Document 1684X3jb5RXoJLy8ybd5Yp5m

FILE NAME Marbletite PMM DATE 1968-1977 DOC PMM004 DOCUMENT DESCRIPTION Plant Formula Worksheets Februar1y1 1974 Supercedes November 16 1973 formula MIAMI PLANT FORMULA PREMIX CONCENTRATE M Concentrate ) . DESCRIPTION OF PRODUCT Marbletite Concentrate for the manufacture of Stucco FORMULA . Raw Material Asbestos SG210 Zinc Stearate Emathlite Function Bulking Agent Waterproofing Workability R.M. Spec No. 13 53 15 % 13.75 .50 78.75 batch WORKING CONSISTENCY ~ Refer to plant testing procedure No. 1 * Denotes Change EXHIBIT 3 Premix000001 . . spunod 0g HOLVa S82 009 6LT MASTER MASTER WALTEX ZOCXIWA2Y-yP]UBH Syous WALTEX WALTEX 49 MATERIAL soes O B 3 9 oY ra FORMULATION FORMULATION FORMULATION A. g - 64.20 HOLVE spunod O06E 17.60 64.20 O42 OOE sxjoesWOVS 9 g eh TS ot OZT . L2T 13250 GH 27 3900 ASBETOS spunodHOLVG OSE. 0.75 0SZ 002 org gt SE 90T OT d FTOS LIGHYA < ATAGEL WOS STRIPE GLUE syoes 69 0.75 S g LNBOUHELHDLAM 0249 0.15 . at <0S 7 SL0 2TZ 0%*0 -STO I 67-W otzps GANT XGLTIVM Z106 Len TWIUSL TIGUVN OTVL OS <TS 704 EWL AdlaLs VN OF SZ UHH HOVIS SOLHasy TEDVLYV - OWO dq SAIOTN BALOINVA LONGd August 15 1974 . Superas lleprd eve ios us formul^s MIAMI PLANT FORMULA WALLTEX WALLTEX 49 ae DESCRIPTION OF PRODUCT An animal glue and starch based wall texture FORMULA Raw Materials * # Marble 325 Talc Huber 90 Clay Starch 747 Asbestos SG210 * Attagel 50 CMC - 7MT Red Stripe Glue Colloids 513D | * Vanicide 51Z_ Function Filler Filler Filler Plasticizer Hardener Bulking Agent R.M. Spec No. 5 17 26 31 12 Bulking Agent 16 Plasticizer 100000 Adhesion 100000 Adhesion 100000 Thickener 100000 Fungicide 100000 % 64:20 17.60 batch 5.02 4.18 5.03 | 0.75 0.75 2.12 0.20 0.15 WORKING CONSISTENCY - Refer to plant testing procedure No. 1 T.C. Specifications Maximum Minimum Average 72 54 66 WORKING PROPERTIES - Refer to plant testing procedure No. 3 CRACK RESISTANCE ~ Refer to plant testing procedure No. 4 BONDING PROPERTIES ~ Refer to plant testing procedure No. 5 * Denotes Change EXHIBIT 3 Premix000003 ra MARBLETITE PRODUCT FORMULA LOCATION MIAMI _ EXPERIMENTAL CODE NO #4 _- PRODUCT GROUP EFFECTIVE DATE PRODUCTION DATE PRODUCT GLAKE DESCRIPTION OF SNOW SNOW GLAKE GLAKE 20lbs 20lbs 15 AXS 5016BAG 5016BAG + 20lbs AXS . FORMULA RAW MATERIALS POLYVINYL POLYVINYL POLYVINYL 5235 HAHACE 267 TITANIUM TITANIUM TITANIUM FUNCTION METHOCEL METHOCEL . 9 MARBLE MARBLE CLAY BENTONITE _ BEAD TBLC 3X VANCIDE : FA MICA PYROPHYLLITE PYROPHYLLITE PYROPHYLLITE PYROPHYLLITE COLLOID 5130D ', WORKING CONSISTENCY SPEC NO _ - % BATCH 10165 _ 20163 20163 _. 4165 102 + 30165 12/202 12/202 8A4 _ +40165 " koh _ . 2016s _ 25165 . - _ 160 lbs 12/02 12/02 12/02 _ 2016 . _ 4016 M 502 . T.C. SPECIFICATIONS MAXIMUM MINIMUM MINIMUM AVERAGE TENSILE STRENGTH TEST WORKING PROPERTIES COLOR PLANT MANAGER CONTROL MGR PRODUCT PRODUCT DEVELOP PRESIDENT PRESIDENT EXHIBIT 3 Premix000004 February 11 1974 Supercedes November 16 1973 for ORLANDO PLANT FORMULA L SNOWFLAKE 0-43 DESCRIPTION OF PRODUCT A vinyl based ceiling spray using Polystyrene aggregate FORMULA . Raw Materials ty Gtefis 4610 4610 Function Spec No. % batch 900 Polystyrene Bead Aggregate 8.08 . 61 + Fibereee 326194 98 325 Talc Bulking Agent www a 29-94 29-94 | Filler P8OF Mica - _ Attagel 50 2027 Filler 2027 Bulking Agent 16:63 2510 3.33 1.92 500 100 - # Marble Plasticizer 650 Filler 650 Polyvinyl Alcohol Adhesive - 28 Attagel # Bulking/ 7661.42 7661.42 7661.42 50 39-92 537 1200 1766 194 50 M Tertehnoed ncAlcoe hol l BOMa Marble 0:03 Thickener- -3,6 ..------ 0760 Plasti cizer Plasticizer Plasticizer 5 58 580:03 0:03 -Filler O seen ee - Polyvinyl Alcohol 54... 10-33 10-33 . Cc Adhesion Adhesion 28 -1-20 -1-20 -1-20... 1 10 36 36 WORKING CONSISTENCY 2-400 Refer to plant testing procedure No. 1 T. C. Specifications Maximum Minimum ~ Average 100 108 116 WORKING PROPERTIES ~ Refer to plant testing procedure No. 3 CRACK RESISTANCE - Refer to plant testing procedure No. 4 BONDING PROPERTIES - Refer to plant testing procedure No. 5 VINYL SPOT TEST - Refer to plant testing procedure No. 2 EXHIBIT 3 Premix000005 QO0xIUELy-el Pre SNOWFLAKE SNOWFLAKEAe OVE aoe MATERIAL TOS FORMULATION : | HOLVE spunod OVS = OZT Syaes oe 39.92 SL ATGEL 13 BT__ | ~6E on ALCOHL13 CE Soy 1.66 1.66 Gor 1 Goel 50 BE a>}. O39 ZF 35 FE =, = L006 ra Gf Sarch ) eT Sxoes ATAGEL ce 070070 2 ae T ay z | a METHOCEL e| 0.6 INwOWGd -"9*6|- _ THOTAM Que -0633- 0.03 cere 99T 26 99T oro -0633- OE -30 ALCOHOL c 1.20 Phy 8 ges Sy ~EO*O <460e"t y.. ; RE ak oe Vent a OW (') 210 (2)-05#FISOVELY _9ga-qnoeta ay TOH10g4-OT. ieee) POOF 2225 oa (9) Ro PROT me-CH@ ~ (63) Bs z 170 3-0-7 OS# LTC (OYA LY (2) OEE OLS DOL Byouys 25 DIVE VOIN ves... TANT >aeseals BesTOS SG THDVLY aaa 210 Hantak WPFEX 210 AEEA Sze 108d EXHIBIT NREL GfA10Rd~ 7A February il 1714 Supercedes November 1973 formul poy "|" ORLANDO PLANT FORMULA { SNOWFLAKE CONCENTRATE 0-53 Pte men! enue, emente ame DESCRIPTION DESCRIPTION OF PRODUCT : Premixed concentrate for the manufacture of Snowflake Ce I mae Materials ; Raw AttageMlaterials ab wt | Materials - Function Spec No.. Bulking Agent. + Plasticizer 61000 ~ ' 20.06 20.06 batch ; Methocel 228 ' Thickener 61000 . . 16.48 Trend Soap _ Plasticizer, - 58 os. .0.56 PolyvinylPolyvinyl Alcohol i Mica PSOF Adhesion Plasticizer 28 33.52 Poe : Filler 4.1 19.96 Refer plant procedure ' WORKING CONSISTENCY = T. C. Specifications to testing 6 Maximum _ Minimum , No. 1 Average ' , i ates - ary - PROPERTIES PROPERTIES No. WORKING 3 i3 j to procedure : - Refer plant 2 . ' testing . . >i 3 to procedure No. RESISTANCE e CRACK testing plant testingprocedure a = ReferRefer toplant i cad re = 474 bie less 7 1 ' rein BONDING BONDING PROPERTIES ~ Refer to ple No h . all a 5 i plant testing No TEST i ; VINYL SPOT : ; ~ Refer to ; i i procedure 2 * Posbe 1 Ie : , . : . ^' 1 ; 4 | F ar . j i j PG i Be p70 . . $ treed rob FR ; Pe : 3 a . fe " . Peo fe bo a " LEODA EXHIBIT 3 Premix000007 * WT SNOWFLAKE 80xIWai4-yejuH. CONETRAE spunod SNOWFLAKE SNOWFLAKE SNOWFLAKE CONCENTRATE FA MOVS OZphoies MATERIAL Hoes WOLVEFpuUnod . on MOVS ALCOHOL EpiG@hus | POLYVINL e HOLVa spunod An OSE eL 60ap, 2162 2162 2-Heatrxe Hove NOVS WaALS OOF syoes $2 "2 =8 ATSHREVT] vi _ HLVUINSO INTOBad <$-0 LHOTEM 90 02 Bot 95O 216 oS" 966T CE AG . AXVTIMONS TWIUSLVN "THOLAN IOHOTY a ~~ THDVLIOS# 8zz dOS Wav TANTAL d08d CNRaL OF 10d YOIN LONToud PREMIX MARBLETITE PRODUCT FORMULA : a offer 005 005 F LOCATION ORLANDO PRODUCT NAME AND NUMBER Snowflake EFFECTIVE DATE 1/4/77 DESCRIPTION OF PRODUCT __ Snowflake _. : PRODUCTION DATE1 RAW MATERIALS Polyvinyl Alcohol Hamaco 267 Titanium Hedman Fiber Methocel # Marble : Bentonite Clay Bead . Tale 3X Vancide AA Mica Pyrophillite L- Colloids - FUNCTION Binder Adhesive SPEC NO . Pigment Bulking Agent _ Thickener Filler } " Hiding Agent . Aggregate Filler 8.15 Bacteriacide Filler . Plasticizer Defoamer . % 1.02 2.03 ~ .37 4.07c .08 .08 65.06 2.68 2.03 16.26 10 2.03 > 4.07 20 BATCH 25 50 } "Oa 100 2 1600 66 50 400 2.5 50 100 5 E.004 WORKING CONSISTENCY | 2459.5 total | T.C. T.C. SPECIFICATIONS TENSILEESTRENGTH TEST WORKING PROPERTIES COLOR BRABENDER VISCOSITY CRACK RESISTANCE BONDING PROPERTIES MAXIMUM MAXIMUM ~ MINIMUM - Z. AVERAGE VALITY CONTROL MGR Product Development PRESIDENT Ruk EXHIBIT 3 Premix000056 ENTER PLANT FORMULA WORK SHEET LABORATORY FILE # PRODUCT NAME SnowflakeSnowflake DATE 11/11/20 11/11/20 OK'ED OK'ED BY EX # Orlando REPLACED DATE REPLACED Plant ; COMMENTS | BARCH SIZE 36-35H 36-35H by Plant Batch GOL MATERIAL IBS UNIT COST TOTAL COST LBS BAGS Hagel #So #So Methacall # 15000 _ | 30 j 10 Vinol RP 251 35 Oris 2276 1/2 Asbestos 7RF9 60 | .1118 . 8500 4840 | ..2276 104820 3.354 4.250 2 16.940 fii +114 | | 2.893 Fiber 2 550 10392 21. 560 i Marb#le 10 Soo 001051 001051 .5.255 , | Chapted Form 301 .2000 7.500 Mica Diamond 1203 So 0039166 0039166 1.958 | ZINC Stearte 1 3420 342 : 1269 641166 | ! | MateCor st a35lH by 1.782 | Cost | -- --" .113 | Labyr Cont .190 Direct Cost - 2085 . 3.21 TOTALS H MIXING INSTRUCTIONS : NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 Premix000059 ~ mn te _ _ Date 11/24/70 Batch Bags Material Pounds atteyl atteyl atteyl atteyl 4 4 he Y Product Ane flake Product flake Yield flake ae l PER Batch | seat 412 a eee ee ae aan f meee) LAFF TT | #2 | Keb 5sLigh | . Y/ af Wa \ MACE AF 7 7 WA . + ~ | eee aie | 1 rae) 7 fe % A BRA? CL. eaidlek 7 if 20 Baye Baye 1 Perpated use Perpated Perpated Se ees EXHIBIT 3 Premix000060 Date 11/2470 11/2470 Product Anc- flake Batch oo > peer ee mle fee oe oe i q admpdemten tenosteme pom mt ane = ~ Material Bags Pounds flake Yield edetaieteluhentenden Seteeded ated PER ee 73 Batch 8 at 35 ne We ame teal ee tree a heey arte Yom slat bese Sm tof seed Seb tee Bee win, ob < XN i attaya v L Bang | 1 TBF9 Page AA 1/4/71 libre 32-1994 32-1994 10 20 Bags | Vingt 217 20 1A col madine madine madinmaedine Jf | hailed /, EXHIBIT 3 Premix000061 a ne | MARBLETITE PRODUCTS INC INTER PLANT FORMULA WORK SHEET ORLANDO PLANT LABORATORY FILE # FEB 2 1972 . EX # PRODUCT NAMNAEME SaSo aoTeake Concentrate REPLACED March DATE March 3 1971 DATE REPLACED OKED BY COMMENTS : MATERIAL LBS GA GAL UNIT TOTAL COST 20 bags BARCH SIZE 20 bags Plant Batch bags oO ~ LBS : lag BAGS 5353 53 lag Attage----...-- ---- -- -- 15,000 , 1200 ----...-- ---- -- -- 1200 Trend Orey R.CHTX 10 250 .1098 .90 .1895 1025 21.94 180.00 1.8950 1.8950 25.6250 25.6250 Aboes Aboes Aboes 4bags a 5 bags 217 Vinyl 400 1060 ATERIAL ATERIAL COST PER J3 . 160.00 390.48 390.48 1952-40 1952-40 1952-40 : bage | Ao e OST OST BAG BAG 1145 TOTAL DIRECT COST 19.6385 19.6385 19.6385 OR .3705 PER LB. i ai TOTALS _, 11060 MIXING INSTRUCTIONS : NOTIFY LAB OF ACTUAL COS^ PER LB. EXHIBIT 3 Premix000062 PLANT FORMULA PRODUCT SNO FLAKE CONCENTRATECONCENTCRATE ONCENTRATE ea MATERIAL POUNDS Attagel 50 15000 an 200 by 200 R- frand Beep only 10 217 Vinyl Yoo 8 Total wt ; Bag & AL Use 1 bag per batch _ Bon &, ," kes Beep || ; PMO EXHIBIT 3 Premix000063 ae a ? ; - | LABORATORY FILE # SHEET INTER PLANT FORMULA WORK PREMIX INC ORLANDO PRODUCTS a FEB 2 1972 EX # Leake Z PRODUCT NAME - REPLACED DATS March 1971 DATE REPLACED . OK a OK'ED BY COMMENTS : MATERIAL Bead | attagel attagel Mica | Selse 21 | 10 Mackle 3 _ oo LO | | = LBS GAL UNIT COST TOTAL COST 62 / 17 min 13621 |22.6312 254 BARCHPlant 70bago 254 Lage LBS 35 . * 50 .1098 5.49 / 100 | .0278 2.78 TT yy 1100 | | .0398 43.78 22 . _ 1000 .0112 11.20 . 20 17 17 Vinyl 50 40 20.00 HI 1; TRE9 60 | 0606 3.6360 I M | Encentrale Encentrale 153 ]- 13705 . 19.6365 19.6365 foo: a 2475 129.1539 129.1539 2 1| | 35th JATERIAL COST PER 35th , COST OF BAG -ABOR COST ae _ _ 1.8264 .1373 1917 1917 HTT | ; ITAL DIRECT COst _ 2.1853 2.1853 . TOTALS 124752 MIXING INSTRUCTIONS : 7 | NOTIFY LAB OF ACTUAL COST PER LB. of EXHIBIT 3 | 2.1853 2796 24649 : Premix000064 - . PLANT FORMULA fay PRODUCT 840 FLAKE enzscaruramammamme so ye MATERIAL , Bond POUNDS 62 # ' min Atagel 50 . DATE 303-71 ee BAGS | GALLONS 1 Mics Fibre $ 10 ) 100 2 1100 22 \ 1000 eS pea 20 SE: In Wool Machine , . 217 Vinyl ; 50 so | 5R01 Asbestoes or 7RFY7RFY 60 . 1 eae Total wt Bag at Makes 70 plus 280 24751 35 EXHIBIT 3 Premix000065 PLANT FORMULA PRODUCT FLAKE CONCENTRATE MATERIAL POUNDS . DATE TAGS | July 13 1972 GALLONS Attagel 50 200 4 Methocel 228 300 6 | Trend Soap Only . 10 AWD # 9 Marble 217 Vinyl 160 | 170 7 400 . 3 & 10 3 & 20 500 Total Weight 1240 Bag at 62 - Makes | 20 Bags G Use one bag per batch CONCENTRATE PER BATCH ~ Attagel 50 . 10 Methocel 228 15 Trend Soap lik Titanox AWD 00 9 NCS 217 Vinyl 00 20 Total Weight per sx 62 PMO EXHIBIT 3 Premix000066 PRODUCT PLANT FORMULA FLAKE CONCENTRATE MATERIAL POUNDS | Attagel 50 200 Methocel 228 300 DATE __ July 13 BAGS GALLONS ele Asbestos 4 462150 462150 1972 Forme -- -- ----, 19 350 6 350 2 Trend Soap Only 10 12 AWD # Marble 160 170 & 10 200 4 3 & 20 217 Vinyl 400 8 Mica Mica Total Weight 424 1240 Bag at 62 - Makes 20 Bags ~- Use one bag per 1/3 CONCENTRATE PER BATCH , Attagel 50 10 Methocel 228 15 Trend Soap HIN | Titanox AWD 00 # 9 NCS 217 Vinyl Total Weight per sx - lat 20 62 PMO EXHIBIT 3 or 2bage Concentrate ( bage Mica +25.23.1 175 175 } A| a) 10 10 +25.23.1 +25.23.1 17.5 " " 10 /A Be 424 | 21.2 Premix000067 perfetchperfetch PRODUCT FLAKE MATERIAL Bead . Attagel 50 Mica 325tale 325tale 7 Fibre # 9 NCS Marble IN WOOL MACHINE . ) 62 . , DATE _ July 13 GALLONS 1972 Nobit ( _ 50 100 : 1100 1000 1 Abay . 1 bag 5 2 2 bags bags i | 22 . logs 200 18 200 Lp Lp 1400 1400 10 bage 325 8 20 24 05 bays 12.50 12 217 Vinyl ASBESTOS 59-210 HEE Asbestoes ae 7RF9 50 60 38 60 | Concentrate 62 Supplemer mertal Concentrate Concentrate Total Weight Bag at 2475 | .. 35 Makes 70 bags plus 25 , 50 56 1 bbaag g3300 the I ing 30 ing 3 boge .- boge 3 b -- -- -- ---- -- a -- -- -- 62 118 50 # Watch Watch Grays te hte a eeen | Grays ees, 12,5 wwwww.warin : 20 Lago Lago a Lago Aan of dastaria? MP 7022 7022 w CVinge CVinge CVinge 40 fms @ t 50.0 50.0 PMO EXHIBIT 3 Premix000068 MATERIAL attigel 50 POUNDS 200 | BAGS 4 GALLONS RCH X 250 ' titol NT 6607 PMO PLANT FORMULA PRODUCT SNO FLAKE CONCENTRATE DATE 3-3-72 MATERIAL POUNDS BAGS | GALLONS a Attagel 50 800 METH CEL 2O 29 | "# . # p Vinyl 1604 | 2 57 a 33x 33x 20 Total wt Bas at 623 Use 1 bag per batch SS. oe = ae mikes 20 Brep CONCENTRATE ATTAGEL 50 METHODEL 15000 CONCENTRATE - 10 157 PER BATCH TREND SOAP 2 TITANOTXITANOX AWD # Nes 84 81/2 217 VINYL TOTAL OUT PER Sx 20 Est attagel ' 15000 15000 mitol mitol trend TRF9 pehethse. RCHTX 200 200 10 400 250 GALLONS 4 4 77 ' totanlt 1060 Beg at 537 -- -- -- one per Batch . PMO EXHIBIT 3 Premix000071 PRODUCT ne MATERIAL PLANT FORMULA slike . POUNDS # DATE ' BAGS 1/4/71 GALLONS 7RF9 abratara mica fibre # 2 # 10 100 1100 1100 1000 / 2 22 20 wool machine 217 Vinyl fibre 2 fibre toteMtl. 70 100 2624 1720 1720 2 maker 75 Begont Begont 35 EA PMO EXHIBIT 3 PremixC00072 Bead atagel sured fibre fibre 10 PLANT FORMULA. POUNDS 625 Tin 50 100 1100 1000 / 2 22 20 GALLONS 217 Ving 5R01 asbestora 70 600 # | 20 tatol mit 2495 B35 Makes 70 * 25 PMO EXHIBIT 3 Premix000073 2 Mees. PRODUCT SNO FLAKE MATERIAL Bead Atagel Mica PLANT FORMULA POUNDS 62 # 7 min 50 100 1100 1000 ee DATE 3-3-71 BAGS GALLONS 1 22 20 In Wool Machine 217 Vinyl 5R01 Asbestoes or TTRFYRFY FO HS 60 1 ime Total wt Bag at Makes 70 plue 25 24751 35 PMO EXHIBIT 3 Premix000074 ERTER PLANT FORMULA WORK SH^ T Orlando Orlando Orlando LABORATORY FILE # PRODUCT NAME Flo - Spray Spray DATE 1 /20/20 11/20/20 1/20/20 OKED OKED BY CONTENTS : e SAV MATERIAL : y LBS GAL UNIT . | 65 .0375 15000 | " .85 Diammonium Diammonium Diammonium Phosphate 1133 Amaran Bibale Bibale . 1545 +3750 Casens Dow A | 50 1 3553 6604 Berd 5 .40 EX# REPLACED DATE REPLACED TOTAL COST BARCH SIZE - 32 bag Plant Batch LBS BAGS 2.438 | 6.380 - 2.009 ' 2.200 7! rr 17.765 Thi Asbestos SRol SRol RCHT Marble 10 Fiber ##2 Take VHT M 100 1050 250 300 1974 Material Material Cost for 32 By Cost Laber Bay Cost 10178 1025 vow 2 0342 10193 TOTALS _. j MIXING INSTRUCTIONS: NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 ~ Premix000075 ENTER PLANT FORMULA WORK SHET LABORATORY FILE # EX # PRODUCT NAME Fb- REPLACED DATE 11/10/70 DATE REPLACED | = OK'ED OK'ED BY __ COMMENTS : a BATCH 52 59 | " MATERIAL LBS GAL COST ; TOTAL COST Plant BAGS | . SPV * 1300 | Cellucize 91 Aa mmin Bibit 182 Dammitin Phosphate | 182 | DAN A 52 Cascin 1300 ; 3107 . Maternal Cost per lang at 52 Cost of bay PISA PISA Cost Concentrate . Cost per pound all Its | | ; _ . 10375 | .9000 48.750 81.900 81.900 3750 __ -1545 | .6604 .6604 50.050 28.19 34.341 .3453 | 448.890 692.050 692.050 i DPV 65 1 1 meth Saw | 7 ! | J'has 13 325 _. 82.50 1545 3 B.b. .2750 2 Casin DA So .3853 17 Ts 6450 I Bead 69 You 21 13.3097 13.3097 Worl 30 ies _ it . 1013 SRO Worl 1018 30 13.4100 13.4100 13.4100 Hil RCHT ft 100 1025 101 2254 |p 10 1050 15 110 [itl VHT 300 = 57 2 250 372 930 100 1974 5 lbi lbi TOTALS MIXING INSTRUCTIONS : 324 Gibe Gibe t NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 Premix000076 ENTER PLANT FORMULA WORK SHET LABORATORY FILE # EX# PRODUCT NAME Flo Flo Spray Spray REPLACED DATE 11/10/20 11/10/20 11/10/20 DATE REPLACED OKED OKED BY COMMENTS : MATERIAL LBS GAL UNIT COST ; 'TOTAL COST SIZE BAICH Plant bag Batch peri; LBS BAGS Bead 10 min 72.1875 72.187N5Y .3886 .3886 .3886 28.052 - Wool bay 30 .0500 1.50 1 | Asbestos 5Rol | IS .10178 1.527 | | Concentrate bass | 119 2254 | 26.823 ||] | -AF950 So 001334 .667 RCHTX | | 150 009275 13.912 | Marble -Wingble white 1000 01376 13.760 | Pale VHT Soo .01660| 8.300 : 1936.1875 1936.1875 94.541 94.541 a ell Mcked of cos3t 4 bay 1.6882 | Labanc -Direct Cost Suga _ 1900 a - ON jp 19889 i] ie 3.06 fl} \ /\ } Pa 4_ =s a MIXING INSTRUCTIONS NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT3 concelled concelled Hantak Premix000077 ENTER PLANT FORMULA WORK SHESTHET ) ke 1 i | . , | LABORATORY FILE # EX # tS REPLACED concentrate entate PRODUCT NAME Flor Spray DATE REPLACED _ 4 DATE 11/10/20 . OK'ED OK'ED BY . COMMENTS : MATERIAL LBS UNIT COST GAL _. ; TOTAL COST BATCH SIZE 52 @ 5%9 Plant Batch . IBS BAGS | Sev Cellucize Cellucize AB | Dammo Phosphate Daw A | Casein Casein i s 1300 91 182 182 | 52 1300 3107 Maternal cost per bag at 52 tong Cost of bay PISA Cost of Concentrate 5 1/163 pound | Cost per per pound 551/163 .0375 | 9000 2750 | 1545 | .6604 3453 | 48.750 48.750 81.900 50.050 28.49 28.49 34.341 448.890 692,050 692,050 i JpV 65 | seth Save 71 cha 325 8250 6.19 Ti phos 13 1545 [i Bb 8 .2750 220 Casin So .3553 1776 1.29 DA ty ye 1.29 Bend 69 40- 40- 2760 13.3097 13.3097 Wool 30 ios 150 , 1013 5201 30 0018 306 13.4100 13.410 Al] RCHT | 100 f , 2254 Frere ow ac |i 10 VHT 1050 300 1025 105 193 10.25 1103 ~ 579 12 1250 322 9 1 1000,4 19744 5lbuss 5lbuss TOTALS MIXING INSTRUCTIONS : ' { 324 tb) be | | j 165 NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 , F'remix000078 10/102/2/7/0 710/20/70 es Spray concentrat pounds BAGS 89 112 # 112 EXHIBIT 3 Premix000079 EXHIBIT 3 : Premix000080 _ 11/19/70 Product con engi Date _Batch . . mma fere wean tate mor mh Aa tem re ee Ht ar aeTorn won et mw on ates Yield PER Batch 4 ome + tom Fase see ere afm sees one om iain eee Se oom ete tor Panpe Menpenn Sen eerete rey Material | Bags Pounds SPV 8 -- -- ---- Bozati 190 p 1 x 90 15000 15000 mz |? 40 s Lpaerereninsver # 1 adcomentate adcomentate 120 1260 Boek : 2900477 29004772900477 Begat Begat 486 Begat A? Men 60 Lredee 3Bags oe 3 Han Pree UST , Date 11/16/70 Batch eee ene ee 20 Product flfolo SSpepcyecy __. ned| Yield PER Batch e bo ens mat elf mtr ie oan fren von man ahd ma Om ant hte VaR Set few Om or > deat tee gor Oh wae Material | Bass Pounds SPV LO Yeap Dow : Borate i 20 140 Carline 10 Backs Braut Braut 6.3 make 40 Bags Bags - Date Batch 11-16-70 pe a 11-16-70 Product FLOSPRRY Yield PER Batch er em pans webb 4- ab Dm ees eres ate ee Cer CD Ce ate cet Cie (a Material | Bags Pounds SP.V 15,000 | 11 | PHOS PHOS 7 BiB " | CASEIN 50 BEAD 10| 66 | WOOL 186. 30 RO 30 PCHTX # 10 ... 1100 550 600 26950 50 Concentrat ConcentrCaotncentrat ConcentratConcentrat 11/3/701/3/7011/3/70 fl Date __ Batcheng ey ota em Sn nn nine ging ate mm Product fl hero. Yield PER Batch Se oe ee Product alfentanil me om ere ain mr nme ne af et ew mn 7= Material | Bags Pounds 1 phosphate 70 228 1B | d 15 Eft tt 3 abel. TIT . POT ZaYa\ aleuey-m fle PRODUCT MATERIAL . Spray Spray comentats POUNDS DATE 11/8/711/80/70 BAGS and % is cv 228 phosphate j 55 6/4 6/4 ## 1 /9/701 /9/70 11/9/70 70 # Pann av craal craal TROT RCH 50 3 40.200- 40.200- / # 10 - 12 VHT 18 ce a eebee | ~... STRUCTIONS - shew ee eo ese dat eos | eae | oe + 4 5 A LA sees EXHIBIT 3 Premix000085 PREMIX PRODUCTS INC 300 N. E. 72ND STREET MIAMI FLA JOB ADDRESS & PHONE 11/7/20 11/7/20 SPV 80LB. | > 15,000 5/56 11/17/70 | | CASEIN | 46 PHOS 4 | | BiB 4 2 EF- # 132 # 520-1 Week Week 30 IBG BCHTX | 150 CONTRACTOR 11-5-70 11-5-70 TERRITORY SALESMAN REMARKS Wing Wing 40-200 600 | 100 # 10 300 Vee 11/71/1/47/040 11/7/40 11/7/70 P 101 BARNETT'S MIAMI - EXHIBIT Premix000086 # 12 70 Beaut Date 2 Product - _Batch#__ en a La -peenpecenia= ee | Yield PER Batch en a ee eee me ee Material | Bags Pounds y 4 A SPV 40 a 7 haa 8 | 27 if tan | 5h01 30 AY 15 RCHTX RCHTX aa 50 | 4 re 10 850 #T _ 300/4 Anne | fs lesa |7 47 | 0087 # 70 _ Date Product flo ___ Batch pane ny peeenno flo Spay Ae Material | Bags Pounds Vield yout 58 * PER Batch agen Spey NRE SO eres eeeeees eect SPV 8 Bays 228 Dag 30 | els Lie oF thaphte | likey bof bel Loo * Low be 5/0 5/0 | Cosaint 10 -- -- _ | EXHIBIT 3 Premi mx000088 #1 108 ADDRESS & PHONE CONTRACTOR REMARKS Dow SPRAY CONC ; 128 64 LB. 902.90 | 5.81 |: AMM BIB # 80 73.86 73.86 RMM PHOS 7 aa | # 80 CASEIN | R.CH.T.X. R.CH.T.X. 500 # 850 17 Bath 45.45 45.45 7727 7727 500 Days Days 494 MAKES & BAGS AT 502B +40 BRGS TO EACH BATCH EXHIBIT EXHIBIT 3 Premix000089 Concentrati Date 11/19/70 11/19/70 Product 5 oy 11/19/70 11/19/70 _ Batch #__ Lj flo- flo- Sorry | Sorry Yield PER Batch ee 7 Material | Bags Pounds SPV 13 Boys cst | |# Down 5/0 2 } shephate shephate 2 By 607 13 ha -- -- -- 11/25/70 33 -- -- -- 11/30/70 q Boste Caguine 10 Boste Boste Se ego 2910 2910 he en cas Aa|s?aedNY pee EXHIBIT B Premix000090 INTER PLANT FORMULA WORK SHE boo LABORATORY FILE # PRODUCT DATE NAME Flo- Flo- 11/10/20 11/10/20 11/10/20 1 /10/20 1 /10/20 Spray Spray OKED BY COMMENTS 1 | MATERIAL ; LBS GAL UNIT COST Bead Wool Asbestos 10 Mimeter SRol bay 72.18757 | 30 1S |. 3886 .0500 .0500 10178 --Concentrate bus |} 119 2254 AF 950 RCHTX RCHTX . Marble winable white white | Tale VHT So |_| 01334 150 .09275 1000 01376 Soo 001660 | a 1936.1875 1936.1875 Mckerd 34 of 3H 4H 34H bay Cost of Bay Later EX # REPLACED DATE REPLACED TOTAL COST BARCH SIZE 56ba LBS Plant Hatch 28.052 28.052 1.500 | : 1.527 15 26.823 | i : .667 | 13.912 13.760 8.300 94.541 94.541 [1] 1.6882 |- ! .1107 1900 a aan a | Sugg Price 3.06 / f Sy ion TOTALS Si MIXING : INSTRUCTIONS Cancelled NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 Premix000091 ENTER PLANT FORMULA WORK SHEET LABORATORY FILE # PRODUCT NAME Flo - Spray Spray DATE 11/20/20 1 /20/20 1 /20/20 OKIED OKIED BY COMMENTS : MATERIAL LBS GAL COST SAV | s Methoull 15000 Diammonium Diammonium Diammonium Phosphate Peni 3. . Casens Dow . Bend 65 00375 fl " .85 13 . 1545 g .2750 So 13553 2 -6604 69 40 Asbests SRol SRol 30 RCHT Marble 10 Fiber# 2 Take VHT . 100 1050 250 300 1974 Material Cost jier By By Cost of Bag Laber Cost 10178 1025 01691 10302 .0193 EX # REPLACED DATE REPLACED a. TOTAL COST BARCH SIZE 4- bags Plant Batch LBS BAGD 2.438 6.380 : 2.009 2.200 , 1 iT} 17.765 TLE 1.321 lil 13 27.6027.6000 /! a ~ ~~ ; 7 3.053 10.250 11.036 9.800 7: _| 5.790 TOTALS MIXING INSTRUCTIONS : NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 ~ Premix000092 1-7-77 I FLO - TEX o ~ e ee i 9 _ | MARBLE AA MICA 406B5 406B5 20LBS 10LBS LBS LB +402 1002 + _ VANCIDE VANCIDE _ TITANIUM TITANIUM _. COLLOIDS COLLOIDS COLLOIDS _ _ I METROCEL . _ X = || VINYL STARCH NYTAL NYTAL 99 HER FIBRE 1/202 4oi 02 ,, 02- 4/201 4/201 602- | 10/03 10/202 1/402 1/402 2... 1 1/2 2/402 2/402 3 5/402 | 5 You 1/8071 1/8071 1 802.1 802.1 402-1 402-14.02.1 4.02.1 11/8028 202.0 202.0 218021 25/802 25/802 EXHIBIT 3 Premix000093 Marbletite Premix Premix aw ' Marbletite Let's Finish Together . . . MFG CO INC | INTEROFFICE MEMORANDUM MIAMI 3009 N.W. 75th Avenus 33122 ORLANDO HOUSTON Oviedo & Sanford Road 32707 8321 Hempstead Road 77008 Phone 305-692-5000 = Phone 305-323-2830 Phone 713-869-6341 FROM SUBJECT / FLOTEY FLOTEYFLOTEY _MATERIAL #GMARBLE AA AA NICA : PYRAY BOR WA VAN CIPE TITANIUM TITANIUM CONSOLDS CONSOLDS . eempeies METHOCEL 3 VINYL VINYL IbsLoz Loz 46 28 317 317 317 Fore 4 3 j 4 eo 10th 10/2 10/2 Location AMI AMI EXHIBIT 3 Premix000094 e 1 EXHIBIT 3 Premix000095 ENTER PLANT FORMULA WORK SHET SHET MIZH Plant : LABORATORY FILE # | PRODUCT NAME Concote EX # REPLACED DATE ORTED BY 11/12/20 4 DATE REPLACED COMMENTS : MATERIAL LBS GAL UNIT COST | BARCHSIZE 13- Batch@ 70 TOTAL COST LBS BAGS | C Tarter 1/4 .474 -119 | Air Entrained Live So 101980 990 ! MouldingMoulding Plaster | Ganging Plaster Plaster Keenes Comment Bj 0184 1.840 i _ So -0184 .920 i So 00344 11720 Ji __ | 40-200 Marble 250 250 0102 0102 2.550 | Asbestos Wh .049 .245 Asbestive Fiberty | .0356 | Wh .0356 .107 un fibered Gypsum Gypsum 150 PA Marble 200 .0141 101019 31115 2,038 | white Cement | | Materal Cost by 47 906 0196 | | .921 14.285 || 1.0988 1.0988 + Bay Cost 1116 Loker Cost Drect Cost _ 1190 1190 | 1.4004 1.404 ! | Sugg Price | 2.15 | TOTALSCument Roa 220 ft MIXING INSTRUCTIONS: A ! NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 Premix000096 53.08.04 53.08.04 53.08.04 LOCATION MARBLETITE Experiment Experiment Experiment Orlanda RhODUCT FORMULA Orlanda EXPERIMENTAL CODE N NOO PRODUCT GROUP EFFECTIVE DATE PRODUCTION DATE 1-9-77 1-9-77 L DESCRIPTION OF PRODUCT Color Flotex match to match - . new new . carling carling carlsprai y spraynspg ray carling spray oo FORMULA RAW MATERIALS 49 MccleMccle Pycophull Pycophul Pycophull the ARD Ln line ches Matha Starcen StarcSentarcen Clay Bentonite Clay BentoniteBentonite Clay Hedman Hedman Fit FUNCTION pores : WORKING WORKING WORKING CONSISTENCY CCOONSNISSTEINCSY TCEONNCSCOINYSISTSENCYTENCCOYNSICSTOENNCSYISTENCY R.M. R.M. SPEC NO een . 291 1 _ len i _ _ _ _ ; . LBS BATCH 2100 150 202 25.0 10.0 '@ 27.5 a50.0 | 50.0 t : ae 2654 2654 2654 T.C. SPECIFICATIONS MAXIMUM MAXIMUM TENSILS STRENGTH TEST MINIMUM MINIMUM AVERAGE WORKING PROPERTIES { \ COLOR . brumers brummersbrummersPRODUCT QUALTIY QUALTIY CONTROL MGR PRODUCT DEVELOP } PRESIDENT PRESIDENT EXHIBIT 3 Premix000097 a? CONCOTE SMALL MIXER 1/4 1/2 1/2 2-1 vwi 1-1 2-1 1-1 1/2 lbs SX SX SX SX SX lbs lbs SX _ gx . lbs - SX POUNDS POUNDS POUNDS 2, 50 Cream of Tartar 50,000 100,000 100,000 100,000 10 ,0 0 FiJ Lime Moulding Plaster 50,000 Gauging Plaster 50.000 250,000 250,000 Keenes Cement 40/200 Marble ; _. aan 5,000 3,000 3,000 150.000 150.000 7TFL Asbestos 7TFL 7TFL Asbestine Unfibered Gypsum P.A. Marble VINYL 200,000 1.500 251 ) 47,000 47,000 White Cement 906.750 3/4 lbs per sx sx per mix 70 lbs 12.95 35.5 12.95 11/13/70 11/13/70 EXHIBIT - Premix000098 October 11 1973 Supercedes all previous formulas ORLANDO PLANT FORMULA TOPCOTE 0-14 DESCRIPTION OF PRODUCT A mix of aggregate and cement for use on patios and pool decks se FORMULA Raw Materials White Cement OZ Marble Sand Finish Lime Zinc Stearate Emathlite Function Strengthener Aggregate Aggregate Strengthener Plasticizer Water Proofing Plasticizer R.M. Spec No. 2500 2500 2500 10 53 15 % 30.74 32.71 32.71 2.04 0.26 1.55 7 batch 1504 1600 1600 100 12 76 WORKING CONSISTENCY w Refer to plant testing procedure No. 1 T. C. Specifications Maximum Minimum Average EXHIBIT 3 Premix000099 TEC rs | Water Ta 131 I | DATE WT DAS e J Oe. ppe xs Sapp wt fp tA BONWOCL) GL) tepy? O47 jsa ecot Marble ad 2850 Hu TOTAL- LBS when when 7 when when Rams , emulsion ; OPERATOR (El \ \ OPND OPERATOR S27, yy 9H/ oat ISP ova |) NOTATION NOTATION Sa} Yr? for viscosity viscosity I wh MACHINE MACHINE MACHINE a WOT Fa MACHINE MACHINE sopsaq : : SREC) (1 sy oe o : 3^' . ETN | 7 Fick's | 201 Moter Molso ; | Vino 131 = : ml Teamol | } . |= Celvito | ( Celvito Natrosol | - Lir Asbestos , | a. sf when Toflemuls when Sai NOTATION Wseadry th, as with Wseadry Toflemuls with Toflemuls der . emulsion MACHINE MACHINE \ a \ ssVee =Mt AACGHIANMENEACHINE MACHINE April pre =| ; | appape a oa tp. 4a. ya. peel 7 (area sd | isa) yaee ile [ae [. 4g) a ( ] ym Wseadry bS! 89. SE qs ; Fy i] HantaklPremix^' Qo << Oo NAMES OF MACHINE OPERATOR OPERATOR & CREW NAMES TIME STA | TIME FINISHED FINISHED . oe enr en enioe ~ 26 + 60 See See Form Hater Hater Naleo EmulsionEmulsion 1826.00 7.50 300,00 Glycol Troysan Gelvital Natrisol Natrisol Natrisol Asbestos MarbleHust Hust Texinol Texinol 18.00 3.50 28.00 22.75 455.00 455.00 157.00 2850.00 2850.00 18.0 18.00 18.00 18.00 ChanChgaensges Changes Changes Changes ; April 14-7200 14-7200 aan ve 7 4/13/472/13/72 4/13/724/13/72 % 32.041 .15 CHANGE | | Pounds Pounds GAI 30.08 212 5.26 .31 7.26 .06 .49 .40 | 7.98 2.75 | 50,00 50,00 .31 SUVE IAT February 11 1974 ' Supercedes November 16 1973 i formula | MIAMI PLANT FORMULA TOPCOTE 14 DESCRIPTION OF PRODUCT A mix of aggregate and cement for use on patios and pool decks FORMULA Raw Material Function Sand Marble- --- enen- Aggregate Aggregate ------ White Cement . Finish O LLIME IME Strengthener Strengthener pom Workability R.M. Spec No. % batch 2 32.95.72.5 32.95.723.2.955.72.5 - 7 wee 32.71 8 30.7420.0 30.7420.0 30.7420.0 30.7420.0 30.7420. 10 2.05 7.5 5- 00 ee 1-55 1-55 160 WORKING CONSISTENCY - Refer to plant testing procedure No. 1 EXHIBIT 3 Premix000104 . MARBLETITE PRODUCT FORMULA LOCATION MIAMI EXPERIMENTAL CODE NO PRODUCT GROUP MARBLE CHIPS WHITE EFFECTIVE DATE 11/4/76 PRODUCTION DATE DESCRIPTION OF PRODUCT FORMULA RAW MATERIALS OZ Marble MATERIALS Water Perfume . FUNCTION Aggregate Aroma _ R.M. SPEC NO 291 - . BATCH 1500 _ _ 1 gal oO, 202 202 WORKING CONSISTENCY T.C. SPECIFICATIONS MAXIMUM TENSILE TENSILE TENSILE STRENGTH STRENGTH TEST WORKING PROPERTIES MINIMUM AVERAGE John Couce 6 PRESIDENT DUALITY CONTROL MGR PRESIDENT PRODUCT DEVELOP EXHIBIT 3 Premix000105 Troyson . 7 Gelvetol : TT aes "xs | TREGE PXS ZE mcsEXTREMACHINE EXTREMACHINE os EXTREMACHINE EXTREMACHINE T lbs 5/00 SST Trot. Toms Babi Babi * adel OPERATOR OLY, minke Premix 9/30/70 Mixing Procdure for Wet Mixer A. Starting Water 220 gals B. Nales 7LBS or I quart C. Vinyl 300 Clear 131 D Proedure adding filler to wet mix is ) Atad dumping the remioning 1,350.00 LBS of 10 EXHIBIT 3 Premix000108 i Le te : ~e N N Cont Cont Cont Cont Cont om oa, ) a Terry Terry Terry and and las las 9 put put put 1, m7 waar - re ^' 4 oon, er ~e . ar . uf eye : Zo cnr ty ov ! bine ae 1 Se od . ot EXHIBIT 3 Premix000109 LABORATORY FILE # PRODUCT NAME Joint DATE OKIED OKIED BY 10/3/20 10/3/20 ENTER PLANT FORMULA WORK SHET EX # OrlandOrolando Cament -liquid . REPLACED DATE REPLACED COMMENTS : MATERIAL Water rethocell 228 Collads # 60 Vinyl CA 100-310 100-310 LBS GAL UNIT COST y 1922 221 e | 19 = .8250 6 .2923 486 .11500 .11500 TOTAL COST Ne 15.675 15.675 1.754 55.890 Die Haylene Glycol Asbestos 7RF9 135 Diamand Min 200 AAA MICH 200 raged . Dow 100 1000 1 12ble 12ble # 10 2000 6049 Cost per cost per Sqaclam Cost** Can La ** Cost Divat Cost Suy Price .0950 | .04822 0039166 002800 7.600 6.510 6.510 7.833 | S.boo S.boo 01299 1.0390 12.990 12.990_ | 1.559 .01051 .01051 21.020 136.431 136.431 Camp Camp 7744 11900 24005 24005 | 31A BARCH 95 5gal.com 5gal.com ; Plant Batch 475 |! j t; : | : -- -- ---- 1.1488 ae ey 16441 | TOTALS | MIXING INSTRUCTIONS: NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 Premix000110 . ELL PRODUCT QOXWalg-ye,ULY . PUTICOTE PUTICOTE PUTICOTE 34 052 OSl OSEE MASTER BATCH SHOS 4M WOVS MATERIAL MATERIAL OZ tt <4 PERCENT WEIGHT SACK [| | - MARBLE MARBLE 06f 00 5.93 5.93 og.1050 LIME SHOBSOT 61 g oss oT GAUING PLASTER * : HoLVA spunod OOoT oo% OSOT Sete 059 7025 11 HOLVE WOVS a WALSVN OOT Syoes 9T 4 Z0T #99 er || LNYOUad LHSTaM Lese <6SELST Le*L 0z*6 ie } YE-N , TIGHVW/0S< GLorlEnAa TIGVW INGE NIT Walevid vTWiIadl 02/07 aNGaH HSINDE ONTDAV LoNdu SES February 11 1974 ye Supercedes November 16 1973 formula ae sem enter m MIAMI PLANT FORMULA PUTICOTE 34 hire e DESCRIPTION OF PRODUCT A Keene cement and lime based putty plaster FORMULA R.M. R.M. Raw Materials Function Spec No. % batch 40/200 Marble ' 30/50 Marble Keene Cement Aggregate 6 Aggregate fow Set Strengthener 42 22.37 5.93 15.13 Finish Lime Plasticizer Strengthener . 47.37 Gauging Plaster Set 44 9.20 WORKING CONSISTENCY - Refer to plant testing procedure No. SET TIME - Refer to plant testing procedure No. 9 * Denotes Change EXHIBIT 3 Premix000112 October 11 1973 Supercedes all previous formulas ORLANDO PLANT FORMULA PUTICOTE 0-34 DESCRIPTION OF PRODUCT A keene cement and lime based putty plaster FORMULA - Raw Materials Pyrax B Lime Finish Keenes Cement Unfibered Gypsum Bestwall only 40/200 MarbleMarble 30/50 or PA Marble Asbestine Function Filler Strengthener Plasticizer Strengthener Setting Quality Aggregate Aggregate Filler R.M. Spec No. 14 10 78 Zwart Zwart Zwart Zwart ; % 2.98 47.62 . 14.88 - ; 8.93 17.86 6.0 1.79 batch 50 . 800 250 150 300 100 30 WORKING CONSISTENCY - Refer to plant testing procedure No. 1 T. C. Specifications Maximum Minimum Average SET TIME 1 Refer to plant testing procedure No. 9 EXHIBIT 3 Premix000113 ENTER PLANT FORMULA WORK SHEET # Mixes LABORATORY FILE # PRODUCT NAME Puticote , DATE 11/12/20 EX # REPLACED DATE REPLACED e* 7 : OKED BY | COMMENTS : MATERIAL LBS G^ LUNIT COST _. TOTAL COST BARCH SIZE 24- not boys IBS Plant BAGS Pyrey B Finish line ; So s | 800 Keene's Cement 250 unfibered unfibered Gypsum Gypsum Marble # 40/200 Marbl#e 30/50 Asbestine Fibert 150 300 | 100 30 a | 1680 .0604 1 02037 02037 .0344 .0141 . .0102 01115 .0356 | 3.020 16.256 | : 8.600 if 2.115 TH 3.060 1.115 | 1.068 1.068 35234 | Maternal cost of 70 st bay | - Buy cost p.4 haby Cost | ae 1.4681 He +1116 . .1900 Itt * Direct Cost Suga Price + Coment Bo | | | a 1.76197 .7697 ! ; 2.72 2.45 iil i a . . | _ ; nl an a 7 > . TOTALS MIXING : INSTRUCTIONS NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 i | a r% F'remix000114 F'remix000114 ve Seweta GL9E ee mt Le 9 YGINOTS 34 Malem ote, FOWL L EOR WeDo we XOGO iN 3-30-77 3-0-7 3-30-7 3-30-77 3-30-37-730-77 3-30-73-30-3-730-77 SOLA _20y g $a 347 OT hSeei nt \UXa 3-30-7 3-0-7 -- ---- 3-30-7 3-30-77 XO r GL SOVE LOXIWSiq-ye}ULH SOVa ONidHS dadd TIVALNW SNFTAHLIOd < LIGHXa -pegre FRO G&fF A SMS4 ty 29oD Go - F79S7 aa eeWeS? 9} 3-07 a rea ns f? 1200 i qa -? pe fy | - C + UMP . re sar CALCIUMJMBBa:s < ror . LIGHXa * a y_ Ang4e? hays sah % AW any) . 10 eee ITEMS 327 PER BAG 1641 __ _ 1641 Oh j 7 om Vy ~ 32 250 25 < oe en ete tte eet OAaa - _ _ EXHIBIT 3 meee 4 ee #t Premix000117 FORMULATION BEDINGCOTE BEDINGCOTE 00Z COb Of76 MASTER BATCH BATCH FORMULATION FORMULATION LHS gL poow' BEDIN BEDIN Ss | SyoesOVS -4ejUeH "4K SC PERCENT PERCENT Of SACK 100 7 OL MATERIAL MATERIAL . MARBLE MARBLE OOFer 00h 4.54 4.54 {es O0fr 400 400 Aes eS SZPb | CEMent - | CEMent AA LIME 17.04 17.04 Bl 7 eo / FINSH ODS )} 7RF97RF9 O0h 2.49 4.53 OSL OSE 200 350 SO OS eos aa ZINC STEAR STEARTE | .63 | 4 ] EMATHLITE OOT syoes PE I .85 .85 SI L @ 68 PYRAX || | LNEOWTd THDIEM Ce lth Ase OBLPoLi FG ESF 8031 80317 LS . ig PLG | SasRIsy BLITHY PrGoCYAOPWEDFGI PDA ITS Bury bIGL DLvey a wot "TWLUaVAN GY Bury rig xe Londu eS COLOR Or PLAY FeTrg AY ONE, Ue AA. - October 6 1969 FINISHCOTE Small Mixen Spr Small Mixen - sx plus -lbs lbs - lbs i. . lbs lbs aa + ons ' te . tes 4 thee uy . 80 lb. sX , Sand Lime ( BlueBag FIBRE FIBRE Asbestine Keene's Cement FIBRE . Attagel 50 te tet on pa, eh aan * wat poe ye a . , a, . . . Bee rite a, ee re we ~F . * m , , EXHIBIT 3. , 2 . , . v - t 7 . v Me *' 7. - . :, : Premix000119 AUGUST 15 1968 PLASTER PLASTER LT BLUE 6 lbs BLUE , 3 lbs BLUE . 3/4 BATCH 1/2 BATCH 4 lbs BLUE S 3 Ibs BLUE 2 16.4 oz BLUE : _ FLAMINGO PINK i ' LT GREEN 6 lbs INT GREEN i 3 lbs INT GRREN | TURQUOISE .* 18. oz INT GREEN ; BUFF _ 4 lbs LEM YELL 2 lb. RAW UMBER . 2 lb. 6 oz RID ; 3 lbs L. VELL $ 1 lb. 9.02 RED 2 lbs b YELL ., od 4 lb. 8 oz INT GREEN my . oe a: , _ 2 lb.4 oz INT GREEN ; 1 lbs INT GREEN 1 lbs INT.GREEN INT.GREEN BLUE 14 lb. BLUE 3 lbs : | oz INT GREEN- 9 oz INTGREEN 3 lb. LEM VELL 1 1b RAW UMBER 2 lb. lb. LEM YELL - 1 lb. RAW UMBER CORAL 3 lbs RED 1 lb. 14 oz LEM 2 lbs RED 1 1/4 lbs LEM . 2 lb. RAW UMBER - 1lb. RAW UMBER 1 16 RAW UMBER - EXHIBIT 3 Premix000120 PLANT FORMULA WORK SHEET # OE hy FIBAT FIBAT LABORATORY FILE # PRODUCT NAME Acousticote 11/12/20 1 /12/20 OK'ED OK'ED BY COMMENTS : MATERIAL LBS Perlite - Regular Perliteline Attagel #So 12 Days 300 400 So Asbestos 7TFI 100 ZING Vinyl | Stearate 217 1 5 .854 Dested Cost per 45 bag Post Bay *fotel Direct Cost Suggested f Cement Price REPLACED DATE REPLACED | BATCH SIZE 19-45 19-45 UNIT COST TOTAL COST LBS | BAGS 2 ! 00446 13.33 | 8.128 02032 mn ; .1036 5,180 = : 00490 | 4.900 0342 .342 .342| .480 2,400 | 34.288 34.288 1.8046 .1538 : 21484 | 331 3.00 I} " : TOTALS MIXING INSTRUCTIONS : NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 1 | | | - Premix000121 MARBLETITE PRODUCT FORMULA LOCATION LOCATION Orlando EXPERIMENTAL CODE NO PRODUCT GROUP Snowflake Coarse - Ecker EFFECTIVE DATE 1/30/16 PRODUCTION DATE 76 DESCRIPTION OF PRODUC_T_ FORMULA ; /// RAW MATERIALS # Marble ; FUNCTION Filler R.M. SPEC CellufX lo 2EL Bulking Agent x Bead Aggregate - Vinyl Binder Methocel | Thickener Colloids Vancide Titanium Attagel 5 Hamaco 267 Defoamer Bacteriacide Pigment : Thickener Adhesive ASP 170 Hiding Agent _ . NO Sen Sen 4.7 7 ee 4.4 ane T. oe .41 * .80 .80 75 Seana _ 20 . 7 41 7 .06 | 1 3/4 ~ 53 9 2 34 72 34 , ~2 34 WORKING CONSISTENCY oo T.C. SPECIFICATIONS SPECIFICATIONS MAXIMUM TENSILE STRENGTH TEST MINIMUM AVERAGE 7 WORKING PROPERTIES . COLOR .* f) TANT MANAGER a . CONTROL QUALITY CONTROL MGR- PRODUCT DEVELOP Jay Jay PRESIDENT PRESIDENT EXHIBIT 3 Prernix000122 GRIN GALLONS POUNDS METHOCAL 000 THYLINE THYLINE THYLINE CLYCOL CARBITOL ACETATE NOPCO N.5oro SNOWFLAKE 79 ASP 400 TITANIUM DIOXIDE QUTILE E..A 100 ; Ab 14 . 5.7 5.7 3.0 5.0 | 250,0 200,0 300 LET LOWNLOWN LION &f 105 40 ANGONIC ATP 6.5 ADD COMPONENTS IN ORDUN ORDUN SHOWN GRIND TO SMOOTH FALTE 1.5 LET DOWN DOWN EXHIBIT 3 . Premix000123 PRODUCT P.V.L. FILLERCOTE MATERIAL POUNDS MOULDING PLASTER GAUGING PLASTER ASBESTOS 7TF1 FIBER # 40/200 MARBLE UNFIBERED GYPSUM 200 lbs 100 LBS 6 ibs 6 lbs 41 105 Lbs, RAGS , i 3 F GALLONS TOTAL LBS PER BATH WEIGHT PER BAG BAGS PER BATH 1987 80 + 12 hs TIS THIS FORMULA IS FOR SMALL MIXER INSTRUCTIONS INSTRUCTIONS * EXHIBIT 3 Hantak Premix000124 October 6 1969 BEDDINGCOTE Small Mixer 5 2 2 1 2 27-1 6 I 1/2 7 1089-21 SX SNe SX SXe SKe lbs . lbs lbs SXB lbs . lbs Sand . White Cement Lime Blue Bag Lime Aquaseal S.A. Marble Asbestos Asbestine R 901 75F17-5F175F1 FIBRE #L FIBRE 40/200 Marble Zinc Stearate LUT W_T per sx 80 lbs No. of sx per mix 13.5 EXHIBIT 3 t Premix000125 spunod 008 GLAT. GEL Lz TF MASTER 9eLO0XILE GE fionva ai PRODUCT AM P.OVL.0L-3 syoes ZE 26z BA q-yej}UeH MATERIAL MATERIAL LIME REGULAR OStt Gzsz 60.29 60.29 Se LOT | SG210 4G #0S 8 523S syoes KENS spunodHoLVa G2tt OOTZz S6L Ge Ge Sere ~ < HOLVE . wovs TaIHXA DO Syoes ot PAu 29 OOT Lb BuLA INWOwadLEOLaM 6L Ze 62 09 LG S TE 72 0 UaXIW AG iL AVINGLYN SOLSHASY alTmd <e7-0 av TATA Ino ga OTZDS ANT Stee TNE . diod ALT LON LONI Ted HOLNe TENTA GUNES od LZ LOX!Wad-HP} spunod a, AE TOPCOTE 08 - COST Oost MASTER MASTER BATCH FORMULATION eH | SsyoBs aM - MATERIAL MOPS OZ PERCENT PERCENT PERCENT - . 32.95 HOLVEspunoa OOTE 32.71 amore ... 2600 2600 . - syoesWOVS ... 175 Le 2.05 Te . OST EMATHLIE HOLVaspunod 0092 0097 Hs GAL 7944 7944 < LIGHXxA4 HOLVa MOVS Be 92 9 92 2 BSLYN OOTSyoes - LNsTHDTSM GS6e TLZE WL*OE 40? 6ST AG TW BLOdOL. TV WIGevW DNaO WWUL LT LEEL VA anys ZO hb THM HSINLA THEVA Londod PLANT FORMULA PRODUCT Brushcote Brushcote Brushcote . . MATERIAL POUNDS DATE 6/29/71 6/29/71 6/29/71 BAGS . i White Cement Finish Lime Type 83 CLAY Barium Chloride | |, Zinc Stevato 376 150Lbi 50Lbi 10 Lbs 5 Lbs 4st 4st sx st GALLONS Total Libs Batch Weight pu Bag | Bags per Biratch | 591 Lbc 40 Lbs 145x +31 as INSTRUCTIONS * EXHIBIT 3 Premix000128 PLANT FORMULA MARION Mixer _ __ PRODUCT Beddingcote Beddingcote Beddingcote MATERIAL POUNDS DATE 6/10/71 6/10/71 BAGS Y GALLONS SANd White White Cement Finish Lime 2000 752 400 400 20 st 80 8 St A Lime XO XO MARble Asbestos - 7JEL 901 | Fiber # 2 | Titanium Titanium 40/200 MARble 200 640 110 24 fi" fl _ 200 4 St | 6st + 40 Lbs st 10 Lbs 2 Sx Zinc Sterate- 28 VMP 3000 37 | Jotal Lbs per Batch | Weight Weight per Bag ; | 4395 Lbs 80 Lbs | Supercedes Supercedes Formule Formule dated 4/15/71 _ | 901 Use - TiTANIUM 901 TER PLANT FORMULA WORK SHEIT MIAMI PLANT 3009 N. W. 75th AVENUE MIAMI FLORIDA 33122 LABORATORY FILE # PRODUCT NAME DATE M JOINT CEMENT . OK'ED BY COMMENTS : MATERIAL LBS GAL ANIT COST Starting Starting Nalco Water Vinol 131 UCAR Troysan EMPIO 220 71/2 300 3 1/2 Gelvatol 20/30 P 28 Mitrosol 250 HHXR Diamond Mica 22 3/4 455 " Marble Asbestos 7RF9 2850 157 Totals 45/16 3/4 Material Cost Per Cal Can Costof Can Labor Cost = === TOTAL DIRECT COST = 4187 1400 1.0600 .5500 .8200 .0398 .01088 .0606 - REPLACED P 3.75 5 gal DATE REPLACED4/1/72 TOTAL COST Batch cans BARCH SIZE Plant Batch LBS BAGS . N 5 3.1402 2 42.00 fi a 3.71 i . ly 15.40 18.6550 _|I! 18.1090 31.0080 9.5142 9.5142 : 141.5364 . 4898 .80 _ .1917 . a 2.4815 on TOTALSTOTALS 45/16 yi ty a MIXING INSTRUCTIONS rod i : UCAR 300 Vinot 1311 22 inches se - ACTUAL COST OF : LAB "yy 78) ye . 1B ots Sate Syy er as : nt y PRODUCT ROOFCOTE ROOFCOTE | MATERIAL POUNDS mannan aemetenainied | WHITE CEMENT 564 | DATE BAGS | 2 GALL C TITANIUM TITANIURM 901 1 | 12B 12B | # 10 MARBLE MARBLE | 1200 24 | ViNAC ViNAC 217 | K Mick 4 _ | LB. 444 2B ZING STERATE | 10 10 LB. | oo a j i TOTAL 1859 BAGRT 80LB EACH INSTRUCTIONS EXHIBIT 3 Premix000131 November 16 1973 Supercedes Oct. 11 73 formula - MIAMI PLANT FORMULA CEMCOTE M a So DESCRIPTION OF PRODUCT Dry mix powdered paint which is to be combined with water to produce a smooth textured readily applied coating for all masonry surfaces FORMULA Raw Materials # Marble . White Cement Finish Lime Zinc Stearate . Salt ee Attagel 50 Polyvinyl alcohol Function . R.M. Spec No. Filler 5 Strengthener 8 Plasticizer 10 Water proofing | 53 AiErntrainment 4-6 Accelerate Set : 57 Bulking Agent- Slip 16 Adhesive 28 % 36.17 36.17 42.25 16.12 0.64 3.22 0.64 0.96 x batch see over WORKING CONSISTENCY Fmpl Refer to plant testing procedure No. 1 T. C. Specifications Maximum Minimum | Average - 50 36 45 WORKING PROPERTIES - Refer to testing procedure No. 8 COLOR White - Colored Shall match standard white sample - Shall match color for said sample see color formulas * Denotes Change EXHIBIT 3 Premix000132 | 7.1- 8 73 PRODUCT WAL TEX ; MATERIAL 7 POUNDS Laine Tacces Laine Laine BAGS GALLON # Marble 300 | Concentrate Concentrate Concentrate 128 L a Asb TRE39 TRE39 Staramic Staramic Staramic Staramic 330 400 _[ HERMA9N.6 1/18/17 o 125 | Stripe | STAR 125 out . Stripe Huber 90 clay | 200 BENT a| Talc 325 700 | 9 Marble Marble 2000 | : Attagel Attagel Attagel 5050 900 Tilanox RANT | 1500 Colloids 513 DD | ' | mimites Mix together together . for without 1 addingotheringredi E INSTRUCTIONS EXHIBIT 3 i. ~~ Premix000133 _ WALLTEX WALTEX - 0502 009 SLT . OST MASTER MASTER BATCH FORMULATION FORMULATION FORMULATION = TESE bE LO0xIWA} PRODUCT d-yeJUH Movs 4M PERCENT PERCENT 100 TT 20 . SHOVSOZ MATERIAL ' 57.81 17 382040 Spinod90CLAY 00st ogor 17.60 17.60 009 St 875 LET 382040 888-90 5.02 | =f 90CLAY . 4.18 4.18 9 7RF9 [OL 7RF9 ASBESTOS te. | | 3882040 8888888-8990 Spunod GOT ATAGEL 50 9 38 006s Ste 0.75 0.75 00g SE | Ot oT 8 8 8 8-89 0 GTUVN CMC cua | |. ATURVI GLUE 89 dt 2.12 2.12 GLUE RED 513 . 106 -| 6# GF JO FTIA COLLOIDS | | - a A SOLHISY -, DHISM te*Zg ye 0.25 0.25 90 4993 4993 20 0&0 G2"0 (LHDIGM OT AG =f TVOUT Wd 7 HDIM _ ADHESIV GUATSNYWOINVLDE SEPARTE ASBESTOS TdIULS GRIND a HUNTS - WITH Cig ASBESTOS MARBLE W OTv SalOTION ADHESIVES SOLSEaSY WOTNVEL HETOMG TLvags THOVLY OF S26 .WanH Hogs ea Cay ONTHD LONdoUd uctober 11 1973 Supercedaelsl previous formulas MIAMI PLANT FORMULAFORMULA WALLTEX 49 DESCRIPTION OF PRODUCT An animal glue and starch based wall texture FORMULA Raw Materials # Marble 325 Tals Huber 90 Clay Starch 330 Asbestos 7RF9 Titanium Attagel 50 ; CMC - 7MT . Red Stripe Glue Colloids 513D Dowicide A A ' Function R.M. Spec No. Filler 7 Filler _ Filler Plasticizer Hardener Bulking Agent . Whiting Bulking Agent Plasticizer Adhesion Adhesion Thickener Fungicide 5 17 6720 6720 6720 6720 6720 16 000 000 34 IN % 57.81 17.60 batch 5.02 4.18 10.06 1.26 0.75 | 0.75 2.12 0.20 . 0.25' WORKING CONSISTENCY - Refer to plant testing procedure No. 1 T.C. Specifications Maximum Minimum Average WORKING PROPERTIES - Refer to plant testing proceduNroe. 3 CRACK RESISTANCE - Refer to plant testing procedure No. 4 BONDING PROPERTIES - Refer to plant testing procedure No. 5 PRODUCTION NOTE " a Grind Titanium with equal weight of # Marble separate adhesives from Asbestos with # Marble EXHIBIT 3 Premix000135 November 16 1973 Supercedes Oct. 11 oi 73 formula MIAMI PLANT FORMULA - DESCRIPTION OF PRODUCT WALLTEX 49 4 An animal glue and starch based wall texture FORMULA Raw Materials * # Marble 325 Talc Huber 90 Clay nr Starch 330 WP angie angieangie Asbestos 7RFO - a (aes G Attagel 50 CMC - 7MT Red Stripe Glue Colloids 513D 4 * Vanicid51eZ _ Function Filler Filler Filler Plasticizer Hardener - Bulking Agent Bulking Agent Plasticizer Adhesion Adhesion Thickener Fungicide Spec No. 57 17 26 31 12 16 16 38 40 .3.4 { 50 2 Me yt % batch 59.17-64.20 59.17-64.20 59.17-659.17-642045.9.127-640.20 17.60 5.02 4.18 10.06-503 . 0.75 0.75 2.12 0.20 0.15 ~ WORKING CONSISTENCY - Refer to plant testing procedure No. 1 T.C. Specifications Specifications Maximum Minimum Average 72 54 66 WORKING PROPERTIES 1 Refer to plant testing procedure No. 3 CRACK RESISTANCE - Refer to plant testing procedure No. 4 BONDING PROPERTIES - Refer to plant testing procedure No. 5 * Denotes Change EXHIBIT 3 Premix000136 Company Company emagia Marble Tanox | ulf CoastChem CoastChem CoastChem excules : LLOIDS of CaRyling CaRyling H. Ross 7 | | ht Tak | Haywo b RClay Co. | taley 14fg | iBling Co. eorgia Marble Walltex - Raw Material Price List Material Material # MarbleMarble Titanox A.W.D. LBS 300LBS 300LBS Price PER 1b 4011038 4011038 523 LBS .24 Attagel # 50 7MT LBS 30 LBS - .0995 .47 Colloids 513DD _ | DOWGIDER DOWGIDER 8LBS 10lbs 10lbs .3881 , 7740 Tale 325 700 LB3 .03662 Asbestos 7RF9Q 7RF9Q 400LBS 400LBS .045337 .045337 Huber Clay 90 200 LBS StaRamic Starch 166 LBS RED StripE FOOD ADHESIVE 84 LIS .0644 .1761 4150 # Marble 20004BS 3978 3978 2.731 2.731 PRICEPRICEPERI 3.31 12.00 299 14.10 3.10 7.74 2563 18.13 12.88 | 29.23 29.23 34.86 22.08 ; 186.05 Total Lbs per Batch | total bags p-- RBatch | Total lbs per Bag 3978 Uss 79.6 50lbs 50lbs i Total PRICE PER Bag = 2.34 EXHIBIT 3 Premix000137 October 6 1969 WALLTEX - DRY SPRAY - Small Mixer 20-1 1/2 15 1/2 2-1 1 1/2 1155-1 bags bag lbs bag lbs bag lb. lbs 10 Georgia Marble Attagel 50 Vinac 251 Vinol 522 | 1 GEPON AC 200 or 4K Mica Orvis MIXING INSTRUCTIONS: After everything is in batch- mix for at least 5 minutes 45 lbs per bag 26 bags per mix , EXHIBIT 3 000138 2.7 ff WALLTEX WALLTEX Ibs fe ' HEDMAN HEDMAN STARCH STARCH / i ( 400- 125 125 BENTONITE pe BENTONITEBENTONITE BENTONITE 200 3 20 MARBLERY MARBLERYMARBLERY _ Zooo fo - -- --...-- 7MT Colloids513DD Col oids513D Colloids513DD Coloids513D Colloids513DD Coloids513D 256 Dowicide Dowicide A 4 Na \ . a. So 300=f ; Ye a <= 12 , wn mixes | SO | oe , a oe caren en a we Need Need 4. Bean Bean Concentrale Concentrale Concentrale per per batch batch . EXHIBIT 3 Premix000139 Methocell Methocell 15000 i AVtItNaOgLel5252 22 Asbestine Fiber 2 Iceburg Iceburg Clay 10 Marble Asbestos Asbestos Asbestos JTFI 1 Pound 38 Pounds 40 Pounds or 1'BA91'BA9 ww | iBAg iBAg 20 Bags BAg BAg _ 2 MARBLECRETE SPRAY MATERIAL "7 POUNDS DATEJuly 13 1972 - BAGS | GALLONS | White Cement 1410 . | 15 SA SA Marble A Marble _ 1600 | 1600 | 20 20 Reg Lime 850 17 | Concentrate Zinc Stearate 31 : 50 2 . 2 Emathlite | | 50 Air Ent Lime 400 Sand 3000 1 8 | 30 per MR Total Weight = Bag at 80 Makes 112 bags & 31 8991 For color in small mixer use batch PMO EXHIBIT 3 Premix000141 PRODUCT MARBLECRETE SPRAY MATERIAL POUNDS White Cement SA SA Marble PA PA Marble 1410 _ 1600 1600 Reg Lime Concentrate 850 31 Zinc Stearate 50 Emathlite Emathlite Air Ent Lime 50 400 Sand 3000 _ DATEJuly 13 1972 BAGS GALLONS 15 20 20 17 2 2 1 8 per MR 30 Total Weight Bag at 80 Makes 112 bags & 31 8991 For color in small mixer use 3 batch PMO EXHIBIT 3 Premix000142 PRODUCT PLANT FORMULA MARBLECRETS th For Marion Mixer MATERIAL - POUNDS | - AT BASS White Cement Concentrate Finish Lime Premix - X 1880 146 800 1600 _ 20 | 4 , . 16 16 July 13 1972 GALLONS Air Ent Lime Sand | 400 5050 8 50 Total Weight Bag at 80 # Makes 123 bags & 36 9876 | For Color figure for 120 Bags Make Oyster White only this mixer PMO , EXHIBIT 3 . ; Premix000143 WORK UMLANDU PLANET ENTER PLANT FORMULA ORLANDO SHET SHET PREMIX - MOBLETITME OBLETITE C TURING CO PLANT PLANT ( ra LABORATORY FILE # . PRODUCT NAME MARBLECRETE SPRAY DATE OKIED BY COMMENTS : MATERIAL MATERIAL MATERIAL GAL LBS LBS UNIT CUST . _ White Cement Marble PA Marble - Reg Lime ' 1410 : 1600 1600 . - 850 Concentrate 31 1/4 , Zinc Sterate -_1 50 Emethelite Air Entraining Lime Sand __ Totals 50 400 3000 8991 0201 0105 .0105 .0236 .0236 .0726 .0726 .03420 .0160 .0241 .0057 __ Cost of Bag Labor Cost TOTAL DIRECT COST EX # REPLACED P 2.45 DATE REPLACED 4/7/72 TOTAL COST Batch BATCH SIZE Plant 112 LBS BAGS r # 80 BAGS .. 28.3410 | 15 16.80 ine, 20 16.80 a 20 myles 20.06 ae 17 _ 2.2687 17.10 .80 9.64 it! yon I oo 1 17.10 pr 128.9097 128.9097 1.1510 1216 .2216 1.4942 $ | r i! |itl ". 2 25 50 bag or 2sx 1 8_ 30 4 UF TOTALS 8991 MIXING INSTRUCTIONS . - a 0 .3093 SHETSBLETITE TER PLANT FORMULA WORK SHETSBLETITE SHETSBLETITE . MANUFACTURING CO ORLANDO PLANT ae Ley - LABORATORY FILE # PRODUCT NAME DATE OK'ED BY CONCENTRATE FOR , MARBLECRETE EX # REPLACED DATE REPLACED 4/1/72 COMMENTS : MATERIAL | Fibre 2 Zinc Sterate _ + --.... LBS GAL NIT COST 15 375 10 250 .0398 .3420 y- |= TOTAL COST om BARCH SIZE Plant 26 bags Batch LBS BAGS 36 1/2 ba 14.9250 |: Pg 7 & 24 wok - 85.50 - 5- 3,000 300 .0160 | = 4.80 - 6 = Natrosol HXR 24 302 .82 19.68 son - Totals 949949 124.9050 CONCENTRATE FOR 92 BAG BATCH OF MARBLECRETE {i 2 Fibre . 30 2 ; an : s Sterate 45 Emathlite _ 34 1/2 mo, | Material Cost Per 36 1/2 sx Cost Bag TOTAL DIRECT COST * ; ; TOTALS MIXING INSTRUCTIONS : a * 5 NOTIFY LAB OF ACT COSU T PEA R IL B 2 - 4.8040 _. ; .1145 4.9185 OR t ul | | i { | ; 1347 LB. . | , MARBLETITE MANUFACTUR ENTER PLANT FORMULA WORK SHET FREMIX - FREMIX | po | LABORATORY FILE # PRODUCT . NAME MARBLEGRETE | | DATE _ | ZA OK'ED BY ry ^' . ee 2b cde all COMMENTS 24 | INIT INIT COST MATERIAL LBS GAL EX # REPLACED DATE REPLACED / 2.25 4/1/72 4/1/72 TOTAL . COST Batch BARCH SIZE Plant Batch LBS _ BAGS = 80 Bags White Cement . | 1880 .0201 37.7880 | 20 . 4 _ * 146 .1347 19.6662 __- Concentrate ___ 3 16 800 0236 18.88 Lime _ : Finished 10.08 yi 12 nolo .0105 : 960 SA Marble Air Entraing Lime PA Marble Sand 400 640 _ 5050 .0241 .0105 | .0057 --- 9..64 8 it a -6.72 28.7850 its: 8 8 50 1/2 OYSTER WHITE FOR COLOR FIGURE FOR 120 BAG a MAKE OYSTER ONLY THIS TTR MIXER ! | eee 131.5562 131.5562 Totals 9876 1.0652 | Per 80 st __ Material Cost a 1022 Cost Bag .2216 it _.Jabor Cost | ; TOTAL DIRECT DIRECT COST . . 1.3890 f \j _ ' a TOTALSTOTALS . 9876 . . MIXING : INSTRUCTIONS INSTRUCTIONS i . - : O .3093 an ' i 4 \ , ie ar y - Caan oe , i+ a ; 7. ea wot, : . * . a FORMULA WORK , ENTER PLANT FORMULA WORK SHET MARBLETITE MANUFACTURING CO a ORLANDO PLANT hy Ay LABORATORY FILE # PRODUCT NAME . DATE MARBLESPRAY ; EX # REPLACED 7 DATE REPLACED = 4/7/72 os OKED BY . : COMMENTS : __ 4 BATCH SIZE 65 Batch Plant Batch a MATERIAL | White Cement LBS GAL INIT COST TOTAL COST LBS BAGS 75 7| , 1128 0201 22.6728 12 7 | yt | Finish Lime Fibre # ; | Zinc Sterate * | 400 30 28 .0236 | | .0398 .3420 - 758 | | Blue Color Concentrate } 3/4 | 1742b _ Titanium 901 AWD 1979 .2450 9.44 1940 9.5760 1484 9800 _ a ble tf A ; oh ie 1: i 8 __ | Air Entraining Lime 200 : 40/200 Marble | Sand 2000 | 2200 .0241 .0094 .0057 4.82 18.80 12.54 Totals 5990 3.4 80.1712 4 I 22 22 Material Cost of 75 sx : Cost of Bag .. ; 1.0037 .1216 Labor Cost i 2216 ; TOTAL DIRECT COST 1.3469 1.3469 : T TOTALS 5990 4 MIXING INSTRUCTIONS: . 4 n. . ; , rast cr 42 e ** NOTIFY OF ACTUAL COST PER LB. ~ : ao x ed . , + , vo tad ~ > aE = ae rt "= aad awe - eee ne . EXHIBIT ay. . oe _ - digg ro a wr ow cgtots oe Bre x VT EXHIBIT RD 2 ental ie ad we Moos -* 1 . MER Pt if g ormy2) ei! a ir RE Sige I RU a. Rasage | . 4 7 to ENTER PLANT FORMULA WORK SHETSHET : - MARBLMEAMRARBTLETITEBLIETTITEE MANUFACTURING CO ORLANDO PLANT yo, mo LABORATORY FILE # EX # PRODUCT NAME DATE ; MARRFL OR E MARRC LECR RETE E ST PRE AYREPLACED DATE REPLACED ___. OKED OKED BY COMMENTS MATERIAL RCHTY _ASP 170 Emethelite INIT COST LBS GAL 3121/2 . 750 500 1025 .0669 ..0160 ..0160 BATCH SIZE bage 1/2 # Plant Batch TOTAL COST IBS . BAGS 31 # , 32.0312 50.1750 i| { _ 12 1 1/2 /2 ened 15 . 8.00 _ 10 Total 1584 1/2 . Material 31 1/2 # sx Bag Cost otal Direct Cost 108.2462 2.1649 .1145 2.2794 a aaa byt OR _ .0726 PER LB. _ , Drepees ye en TOTALS 1584 1/2 = INSTRUCTIONS : aw i ~ Lj ii Ly: _ i: q rl | i 1 ; iq \i n MARBLESPRAY MATERIAL POUNDS ) White Cement 1128 Finish Lime 400 Per EMR This date 7/23/71 DATE BAGS July 13 1972 GALLONS 12 8 Fibre # 2 30 _ Zinc Stearate 28 Blue Color Conc 758 3/4 AWD Air Ent Lime Premix 4 1t 200 2000 he 20 Sand 2200 22 Total Weight _ Bag at 5990 3/4 .75 Makes 79 bags plus 65 3/4 lbs Small mixer as is ~ ~ Large Marion Mixer use twice as much PMO EXHIBIT 3 Premix000149 * lrssiD EERE la dG Eb OM INTER PLANT FORMULA WORK SHEET 7 MIAMI 75th AVENUE i 3009 ; MIAMI FLORIDA 33122 ; LABORATORY FILE # ,; EX # % 26.5 PRODUCT NAMEMARBLECRETE SPRAY ee DATE '. REPLACED S _ 2.45 DATE REPLACED 4/1/72 | OK'ED BY COMMENTS : MATERIAL - LBS GAL UNIT COST TOTAL COST Plant BARCH 59.16 sx LBS BAGS 80 bag White Cement . 752 .0194 14.5888 | 8 - SA Marble *_| 800 .0109 8.72 = 10 PA Marble | .800 .0109 8.72 ;: H 10 Sand 1600 0072 11.52 at 16 7 Finish Lime 500 .0244 12.20 10 Lime Concentrate 200 .02496 4.9920 | & 84 _{ .1409 11.8356 2 : Me Totals 4736 72.5764 72.57672.45764 Material Cost Per 80 sx 1.2301 Cost of Bag PM A .1022 | Labor Cost - .1917 TOTAL DIRECT COST _ 1.5240 TOTALS 4736 , MIXING INSTRUCTIONS 0 | is . (bg . * oe scree-A)SESKsE SI Rate 5 kasd MIAN PLM AVENUE ; INTER PLANT FORMULA WORK SHET SHET 3009 N. W. 75th MIAMI FLORIDA 33122 LABORATORY FILE # EX # 24.4 PRODUCT NAME MARBLECRETE : " DATE REPLACED P 2.25 DATE REPLACED 4/1/72 OKED BY COMMENTS : MATERIAL _ LBS GAL UNIT COST TOTAL COST BATCH SIZE Plant 61.4 bags Batch LBS BAGS 80 bag Sand . | 2500 | .0072 18.00 : 25 i XO Marble , 800 .0113 9.04 8_ White Cement - Finish Lime 940 400 .0194 .0244 18.2360 9.76 | +1 G yy 10 8 E Lime Concentrate 200 : 73 Totals ___. _ Material Cost per 80 sx Cost of Bag PM A _ Labor Cost 4913 : TOTAL DIRECT COST 02496 .1189 4.9920 8.6797 68.7077 1.1263 .1022 .1917 ; 1.4202 4 2 i Ja TOTALS 4913 MIXING : INSTRUCTIONS tad te we, ENTER PLANT FORMULA WORK SHET SHET Fe, Te LOTT) ~omtee ORLANDO ORLANDO ORLANDO ORLANDO ORLANDO PLA THENS THENS CO ay * LABORATORY FILE # ; PRODUCT NAME MARBLECRETE DATE OKIED OKIED BY COMMENTS 2/2 MATERIAL MATERIAL 135. " GAL NIT COST White Cement ___ Concentrate Finished Lime SA Marble 1880 i 146 800 960 0201 1347 .0236 .0105 EX # REPLACED DATE REPLACED P 2.25 4/1/72 Patcl BARCH SIZE Plant Patcl TOTAL COST _ LBS . BACL 80 Bags 1 If 37.7880 4! 20 at 19.6662 4 13.88 10.08 7 16 12 Air Entraing Lime PA Marble Sand 400 640 5050 0241 .0105 .0057 FOR COLOR FIGURE FOR 120 BAG MAKE OYSTER 9.649.64 6.72 . 3i 28.7850 1) THIS WHITE WHITE ONLY THIS MIXER 001 8 50 1/2 Totals MaterCi ostaPl er 80 sz 9876 _ Cost of Bag __ Labor Cost TOTAL DIRECT COST . 131.5562 TTT a 1.0652 |i 1022 a j | .2216 Hae 1 qt 1.3890 |', eT : TOTALS 9876 F; MIXING INSTRUCTIONS: a H .3093 NOTIFY LAB OF ACTUAL COST PER IB EXHIBIT 3 an ' t { q ~ 000152 tee =: ~~ _TER PLANT FORTULA FORTULA WORK IFL PR tre LABORATORY LABORATORY LABORATORY FILE # / EX fi DATE DATE REPLACED 4/2172 4/2172 OKED OKED BY COMMENTS : MATERIAL White Cement Finish Lime LB5 GAL MIT COST 1128 400 .0201 .0236 .0236 TOTAL COST os ARCH SIZE PlanBatch PlanBatch PlanBatch 35 . SAGS 22.6728 |; 12 9.44 2 Fibre 2 Zinc Sterate 758 Blue Color Concentrate _ Titanium 901 Air Entraining Lime 30 28 3/4 4 200 40/200 Marble 2000 Sand | 2200 Totals 5990 3/4 . : Material Cost of 75 sx Cost Bag Labor Cost TOTAL DIRECT COST .0398 .3420 .3420 .1940 - 9.5760 .1979 .2450 .0241 .0094 .0057 1484 .9800 4.82 18.80 12.54 80.1712 1.0037 1216 .2216 1.3469 . ~ _ : i 4 it 20 || 22 Ly ! i ji! ft i i i a Pay. 3# ee & TOTALS 5990 3/4 MIXING INSTRUCTIONS . H . = .3093 NOTIFY LAB OF ACTUAL COST PER LB. aM Re " -EXHIBIT -EXHIBIT 3 a { . Hantak x000153 0 ema rae GRLANDGRLOANDO FUNT _CER PLANT FORMULA WORK CHEIT CHEIT "KLA30 Punk ) LABORATORY FILE # a PRODUCT PRODUCT NAME CONCENTRATE FOR MARBLECRETE DATE EX # REPLACED DATE REPLACED 4/1/72 OKED OKED BY CONTENTS : MATERIAL Fibre 2 Zinc Sterate ___ VMP 3,000 LBS GAL INIT COST 15 . 375 10 250 12 300 .0398 .3420 .0160 TOTILL COST BANCH SIZE 26 bags Plant Patel IBS BAGS 36 1/2 bat 14.9250 14.9250 4) 5 85.50 & 24 5 _- _ 4.80 | 24 .82 19.68 - Natrosol HXR 30z Totals 30z 124.9050 CONCENTRATE FOR 92 BAG BATCH OF MARBLECRETE riot |i a. Zinc Sterate Emathlite mie 45 34 1/2 Material Cost Per 36 2 sx \ | of Cost Bag TOTAL DIRECT COST a | t lt Lo 4.8040 LL 1145 ti 4.9185 I |i}. OR .1347| .1347 PER LB. ili t i iz _. i ee TOTALS MIXING INSTRUCTIONS: NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 e Premix000154 - oO LABORATORY FILE # INTER PLANT FORMULA WORK SHEIT PREMIX MARBLETITE MANYFACTURING CO ORLANDO PLANT EX # PRODUCT NAME DATE OK'ED BY CONCENTRATE FOR MARBLECRETE SPRAV REPLACED DATE REPLACED COMENTS : MATERIAL - RCHTX ASP 170 LBS GAL NIT COST 312 1/2 * 750 1025 0669 TOTAL COST BARCH SIZE 50 bags 9 1/2 # LBS BAGS 31 1 # 0312 50.1750 ! ; i 6 12 / % 15 ast Emethelite 500 _Natrosol _ 22 | Total __ 1584 1/2 Z Material Cost Per 1/2 ! #sx #sx Bag Cost. ~ Stal Direct Cost ..0160 ..0160 .82 8.00 18.04 108.2462 2.1649 .1145 2.2794 tt 10 | ak . | | OR 0726 PER LB. TOTALS 1584 1/2 ga MIXING INSTRUCTIONS , Pa - NOTIFY LAB OF ACTUAL COST PER LB. EXHIBIT 3 { t i - Hantak Premix000155 Premix000155 INTER PLANT FORMULA WORK SHET MARBLETITE MANUFACTURING CO ORLANDO PLANT r LABORATORY FILE # 4 Fd PRODUCT NAME DATE MARRLESERAY EX # : REPLACED DATE REPLACED 4/1/72 4/1/72 ye OK'ED BY COMMENTS : MATERIAL LBS GAL UNIT COST TOTAL COST Batch BARCH SIZE 79 65 # Plant Batch LBS BAGS 7575 White Cement ; Finish Lime Fibre 2 Zinc Sterate ee 758 Blue Color Concentrate 1128 400 30 " 28 3/4 Titanium 901 4 Air Entraining Lime 40/200 Marble Sand 200 2000 2200 Totals 5990 3.4 Material Cost of 75 sx Cost of Bag Labor Cost TOTAL DIRECT COST 0201 .0236 .0398 .3420 .3420 .1979 .2450 0241 .0094 .0057 22.6728 9.44 .1940 9.5760 . .1484 .9800 4.82 18.80 12.54 __| 80.1712 1.0037 .1216 .2216 1.3469 ti i Tt air a a li 7 | . iF | 12 8 a 4 20 " fof- i. 7 TOTALS 5990 MIXING INSTRUCTIONS: aa ; H .3093 NOTIFY LAB OF ACTUAL COST PER LB. rok A, ves oa ceed eee Tse gh EXHIBIT i ewes Premix000156 ENTER OPRLLANATNDFOORPMLUALNATWORK SHEITSHEIT PREMIXPREMIX - MARBLETITE MANUFACTURING CO ORLANDO PLANT ay . Od LABORATORY FILE # . PRODUCT NAME MARBLECRETE SPRAY DATE OKED OKED BY COMMENTS : MATERIAL LBS GAL I.NIT COST White Cement Marble _M_a PArble Reg Lime Concentrate Zinc Sterate Emethelite Air Entraining Lime Sand Totals 1410 1600 1600 850 31 1/4 50 50 400 3000 8991 0201 0105 .0105 .0236 .0726 .03420 .0160 .0241 .0057 Material Per 80 _ Cost Bag : t Labor Cost _ TOTAL DIRECT COST EX # REPLACED 2.45 DATE REPLACED 4/1/72 TOTAL COST BAICH SIZE 112 Plant Batch LBS BAGS # 80 BAGS . 28.3410 16.80 | 7 bee 16.80 20.06 a i] . * i ne 2.2687 17.10 ii! yo ! .80 9.64 17.10 15 20 20 17 at. .. 2 25 50 bag or 2sx 1 | 8 30 128.9097 1.1510 | is 1216 | .2216 i | 1.4942 . pil 77 | 4 TOTALS 3 8991 MIXING INSTRUCTIONS H .3093 NOTIFY LAB OF ACTUAL COST PER LB. i { H EXHIBIT 3 ~ - Premix000157 -\ PRODUCT CONCENTRATE FOR MARBLECRETE MATERIAL POUNDS : DATE - MAGS July 13 1972 GALLONS Fiber # 375 : 7 & 25 | Zinc Stearate 250 _ ' 10 V.M.P. #Emathlite - 300 6 Total Weight 925 Bag At 37 Makes 25 bags per batch CONCENTRATE FOR ONE BATCH Fiber # 15 Zinc Stearate . Emathlite VMP 3,000 10 ; 12 Total Weight 37 PMO EXHIBIT 3 Premix000158 PRODUCT MATERIAL AWD Titanox 9 NOS ASP 170 _7 Emathlite . PLANT FORMULA POUNDS DATE -{ - BAGS | | a 100 GALLONS _ 212 4 & 12 750 15 500 10 4/2/71 : Total Weight - 1562.5 Bag at 31 4/2/71 Makes 50 bags per batch CONCENTRATE PER BATCH . AWD Titanox Makes {% sxs 4 # NCS ASP 170 . 8.5 , 30 Emathlite 20 Totla Weight 62.5 PMO EXHIBIT 3 Prernix000159 MATERIAL White Cement | Premix - X Lime Concentrate Air Ent Lime Sand PLANT FORMULA POUNDS ; | 940 | | 800 400 .73 200 2500 | 10 8 8 2 4 25 | Total Weight . = Bag at 80 # Makes 61.41 Bags 4913 For Color figure 60 Bag Batch Changed to Air Ent Lime 7/16/71 per R. CAKEONS 1 Bag BatchBatch 15.3 lbs 13.0 lbs 6.5 lbs 19 028 3.25 lbs 40.7 lbs 80 lbs PMO EXHIBIT 3 Premix000160 oe spunod LOXWues 08 foLva oogTt 00ST 2697 GTt ye | | | TOPCETOPCOTE 14 TOPCOTE O4 MATERIAL eS gL PERCENT gt Hobvd $puno WL6Z 002 ae 2600 MOVs Octgoes Te Tt te Fy ie e 2444 EMATHLITE | bf ad Hoavasprnod 0092 oo9e YZ GAT Ce 1967 744 ee WOLVE | | || OVS EAG 2z 9% 92 Oz GALS OOTsyoes vn _ TNZOURETHOTaMte The HL GO % OF 64 T Za | WoW Tw"e_t Ghodon TVINSL ATGaYN C RAREO WNL BLYUVELS TTLLE TN avs ZO MCRL HSINdZ Ors VNG ctondu _ . Z9 LoxWwiald-NpIueH FORMULATION 0 008 8 WOTWa Spurod Oost MASTER MASTER wonilal FORMULATION . TOPCOTE TOPCOTE 0-14 OL Syoes at PERCENT aL MATERIAL YORG | HOLVa Spunod OTE OtE HOS 608 2600 APE SyoesNOWS % 2444 CTE Te TE Oct STEAR < spanod Aate HOnva 1.55 1.55 wre cEt " 125 LIGiHXa || 7944 NOLVE MOVs Se Oe 92 Oz 7344 Walbs OOt Syoes vw || GNOUEdL2HDLdHMee vara AL*OC Gore AtOg corr FT=0 TitESOT TVURLV TE aLOdOL FaIN Teo Gil THE ZO BOTAN ASIid Z WWa LOACoud e October 11 1973 e Supercedes all previous formulas MIAMI PLANT FORMULA TOPCOTE 14 DESCRIPTION OF PRODUCT . of A mix aggregate and c-ement fo- r use on patios and pool decks FORMULA . Raw Material Sand OZ Marble . White Cement Finish Lime Zinc Stearate Emathlite Function , Aggregate Aggregate Strengthener Strengthener Water Proofing Workability R.M. Spec No. 250022 250022 250022 .10 250022 250022 250022 % 32.71 | 32.71 30.74 2.05 0.24 1.55 batch - WORKING CONSISTENCY T. C. Specifications Refer to plant Maximum . testing procedure No. 1 Minimum Average EXHIBIT 3 Premix000163 16 February 11 1974 Supercedes November 1973 formula _ _ ORLANDO PLANT FORMULA ACOUSTEX 0-48 DESCRIPTION OF PRODUCT A vinyl based ceiling spray with perlite as aggregate FORMULA Raw Materials Attagel 50 a Methocel 228 Polyvinyl Alcohol Asbestos SG210 Fiber 2 9 Marble Perlite P8OF Mica Zinc Stearate Soap Function Bulking Agent Plasticizer Thickener Adhesive Bulking Filler Agent Bulking Agent Filler Aggregate Slip Water Proofing Plasticizer R.M. Spec No. 010003 010003 28 010003 044 044 044 / moo moo : % 1.61 0.32 2.58 0.98 35.47 3232..2381 3.22 0.06 0.03 Lbs batch WORKING CONSISTENCY - Refer to plant testing procedure No. 1 WORKING PROPERTIES - Refer to plant testing procedure No. 3 CRACK RESISTANCE - Refer to plant testing procedure No. 4 BONDING PROPERTIES m Refer to plant testing procedure No. 5 VINYL SPOT TEST - Refer to plant testing procedure No. 2 EXHIBIT 3 Hantak Premix000165 ACOUSTEXan ACOUSTEX 0-48 0-48 Q9LOXIWA! 4-ye}HE aM MOVS : O4 SHOeS MATERIAL 50 ALCOHOL ALCOHL : SG210 . sao . OST es 550 S| FIBER _ HoOdva spunod ~ 364 23.48 GZ oF ST 14 005 3.64 S 0 G* | 64ST < LIatHxa P8OF HOVS = SOAP SyoesOOT & Ti Tr Or SAT . - 1549.5 LNaOugdDLEOLEM T9T ZE*O BSZ 36.70 LAGE TE*SE Bre SOE <00 AG | Si-O Sez TOH'TY OTZDS XHLSOo OS# IANTAL ef TIGUVA ML VOIM TWINSLVW THOVLY THOLEW 10d SOLEISY UaLy 6# Tadd d0gd dOs LONGd ACOUSTEX Go 0-480-48 Z9LOXIWS . 4-42: ueHy AM MOVE OZs70RH MATERIAL YORS HOLVE Spuned ALCOHOL | O2TSyVeEs MARBLE HOLVEspunod 500 S* < $ 0 23.48 GT 23.48 OF 0S ay 14 364 6ST 364 ee LIGHXA} | 5050 - MICA WOWS = . SOAP -oNet Syoes TT onSIT Ta ' SOAP | _ INaoUadDHTaM TOT eeto Pyare 36.0 LA* GE Tee Bee 1549.5 <% <0 O AG . TANL'IO< XYELSnoy, TOH'TY Si-O OS# S.22 OTZDS TWINED THDVELY LTHEOHN SOLHESY eUaHLe T6aN ATHLGLd dVoOgIdM dvos donud formula 16 February 11 1974 Supercedes November 1973 ORLANDO PLANT FORMULA ACOUSTEX 0-48 -- --,, -- -- -- --,, -- ------,, -- -- DESCRIPTION OF PRODUCT A vinyl based ceiling spray with perlite as aggregate | | FORMULA Raw Materials Function Attagel 50 - Bulking Agent Plasticizer Methocel 228 Thickener Polyvinyl Alcohol Asbestos SG210 Fiber 2 Adhesive Bulking Agent Bulking # Marble Perlite P8OF Mica Bulking Agent Filler Aggregate Slip Stearate Zinc wwe ws Soap * Water Proofing ee Plasticizer- R.M. . Spec No. % 0.32 28 2.58 13 0.98 60 | 35.47 5 1 32.31 41 .3.22 - 53 0.06 58 7 yawn -0.03 batch WORKING CONSISTENCY ~- Refer to plant testing procedure No. 1 1 WORKING PROPERTIES . { } plant Refer to F testing proceduNroe. 3 F F CRACK plant ae hee RESISTANCE - Refer to ctw i testing procedure No. 4 . 1 BONDING PROPERTIES - Refer to plant testing procedure No. 5 : VINYL SPOT TEST - Refer to plant testing procedure No. 2 ? EXHIBIT 3 Premix000168 February 11 1974 Supercedes November 16 1973 formula . ORLANDO PLANT FORMULA r H i i t 4d DESCRIPTION OF PRODUCT A Lime Based ceiling texture containing perlite as the aggregate FORMULA . Raw Material Perlite Regular Finish Lime Asbestos SG210 Vinyl 523 Keenes Cement . Function Spec No. Aggregate 1 Plasticizer Strengthener Bulking Agent 10 ~ 13 Adhesive ; 28 Setting Quality 42 ; % 32.19 - 60.29 5.57 1.11 0.84 . batch WORKING CONSISTENCY - Refer to plant testing procedure No. 1 T. C. Specifications . Maximum 108 Minimum 90 Average 100 - VINYL SPOT TEST - Refer to plant testing procedure No. 2 WORKING PROPERTIES - Refer to plant testing procedure No. 5 tone Product shall be very white in amount of aggregate and contain a generous EXHIBIT 3 . Premix000169 PREMIX MARBLETITE PRODUCT FORMULA LOCATION PRODUCT NAME AND NUMBER EFFECTIVE DATE | 8/2/77 Woncate Woncate Woncate 3m 8/2/77 _ PRODUCTION DATE DESCRIPTION OF PRODUCT 7016 5016 5016 = 2 - > " fl - sand i O a Ox FORMULA RAW MATERIALS LIME MOULDING MOULDING MOULDING GAUGING GAUGING 5 # MARBLE MARBLE . FUNCTION PLAS --- ~ GYP FILLERS FILLERS FILLERS FILLERS FILLERS FILLERS FILLERS R.M. . SPEC NO % 165016 1100.1 11001.1010.1 1100,15 1100,111050,15 165015 165015 165015 165015 - 5050070 5050070 5050070 5050070 IBS BATCH oleeee 15 bi 7- bngiy. 10.16 10.16 ' 7-142210162 7-142210162 7-142210162 7-142210162 23402 23402 15 WORKING CONSISTENCY T.C. SPECIFICATIONS| ' TENSILEESTRENGTH TEST WORKING PROPERTIES COLOR BRABENDER VISCOSITY CRACK RESISTANCE BONDING PROPERTIES VINYL SPOT TEST MAXIMUM MINIMUM AVERAGE PLANT MANAGER QUALITY CONTROL MGR Product Development EXHIBIT 3 PRESIDENT PRESIDENT Premix000170 LZ0xIWwaig-ye}uY fe MarblecrteMarblecrte PRODUCT 4a WOVS ve , MATERIAL Asbestos OLSores ; Emathlites Stearte |" WOYS OT syses : , NOLVIWHOE HOLVASpunod 009 ose OSeT ote. < HOLVE MOV|S " | LialHxXa : Gals OOT syoes Oz (OT! Ge VN - 6-6 4| eqrueog uANROUEdLHOIGH ^'o2e. C:SCLE*ST 009 1a | - eqmoTaey EVIGELoles pyereg SeTAT soaseqsy outz em == Vi LONCONd February 11 1974 Supercedes November 16 1973 formula ORLANDO PLANT FORMULA MARBLECRETE 0 6 DESCRIPTION OF PRODUCT A mixed white domestic portland cement and marble silica aggregate composition which includes a water proofing producing a durable and weather proof exterior stucco finish FORMULA Raw Materials White Cement Finish Lime XO Marble E Lime Sand Asbestos SG210 c Zinc Stearate c Emathlite c Function Strengthener Strengthener Plasticizer Aggregate Plasticizer Aggregate Bulking Agent Water Proofing Plasticizer R.M. Spec No. 8 10 . 4 11 2 13 53 15 % ~ 19.12 8.13 16.26 4.37 57.30 .23 .10 .49 batch WORKING CONSISTENCY - Refer to plant testing procedure No. 1 C. C. Specifications Maximum 25 Minimum 20 Average 20 TENSILE STRENGTH TEST ~ Refer to plant testing procedure No. " WORKING PROPERTIES - Refer to plant testing procedure No. 7 COLOR - White Color shall be snow white - Shall match color for said See color formulas sample EXHIBIT 3 Premix000172 Marblecrte MarblecrteMarblecrte 0-6 MASTER FORMULATION Os7 006 MASTER BATCH BATCH FORMULATION Marblecrete MOVES "4M 3 6 . Syoes MATERIAL STT OL ard pounds MATERIALWhite ~ HOLVa Spuod OBST 008 O00T OOF UOUS az OT 650 6516. SOVS Ozt SyoeS Oz ot i a OS 4 Asbetos ( c e251 O59OOeT OSE OTY si 8 8 C661 Emathlite ) Z 2OT CT CT TY syoesOOT - UIST { 21LNG Zt Crs Se Lore OC oye or eye 6L OT - @ 21 9-0 ; (3) (Oo) #1e% eqtosTaey RRL erQUDTIO SOISY Syersyg 20RCOUd ' COTES (Oy 87 VueMsy SEPT STAE SHT Sr Sato UStita OX 177 DUES EXHIBIT3 ELOXIWAY Conqu YEJUEH ' LIGiHX February 11 1974 Supercedes November 16 1973 formula | ORLANDO PLANT FORMULA PREMIX MARBLECRETE SPRAY CONCENTRATE 10-7 DESCRIPTION OF PRODUCT ' Concentrate for the manufacture of marblecrete stucco spray FORMULA . Raw Material Zinc Stearate Emathlite Asp 170 Clay Function R.M. Spec No. Water Proofing 53 _ Slip Filler Plasticizer _ 1 15 19 119 % 6.11 65.65 28.24 batch see over WORKING CONSISTENCY - Refer to plant testing proceduNroe. 1 nen eee ee - * Denotes Change . EXHIBIT 3 Premix000174 GAL OXIWS1q-ye}UHY Marblecrte Marblecrete Marblecrte Spray ham MOVS ry O04 syoes Stearte Stearte HOLVA spunod [| AOVS Ost syoes NOTLVAWHU < _HOLVa spunod 0% GEE S661 LIGIHXH HOLYE MOVS O H | syoes Was 27-0 ve OOT 47 92 2TT || e9aQques0g BNHOUd LHSIM TT*S 69 V2" 2a 49 ge 7 Aeadg SV eqgaostquey AyTaLeqresyg eTo ETUA oLT LOACUd sutZ EUR dSv February 11 1974 = Supercedes November 16 1973 formula ORLANDO PLANT FORMULA | MARBLECRETE SPRAY 0-8 DESCRIPTION OF PRODUCT ; Mix for application with a cement block or cement a spray scratch gun on surface FORMULA Raw Material * Sand 40/200 Marble White Cement Finish Lime - * / Lime Zinc Stearate c * Emathlite c Asp 170 Clay c Function R.M. Spec No. Aggregate 2 Aggregate 6 Strengthener 8 Strengthener 10 Plasticizer 11 Water proofing 0073 Slip Filler two - Plasticizer wn, 15 19 % 36.61 33.07 18.65 6.61 3.31 ~ .10 1.07 . .58 batch see over WORKING CONSISTENCY - Refer to plant formula testing procedure No. 1 T. C. Specification Maximum Minimum Average 25 - 20 20 TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES ~ Refer to plant testing procedure No. 7 COLOR - White shall be snow white standard Colored shall match standard see color formulas * Denotes Change~ EXHIBIT 3 000176 February 11 1974 Supercedes November 16 1973 . formula ORLANDO PLANT FORMULA PREMIX CONCENTRATE 0-5 i DESCRIPTION OF PRODUCT A concentrate for use in manufacture of Marblecrete Stucco FORMULA Raw Materials *** Asbestos SG210 *** Zinc Stearate *** Emathlite . Function - Bulking Agent Water Proofing Plasticizer R.M. Spec No. 223 53 15 % 27.69 12.31 60.00 batch WORKING CONSISTENCY 1976 Refer to plant testing procedure No.1 * Denotes Change EXHIBIT 3 Premix000177 February 11 1914 1914 . Supercedes November 16 1973 formula | MIAMI PLANT FORMULA MARBLECRETE M DESCRIPTION OF PRODUCT . A mixed white domestic portland cement and marble silica aggregate composition which includes a water proofing producing a durable and weather proof exterior stucco finish 0 Lbs oo iW .03805 , FORMULA . Oo R.M. Materials Function | 7 . Spec No. White Cement - ' - Strengthener 15.30 8. 19:12 5822 Finish Strengthener 6.50 - 6318 2067 ty) Plasticizer Plasticizer . 10 -8713- 2067 -8713- | XO Marble | E Lime i Aggregate . | 13101 4 .0158 16.26 2056 . Plasticizer 3.50 11.02696 - 11.02696 4.37129.094 4.371299.0944 Sand Aggregate 41:04 2 0093 51.30 4.371299.0944 Agent .3817 Asbestos SG210 c , _. Bulking Agent 18 13 10915 .23 ..0165 10915 Zinc Stearate c | * Water Proofing .08 .08 53 64 | 010 0512 Emathlite Plasticizer 136 | 0512 2004 | 9 20049 2049 So - WORKING CONSISTENCY T. C. Specifications | TENSILE STRENGTH TEST oo as Refer to plant testing procedur Noe. 1 1.54 sO Maximum =. Minimum Average .25 20 20 - Refer to plant testing procedure No. 6 - WORKING PROPERTIES - Refer to plant testing procedure No. 7 , COLOR - White .Color shalble snow white - Shall match color for said See color formulas sample EXHIBIT 3 : Premix.000178 February 11 1974 Supercedes November 16 1973 formula C anal MIAMI PLANT FORMULA PREMIX MARBLECRETE SPRAY CONCENTRATE M DESCRIPTION OF PRODUCT _ Concentrate for the manufacture of marblecrete stucco spray FORMULA Raw Material Zinc Stearate , Emathlite * Asp 170 Clay = Function Water Proofing R.M. Spec No. 53 . Slip Filler Plasticizer | 15 aan . 19 119 % 6.11 65.65 65.65 ; 28.24 batch see over WORKING CONSISTENCY Dv Refer to plant testing procedure No. 1 * Denotes Change EXHIBIT 3 Premix000179 ~~ | spunod oe HOLVA __ MARBLECRTEMARBLECRETE SPRAY MARBLECRET ABS SPRAY er4: O04 | $ Weuvaputo sovs oStHOVS 170 DYINUCOLMAY HoLvaspuno Oz oot GES ~ te | HOL Fa SOvS VALS LW OOFsyoes TT VW BLVENAOD te" INaouadLHDIGM TL"9 GO*.9 Be Ra 2VUdS Tmodta ALVUELS Ry1o THALNTY @LT inl OLT ain a ONIZ Va dsv Se LONCOEd February 11 1974 Supercedes November 16 1973 formula MIAMI PLANT FORMULA PREMIX MARBLECRETE SPRAY CONCENTRATE M DESCRIPTION OF PRODUCT Concentrate for the manufacture of marblecrete stucco spray FORMULA Raw Material Zinc Stearate EmathliteClay Asp 170 Clay Function Water Proofing R.M. Spec No. 53 Filler Plasticizer 19 % 6.11 batch see over 28.24 28.24 WORKING CONSISTENCY ~ Refer to plant testing procedure No. 1 * Denotes Change EXHIBIT 3 Premix000181 _-ze1goxuiald: PRODUCT 02 MARBLECRTEMARBLECRTE MATERIAL MOVS ARIUEL STEARATE STEARTE ZINC STEARTE HOLVaCLAY CLAY S370 OT eS NOLVIWU HOLVEspunod OZT oOO < SLS *T 38-84 HOLVE MOVS esd 4 YLS Z-W OOL syoes 9% ET VN GLVUNAOD LNGLHDIGM Tt"9" Gad IG G9S9 8102 ZVUdS BLAM AYTO ALVaRLS AIAN ait OT THE TVIURLN ONIZ VN dsv LoONdo 81 0OXIWiag-yeqUH MarblecrteConcetrae y MATERIAL MMAATTEREIRALIAL MOVS OL ECS Asbestos SG210 . | Wonvd spunod Movs OzT Syoes NOTLVIWHOS < HOLVdSpuriod Ove Gel GEqT 06T LIGHXA HOLVE MOYS YELS OOT syoes g mG 8S VN | DN LHDISM 6-0 GL ET OS*L GL" Sh Ig - 2% efrquscg eqsodtqauey eT OTENS OTers . RRR TT SOTSUSY yg SUEZ SyTUyeu LONd PS PRODUCT 0S Marblecrte Spray 0-8 WoL OSE OO? a ey) Te oL65 LOXIWa W=Ti-e g-MejUeH AM MOVG 018g oes Od "Oe 6t TT, 100 aH pounds BH ~T | Marble HOLVd ca e O0Ze 9B2T Osy UE oT 2650 TT <656_ . : MOVS iS) g ; Emathlie Te S86 . , OZT c Ze St eT a HOLVA O06e OGGST OSS Ose 86 Le " < LIGHX# . 170 ~ MOVS ' Te TELS 9 OOT be oT TT ; Concentrate 20 for Or , colors ZOE. GOT TD ST Tet 20 T es | g~o , ; Aeidg Y TopTOS [Oy #0Z doy sqoreTty WUAPSTL STELSI (8) O STICH Twos) T Sup T Sat Sa iOLpT eqeBaque LOAdo preg 0/07 STI USTrEs a/V EXHIBIT EXHIBT ae duo) THO February 11 1974 Supercedes November 16 1973 formula i ORLANDO PLANT FORMULA PREMIX CONCENTRATE 0-9 Concentrate C DESCRIPTION OF PRODUCT . Concentrate for Stucco i the ! manufacture of Marbletite FORMULA Raw Material * Asbestos SG210 Zinc Stearate Emathlite Function Bulking Agent Waterproofing Workability R.M. Spec No. 13 53 .15 . % 13.75 7.50 78.75 78.75 batch testing procedure No. 1 CONSISTENCY - Refer to plant WORKING sae a * Denotes Change EXHIBIT EXHIBIT 3 Premix000185 February 11 1974 Supercedes November 16 1973 formula| MIAMI PLANT FORMULA MARBLECRETE M ' DESCRIPTION OF PRODUCT A mixed white domestic portland cement and marble silica aggregate composition which includes water proofing producing a durable and weather proof exterior stucco . finish . FORMULA Raw Materials White Cement Finish - XO Marble . E Lime Sand - Asbestos SG210 c Zinc Stearate c Emathlite Function oe R.M. Spec No. ' Strengthener Strengthener Plasticizer Aggregate Plasticizer Aggregate .. Bulking Agent Water Proofing Plasticizer g -10 amen 4 11 2 13 53 -15 % batc 19:12 '\ 13- 13- | 16.26 403712189 403714037212189 140371218984037912189 5. 1..3230 40371289 10 49 49 a i A WORKING CONSISTENCY ~ T. C. Specifications | TENSILE STRENGTH TEST Refer to plant testing procedurNoe. 1 Maximum - Minimum | Average 25 20 20 -Refer to plant testing proceduNroe 6 WORKING PROPERTIES - Refer to plant testing procedure No. . 7 COLOR - White : .Color shall be snow white 11 Shall match color for said See color formulas sample EXHIBIT 3 Premix000186 MARBLECRTE spunod G1 MARBLECRETE 6 Tg0T $5) MASTER MASTMEARSTER BATCH FORMULATION FORMULATION OE | PERCNT |. MOVESyoes 100 OM BATCH PERCENT 6 62 WEIGHT CEMENT yoesg OZ | 8.13 HOLVEsputiod 16.26 8.13 OO9T 1313 000% 130 a syoes 4037 MOVS | 41 51.30 51.30 9T 0S OCT 0.23 | yf 7 _ | - STEAR 18 / TALS spiunod <a HOLVE -.049 0.10 OO <TS88, OOTY -.0049 EMATHLITE NOVS a | GOT syoes 9T <LT e TY vit || wane NHOUmdZHOTUM SL ^'t ET. 92 ces OT OfTS aT Ot'O ig | _. | =|. Q-N (2) (9) <8 TWLUEVA EXHIBT aLvans HSIN BLauos . GW DOfS T-L LNGINTO IGavW Tau AWIT TEM NYS oO T X #/ EXHIBIT Lopd Date Le0xIWelg Sack \e1UeF| 70 ; oo RP nee an < a LIGHXA ns a , ; . tT t OSV ULES NOG Nov 16 / 73 . Supercedes all previous formulas . MIAMI PLANT FORMULA MARBLECRETE M i % - DESCRIPTION OF PRODUCT A mixed white domestic and marble silica portland cement which includes aggregate composition a water proofing producing a durable and weather proof exterior stucco finish FORMULA Raw Materials White Cement Finish Lime XO Marble : E Lime Sand Asbestos SG210 c Zinc Stearate c Emathlite c . WORKING CONSISTENCY T. C. Specifications TENSILE STRENGTH TEST ae Function = ' R.M. Spec No. Lbs Strengthener Strengthener . Plasticizer - Aggregate Plasticizer Aggregate Bulking Agent | - Water Proofing ' Plasticizer . . Refer to plant testing g 19.123911 19.123911 0772334 0772334 0772334 0772334 - 0772334 15 ' 8.13 16.26 4.377707 4.377707 51.30532 51.30532 .230.22 1100.1030 1100.1030 0.49 : . Sy procedur Noe. 1 . Maximum 25 Refer to plant Minimum - Average 20 20 testing procedure No. 6 | batc WORKING PROPERTIES ~ Refer to plant testing procedure No. 7 ft COLOR J- White shall be snow white - Color - Shall match color for said sample See color formulas EXHIBIT 3 000188 FORMULATION FORMULATION L07o aueane Qe 6sSpuriod Teor OST 006 O5 0062 82 Le es a PERCENT MATERIAL BY ee 3.4 WOVS OZ CEMENT OES WEIGHT WEIGHT 6 G 6% sputiod Rie HOLVE 16.26 16.26 009T 00% 0005 1332050 aOFs Li pte SOVS ) syoes Oz oT 9T g "0S wa EMATHLIE HOLVGsptmod 0.49 0.49 OOET See OOTY 832 39 6 S61,cabs aml LOW X ParsvnHOLVE | SOVS % OOT Syoes POT <L eT TY t WZ | LNwOUNE LHDLAM we CL g 92 9T pe"ge 1s e0 geo An 649 AT of. . O-K (0) (0) gle SLTHLYNE ZLVYINFO avars IELaaMuOT ENGIED EWIT HIS GWT DOTSe (2) ' VIM SOLHESY Vil ATM HSINTA O X a/v aqys IBIT LONGO - October 11 1973 Supercedes all previous formulas MIAMI PLANT FORMULA MARBLECRETE M DESCRIPTION OF PRODUCT A mixed white domestic portland cement and marble silica aggregate composition which includes a water proofing producing a durable and weatherweather proof exterior stucco - finish.. White Cement Finish Lime / Lime Asbestos 7RF9 Zinc Stearate Emathlite c c c Function Aggregate Aggregate '. Strengthener Strengthener ~ Slip Strengthener ~ Slip ; Bulking Agent Water proofing Workability R.M. Spec No. 2 ho) 8 H , % . 50.88 16.28 19.15 | 8.14 . batch , see over ; . HUKE HUKE HUKE HUKE 4.07 0.60 0.40 | 0.48 WORKING CONSISTENCY M T. C. Specifications Refer to plant .> Maximum- testing procedure No.1 Minimum Average TENSILE STRENGTH TEST - Refer to testing procedure No. 6 _ WORKING PROPERTIES - Refer to plant testing procedure No. 7 COLOR ~ White Color shall be snow white ~ Shall match color for said See color formulas sample EXHIBIT 3 000190 PRODUCT_ L6OxiWjad-YeIUH MARBLECRTE TROT 0062 006 MASTER MASTER BATCH BATCH FORMULATION FORMULATION MARBLECRET MARBLECRETE MOVS BATCH MATERIAL Sxoes MATERIAL 3A PERCENT O4 6% PERCENT 6 100 Hobva Sspunod 000% 0097 16.28 00g 13 6S 1300 hy 696 | CEMENT O@t sxoes Os OT 0% 9T g Le 4.07 ASBETOS STEARTEc oot? ~O0 <t 0.40 0s9 GEE gy 32 6 <2208 EMATHLITE ) _ oa SHOCS SET 9T 25 9 WLS | OOT Ti <T. - | VW @21 38 05$2" OT GT6T qT". ZO7-09 0 "0 37 00 AE Q-N (0) (0) #iz BLAUOT Fat SLVNGO SLITHYWGDLVELS TiMaiW ' 6f8L (8) IG WALT AVN mT : TWidSLvN anys O x @LlHM HSINA W/V SOLHESY ONTZ Londoud MARBLECRTE MARBLECRETE MARBLECRET CONETRAE 4h MOVE MATERIAL Hoes ofsyoers HOLVE spunod MOS OZT sxyoes NOILVANUOT < HOLVG spunod 009 "OSz OSeT O0T*z LIGHX] HOLVE . SOVS UaLS OOT Syoes Oz Of SZ VN $"M SLVUINTOD WINHGEOLHDIGM 692 TE2T 009 ZT OTz ALTWOEaN OS HLVAEL A, TWIVSLN SoLHasy ONTZ TUL Yer LOAGONd 1974 February Supercedes November 16 1973 form MIAMI PLANT FORMULA PREMIX CONCENTRATE M DESCRIPTION OF PRODUCT A concentrate for use in manufacture of Marblecrete Stucco FORMULA Raw Materials *** Asbestos SG210 | *** Zinc Stearate *** Emathlite Function Bulking Agent Water Proofing Plasticizer R.M. Spec No. 13 53 15 % 27.69 12.31 60.00 batch WORKING CONSISTENCY S Refer to plant testing procedure No. 1 - * Denotes Change EXHIBIT 3 Premix000193 February 11 1974 Supercedes November 16 1973 form Concel MIAMI PLANT FORMULA PREMIX CONCENTRATE M DESCRIPTION DESCRIPTION OF PRODUCT A concentrate for use in manufacture of Marblecrete Stucco FORMULA Raw Materials * Asbestos SG210 Zinc Stearate * Emathlite Function - Bulking Agent Water Proofing Plasticizer R.M. Spec No. HUL 53 HUL % 27.69 ~ 12.31 60.00 . batch WORKING CONSISTENCY 1 Refer to plant testing procedure No. 1 4 t. * Denotes Change EXHIBIT 3 Premix000194 CONETRAE MARBLECRETE CONCENTRATE 5 CONCENTRATE | | MARBLECT SM oes YOFS oO Syoes HOLVE spunod OVS : N OstSHOPS OLVINOL HOLVG spunod 009 0Sz OS2T-00T HOLVE MOVS Sz FRESH OOT Smoes 0g OL Ge { S-i ALVYNEOD LNFOUGgLHDTEM 6942 Le*eT 9009 ae | HLM OTZ STE aw DS RLVELS LID TWIMSL VT SoLsagsy ONTZ WLW Londoud $61 0xIWAsd-ye]UHY ~. a -t es Ge L_LENHXA rE r | ate February 11 1974 Supercedes November 16 1973 formula MIAMI PLANT FORMULA MARBLECRETE SPRAY M DESCRIPTION OF PRODUCT : with Mix for application a cement block or cement a spray scratch gun on surface FORMULA Raw Material * Sand * 40/200 Marble * White Cement *Finish Line * E Lime * Zinc Stearate * c Emathlite- 170 Clay c Function R.M. Spec No. Aggregate Aggregate 2 . 6 Strengthener 8 Strengthener Plasticizer Plast 10 11 Water proofing 53 __ 36.61 33.07 + 18.65 --6-67 3.31 11.57 0.10 batch see over . Slip Tiller 3 PlastiPlacsticiizezr Plaesticirzer meter ( " -1 ervey, : oi a. 058 058 - WORKING CONSISTENCY Refer to plant formula testing procedure No. 1 T. C. Specification Maximum Minimum | Average 25 20 20 TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES - Refer to plant testing procedure No. 7 COLOR - White shall be snow white Colored shall match standard see color formulas * Denotes Change EXHIBIT 3 Premix000196 pean _ spunodSPRAY TL O0e QO6T MASTER OSE MARBLECRETE ~} 9 Co FORMULATOINSE FORMULATION FORMULATION Z6LOXIWAY-yejUH Syoes MARBLECRET me "IM MARBLECRTE Of 6T TT hi 3BH OZ MATERIAL yOBS | -f ie sacks on 2650 sacks HOLVa spunod 3.07 36.61 9827 agg 2650 3535 me MOVS Te e g OZT Syoes S < 6.61 6T - <T 550 veneer n te: e | Pine _ < STEARTE HOVEspunod 1:07 1:07 HOST 0S Qn g io 3S865 : LIGHXS) . ) CLAY BOYS mee syoes etn UELS ra=e OOT 6% Zoz QT. TI . nn VL | |. Eter | wen ZNBOUd LHDISM @~ T996 LOvE s9gt T9 9 oxnas) OE BG) Ad Goenna a CONCENTRATE- |. pn semn ; ht HLGUOR ennttn <n (2) OE O-)ee -OHEVANTO TAU t 7 . qIaUyW INGWG MIT TWIMELVN CNVS 0Z/O% LTH HSINTA LOndou ALVELS (D) RYT Do SETE Od EE EE EXHIBIT PEST SY : November 16 1973 Supercedes Oct. 11 v, 73 formula MIAMI PLANT FORMULA MARBLECRETE SPRAY M % DESCRIPTION OF PRODUCT Mix for application with a spray gun on a cement block or cement scratch surface FORMULA Raw Material Sand 40/200 Marble White Cement Finish Lime E Lime Zinc Stearate c Emathlite c Asp 170 Clay c Function R.M. Spec No. % Aggregate 2 Aggregate 6 - Strengthener 8 Strengthener 10 Plasticizer 11 Water proofing 53 34141 362261 - 33.07 18.65 18.65 6.61 3.31 10093 10093 ae) batch see over - Slip 15 Filler W Plasticizer 19 1.07 0.58 WORKING CONSISTENCY ~ Refer to plant formula testing procedure No. 1 _ T. C. Specification Maximum , 25 Minimum 20 Average wa TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES ~ Refer to plant testing procedure No. 7 / COLOR Ove White shall be snow white Colored shall match standard see color formulas . * Denotes Change EXHIBIT 3 Premix000198 November 16 1973 Supercedes Oct. 11 v, _ 73 formula e MIAMI PLANT FORMULA MARBLECRETE SPRAY M 33 DESCRIPTION OF PRODUCT Mix for application with a spray gun on a cement block or cement scratch surface- FORMULA Raw Material Sand 40/200 Marble White Cement Finish Lime E Lime Zinc Stearate c Emathlite c Asp 170 Clay c Function R.M. Spec No. .% batch Aggregate 200007 Aggregate 200007 - Strengthener 200007 Strengthener 200007 Plasticizer 200007 Water proofing 53 36.41 352861 - 33.07 ~ .18.65 .18.65 6.61 3.31 110 0-33 aed) see over Slip 15 Filler - m Plasticizer 19 1.07 0.58 WORKING CONSISTENCY - Refer to plant formula testing procedure No. 1 _ T. C. Specification Maximum 25 Minimum 20 Average me TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES Man Refer to plant testing procedure No. 7 ^' COLOR ~ White shall be snow whitestandard Colored shall match standard see color formulas * Denotes Change EXHIBIT 3 Premix000199 . . . D MARBLECRTE OZXIWeLG-HE HOLVESpunod 002 OO6T TEOT Ose 002 GEA 09 9% O08 SPRAY MARBLECRET SPRAY SPRAY 8 TT 4 OZ 4RG Woes - ft ff ua Date Gs at sacks HOLVasptunod36 ood 984T Stageon Stageon 2900 COT ry 2650 Glo -3500-3500 : i MOVS O27 sy0es St 18.65 6T Stageon Stageon - 650 oO STEAR _ : spunod-HOLVE 0062 os9z : Stageon Stageon Sek 98. LE OA 10. STARK EMATHLITE YOWS % CLAY OOT BYOCS 62 9% QT, TT S 44 VN DNWOUHdDHOTHM a ERE TE S-W LO" 59 T9"9 S820 LO T 8S*0 , = * a * <E98T 29 .88 CONCENTRATE ElguoRTayM (9) (9) #0%7 ELVELS ' (9) HIUVW ENGWHO WET AVIO . ALVUNTO = = AWTT OLT TIVUSLVW SLUTYWG LONdou aNvS 02/07 SLTHM HSING 8/ ONIZ asv . EXHIBIT November 16 1973 Supercedes Oct. 11 v, _ 73 formula MIAMI PLANT FORMULA MARBLECRETE SPRAY M 5 . DESCRIPTION OF PRODUCT } Mix for application with a spray gun on a cement block or cement scratch surface FORMULA Raw Material * Sand * 40/200 Marble * White Cement * Finish Lime * E Lime * Zinc Stearate c * ' * Emathlite c * Asp 170 Clay c - Function R.M. Spec No. _ \ ' batch Aggregate Aggregate Strengthener Strengthener Plasticizer Water proofing . 2 6 8 10 11 53 36.61 3561 - 33.07 * 18.65 18.65 6.61 3.31 110032 110032 . see over Slip 15 Filler www 7 Plasticizer 19 1.07 0.58 to WORKING CONSISTENCY - Refer plant formula testing procedure No. 1 _ T. C. Specification Maximum _ 20 Minimum 20 Average aa? TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES TOLD Refer to plant testing procedure No. 7 . y COLOR - White shall be snow white Colored shall match standard see color formulas . * Denotes Change EXHIBIT 3 Premix000201 November 16 1973 Supercedes Oct. 11 v, | 73 formula MIAMI PLANT FORMULA MARBLECRETE SPRAY M 5? DESCRIPTION OF PRODUCT Mix for application with a spray gun on a cement block or cement scratch surface FORMULA Raw Material Sand 40/200 Marble White Cement Finish Lime E Lime Zinc Stearate c Emathlite c Asp 170 Clay c Function R.M. Spec I batch Aggregate aan . Aggregate aan Strengthener aan Strengthener 10 Plasticizer up Water proofing up . 36161 305261 - 33.07 * 18.65 6.61 3.31 1100-235 1100-235 1100-235 see over - Slip H Filler - Plasticizer H 1.07 0.58 0.58 WORKING CONSISTENCY -m Refer to plant formula testing procedure No. 1 _ T. C. Specification Maximum 25 Minimum 20 Average ao TENSILE STRENGTH TEST - Refer testing procedure No.6 WORKING PROPERTIES 7 Refer to plant testing procedure No. 7 4 COLOR - White shall be snow white standard Colored shall match standard see color formulas * Denotes Change EXHIBIT 3 Premix000201 _ 9 spunod BATCH 00% OO6T TEOT OS < 002 09 ffry h/ HOLVE MARMBARLBELCECRREETTEE os 3 ZOXIWAE-4gUH Ssyoes MARBLECRET MARBLECRET Oz 6T a d vi eg OL ? ontg 49eg & .HOLVE spurnod 36 . , 99LT 0s9 OO < 2900 2650 <OT ary 3500 Syoes 650 BOVS 9 GE Ze 6T eT O2T 650 STEARTE | c spunod-HOdVa 0062 0492 } OSS" Ose LE , ' < LIGHX3 EMATHLITE NOVS oy 44 OOT ByNOeCS 6% 29% OT, TT S 170 || Qe INEOUSd THOTEM e-W eS LO* S9 T9 9 TET BS L0 T gS 0 *= 9E Ce ST Ia CONCENTRATE (2) (9) #0%: ' (') SLAUOTIENW . HIGUVN INEWGO SMT ZAIO GLVUELSAMI OLT SLOWING ALVENZO TVIALVW Londw CNVS COZ/OF SLIM HSINTA a/ ONIZ dSV October 11 1973 Supercedes all previous formulas MIAMI PLANT FORMULA MARBLECRETE SPRAY M A DESCRIPTION OF PRODUCT Mix for applicatiwiotnh a spray gun on a cement block or cement scratch surface FFOROMURLAMFUORMULLA AFORMULA Raw Material . Function R.M. Spec No. Sand 40/200 Marble White Cement Aggregate 200272229 Aggregate . . . 6 Strengthener 8 Finish Lime E Lime . Strengthener Plasticizer 200272229 200272229 Zinc Stearate c ) Water proofing | 200272229 Titanium Dioxide c Whiting 200272229 Emathlite c Hardener - 200272229 Asp 170 Clay c Filler.Fi-l er.- Adhesion Plasticizer . - 19 % 36.32 33.02 18.63 6.60 3.30 0.46 0.02 1.16 0.49 batch - see over WORKING CONSISTENCY - Refer to plant formula testing procedure No. 1 = T. C. Specification Maximum Minimum | Average TENSILE STRENGTH TEST - Refer to testing procedure No. 6 WORKING PROPERTIES - Refer to plant testing proceduNroe. 7 COLOR - White shall be snow white ; Colored shall match standard see color formulas EXHIBIT 3 Premix000203 i spunod Og MARBLECRTE OO0E MASTER 109 606T HEOT MASTER T BATCH FORMULATION FORMULATION MARBLECRTE POZX!Wald- syoesMARBLECRETAN a 02 Z PERCENT F PERCENT OZ BATCH oes MATERIAL ejuey 9 spunod z MARBLE OOge 33.02 3 .02 085 OO < Ty OTT ca 0796 MOVS OT syoes cE Ze 6.60 & 9 OT ZINC c EMATHLITE x ) 059%. 0068 0.02 056 0Sz LE 26 oO Ge08 < ) 1.16 1.16 ^'z 90.49 it g LIGIHXS g ASP cCLAY INA B-N LHDIHK Ze9E ZO" ee aT 09 5Of*E 970 Z0 O OTT 67 0 2 CONETRAE (0) (9) TIANUM ELVUELS FOR WOINVET COMORS ENG eos GIT (9) (9) ZIO SIT SLT a OLT aNYS 02/07 SLIBM ESINTA B/V ONIZ Toy dsv LONCoud SUOWD #O% Udut fi BLYNAOD WATLNIYEWLOT