USP 30 - talc monograph________ Aerobal Microbial Counts - Oral
USP 30 - talc monograph
Total Molds & Yeast - Oral
USP 30 - talc monograph
Microbial Contamination, Aerobic Bacteria
USP 30 - talc monograph
Microbial Contamination, Fungi
Date Sampled: 10-12-2007 Date Received: 10-15-2007
Date Analyzed: 10-15-2007
Results <0.001 0.3 0.6 18.4
Units W t% W t% w t% Wt%
Negative 1010 10 1010 10 1010 10
cfu / g cfu / g cfu / g cfll/ g cfu/g cfu / g
Initial: 11-05-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 5
ITA-Ratcliff-000169
t
Intertek
Report of Analysis 2007-012958-BRPK
Sample ID : 2007-012958-DRPK-002 Sample Description : ID: Guangxi 2 M.V. "Wina"-1
Product: Powder
Method EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph Identification C
EP 04/2005:0438 talc monograph Acidity / Alkalinity
EP 04/2005:0438 talc monograph Water-soluble substances
EP 04/2005:0438 talc monograph Aluminum
EP 04/2005:0438 talc monograph Calcium
EP 04/2005:0438 talc monograph Iron
EP 04/2005:0438 talc monograph Lead
EP 04/2005:0438 talc monograph Magnesium
EP 04/2005:0438 talc monograph Loss on Ignition
EP 04/2005:0438 talc monograph Microbial Contamination, Aerobic Bacteria
EP 04/2005:0438 talc monograph Microbial Contamination, Fungi
FCC V talc monograph
Identification A
FCC V talc monograph
Identification B
FCC V talc monograph
Acid-soluble substances (as S04)
FCC V talc monograph
Arsenic
FCC V talc monograph
Free alkali (as NaOH)
FCC V talc monograph
Lead
FCC V talc monograph
Loss on Drying
FCC V talc monograph
Loss on Ignition
FCC V talc monograph
Soluble salts
HTM_059
Lead
USP 30 - talc monograph
Identification A
USP 30 - talc monograph
Identification B
USP 30 - talc monograph
Identification C
USP 30 - talc monograph
Acidity / Alkalinity
USP 30 - talc monograph
Loss on Ignition
USP 30 - talc monograph
Water-soluble substances
USP 30 - talc monograph
Iron
Date Sampled: 10-12-2007
Date Received : 10-15-2007
Date Analyzed: 10-15-2007
Results
Pass
Pass
Pass
Pass
<0.1
0.6
0.27
0.01
3.3
18.3
5.3
670
20
Pass
Pass
0.8
<3
<1
<5
<0.1
5.3
0.17
2.01
Passes Test
Passes Test
Passes Test
Passes Test
5.3
<0.1
0.01
Units
W t% % %
%
ppm % %
cfu / g cfu / g
% mg /kg
% mg/kg
% % % ppm (Wt)
W t% W t% W t%
Initial: 11-05-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, vvww.intertek-cb.com
Page 4 of 5
ITA-Ratcliff-000170
r J ' *
1
Intertek
^
Report of Analysis 2007-012958-DRPK
Sample ID : 2007-012958-DRPK-002 Sample Description : ID: Guangxi 2 M.V. "Wina"-1
Product: Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 10-12-2007 Date Received: i 0-15-2007
Date Analyzed: 10-15-2007
Results <0.001 0.3 0.6 18.6
Negative 670 20 670 20 670 20
Units W t% W t% w t% w t%
cfu / g cfu / g cfil / g cfu / g cfil / g cfu / g
Initial: pA s\--
11-05-07
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 5 of 5
ITA-Ratcliff-000171
Iritertek
Report of Analysis 2007-014287-BRPK
Client: Contact: Client Reference No:
Luzenac Mr. John Poston
Intertek Caleb Brett 1114 Seaco Avenue Deer Park TX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Date Requested: Date received: Collected By:
11-30-2007 11-30-2007 Client
Client Sample Description Guang Xi 2 11/23/07 MV Hellenic Sea
RESULTS:
SEE ATTACHED SHEETS
Product Powder
Sample ID 2007-014287-DRPK-001
Intertek Caleb Brett
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative of the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
01-03-08
Page 1 of 3 ITA-Ratcliff-000172
Intertek
Report of Analysis 2007-014287-DRPK
Sample ID : 2007-014287-DRPK-001 Sample Description : Guang Xi 2 11/23/07 MV Hellenic Sea
Product: Powder
Method EP 04/2005:0438 talc monograph Identification A
Test
EP 04/2005:0438 talc monograph Identification B
EP 04/2005:0438 talc monograph Identification C
EP 04/2005:0438 talc monograph Acidity / Alkalinity
EP 04/2005:0438 talc monograph Water-soluble substances
EP 04/2005:0438 talc monograph Aluminum
EP 04/2005:0438 talc monograph Calcium
EP 04/2005:0438 talc monograph Iron
EP 04/2005:0438 talc monograph Lead
EP 04/2005:0438 talc monograph Magnesium
EP 04/2005:0438 talc monograph Loss on Ignition
* EP 04/2005:0438 talc monograph Microbial Contamination, Aerobic Bacteria
* EP 04/2005:0438 talc monograph Microbial Contamination, Fungi
*FCC V talc monograph
Identification A
FCC V talc monograph
Identification B
FCC V talc monograph
Acid-soluble substances (as S04)
FCC V talc monograph
Arsenic
FCC V talc monograph
Free alkali (as NaOH)
FCC V talc monograph
Lead
FCC V talc monograph
Loss on Drying
FCC V talc monograph
Loss on Ignition
FCC V talc monograph
Soluble salts
HTM059
Lead
USP 30 - talc monograph
Identification A
USP 30 - talc monograph
Identification B
USP 30 - talc monograph
Identification C
USP 30 - talc monograph
Acidity / Alkalinity
USP 30 - talc monograph
Loss on Ignition
USP 30 - talc monograph
Water-soluble substances
USP 30 - talc monograph
Iron
Date Sampled:
Date Received: 11-30-2007
Date Analyzed: 12-14-2007
Results
Pass Pass Pass Pass <0.1
0.5 0.2 0.03
4 19.0 5.6 2210
10 Pass Pass
1.0 <3 <1 <5 <0.1 5.6 <0.1 <0.1 Pass Pass Pass Pass 5.6 <0.1 0.03
Units
W t% % % %
ppm % %
cfu / g cfu / g
% mg/kg
% mg/kg
%
% %
ppm (Wt)
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 01-03-08
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
ITA-Ratcliff-000173
4.
Intertek
Report of Analysis 2007-014287-BRPK
Sample ID : 2007-014287-DRPK-001 Sample Description : Guang Xi 2 11/23/07 MV Hellenic Sea
Product: Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph * USP 30 - talc monograph * USP 30 - talc monograph USP 30 - talc monograph ^ USP 30 - talc monograph * USP 30 - talc monograph USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: Date Recejve(j. 11-30-2007
Date Analyzed: 12-14-2007
Results <0.001 0.2 0.5 19.3
Negative 2210 10 2210 10 2210 10
Units W t% W t% w t% w t%
cfu / g cfu / g cfu / g cftl/ g cfu/g cfil / g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN INDEPENDENT LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
(
Initial: /'r ''- - ^
01-03-08
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 3
ITA-Ratcliff-000174
Intertek
Report of Analysis 2008-000710-DRPK
Client: Contact: Client Reference No:
Luzenac Mr. John Poston
Intertek Caleb Brett 1114 Seaco Avenue Deer Park, TX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Date Requested: Date received: Collected By:
01-15-2008 01-15-2008 Client
Client Sample Description ID: Ore Type: Guangxi 2A 1/15/08 (M.V. Iguana) 1/2008
Product Solid Sample, Powder
Sample ID 2008-000710-DRPK-001
REVIEWED
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative of the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
03-04-08
Page 1 of 3 ITA-Ratcliff-000175
Intertek
Report of Analysis 2008-000710-DRPK
Sample ID : 2008-000710-DRPK-001 Sample Description : ID: Ore Type: Guangxi 2A 1/15/08 (M.V. Iguana) 1/2008
Product: Solid Sample, Powder
Method EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph H TM 059 USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled 01-15-2008
Date Received 01-15-2008
Date Analyzed 01-15-2008
Results Passes Test Passes Test Passes Test Pass <0.1 0.4 0.22 0.01 0.6 18.3 5.3 1600 10 Pass Pass 1.5 <3 <1 <5 <0.1 5.3 0.2 0.76 Passes Test Passes Test Passes Test Passes Test 5.3 <0.1 0.01
Units
W t% % % % ppm % %
cfu / g du / g
% mg /k g
% mg /k g
% % % ppm (Wt)
W t% W t% W t%
REVIEWED
-MAR-9
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536
q >.,j
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, wrvw.intertek-cb.com
Page 2 of 3
ITA-Ratcliff-000176
Report of Analysis 2008-000710-DRPK
Sample ID : 2008-000710-DRPK-001 Sample Description : ID: Ore Type: Guangxi 2A 1/15/08 (M.V. Iguana) 1/2008
Product: Solid Sample, Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 01-15-2008 Date Received1 01-15-2008
Date Analyzed: 01-15-2008
Results <0.001 0.2 0.4 18.3
Negative 1600 10 1600 10 1600 10
Units W t% W t% w t% w t%
cfu/g cfu / g cfu/g cfu/g cfu/g cfu/g
REVIEWED
ITA-Ratcliff-000177
Intertek
Report of Analysis 2008-002747-BRPK
Client: Contact: Client Reference No:
Luzenac Mr. John Poston
Intertek Caleb Brett 1114 Seaco Avenue Deer Park. TX 77536 Ph: (713) 844 3200 Fax: (713) 844-3330 Email: dptechctr@intertek.com
Date Requested: Date received: Collected By:
02-27-2008 02-27-2008 Client
Client Sample Description
ID: Guangxi 2A 2/22/08 M.V. "Wina" ID: Guangxi 2 2/22/08 M.V. "Wina"
RESULTS:
SEE ATTACHED SHEETS
APPROVED BY:
Intertek Caleb Brett
Product
Solid Sample, Powder Solid Sample, Powder
Sample ID
2008-002747-DRPK-001 2008-002747-DRPK-002
REVIEWED
This report has been reviewed for accuracy, completeness, and comparison against specifications when available. The reported results are only representative of the samples submitted for testing. This report shall not be reproduced except in full without written approval of the laboratory.
(
03-24-08
Page 1 of 5 ITA-Ratcliff-000178
Intertek
Report of Analysis 2008-002747-DRPK
Sample ID : 2008-002747-DRPK-001 Sample Description : ID: Guangxi 2A 2/22/08 M.V. "Wina"
Product: Solid Sample, Powder
Method EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc *EP 01/2008:0438 talc *EP 01/2008:0438 talc *FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM_059 *USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled: 02-13-2008
Date Received: 02-27-2008
Date Analyzed: 02-27-2008
Results
Pass
Pass
Pass
Pass
<0.1
0.3
0.28
<0.01
1.0
18.7
5.4
730
60
Pass
Pass
0.6
<3
<1
<5
<0.1
5.4
<0.1
0.6
Passes Test
Passes Test
Passes Test
Passes Test
5.4
<0.1
<0.01
Units
Wt% % % %
ppm % %
cfu / g cfu/g
% mg/kg
% mg /kg
% % % ppm (Wt)
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN OUTSIDE LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 03-24-08
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 2 of 5
ITA-Ratcliff-000179
Intertek
Report of Analysis 2008-002747-BRPK
Sample ID : 2008-002747-DRPK-001 Sample Description : ID: Guangxi 2A 2/22/08 M.V. "Wina"
Product: Solid Sample, Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph *USP 30 - talc monograph *USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 02-13-2008 Date Recejved; 02-27-2008
Date Analyzed: 02-27-2008
Results <0.001 0.3 0.3 19.1
Negative 730 60 730 60 730 60
Units W t% w t% w t% w t%
cfu / g cfu / g cfu / g cfu / g cfu / g cfu/g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN OUTSIDE LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 03-24-08
-- - Intertek Caleb Brett
1114 Seaco Avenue, Deer Park TX 77536
Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 3 of 5
ITA-Ratcliff-000180
Intertek
Report of Analysis 2008-002747-BRPK
Sample ID : 2008-002747-DRPK-002 Sample Description : ID: Guangxi 2 2/22/08 M.V. "Wina"
Product: Solid Sample, Powder
Method EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc EP 01/2008:0438 talc *EP 01/2008:0438 talc *EP 01/2008:0438 talc *FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph FCC V talc monograph HTM_059 USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph
Identification A
Test
Identification B
Identification C
Acidity / Alkalinity
Water-soluble substances
Aluminum
Calcium
Iron
Lead
Magnesium
Loss on Ignition
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Identification A
Identification B
Acid-soluble substances (as S04)
Arsenic
Free alkali (as NaOH)
Lead
Loss on Drying
Loss on Ignition
Soluble salts
Lead
Identification A
Identification B
Identification C
Acidity / Alkalinity
Loss on Ignition
Water-soluble substances
Iron
Date Sampled: 02-13-2008 Date Recejved: 02-27-2008
Date Analyzed: 02-27-2008
Results Pass Pass Pass Pass <0.1 0.1 0.15
<0.01 1.1
18.6 5.1 160 40 Pass Pass 0.3 <3 <1 <5 <0.1 5.1 0.1 0.5 Passes Test Passes Test Passes Test Passes Test 5.1 <0.1 <0.01
Units
W t% % % %
ppm % %
cfu / g cfu / g
% mg /kg
% mg/kg
% %
%
ppm (Wt)
W t% W t% W t%
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN OUTSIDE LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 03-24-08
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
ITA-Ratcliff-000181
Intertek
Report of Analysis 2008-002747-BRPK
Sample ID : 2008-002747-DRPK-002 Sample Description : ID: Guangxi 2 2/22/08 M.V. "Wina"
Product: Solid Sample, Powder
Method USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph USP 30 - talc monograph *USP 30 - talc monograph *USP 30 - talc monograph
Lead
Test
Calcium
Aluminum
Magnesium
Absence of Asbestos A
Aerobal Microbial Counts - Topical
Total Molds & Yeast - Topical
Aerobal Microbial Counts - Oral
Total Molds & Yeast - Oral
Microbial Contamination, Aerobic Bacteria
Microbial Contamination, Fungi
Date Sampled: 02-13-2008 Date Received: 02-27-2008
Date Analyzed: 02-27-2008
Results <0.001 0.2 <0.1 18.3
Negative 160 40 160 40 160 40
Units W t% W t% w t% w t%
cfu / g cfu/g cfu / g cfu/g cfu/g cfu/g
THE ANALYSIS RESULTS DENOTED (*) WERE PERFORMED BY AN OUTSIDE LABORATORY. INTERTEK CALEB BRETT CANNOT ACCEPT LIABILITY FOR THE ACCURACY OF ANY RESULTS NOT PERFORMED BY ITS OWN LABORATORIES.
Initial: 03-24-08
Intertek Caleb Brett 1114 Seaco Avenue, Deer Park TX 77536 Ph: (713) 844-3200, Fax: (713) 844-3330, Email:dptechctr@intertek.com, www.intertek-cb.com
Page 5 of 5
ITA-Ratcliff-000182
Intertek
Job Reference:US785-0015015 Job Location:Deer Park, TX, USA
Client:Luzenac, Inc. Contact:John T. Poston Address:17509 Van Road
Houston, TX 77049 USA
Report of Analysis
Deer Park Technical Center Laboratory 1114 Seaco Avenue Deer Park, Texas 77536 USA Tel: (713)844-3200
Date Job Created:04-Sep-2008
Job Description:Analysis only of Talc, Submitted, 9/4/2008 at Deer Park, TX, USA, Deer Park.
Sample Summary
Ramnle Nnmher 2008-DRPK-004497-001
Date CnmnlpfpH 25-Sep-2008
npfsr.rintinn
ORE TYPE: GUANGXI #2 GRIND DATE 9/2/08 SHIP NAME: M.V. "SHI DAI#3' ARRIVAL: 05/2008
Page 1 of 3
REVIEWED
OCT 15 2(]08
QM:_
07-0ct-2008 12:58 PM US785-0015015
ITA-Ratcliff-000183
Intertek
Report of Analysis
Sample ID2008-DRPK-004497-001
Date Taken:04-September-2008
Drawn By:Client
Date Submitted:04-September-2008
Sample Designated Asrtalc
Date Tested:25-September-2008
Representing:ORE TYPE: GUANGXI #2 GRIND DATE 9/2/08 SHIP NAME: M.V. "SHI DAI#3' ARRIVAL: 05/2008
Method
USP 31- NF 26
".01
FCC V Talc ITM 1059
Test Result
USP 31 MONOGRAPHS Identification A
Pass
Identification B
Pass
Identification C
Pass
Microbial Limits, Topical - Total Aerobic Count
620
Microbial Limits, Topical-Total Mold and Yeast Count
10
Microbial Limits, Oral - Total Aerobic Count
620
Microbial Limits, Oral - Total Mold and Yeast Count
10
Acidity / Alkalinity
Pass
Loss on Ignition
5.1
Water Soluble Substances
< 0.1
Iron 0.01
Lead
< 0.001
Calcium
0.2
Aluminum
0.4
Absence of Asbestos - A
Negative
Magnesium
18.7
EP Talc Monograph Identification A
Pass
Identification B
Pass
Identification C
Pass
Acidity / Alkalinity
Pass
Water Soluble Substances
< 0.1
Aluminum
0.4
Calcium
0.19
Iron 0.01
Lead
0.3
Magnesium
18.7
Loss on Ignition
5.1
Microbial Limits, Topical - Aerobic Bacteria & Fungi Count
620
Microbial Limits, Oral - Total Aerobic Microbial Count
620
Microbial Limits, Oral - Total Fungi
10
FCC Talc Monograph Identification A
Pass
Identification B
Pass
Acid Soluble Substances
0.8
Arsenic (as As)
<3
Free Alkali
<1
Lead
<5
Loss on Drying
<0.1
Loss on Ignition
5.1
Soluble Salts
<0.1
Metals by Aqueous Matrix by ICP-AES
REVIEWED
Units
cfu/g cfu/g cfu/g cfu/g
% % % % % %
%
% % % % ppm % % cfu/g cfu/g cfu/g
% mg/kg % mg/kg % % %
Page 2 of 3
OCT 1 5 2008 nim- ^
07-0ct-2008 12:58 PM US785-0015015
ITA-Ratcliff-000184
Intrtek
Report of Analysis
Sample ID:2008-DRPK-004497-001
Date Taken:04-September-2008
Drawn By:Cllent
Date Submitted:04-September-2008
Sample Designated Asrtalc
Date Tested:25-September-2008
Representing:ORE TYPE: GUANGXI #2 GRIND DATE 9/2/08 SHIP NAME: M.V. "SHI DAI#3' ARRIVAL: 05/2008
Method
ITM 1059
Test
Metals by Aqueous Matrix by ICP-AES Lead
Result
0.182
Units
ppm Wt
o
Page 3 of 3
r eview ed
OCT1.5 2 P
07-0ct-2008 12:58 PM US785-0015015
ITA-Ratcliff-000185
Intertek
(
Report of Analysis
Deer Park Technical Center Laboratory 1114 Seaco Avenue Deer Park, Texas 77536 USA Tel: (713)844-3200
Job Reference:US785-0015243 Job Location:Deer Park, TX, USA
Date Job Created:01 -Oct-2008
Job Description:Analysis only of Talc, Submitted, October 1, 2008 at Deer Park, TX, USA.
Client:Luzenac, Inc.
Contact:John T. Poston
Address: 17509 Van Road Houston, TX 77049 United States of America
Sample Summary Sample Number______________________ Date Completed___________________ Description__________________
2008-DRPK-005257-002
15-Oct-2008
Guangxl 2 9/29/08 "Hellenic Sea"
(
Page 1 of 5
REVIEWED
06-NOV-2008 10:23 AM US785-0015243
ITA-Ratcliff-000186
Intertek
Report of Analysis
Page 2 of 5
06-Nov-2008 10:23 AM US785-0015243
ITA-Ratcliff-000187
06-NOV-2008 10:23 AM US785-0015243
ITA-Ratcliff-000188
Intertek
Report of Analysis
Sample ID:2008-DRPK-005257-002 Drawn By:Client Sample Designated AstTalc RepresentingiGuangxi 2 9/29/08 "Hellenic Sea"
Method
USP 31- NF 26
'.01
FCC V ITM 1059
Test
USP 31 MONOGRAPHS Identification A Identification B Identification C Microbial Limits, Topical - Total Aerobic Count Microbial Limits, Topical-Total Mold and Yeast Count Microbial Limits, Oral - Total Aerobic Count Microbial Limits, Oral - Total Mold and Yeast Count Acidity / Alkalinity Loss on Ignition Water Soluble Substances Iron Lead Calcium Aluminum Absence of Asbestos - A Magnesium
EP Talc Monograph Identification A Identification B Identification C Acidity / Alkalinity Water Soluble Substances Aluminum Calcium Iron Lead Magnesium Loss on Ignition Microbial Limits, Topical - Aerobic Bacteria & Fungi Count Microbial Limits, Oral - Total Aerobic Microbial Count Microbial Limits, Oral - Total Fungi
FCC Monograph Identification A Identification B Acid-Soluble Substances (as S04) Arsenic Free Alkali (as NaOH) Lead Loss on Drying Loss on Ignition Soluble Salts
Metals by Aqueous Matrix by ICP-AES
Page 4 of 5
Date Taken:01-October-2008 Date Submitted:01-0ctober-2008
Date Tested:15-0ctober-2008
Result
Pass Pass Pass 280 20 280 20 Pass 5.2 < 0.1 0.01 <0.001 0.2 0.4 Negative 18.6
Pass Pass Pass Pass < 0.1 0.4 0.18 0.01 3.3 18.7 5.2 280 280 20
Pass Pass 0.9 <3 <1 <5 < 0.1 5.2
< 0.1
Units
cfu/g cfu/g cfu/g cfu/g
% % % % % %
%
% %
%
% ppm % % cfu/g cfu/g cfu/g
% mg/kg % mg/kg % % %
06-NOV-2008 10:23 AM US785-0015243
ITA-Ratcliff-000189
Intertek
Report of Analysis
Sample ID:2008-DRPK-005257-002 Drawn ByiClient Sample Designated As:Talc Representing:Guangxi 2 9/29/08 "Hellenic Sea"
Method
ITM 1059
Test
Metals by Aqueous Matrix by ICP-AES Lead
--
Signed:
Date Taken:01-0ctober-2008 Date Submltted:01-October-2008
Date Tested:15-0ctober-2008
Result
0.800
Units
ppm Wt
(
Page 5 of 5
O6 -N0 V-2 0 O8 10:23 AM US785-0015243
ITA-Ratcliff-000190
(
(
Page 3 of 5 65464
reviewed
FEB 26 2009
QM:_
18-Feb-2009 4:22 PM US785-0016368
ITA-Ratcliff-000192
Report of Analysis
Sample ID:2009-DRPK-000398-002 Drawn By:Client Sample Designated Asrtalc Representing:Guangxi 2 1/9/9
Method
USP 31- NF 26
.01
FCC V ITM 1059
Test
USP 31 MONOGRAPHS Identification A Identification B Identification C Microbial Limits, Topical - Total Aerobic Count Microbial Limits, Topical-Total Mold and Yeast Count Microbial Limits, Oral - Total Aerobic Count Microbial Limits, Oral - Total Mold and Yeast Count Acidity / Alkalinity Loss on Ignition Water Soluble Substances Iron Lead Calcium Aluminum Absence of Asbestos - A Magnesium
EP Talc Monograph Identification A Identification B Identification C Acidity / Alkalinity Water Soluble Substances Aluminum Calcium Iron Lead Magnesium Loss on Ignition Microbial Limits, Topical - Aerobic Bacteria & Fungi Count Microbial Limits, Oral - Total Aerobic Microbial Count Microbial Limits, Oral - Total Fungi
FCC Monograph Identification A Identification B Acid-Soluble Substances (as S04) Arsenic Free Alkali (as NaOH) Lead Loss on Drying Loss on Ignition Soluble Salts
Metals by Aqueous Matrix by ICP-AES
Page 4 of 5 65464
Date Taken:09-January-2009 Date Submitted:09-January-2009
Date Tested:18-February-2009
Result
Units
Pass Pass Pass 3400 90 3400 90 Pass 5.4 < 0.1 0.02 < 0.001 0.3 0.6 Negative 19.2
cfu/g cfu/g cfu/g cfu/g
% % % % % %
%
Pass Pass Pass Pass < 0.1 0.6 0.30 0.02 4.3 19.2 5.4 3490 3400 90
% % % % ppm % % cfu/g cfu/g cfu/g
Pass Pass 0.3 <3 <1 <5 0.2 5.4 < 0.1
% mg/kg % mg/kg % % %
REVIEWED
Qivi:
18-Feb-2009 4:22 PM US785-0016368
Intertek
Report of Analysis
Sample ID2009-DRPK-000398-002 Drawn By:Client Sample Designated As.talc Representing:Guangxi 2 1/9/9
Method
ITM 1059
Test
Metals by Aqueous Matrix by ICP-AES Lead.
Signed:
'' ^
___ % A K & J J L l x ________
InteVtek
^^
Date Taken:09-January-2009 Date Submltted:09-January-2009
Date Tested:18-February-2009
Result
1.99
Units
ppm Wt
Date
j '1
Page 5 of 5 65464
reviewed
FEB2620j)9^
18-Feb-2009 4:22 PM US785-0016368
ITA-Ratcliff-000194
Intertek
Report of Analysis
Deer Park Technical Center Laboratory
1114 Seaco Avenue Deer Park, Texas 77536 USA Tel: (713)844-3200
Job Reference: US785-0019508 Job Location: Deer Park, TX, USA
Client: Luzenac, Inc.
Contact: John T. Poston Address:17509 Van Road
Houston, TX 77049 United States of America
Sample Summary
Sample Number_________________________ Date Completed
2009-DRPK-011976-001
22-Oct-2009
Date Job Created: 08-0ct-2009 Job Description: Analysis only of TALC at Deer Park, TX, USA on 8 October, 2009
Customer Reference:
Description_____________ GUANGXI 2 10/06/2009
jfeiuuJ Ooif^
(
Page 1 of 3 1go186
02-Nov-2009 9:37 AM US785-0019508
ITA-Ratcliff-000195
Intertek
Report of Analysis
Sample ID: 2009-DRPK-011976-001 oample Designated As: talc
Vessel/Location: DCS Representing: GUANGXI 2 10/06/2009
Method ITM 1059 EP 6.01
USP 31- NF 26
FCC VI (
Test Metals by Aqueous Matrix by ICP-AES
Lead EP Talc Monograph
Identification A Identification B Identification C Acidity / Alkalinity Water Soluble Substances Aluminum Calcium Iron Lead Magnesium Loss on Ignition Microbial Limits, Topical - Aerobic Bacteria &Fungi Count Microbial Limits, Oral - Total Aerobic Microbial Count Microbial Limits, Oral - Total Fungi USP 31 MONOGRAPHS Identification A Identification B Identification C Microbial Limits, Topical - Total Aerobic Count Microbial Limits, Topical-Total Mold and Yeast Count Microbial Limits, Oral - Total Aerobic Count Microbial Limits, Oral - Total Mold and Yeast Count Acidity / Alkalinity Loss on Ignition Water Soluble Substances Iron Lead Calcium Aluminum Absence of Asbestos - A Magnesium FCC Monograph Identification - XRD Identification - IR Arsenic Lead Acid- Soluble Substances (as Sulfates) Free Alkali (as NaOH) Loss on Drying Loss on Ignition Soluble Salts
Date Taken:08-0ctober-2009 Date Submitted08-0ctober-2009
Date Tested 22-October-2009 Drawn ByClient
Result
Units
<1.00
ppm Wt
Pass Pass Pass Pass < 0.1 0.6 0.17 0.02 1.2 18.9 5.7 160 150 10
% % % % ppm % % cfu/g cfu/g cfu/g
Pass Pass Pass 150 10 150 10 Pass 5.7 <0.1 0.02 1.240 0.2 0.6 Negative 18.9
cfu/g cfu/g cfu/g cfu/g
% % % % % %
%
Pass Pass <3 <5 1.6 < 1.0 0.3 5.7 0.2
mg/kg mg/kg % % % % %
Page 2 of 3 190186
02-Nov-2009 9:37 AM US785-0019508
ITA-Ratcliff-000196
Iritertek
Signed:
I
Report of Analysis
Iritertek __^J
MDate: I
Page 3 of 3 190186
02-NOV-2009 9:37 AM US785-0019508
ITA-Ratcliff-000197