Document 1QvEvjM5zVb494wjnj3O9999j
EG 01
---------------------
CODE YE-698-D
< DATE )
L2H32 5527* LBS*
("l o t )
< EST WT )
*-y, /
PROCESSES
CZ/r ( ) YE-698-D <T)
dSBfc
FWP 10/15/82*'
/* COMTYP JOB NAME : 01YE698DMT
BLENDED BACK; CG 1, PQ 98,___ (CODE)
(LOT)
(POUNDS)
EQUIP MENT PREP
1
351 2
NAME: MOLYBDATE ORANGE
i USE I
1 ACCT
|I LBS
N-CODE 1 LBS
| j ,|
4***JZ&fAIN SODIUM SULFATE FOR S-13
|1 84
1 08-A 1 84
2^T CALCULATE 6 SET ON BADGER METER FQ,
16
' I iNITRIC ACID WEAK)
fiYPjX.
!J^_!
33-D
|3T>er
3^TJ3BJAIN SODIUM CHLORIDE FOR S-33
1 734 1 4-A 1 734
4-^^TAIN . SODA ASH FOR S-37
1 146 1 3-A 1 146
FHJ3BTAIN SODIUM SILICATE FOR S-39
1 237 I 32-D 1 237
*H>6BTAIN SODA ASH FDR S-43
1 350 |
|OBT0JM-ANTI MON Y TRIOXIDE FOR S-46
1 70
1----- ------------------------ --------------------------------------------------------
-\
WEIGH SODIUM CHROMATE INTO V-351* ^
i Hill i
3-A 711-B
10-D
t 350 i 70
1 1885
QPTR______ MK^Zf, <?L1%
OPTR_____, MK , _______V.
359 WEIGH IN SODIUM MOLYBDATE. SOLUTLON 3 OPTR._____ , MK _&/, -OPTR _____, MK _, T-_____ , _.__!L%
303
3SR RUN 10* (50 G) WATER INTO V-358
IKti V-359 INTO V-351 6 PUMPKIN, V-351
l^rT-ADJ to 55* (2600 G>
13-t'SlFTIN N-10S-A FROM
STIR 5 MIN & RECORD:! PH/L<,,I_C9^0"IO*0)
1>-r ADJ TO PH 9 *8-9 *9 6 RECORD: jAjLlJj!
I (CAUSTIC SODA SOLUTIONT-------
i:z::ASSUME 50%
ASSUME 66% ___j Lj
7-D 33-D
: ADD N-33-D FROM S 2 USING BADGER METER
ADJ TO 66* (3U21 G) AT 67-69*F
>' RECORD; VOl JIJL* A __JyL*f
\W \ STIR 5 MIN 6. RECORD: PH^l#(7.4-7*6) 6
I G/ML
*080-1 *083)
i NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
i LIST 6 ATTACH, TAKE 1 QT SAMPLE
sv I RUN 20* (996 G) WATER INTO V~_J*// 5 | RECORD N-41-D STORAGE TANK TO PUMP FROM*
CIRCLE ONE: 402 41 411 42 424 425
CHECK WITH CU SUPV:
^STORAGE TANK MUST CONTAIN AT LEAST 2376
mv$ 1982
I GAL: 402=49*, 410=25*, 411=48*, 420=25*,
| 424=25*, 425=31*
i ^STORAGE TANK MUST HAVE STIRRED AT LEAST
I 20 MIN SINCE LAST ADDITION OR ADJUSTMENT
i ^STORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLETE,
\
SET METER FOR 30 G 6 PUMP TO SV
LOT: * EQUIP
MENT I
COMTYP JOB NAME: 01YE698DMT PAGE 02
DATE PRINTED:10/15/82 I USE | N~ |AOUT
lr
I LBS | CODE | LBS
SV 01 5
CONT
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY, 'RECORD BELOW* IF NOT IN RANGE, STOP PUMPING & SEE SUPV.
I I
* PH:,______(2*2-3*?)
* DENSITY: _________ G/ML (1*270-1*323) 23 IF S-22 OK & WHEN S-21 COMPLETE, RECORD
DENSITY ______ G/ML ON TRAPPED SAMPLE
FROM END OF S-21 PUMPING.
24 USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW* NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21*
CIRCLE DENSITY & SETTING IN TABLE BELOW*
**#* TABLE ##**
I - **** *** **** #M*
__ __i
G/ML SETTING I G/ML SETTING f G/ML SETTING|
1 1*270 1678 | 1 .291 1534 | 1 .312 1410 |
1 1 * 271 1670 I 1 .292 1527 i 1 .313 1404 |
1 1 * 272 1663 | 1 *293 1521
| 1 *314 1399 |
1 *273 1656 | 1 *294 1515 | 1 -315 1394 |
i 1 *274 1649 | 1 *295 1509 | 1 .316 1388 1
i 1 *275 1641 | 1*293 1503 1 1 -317 1383 |
i 1*276 1634 | 1.297 1497 | 1 -318 1378 |
1 .277 162? | 1.298 1490 1 1 .319 1372 1
i 1 *278 1620 | 1 *299 . 1484 | 1 -320 1367 1
1*279 1614 | 1.300 1478 | 1 .321 1362 |
i 1 * 280 1607 | 1 .301 1473 | 1 *322 1357 |
i 1 .281 1600 | 1 *302 1467 1 1 *323 1351 |
i 1 *282 1593 | 1 *303 1461
1 1 *324 1346 |
i 1 *283 1586 1 1 .304 1455 f 1 * 325 1341 |
i 1*284 1580 | 1 *305 1449 | 1 * 326 1336 |
i 1.285 1573 i 1.306 1444 | 1 *327 1331 1
! 1 *286 1566 f 1 *307 1438 | 1 *328 1326 |
1 1 .286 1566 | 1 ,307 1438 | 1*328 1326 |
i 1*287 1559 | 1 -308 1432 1 1 * 329 1543 |
i 1.288 1553 1 1 *309 1427 1 1 *330 1537 1
i 1 * 289 1546 | 1 *310 1421
| 1 *331
1532 |
1.290 1540 |.
| 1 *31 1
1415
| 1.332
1526 l
251 SET METER & PUMP
G (RECORD FROM TABLE)
|
1 FLUSH 1LINE WITH WATER INTO SV FOR APPROXIMATELY 1
30 SECONDS
.2.
26| ADJ LEAD NITRATE TO 76* (3625 G) AT 67-69#F.
i |
I RECORD :___
*F
27| STIR 5 MIN & RECORD PH: ___ _ (2. 2-3*7)
1 1
28| IF NECESSARY ADJ TO PH 3.0-3*1
ASSUME 66X1.
1 6 RECORD PH: _
ASSUME 50% |.
NOTE: ;DILUTE N-7 --D~7 0:1 WITH WATER BEFORE ADDING!
29| RECORD :___ ____ G/ML (1 . 143-1.144) IF OUT OF SPEC I
i FILL OUT CHECK LIST & ATTACH*
1
30I STIR AT 67-69*F FOR S-31- TAKE 1 QT SAMPLE-
1
I
I I I I 1- 1 i1 11 l1 1! 11 1i 1 1 11 11 [1 11 11 11 11 1i i i 1i 1i i "1 i i i 1i 1i \ 1 41 -D i 1 57-A i 1i 33-D i 7-D i |i 1i 1 ,i i
V K.
DUP050059661
.; v',\ .*?>'
*v **pmr.v
4t*i II
COHTYP ; JOB NAMEsJOl Y69I)MT/ PACE 02 . DATE PRINT!ED: 11/02/82
- 1>*- ,.
* | USc.
N- ia c c t ;
... ........... ....
:tr'.--v-'HiS-'S-. | |.ft
CODE | LBS .
APPROXp^0^WH3I2EtoNWUTWGto ;?PUMP :;
i
01 CHECK PHVa DENSITY.^ RECORD %EDtol7 IF NOT .
'i :-'? It- : PH^TO^a^i; r"" ,^lilgir
-
IS"- I -* DENSITY;
23-rTF S-22|OK; *t n **-------------- --
^ 1 ' DENSITYfi|fe2S?G/ML?
'R0M.%END0B^21 vPUHPI^C^^^^^^fe^
USING DENSITY; PR0H :S~23^feNB^TE^ SETTING FOR
3i, I SECOND DUMPING IN TABEE>EOOW2!^NOTE5*TABLE'
ACCOUNTS FOR *30 G AllREADY^UHPED IN 5-21. CIRCLE DENSITY 4 SETXING|INSrABLE BELOW*
' ***# TABLE
........| J
. ' . '-y..^ -r.-y-''
'
-4;*. -V^V -rirSF.'' .
J.
G/ML SETTING
G/HL; , SETTING | G/HL SETTING|
1 ..270 4644Ss. 1.. 291?$sS?T504!;fj!i;,.l, 1.312 1382 |
1.271 : 1 637*> 1 '.292i^'4.8?Jfev-4 1.313 1376 |
a; 1.272 1630 - 1.293 !^m9i
1.314 1371 |
T 1.273 1623
1.294 *1485
1 .274 1616-' 1.295*f.&*14?9
1.315 1367 | 1.316 1361 |
1.275 1609 1 I 1.276 1602
1.277 1595
1 .278 1588
1.296^J473 T^97J^H467,
1^2981^1461 1 .299 >f1455'
1 .317 1356 1.318 1351
1.319 ,1345 1.320 S f340
I |
I
1.279 1582 . .I l.i`300
...... 1.321.^/1335
1.280 1575 I 1.301
-1 .322 ,v'y ~.1330
1.281 1568 r | 1 w302
<1 '.l/l'
%
1.282 1 .283'5"
;415556S5Mi*i J
1.303
rJ324| OK' ' " -gjftr,,.,........
...................
1.284 , 1549$S/J -1^3051
1 .285 'T542^|T 1
141i<^^plp274;w1305 ';: |
l < .284 ;,:.53S35^I > 1 .287 1528^-1 1.308^^404^^1-4^329,xg4295
1.288 1522:. :. | 1.39:^3395ji,,-I 1.330^51290
1.289 1515 | 1..310:Sai393t^
I
1 l 1.290 1510 I 1.311 1387- I 1.332 1280 I
-r l .:3$r:*~\ I *88W:4 ''
. -v
s*t,'Tg*y.` ' * , i' < -
|25r^tT METER 6 PUMP /J/2?_G <RECORD FROM TABLE)
I
I | FLUSH LINE WITH WATER INTO SVFOR APPROXIMATELY |
I | 30 SECONDS
I
I2ATADJ LEAD NITRATE TO 3625G=JLZ6*-242/245 6 74.5* I
I | -247) AT 67-69*F
>v
I
I /RECORD: __k____ *F & /CE CONSUMED\ (3304/BLOCK) I330X__
|27T STIR 5 MIN * RECORD RH: UjJt- <2.i-3.7)
|
| | **** USE TITRIMETERTQADJUSTJ^4l-D PH ****
I^
J28T EF NECESSARY ADJ TO PH 3t 0"*3T1
ASSUME 66% I__ *Z,~.
1 | 6 RECORD PH:
ASSUME 50% |______
| | NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING|
I 29t RECQRD : MJMrl G/ML (1.143-1.144) IF OUT OF SPECI
| | /FILL OUT CHECK LIST & ATTACH.
I
I30<STIR AT 67-69*F FOR S-31 . TAKE 1 QT SAMPLE.
I
41-D | 51 10 I
57-A l____ I
1/ 33-D |_i_.
7-D 1_._.
i
DUP050059662
LOT: Louie' MENT I
SV
CONT
COMTYP JOB NAME: 01YE698DMT PAGE 03
DATE PRINTED:10/J5/82 USE N- ACCT LBS CODE LBS
** **
* *
(-- *-- --<m wa. m ~~ <f* ~~ mm mm MM M-- MM mm .<
OBTAIN 1 QT SAMPLES OF S-18 & S-30 SOLUTIONS
6 TITRATE TWICE
NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
7,1-7,4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL
EQUIPMENT 6 REPEAT TITRATIONS). DO NOT
PROCEED IF N-IO-D TITRATION IS OUT OF RANGE
ADJUST V-358 FOR A TITRATION PH OF a. 10 TO 2.201
FROM. FINAL IN-LINE TITRAOON, RECORD LOWEST
PH JrJjtJk 6 ML N-10-D__
sen WHEN S-31 TITRATION OK , STRIKE V-358 THRU
SV BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
6
16-18 MIN
, onA
j f>
RECORD: START J/JsirjtlQ, TOTAL MIN_,,t_OL___
NOTE*. STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
33^ 6 BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
FOR 15 MINUTES 3/f^l DURING S 33, WASH IN V-,358
3S^i STIR 2 MIN 6 RECORD PH_jfe_:_V(1 .8-2.5)
I PBXS,__ibr:_(MUST BE + ) y^c STIR TOTAL OF 15 MIN .FROM S-33 6
RECORD: TEMP__/jLF (67-73F)
DUMP N-3-A FROM S-4
3<>' STIR 3 MIN 3?V> POUR IN N-32-D FROM S-5
STIR 2 MIN
RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN & FLUSH ALUM LINE WITH WATER
4 DUMP IN N-3 FROM S-6
4 STIR 4 MIN FOR S-48
734
115-D
367
390 7
1RUN IN HYDROCHLORIC ACID USING WEIGHT 6 FLOW
| i CONTROL PANEL
MK
mk i___________ ;____%
I DURING S-44 SIFT N-711-B FROM S-7 INTO V-390
I^-^WITH AGITATOR ON IN 1-2 MIN
47^rsrTIR 1-2 MIN TO MILKY SOLUTION
28-D 28-D
105
SV ygr\ WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
8 ! SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV
I WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES,
DUMP IN BLANC FIXE N
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP'OF PAGE 1 -
__
RECORD: CODE
LOT
___ *=
51, r" STIR 20 MIN ^ 4
> RECORD: PH_,,A.-:--Z<5.8-6.0)
33''] IF NECESSARY, ADJ TO PH 5,8-6.0
ASSUME 50%
6 RECORD: PH-____________
ASSUME 66%
FLOOD TO 153" (7298 G) 6 STOP AGITATOR
* START,
,OPTR
.
330W] 128- 330
7 33 -D
DUP050059663