Document 1Q0My0dYnEkeXd5MoR8JMDZmZ
BIODEGRADATION TEST SUBSTANCE Identity: PtoerafsluPoFrDoSde,caFnCe-s1u2l0f,onoarte3,MaSmammopnlieuJm29s0al5t-;1m.a(y1-aDlescoabneesurelffeornriecd acid, 1,1,2,2.33,4,4,5,56,6,7,7.8,89,9,1010,10-
heneicosafluoro-, ammonium salt, CAS # 67906-42-7)
Rbcueetlmyllaorscokellsvl:eosaTonelsdvte3s(7aa.pm5pp%rloewxaiitmsearat)e.mliyxAlt2lu5rve%alotufeeststherseutpbeossrtttasenudcbers,etla3ant7ec.et5oi%nthbwiuasttymelirxtaunrde.
No calculations were made to adjust for the actual concentrationofthe fest substance in the test sample. Test sample was from 3M production lot 164.
METHOD
MTyepteh:odA:erEoPbiAc405.1 GLP: No Year completed: 1991 CIonnotcaulcutmt:ime:So2u0rdcaeyosf inoculum not recorded RESULTS
5-day carbonaceous BOD: 67,000 mgkg
10-day carbonaceous BOD: 600,000 mg/kg
2c0o-pd:ay carbonace1o,0u0s0B,0O0D0:m7g2k0g,000 mg/kg fRallelumobraiirondkaetsge:rdamdoaiTtehitioysn.mianCtdueirrcriaeatnletdhkiannsotwahilspeesdrtgfuleduyoorfisitnhaleitkesedelymcdohiueemetitysotarrnieeddsuacstunigoognne-softsthtehat non-fluorinated moiety, butyl cellosolve. Testing was conducted on the "as-sold" mixture of the subject material in waantderno(t~d2ir5e%ctsluybtjoectthemastuebrjiealc)t. maTtehreiavla.lues reported apply to that mixture CONCLUSIONS Tbhiiosdetgesrtaidnegdiinndiaceartoebditcheatnvtihreobnumteynltcselclaopsaolbvleeomfoiseutpypoisrtliiknegly to be
000112
cbiooudledgbraedfaotiuonnd.thTahtiwsosutluddyalclaonwnfootr rbuiloedoeugtratdhaetipoosnsiobfiltihtey ftlhuatorcoocnhdeimtiicoanls ecvoemnptounaellnyt,benoernrciocuhleddittehaxtclcuodueldthmeetpaobsosliibcialltlyytahlatteratmhiiscrcohoemrigcaanli.sm could
Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY
Reliability: Kiimisch ranking 2. This documentation, characterizationofthe
study lacks sufficient test substance purity,
and
taneasltyetdi,catlhembeiaosduergeramdeanttioonfotfestthceosnoclevnetnrtatcioounlsd. nBotecbaeudsieffaermeinxtitautreedwfarosm
biodegradation of the fluorochemical component.
REFERENCES
Study conducted Minneapolis, MN,
at the request Lab Request
of 3M Company by Pace number J2905, 12/4/91
Incorporated
of
OTHER
Last changed: 5/18/00
000113
05/15/2000
EANRVCIHRIOVNEMDENTFAILNALLABROERPOARTTORY
1
RLAEBQUERSEQTUOERSTNAMNEO:. JS2A9B0/K5PC DPERPOAJRETCMTENNTO:: 90957305012900 DATE RECEIVED: 10/24/1991 DESC: ECOTOX SCREEN - FC-120
CONTRACT EXP COMP
DLAATBE(:S):01P/A2C4E/1992
DATE COMPLETED: 12/05/1991
PPRHOOJNEECTNO:LEAD:
3M FAX NO: 651-778-6176
DO NOT REFRIGERATE SAMPLES
TEST BY WEIGHT - NOT VOLUME
SAMPLE DATE CODE
DESCRIPTION RESULT
MOL or (95% C.I.)
1 10/10/91 FC-120
LoT-164
PACE PACE
CC--BBOODD--1005
**BBOODD--1005 ((CCAARRBBOONNAACCEEOOUUSS))
66070000000MGM/GK/KGG
6000 8000
PACE C-BOD-20 PACE COD-RFX
*BOD-20 (CARBONACEOUS) "COD (DICHROMATE REFLUX)
720000 MG/KG 1000000 MG/KG
6000 50
* = CONTRACT LAB DATA
000114
fp : CA ce--
REPORT OF LABORATORY ANALYSIS
oxcemer 0, 191
PDsx,p
a TR 2
WSB eH. Eonvdieri oncsheentt]al Laboratory
Socm,u
"
Sa Bldg. 2-3-09 ssi
RE: PClAiCeEntproRjeefcetrentoc.e: 93121900259.526
dear Hr. Schell
SEenckloovseerd.251,s t1h9e91,report of laboratory analyses for samples received
tIof tyoountahcatveusany questions concerning this report, please feel free
sin"ce7rely, ~
CPS rioajei ca.t AMarannaagter( DundllTM
i
Enclosures
FrE Tr ionnre
0011s
erie
midll EiiTie
pE SRe5 mRe.
mm
mS
P Q Ps eo
REPORT OF LABORATORY ANALYSIS
39345EnBvuisrhonAmveenntuael Laboratory BStl.dg.Pau2l-,36M-N09 55133
Attn: Mr. Wade Schell
Client Reference: 32905
PDAaCtEe SCaomlplleecteNdu:mber:
DCaltieentRecSeaimvpelde 10:
Barameter
inlts
INORGANIC ANALYSIS
I34NDCIhVeInDlUcAaLl POAxRyAgMeETnERDSemand Method 410 mg/kg BBiloocchheennilccaall OOxcyyggeenn DDeemmaanndd,, CCaarrbb 0150 DDaayy mngg//kkgg Biochenical Oxygen Demand, Carb 20 Day ng/kg
DPAeCcEembPerroje04c,t 1N9u9m1ber: 911029526
B1y0 0C3l8t6e5n0t2 MOL 2109/0259-/191 METHODDATEANALWED 6S0O00 617000000000 EEPPAA 441005..11 1111//0173//9911 66000000 670200000000 EEPPAA 440055.111 1111//1133//9911
MOL Method Detection Limit These data have been reviewed and are approved for release.
SItnaorrlgaaniEcngeCrhemistry Manager
TREE Ski tn
R HEaE
foinrrtarteans
he
000116
orbe ios o APemPsoemeotn
oat .
PACE, INC.
.
2)
Be Sitiged oie
~ EEN Les
1-02] a-sc| o> zon
2
ne
[90fled 1 |
we| aot eors | lie7s [E5T5HJ TY eJIb om|u200s 1|
i
(aad) lose] 1s bolLedn] aor
.
&
To
|
[oo] 22 beela]--plu-- isa|l--7s15-- a||
| rare
Cs 1 ot Jok[sool]--ur|
| |za3ean olnebo
RNS
|
IR
ereescso
I Lio]aavsale]p aLaa a= lo ||
3 | 530/
[oa] a2] pots Looe | 5333
on
san
[orbeled ie [ca |-- |
|
| eer Te bela]
RN 5
[p|l9e61 edeLasLJsLsal 201 |
on
wan | [5]wh I
1b poo | [ep phaentee Lb--
> Jo)" |1 | Do p [65ke absd at n[232]e rpc|
ml | hese JJoga TT
D1 = INITIAL DO Dz = FINAL DOF = _ 2 goreseen vo, 2:08
SEED CONTROL (50) = SEED CONTROL DO DFO: x F 0.48
i
e001?
5 DAY BOD, BOD-0S,
'
`SE CSReOBLboUooBNnLAaECcEEsBaoOsDn,Ss S3BBO0ooL5bb-B153O.60D.bBavavs, CCcOooCgoeRnr
ATE AnALYzED N_I3FlouT 185-91
ErE eEnEa!over p =-- ANALYZED BY,
INCUBATOR #_|
[ovJevcmlwreevosSinusitrs|comemrelpsf M ers]a "ao Jouloe|] 5] 5a-]sc| c "eea cieo e|
| A Hel Phra wor |[200 is[1ol|
\
SH
[20] 32fssfaall 1 [3]w1.5c2
[oo | rage (ss) Joldast aT
|| Jraneo Cond
Q
zo [odlola] medui]
gt |ue0 7 ea Jalal7 [| 3307|
sn | |] bases | Jos]3s]bal bb _
fier | feelwofla 1 1
|
6, co0| [Flsomy mead [221292 ishiel 59 Jug | S73 |
we [3
I fos fon polls fore Tazet |
aw ||| aeLdaLepubie onde
ol cor| =ebb TF
| & oF| [hme] Lbo olal T tT s1
l wo
ol [ale fold ug fos | coor |
aad) bad | os fealelan J]
ox [lasfoe
JuleT ] T} |
39 aoe | [= Folme pd TT
|
ee posse La f jo al s buogl e135s 22| |
wm) thos | Josliof fod| er]lia| |
oe ESSERE |
DI = INITIAL DO D2 = FINAL DOF =
SAMPLE IE Wr *o>
seo c: onto csc) + 55D cone 30 07" x F072
000115.
|
S pay BOD, BOD-OS_______
DATE ANALYZED IN_|I-13-9ouT 2-3-9}
I -- Tocor ee1bb SAMPLE [RESULTS UNITS[lcomMENTS{IPH|(mdf
02]
A
o
"UOLURE
| S#0ENof fered 5peg 22020 Fo E21o I fe|n ie|
SN
es EN
08)49 007) 1g [[18721f9Ae0m8ml0e|G[[EooaoEadp4fbJu5s: 2lo1-- ll]fiaoct [dooenenc|
w | oLtet] [ ladbe llon[l cF oT|
6Al gn?)of [bo|mer]e [fassoilae fbeailnT 5 fon |T seas||
: | Lore||[[5pDoandeTod[dseoona| ravos||
Ap| #51
[A;merfo L leo bebdITe1 ab fen1fo ran]
Le wor | fPezedooepfoblT ] LoT l
58o7ro] [cr2eel|f[ePiPoetfaobl eTe fLoe [7.62|
I ao ||] 2 Poel osbdo]
DT = INITIAL DO DZ =FINAL DOF = _2- SAMPLE SEED VOL. = a2
.
wb
--
000119
