Document 1QNBLJyJaZRyx4QjD1Q27JDod
PPG Industries, Inc. Chemicals P.O. Box 1000 Lake Charles, Louisiana 70602
Bill PMTtf Manager Laboratory Services/Environmental
February 15, 1989
U. s. Environmental Protection Agency Water Management Division Enforcement Branch (6WE) Allied Bank Tower at Fountain Place 1445 Ross Avenue Dallas, TX 75202-2733 Dear Sir:
Attached is the DMR for January, 1989,and attachments explaining five daily maximum excursions for copper, monthly average excursions for copper and solids, a daily maximum excursion for mercury, and a pH excursion. The agency was notified by phone of each of the copper and mercury daily maximum excursions as required by our permit. Also attached is an explanation for lack of BOD data at Outfall 201. If you have any questions concerning this report, please contact Mark W. Wood at 318-491-4450. Pocnor't fill 1 \7
I Manager, Laboratory Services/
Environmental Control WJP/MWW/VC Attachments
SL 24507
ATTACHMENT I EXPLANATION OF EXCURSIONS
DATE
OUTFALL PARAMETER LIMIT
1/3/89
201
Cu 49.3 lb/day 24 hr/comp
1/5/89 1/9/89 1/17/89 1/22/89
49.3 49.3 49.3 49.3
lb/day lb/day lb/day lb/day
EXCURSION
EXPLANATION
+94 lb/day
Upset conditions. Newly completed control equipment not performing according to design levels.
+ 16.1 + 18.3 + 35.7 + 2.5
lb/day lb/day lb/day lb/day
Same as above Same as above Same as above Same as above
January, 201 1989
Cu 18.2 lb/day + 68.6 lb/day The copper control
Mo. Avg.
system (alkaline
precipitation) did
not perform as
effectively as lab
scale design tests. The problem appeared to be that some of the copper is in a soluble
complexed form. Lab tests, however, indicated the addition of a
more powerful complexing agent, resulting in an insoluble copper
complex would solve the problem. Continuous addition of this
reagent began 1/23/89, and has thus far successfully controlled
copper discharge from the system.
1/9/89
101
Hg 0.30 lb/day +0.21 lb/day The Chlorinated
24 hr Comp
Condensate Tank
level filled up and
backflowed through
the main chlorine
header of the
Mercury Circuit
Chlorine Unit.
This allowed the condensate (Hg contaminated) to flow with the
header seal water to the untreated but monitored Mercury Trace
Sewer. This chlorinated condensate is normally recycled but
transfer back to the system or overflow to treatment was inhibited
due to blockage of the level control valve, transfer pump, and the
tank overflow.
SL 024508
DATE
OUTFALL PARAMETER LIMIT
EXCURSION
EXPLANATION
1/22/89 001
pH, Cont.
6-9(60 min)
70 min.
Chlorination of cooling water resulted in th pH falling slightly below pH 6.
A contributing factor was the lack of river water buffering capacity (typical in January and February).
January, 201
TSS, 4270 lb/day +319 lb/day A Settling tank in
1989
Mo. avg.
the Silicas
Production Unit
experienced two
major mechanical
failures resulting
in the overloading
of solids control
filter units. Both
mechanical problems were repaired, additional quantities and types of settling aid wer
added, and extra round-the-clock operator coverage was provided the
last half of January. The solids control system is now performing
satisfactorily and TSS discharges are within permitted levels.
SL 024509
ATTACHMENT II BOD DETERMINATION The dechlorination of the remaining chlorinated streams comprising Outfall 201 (begun in mid-December, 1988) operated successfully in January, 1989. The presence of the dechlorination agent (sodium thiosulfate) has, however, made BOD determinations impossible. No valid data were collected from any of the five attempts to measure BOD on this Outfall.
SL 024510
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MO
DAY
01 01
PERIOD
YEAR
MO
1W ol
OAY :!
i--a
o
CO
RntMgncd omb^Bmcmum ApprowMapirca 12-31-87
I'Li ifl I It
PARAMETER
(J Cmrd Only) QUANTITY OR LOAOINQ
(46-JJ)
{14-61}
AVERAGE
MAXIMUM
UNITS
(4 Card Only) 06-41)
MINIMUM
QUALITY OR CONCENTRATION
(46-11)
(H-61)
AVERAGE
MAXIMUM
UNITS
NO. FREQUENCY OF
ANALYSIS
162-&S
BAMPLC TYPS
(6fl70>
ID, 5-L>AL Li Dt G. C) >3 Ju 2 0 fit LIFN F HC T
1 1DH, TUIAI IFNDED FL'-fi 2 U FI Ml NT NFT
1 A Dill! OA1IIF
1 AD i M UAI 1 IF
IAMPLI MEABUREHCMT
psWr j MAlBMiilBMF
ll ': y'
SAMPLE MEASUREMENT
mffSuLt
*
74
iAiLV AO 4588
4270 nATI V AO
* * X P -A * *
12<38
#***,
DAtLV MX LBS/D'
' .. '
7879
******
11465
******
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THREE- canP2j
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50
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2A42
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WEEK THREE- q^I WEEK
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2 0 Li
14
0. 0 REPORT
0.0 REPORT
***** *
******
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NA THREE- nnMP24
WEEK THREE-
l 1 IF WT NF T UAI 1 IF
hATl V AO DAILY MX LBS/DV
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WEEK
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14.4
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^-*ynLL_ Report
REPORT
******
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******
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**** *** *
THREE; C0MP2-1 WEEK
OROE f'HANE
SAMPLE MEASUREMENT
0. 0
0.2
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E/TITLE PRINCIPAL EXECUTIVE OFFICER
I CtRIlTY UNOCR PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE MFORMATlON SUBMITTED HEREIN ANO BASED
I . G. DROWN
ON MY momAY OF THOSE INCPVIOUALS IMMEDIATELY RESPONSIBLE FOR OBTAININC THt INFORMATION i BCOCVE IMC SUBMITCO INFORMATION
WORLD MANAbl R
S TRUE ACCURATE AND COMF1 ETC I AM AWAAC THAT THEBE ABC SK> NIFiCAMT FCNALTCS FOB SUBMITTING FALSE INFOBMATlQN WtCLUOING
The FOS&I0H.ITV OF FN( ANO *MPfflSt>NMCNT SEE l| USC 3 MX)I ANO 33 USC t 1319 /frnaitte* under theme ((**' ms* tnriitde fine* up tu
IIGNATURC O* PRINCIPAL EXECUTIVE
TYPED OR PRINTED
trtd ltt meatmum tmpntitnmrut uf htUteen InninMa end i \e*m /
OFFICER QR AUTHORIZED AGENT
NA
* x *-k x *x *
Tl[LCPHONK
318 491 - 4501
bm NUMBER
THREE- COMP2I
WEEK THREE, CQMP21
WEEK..
DATE
i/y
y
YEAR
MO
DAY
(ENT ANO EXPLANATION OF ANY VIOLATION* (Reference all uttuihments here)
' ii; L A [ I, iCHNI- N1 FOR' C /LLAMAT I UN OF t ,;U IRS 10N
T*N0 DATA AVAILABLE (SEE ATTACHMENT)
SL 024516 33?01 fRsv 1 0-791 PREVIOUS EDITION TO BE U0CO
< REPLACES ERA
T*44l WHICH HAY MOT BE USCD.1
PAftr
nr
RMITTEE NAME/ADDRESS tlacludr jfi/j Namt /Lotauon tiffddiiGStmrtru)
Si.
DRESS p. XIROX 1000______________
____L&LE
_/o0'2.
;ility CATION
NATIONAL POLLUTANT DISCHAJtM ALIM I NATION SYSTEM \NPOti)
DISCHARGE MOTORING REPORT limit)
_______L_JHL_
(JM|
17
L A000076i
:-oi a
-
PERMIT NUMACR
DISCHARGE NUMBER
PPG
PI HOI CANA)
Fora MMpved 1
OMB^P>4(K04
ApprovKipires 12-31-87
PLoNl' [J
MONITORING
YEAR MO DAY
190*? ui
ul
PERIOD
YEAR
MO
19BS i 11
DAY
si
PARAMETER <JM7>
0 Card Only) QUANTITY OR LOADING
(46-JJ)
04-61)
AVERAGE
MAXIMUM
UNITS
(F Card Only) <--)
MINIMUM
QUALITY OR CONCENTRATION
(XX-JJ)
04-61)
AVERAGE
MAXIMUM
UNITS
NO. FARHEOAoULrIVNiClfV ATMYPPELC
[XI-XJ {64-6$)
(69-JO)
} 1 IYL ENE CHI OR IDE
4 2S 2 0 0 FLUENT MET VALUE
IAMPLC MEASUREMENT .jgggk
0.0
Report DAILY av
0. 2
IHHHHHF
REPORT
******
DAILY MX LBS/D>i
,
****** ******
****** ******
**** **x *
NA THREE; C0MP2'
WEEK WEEK COMP 2-
3'
fRACHI .ORDE 7HVLENE
AMPLE
MEASUREMENT
0. 4
2,5
XXXX XX
X *****
******
NA THREE; C0Mc,2^ WEEK
4 7l> 2 0 0
LLiUTI.-NLI VALUE__
1, 01 CHI. OROE THAME
AMPLE
MEASUREMENT
Report DAILY AV
0.0
REPORT
#*##*#
DAILY MX LBS/D'i
0. 1
xxxxx#
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WEIlK COMPS-
WEEK. 1 NA THREE; C0MP2-
WEEK.
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0. 0
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WEEK
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-F^WWgjMEASSAUMRPELMEENT
REPORT DAILY AV
0. 1
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tEEPORT
3AILY AV
0.2
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******
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0,4
XXXX XX
REPORT
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DA<LY MX LBS/DV
0. 7
******
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xxxxx* ****** ******
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NA THREE; COMP 2WEEK WEEK . C0MP2-
NA THREE COMP 2WEEK
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DICHI QROETHANE
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MEASUREMENT
REPORT DAILY AV
1.3
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3. 2
X xxxx x
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THREE .COl-ir'2' WEEK NA THREE COMP 2- , WEEK
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PERMIT
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REPORT * REPORT
******
DAILY .AY. ..DAILY-MX LBS/DV
******
******
C/TITLE PRINCIPAL EXECUTIVE OFFICER
I . G - DROWN
i CIKTSV UNDER PENALTY OF LAW THAT i NAVE PERSONALLY CJtAMlNED
orANO AM FAMILIAR WITH THE INFORMATION SUBMlTTEO HEREIN AMO BASED
on mv inouirv
those individuals immediately responsible for
OBTAINING the INFORMATION I BCUCVC THE SUBMITTED INFORMATION
t i-t
iniu\. G NANAfiLh1
S TRUE ACCURATE AND COMPLETE I AM AWARE THAT THERE ARE S*G MFC ANT PENAL TWS FOR SUBMITTING FALSE INFORMATION INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT SEC 10 US C I IOOI AND
33 U&C I 1310 ifrMftiri undrt ihtmr jktiiMtPi mi* tneiudr /inn up in 1/iHMi
SIGNATURE OF PRINCIPAL EXECUTIVE
TYPED OR PRINTED
9nd nr fuiimam
nf ftrlufrn | munthn mnd i ink t
OFFICER OR AUTHORIZED AGENT
ENT ANO EXPLANATION OF ANY VIOLATIONS iKrfrrrncr all ulluthmrnls hfrrj
XXXX X X X* 1
TELEPHONE
THREE C0MP2' 1 WEEK
DATE
SIB 4V1 -45U<
,7-
MCA
foot.
NUMBER
YEAR
MO
DAY
SL 024517
m 3320-1 (Rv. 10-79) PREVIOUS edition to re used
(REPLACES EPA FORM T-4 WHICH MAY NOT BE USED.)
PAGE
OP
`IMITTEE NAMC/ADORESI (Include ilit} Warn* /Location r/^crrnf) Mf_______EOjLII^L
NATIONAL POLLUTANT D l*C H AltOX ELIMINATION SYSTEM (tVflJEi)
DISCHARGE MOJ^pRING REPORT (DM*)
tJ-l 6)
02-19)
F
sw._L_ jj
iiOX
_____________________________________________________
LA00O07M
2u i a
______ Li^-E
,_LFu.
______________
PERMIT NUMBER
OISCHANGE NUNBCR
PPG
I ! I I. U
LANhL
PlnNE
Form t
OMB1
I
;<MTY NATION
MONITORING
YEAR
MO
DAY
PNOM tw; 01
01
TO
PERIOD
YEAR
MO
iw: oi
DAY 31--
MOTE: B--d InsIrucUons bstor* comptoting this form.
PARAMETER 0217)
O Cwd Only) (44-55)
QUANTITY OR LOADINQ (5441)
AVERAGE
MAXIMUM
UNITS
(4 Card Only) (54-45)
MINIMUM
(RANGDICHLGROVLLNE
546 2 0 0 F LULU I. UE.1 value:
NVL CHLORIDE
175 2 0 o
AMPLE MEASUREMENT
Mm
Hf j
MEASUREMENT
0. 5 liT 0.0
RERDRT -MlLY MX LBS/
* * K** *
******
#**
******
ELUfcMl. MEL.ttflLUE OW, IN CONDUIT OR F<U I REAT MEN 1 PE AN' ULo 2 0 0
SAMPLE MEASUREMENT
10. 40 lPORT
15.48
****** ******
FLUENT NET VALUE
LOR INC TOTAL
>1D( ial
SAMPLE MEASUREMENT
>00 2 u 1 AUMIt'
LLiLNX NEE VALUE 1 (JR 1 NA I ED HYDROvDONS, GENERAL
SAMPLE MEASUREMENT
552 2 Ft l ADM IF
i nr-kit mft vai hf
l CHI ORtlETHE HE
SAMPLE MEASUREMENT
?0< t
2 (i
i)
1 1 Oil. UE LVALUE
jgQDfl AVS
22 9 DAILY.
f8' DAILY AV
0. 1
REPORT DAILYAV
4
5*7.7
DAILY MX l7
0.3
REPORT -DAILY MX
dIL *** * * *
****** LBS/BY ******
****** BS/OY ******
******
BS/EY
QUALITY OR CONCENTRATION
(44-55)
(54-41)
AVERAGE
MAXIMUM
k-d ** M *
** ****
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***** ******
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UNITS
IHHH
X * ** ****
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****
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**** *** X
*** k *** #
IRCOUCNCY OF
ANALYSIS
(4J-4JJ (44-44)
SAMPLE TYPE
(49-70)
NA THREE C0MP2^ WEEK
THREEifaOMr?'
WEEK
NA THREE / COMP- 2* WEEK
threei Gamp WEEK 1,4
NA CONTI RCORDf NUQUS
CONTJ
nupus u THREE GRAB
WEEK THREE4 GR
WEEK o THREE\ COMP 2
WEEK THREE COI
WEEK
NA THREE COMP 2
WEEK THREEt <?QnP& WEEK
SAMPLE MEASUREMENT
C/TITLE PRINCIPAL EXECUTIVE OPPICCR
T. G. DROWN WllRl G MANAGER
TYPED OR PRINTED
i CERTIFY UNOCK PENALTY OF LAN THAT I HAVE PERSONALLY EAAMINCD ANO AM FAMILIAR WITH THE INFORMATION SUBMITTED HERON ANO BASED
ON MY INQUIRY OF THOSE INOlVlOUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION I BELIEVE THE SUBMITTEO INFORMATION IS TRUE ACCURATE ANQ COMPLETE `i AM AWARE THAT THERE ARC SlG
NfFlCANT PENALTIES FOR SUBMITTING FALSE INFORMATION INCLUDING THE POSSlBMlTY OF FINE ANO IMPRISONMENT SEE 16 U SC * KXH ANO )3uSC i 1H9 iprnaltte* under theme atatutrm mm* include fine* up u* flit taut and <i* ma iinuin tmprtmttnmml ttf hr tween E miuith* and i \ear* t
1ENT AND EXPLANATION OP ANY VIOLATIONS <*r/rr.nr all ull< trolrnf ( hrrr)
b-VM -
T:lephone
310 491 450(.
SIGNATURE OP PRINCIPAL EXECUTIVE
OFFICER OR AUTHORIZED AGENT
mm
NUMBER
DAT*
n
2-
YEAR
MO
(H DAY
SL 024518
*mn.i to
in 7Qi PPtvrnii* rnirtoN to be utto
ihtnachi tPA mom* tod which may not be used.)
page:
of *
1WM1TTEE NAME/AODRUt {Include
stilly Name / Location / different)
Mi___ EEXi-IlM_______________________
drc F. Q. eoTX 10 n 0________________________
______ Lil _L:aAJj'LF-S.^U^ J70hQ2_
NATIONAL POLLUTANT DISCHARE KLIM I NATION SYSTEM {\PDf.S)
OISCHAR K MOTORING REPORT (MfX)
_____________________________________________________________ (17-/9)
F INfu.
L. A0000761
401 A
PERMIT NUMKER
DISCHARGE NUMBER
S1LIC A f' I CiMEH 13
iexplres 12-31-67 DITCH
Sit lo
cation
TQM B.
BROWN,
PARAMETER (-i7)
OW, IN CONDUIT OR RU TREATMENT (LAN 05u 2 0 u FT IJENT NET VALUE
1 URINATED MYDRORLCINS , UENLRAL 052 2 O (i FI ill-NT NET PALI IF
MONITORING PERIOD
YEAR
MO
DAY
FROM iw; Hi
ul
YEAR
MO
DAY
TO iw; U1
i-i
dQRKS
MANAGER (J Card Only) (46-33)
QUANTITY Oil LOADING
AVERAGE
MAXIMUM
UNITE
AMPLE MEASUREMENT
1*****
*
AMPLE MEASUREMENT
(#****
1.7-7.
REPORT DAILY MX MOD
* *****
****** ****
(4 Card Only)
OM)
MINIMUM
******
******
******
******
<2*29) IJO-ip
NOTE: Rd instructions blor complKtlnfl CM* form.
QUALITY OR CONCENTRATION
(46-33)
(34-61)
AVERAGE
ihhuhi#
MAXIMUM
******
UNITE
FREQUENCY
or
ANALTlIf
AMPLE TYPE
[62-63) (64-68)
{69-701
NA THREE /|EST IMf
****** ******
******
41 O
* ** x
X** H
WEEK
THREE/ pEsTIFi? WEEK
NA THREE/(GRK~
******
IREPQRT
* * **
WEEK
THREE4 GRAB
***#
DAILY MX IJB/L
WEEK
AMRLE MEASUREMENT
AMPLE MEASUREMENT
AMPLE
AMPLE MCASURCMENT
SL 024519
AMPLE MEASUREMENT
/TITLE PRINCIPAL EXECUTIVE OFFICER
I.b. BROWN WORTS MANAGER
TYPED OR PRINTED
1 CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SURMlTTEO HEREIN ANO RASED QN MY INQUIRY OF THOSE NOVDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION I BEUEVC THE SUBMITTED INFORMATION IS TRUE ACCURATE ANO COMPLETE I AM AWARE THAT THERE ARE SK* MFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT SEE 10 USC I IOOI ANO 33 U$C I 1310 iPmutUn under thtwe W*lNlra me* include ftnr* up u* tfumut and tt* naiiinitn ifflprtin*ptii *tf /YftifPit | muniL and i >pii* i
ENT ANO EXPLANATION OP ANY VIOLATIONS (.Rtftrrnrt ull ultmhmemt herr)
TELEPHONE
DATE
3IB 491- 4500
SIGNATURE OF PRINCIPAL EXECUTIVE OFFICER OR AUTHORIZED AGENT
AMCA COM.
NUMSCR
YEAR
I'f
DAY
(PLACES KPA POPS* T-40 WHICH MAY NOT BE USED )
PAGE
OP
fMirrtC NAME/AODACtC iinctud< ith hom*/i.acatum tj dtfftrtnt)
41____
iserej^__u_1
.
_____L^IJ: j:iiAlSL_Lft^. 706OI
NATIONAL. POLLUTANT OIHARQI ELIMINATION STSTEM \.NPUKS)
DISCHARGE MO^MPRING REPORT {OMR)
U 16)
LA000076 l'w"
PERMIT NUMBER
3u a A
DISCHARGE NUMBER
PPG
f- I MAI.. CANAL
PL I
Fora Ajscpved < OMB)|^B4(H)0(M ApproraHpJre* 12-31-87
B 2nd flush
iLiur___________________________
AT ION
Mil G- DROWN. iQEL
PARAMETER
H, IN CONIjU 1 T QF< cu i reatmoj r pi. an i5u 2 0 0
RLUFNT HE.T VALUE. ORINATED HYDRO(BUNG, GENERAL >52 2 u o ~l I lf-~N T MET CAL IIP
IAMPU MEAIUMMKNT
RAM RLE MEASUREMENT
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<*W
AVERAGE
******
*###*
.U*f*c*fr*lH*H*t. ******
M `
MONITORING PERIOD
YEAR MO
DAY
FROM 1909 01
01
YEAR MO DAY
iw; 01
31
NOTE: Hssd Instructions bttora i
Bit* I
QUANTITY OR LOADING
i34*n
MAXIMUM
UNIT*
B. 64
(I Card Ortfy) (iWJ)
MINIMUM
******
QUALITY OR CONCENTRATION
(-)
(3*61)
AVERAGE X X ** * X
MAXIMUM
X *****
UNITS
FREQUENCY OF
NAUtt6
624J) <6F-6>
NA
SAMPLE TYPE
(69-70>
RERORT
DAILY MX mu
******
******
******
******
X X *** *
72231}
# #** ****
DAILY INSTAH DAILY imjw
NA
*ih|**#
**** ******
***
******
REPORT
DAILY .t
DAILY DAILY.
SAMPLE MCAIDKMINT
SAMPLE MEASUREMENT
SAMPLE MEASUREMENT
SAMPLE
measurement
SAMPLE MEASUREMENT
C/TITLE PRINCIPAL EXECUTIVE OFFICER
T.G. BFvOWN WORKS MANAGER
TYPED OR PRINTED
I CERTIFY UNDER PENALTY OP LAW THAT t HAVE PERSONALLY EXAMINED
AND AM FAMILIAR WITH THE REFORMATION SUBMITTED HEREIN AND BASED
ON MY INQUIRY OF THOSE INOVOUALS IMMEDIATELY RESPONSIBLE FOR
OBTAINING THE INFORMATION I BELIEVE THE SUBMITTED INFORMATION
4& TRUE ACCURATE AMO COMPLETE *1 AM AWARE THAT THERE ARC SC
MFCANT PENAL T<S FOR SUBMITTING FALSE INFORMATION INCLUDING
the POSSMAiTV OF fine ANO IMPRISONMENT SEC IS USC ft lOOt AND )3 USC I IT IS ffrMfliM tutd+r tke*r limtutn m*v mriudr finr* up U* IlffMfi
ftjtrf r
imp^wMiNruf *4 ArCu-rFu ^ H9ti*l*R ntf 3 >**r t
ENT ANO EXPLANATION OF ANV VIOLATIONS IRrlmncr alt ullachmrnll hrrr)
TllLEPHONE
DATE
318 491 -450t. R
SIGNATURE OF PRINCIPAL EXECUTIVE OFFICER OR AUTHORIZED AO ENT
All(A
CODE
NUMRER
YEAR
>
MO
DAY
3320-1 (Rbv. 10-79) previous edition to re used
I REPLACE
T-AO WHICH HAY NOT RE USED.)
PAGE
OF