Document 1KmKL0N5D7Z3EDjR68v4mKkd

EG** 01 CODE YE-698-D L2H12 < LOT ) si PROCESSED < ) YE-698-D <T> APPROVEI FUP 10/15/82 5527* LBS. ( EST WT ) COMTYP JOB NAME: 01YE698DMT BLENDED BACK: CG 01, EQUIP | -MENT i NAME: MOLYBDATE ORANGE 1 USE 1 LBS I N-CODE ACCT LBS PREP 1 351 359 3 'I TAIN SODIUM SULFATE FOR S-13 i I CALCULATE 6 SET ON BADGER METER FOR S-16 NITRIC ACID WEAK) % OBTAIN SODIUM CHLORIDE FOR S-33 L OBTAIN. SODA ASH FOR 5-37 \ OBTAIN SODIUM SILICATE FOR S-39 I OBTAIN SODA ASH FOR S-43 \/r\ OBTAIN ANTIMONY TRIOXIDE FOR S~46 1 84 1 !_S5__ 1 1 734 1 1 146 1 1 237 1 1 350 1 j 7 I WEIGH SODIUM CHROMATE INTCL V-351 . OPTR 3%, MK ZOo OPTR AsL, MK___ . i ., I I WEIGH IN SODIUM MOLYBDATE SOLUTION OPTR. 4?, MK Ll L, 1-3&Q, \~9M 1 OPTR &M-, MK T-_____ , ______ %i 108-A 33-D 4-A 3-A 32-D 3-A 711-B 10-D 423-D 84 60 734 146 237 356 70 1885 303 358 4 SV 5 10* (500 G) WATER INTO V-358 | !4>^pRtW V-359 INTO V-351 & PUMP IN V-351 I TO 55* <2600 G) I |4^UiFT IN N-108-A FROM S 1 _ . | M<j_|JIR 5 MIN & RECORD: PH__'_>L_<910. 0) | ADJ TO PH 9 - 8-9 - 9 t, RECORD: |^ < CAUSTIC SODA SOLUTION) ASSUME 50% |____ ASSUME 66%I_______ H> N-33-D FROM S 2USING BADGERMETER | ADJ TO 66* <31.21 G) AT 67-69*F } . RECORD: VDL_4it* & _Jl. I iiS^TSTlR 5 MIN 6 .RECORD :PHj|5r<7.4"?.6> & | } 1 G/ML Jj.OljLi'i .080-1 .083) I I ! NOTE IF'g /ML OUT OF LIMITS FILL OUT CHECK | I i LIST & ATTACH. TAKE 1 QT SAMPLE | w RUN 20" <996 G) WATER INTO I . 7-.D 33-D || I I1 |j I1 I2T I RECORD N-41-D STORAGE TANK TO PUMP FROM, v.CIRCLE ONE: 402 410 411 420 424 425 CHECK WITH CU SUPV: ^STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402-49*, 410=25*, 411=48*, 420=25*, <224=25425=31 * ^TOftAerTANK MUST HAVE STIRRED AT LEAST 2 MIN SINCE LAST ADDITION OR ADJUSTMENT Jt-STORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FDR THIS BATCH IS COMPLETf SET METER FOR 300 G 6 PUMP TO SV MOV 2 1982 t W3T ----___ EQUIP | MEN!| | CQHT'YP JOB NAME : 01 YE693DMT PAGE 02 DATE PRINTEDr10/13/82 < USE N- IACCT LBS CODE | LBS SV 122 5I CONT | 23 24 AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH $, DENSITY* RECORD BELOW. IF NOT IN RANGE, STOP PUMPING 4, SEE SUPV. * PH:_____ (2*2-3.7) * DENSITY: _________ G/ML <1.270-1.328) IF S-22 OK & WHEN S-21 COMPLETE, RECORD DENSITY ______k_ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING. USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 . CIRCLE DENSITY & SETTING IN TABLE BELOW. TABLE WKjftt G/ML 1 .270 1 .271 1.272 1 .273 1 .274 1 .275 1 .276 1 .277 1 .278 1.279 1.280 1.281 1.282 1 .283 1.284 1 .285 1.286 1 .286 1.287 1 .288 1.289 1 .290 SETTING ! G/ML SETTING 1 G/ML 1678 1 1.291 1534 1 1.312 1670 1 1.292 1527 1 1.313 1663 1 1.293 1521 I 1.314 1656 1 1.294 1515 i 1.315 1649 I 1.295 1509 1 1.316 1641 1 1.296 1503 1 1.317 1634 1 1.297 1497 1 1.318 1627 1 1.298 1490 1 1.319 1620 1 1.299 . 1484 1 1.320 1614 1 1.300 1473 l 1.321 1607 I 1.301 1473 1 1.322 1600 1 1.302 1 467 1 1.323 1593 I 1.303 1461 1 1.324 1586 1 1.304 1455 1 1.325 1580 1 1.305 1 449 1 1.326 1573 I 1.306 1444 1 1.327 1566 f 1.307 1438 1 1.328 1566 1 1.307 1 438 1 1.328 1559 1 1.308 1432 I 1.329 1553 I 1.309 1427 1 1.330 1546 I 1.310 1 421 1 1.331 1540 1 1.311 1415 } 1.332 SETTING 1410 1404 1399 1394 1388 1383 1378 1372 1367 1362 1357 1351 1346 1341 1336 1 331 1326 1326 1543 1537 1532 1526 25 1261 I 271 1281 II II I29| II 1301 SET METER 6 PUMP _______G (RECORD FROM TABLE) FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS ADJ LEAD NITRATE TO 76" (3625 G) AT 67-69*F. RECORD: ______ ___*F STIR 5 MIN 6 RECORD PH: _____ <2.2-3.7) IF NECESSARY A0J TO PH 3.0-3.1 ASSUME 66%I 6 RECORD PH : _____ . ASSUME 50%|Z_ NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING RECORD: ______ G/ML (1.143-1.144) IF OUT OF SPEC FILL OUT CHECK LIST & ATTACH. STIR AT 67-69*F FOR S-31 . TAKE 1 QT SAMPLE. 41-D | 5110 57-A | 33-D 7-D r DUP050059951 COMTYP JOB NAME: 01YE698DMT PAGE 02 DfrMRim^nm2 I LBS | CODE | LBS AT APPROX 100. G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY * RECORD BELOW. IF NOT IN RANGE, .'STOP PUMPING * SEE SUF'V. * PH:3a-<2.2-3.7) 'ISTTY: ^6j ^(Q/_ G/ML 270-1.328) IF S-22 OK & WHEN 5-21 COMPLETE, RECORD DEj*ITY liCU~ C/ML ON TRAPPED SAMPLE OM END OF 5-21 PUMPING. USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS .FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY 6 SETTING IN TABLE BELOW. **** TABLE k *k * I I 1 G/ML SETTING 1 G/ML SETTING 1 G/ML SETTING 1 i 1.270 1644 1 1 .291 1504 1 1.312 1 382 ! 1 1,271 1637 1 1.292 1487 1 1.313 1376 i 11.272 1630 1 1 .293 1491 1 1.314 1371 1.. i 1.273 1623 1 1.294 1485 1 1.315 1 367 |. j 1,274 1616 1 1 .295 1479 1 1,316 1361 i [ 1.275 1609 I 1. .296 1473 1 1.317 1356 1 I 1.276 1602 1 1 .297 1 467 1 1,318 1351 1 1 1.277 1595 1 1 .298 1461- 1 1.319 1 345 1 1 1.278 1588 1 1.299 1455 i 1.320 1340 I 1 1.279 1582 1 _144&` 1 1.321 1335 i 1 1.280 1575 id .301 1 444V' ' 1 1.322 1330 1 J 1.281 1568 1 1 .302 1438' 1 1,323 1324 1 1 1.282 1562 1 1 .303 1432 1 1.324 1319 111.283 1555 1 1.304 1426 1 1.325 1315 1 1 1.284 1549 1 1.305 1420 1 1.326 1310 ! 11.285 1542 1 1 .306 1416 1 1.327 1305 I | 1.286 1535 1 1 ..307 1410 1 1,328 1 300 1 1 1.287 1528 i 1 .308 1404 1 1.329 1 295 1 1 1.288 1522 1 1 .309 1399 1 1.330 1 290 1 11.289 1515 1 1 .310 1393 1 1,331 1285 1 1 1.290 1510 1 1 .31 1 1387 1 1.332 1280 I .SET METER & PUMP /&QO& (RECORD FROM TABLE) | I ! FLUSH- LINE WITH WATER INTO SV FOR APPROXIMATELY | j i^O'SECONDS | 4 ADJ LEAD NITRATE TO 3625 G <76'-242/245 6 74.5' i I I 247) AT 67-69F j ' 41 ~D I 5110 I I RECORD: Jfi7_____*FA ICE CONSUMED (330$/BLOCK) 1330X6zi 57-A \lA&S> |2>rSTIR 5 MIN % RECORD PH; (2.2-3.7) J ft*** I IUSE TITRIMETER TO ADJUST N-41-D PH **** | || I3T IF NECESSARY ADJ TO EiW-2.0-3.1 ASSUME 66% | _ } 33-D | IJ RECORD PH : _tZZl ASSUME 50% U " 1 7-D J " I i^NtrfE: DILUTE. N-7-D 10:1 WITH WATER BEFORE ADDING j || 128T RECORD: G/ML (1.143-1.144) IF OUT OF SPEC) | | TfLL OUT CHECK LIST 6 ATTACH. I || "STIR AT 6?--69*F FOR S-31 . TAKE 1 GJT SAMPLE. I JI DUP050059952 LOT; 1. EQUIP MEN!' ____I. SV: 31 I ""*5:" EONT I rr k Wt ' .Jr?" . - COMTYP JOB NAME: 01YE698DMT PAGE 03 DATE PRINTED:10415/82 USE N- ACCT LBS CODE LBS OBTAIN 1 QT SAMPLES OF S-18 & S-30 SOLUTIONS 6 TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE 7,1-7.4 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0.10 ML N-1-D <IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS). DO NOT PROCEED IF N-10-D TITRATION IS OUT OF RANGE ml .ADJUST V-358 FOR A TITRATION PH OF Ot W TO 2.GO FROM FINAL IN-LINE TITRATION, RECORD LOWEST PH & ML N-10-D _____ . ' / yf-y? /s33-D 7-D 2 I WHEN S-31 TITRATION OK , STRIKE V-358 THRU sv BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN '".6 16-18 MIN - RECORD: START TOTAL MIN___ M____ NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS & BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER FOR 15 MINUTES DURING S 33, WASH IN V-358 STIR 2 MIN 6 RECORD PH (1 .8-2.5) XS,^_rte__<MUST BE + ) STIR TOTAL OF 15 MIN FROM S-33 6 RECORD: TEMF' <67-73*F) DUMP N-3-A FROM S-4 STIR 3 MIN POUR IN N-32-D FROM S-5 STIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN & FLUSH ALUM LINE WITH WATER 1 734 I 115-D 367 DUMP IN N-3 FROM S-6 STIR 4 MIN FOR S-48 RUN IN HYDROCHLORIC ACID USING WEIGHT MK _____ _____________ %i. DURING S-44 SIFT N-711-B FROM S-7 INTO V-390 I WITH AGITATOR ON IN 1-2 MIN | I- STIR 1-2 MIN- TO MILKY SOLUTION | 28-D 28-D 105 WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP UNTIL FOAM SUBSIDES, I jJ>-L<DUMP IN BLANC FIXE N I50H WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON j i TOP OF PAGE 1 - I RECORD: CODE __________, LOT_________ _ _________ # 4'">'STIR 20 MIN . fECDRD: PH^(gi.Q___<5.8-6.0) . lE^NECESSARY, ADJ TO PH 5.8-6.0 ASSUME 50% & RECORD: PH-_____...______ ASSUME 66% FLOOD TO 153* (7298 G) & STOP AGITATOR I___ 128-A 330 7-D 33-D FINISH OPTR 7&LWM? 7%l Z DUP050059953