Document 10jgXJR0E20gObeXG3Z21Bpz5

PASCAnoalluymtibciaalServices- Created with Analpystt Reporter Printed: 14/02/2010 6:41:00 PM PDraotjaeFctie E02v0a8'1s0bP1rSoamcpPlFeCsstwoinfg inRessturlutmTeanbtlNeame __A0P2I05801000SamplesLoanbg [SampleName ioaossE:002 `AcquisitionDate |2/9/2010 1218.12 AML [injectionVolume [5 `SampleType [(AcqunisitiionMeethocd[|2PtF2CRonstenxLonvg damiarDi[lwuetiigohntFtaocVtoorlme [[ 100000]| FReistuslPtsekSummary Anais RY Gane [eros | PFDOA 1 PFT Prien ores |wow |2mas | mw | owes "o worros| somo omwin| 0 |wa | 13C-PFDoA 161840 0.00 (4.63) 0 NIA No | 13C.PF00A| 161840 | 0005.14) o A No | voeroor| sew Joma | 0| wa | we 48i Sel! Page 158 of 262 52 Logon AnalyticalServices" Cratea vin Ana: Reporer RCSummary eres| opr| ws eae| IE | Roig [roe room| wom | wo [oman| w [raz [ewae| wm | me|omem| ow | [oorros | mam|wwe| we [mas| | owe Lome 0|e wen| ow srcerm sem|wm | we | ava | we | somo e|m wwe s | we| swam || Fras smo | mw |w emo | we] 53 8AnaollyutimciaalServices Created with Analpysst Reporter Printed: 140212010 6:41:00 PM QuantiPteaaktReivvieew K1000968.002 => = ry = om Ian i i- | Ba4se1l3Pi0Fn1Oe6Ac901MiDsased | 41137C.-0P57F2O0A08 Baselinec Missed | B4a6s3e.lP0iE4ne1Nc0A.01Mi0sased | B4a661s.3i0Cn4-s2P3cF.N0MAiDsased Ll lo ow io Lome 7 = cBa4s9e9Pl.iR0nO8eS0c01Mi0sased | cBa5s013e3.i0Cn0-e8P0cF.M0OiSDsased angen HA = od the bo l: + L a] I. Jo "hao Bits] ] 3 7 | Ba5s1e3lP.i0nF4eD6Ac9M10i0s3sed | Ba$s1e15l3.iC0n-4eP7F00OMAiDsased Ea Wag pea =3 . Fo3 563P.F0U51A9A.TDa Baseline c Missed | 56153001-2P7F0U0RADa oBaselie Missed | 599P.R0O80S0T Da Baseline: Missed | 50133C0-1P0F0OS0a oBaseline c Missed - 7 TE 7 ido ed] 613P,F01D3O69A.01 0a cBaselinec Missed | = zl5: IfUFWrIPIREILEN 713P.F06T6e9A.10 0a Baseline o Missed | 611530C/-1P6F0D.00A0a cBaselinecMissed | 7 [ -i le A 611530C/-1P6F9D.00A0a Baseline o Missed 663P0E/6T1A901 0a oBaseinecMissed | 61153C0-/P1F6D9OD.Aa0 Baseline c Missed 0 Before O After Page 160of 262 54 Lo Columabia services: fon Ratio Confirmation RH i PrCinrteead:ted14w/i0t2h/A2n0a1l0y6::4R1e:p0o0rPteMr K1000968-002 -A "| 413.P0F2O69A.20 Da 463,P0F2N19A.20 Da "BasWerloinngoePMeiasksed | BaWrsonegclPMieiasnkseed | nt = - | |I aTmT enLi] a.Ialigsen|[ 563P0F1U2T6A920 Da 599P.F0O9S902 Da GBasWeiloinngecPMeiasksed | BaseWlrionnegMPieasksed| 499.P0F1O99S.20 Da 513P0F26D92A0 Da BaseWlrionnegMPiesasked | BaWsroengolPiMeianskseed = EH = = DI ELL|ilr eeteUOg NTL 613P0E/D16O902 0a 563,P0F11T6R9.20 0a cBasWerloinngecPMeiasksed | Ba WsioengloPiMeianskseed ] hee 713P0F/T1E6A902 Da BaWsreloinnegoPMeiasksed O Before 0 After Page 161 of 242 55 A Columbia AnalyticalServices Crested wih Anapts Ropoter Printed: 15/02/20102:34:00 PM FrDaotmaeFtile EcazosaT0SPamApRtePsonan it iRnessturnumTeanbtlNeame__40921058010003amplessnonedis [S`AacmqpuilseitNiaonmDeate |2i/c6a/2m0m7a0e1010.70434AN [ec`tAcoqunisvitiioanrMethod{|2P2FCKinetexShdoarmt [iSeacmptloenTvyoperame [5] | WDeiliugtihotniFoavcetoirume[ooo | Results Summary [aAnalyte Peak [s|tisam en [RGER | AnalyteRT anamenves | GOST Calc. Conc. .oat P[ropAt rr|e1sncprta| wsnaosomo || s1szsoczenn|| wseamsme | o0o0s | woe | ras worms | wm|amum| wa | ovat pprreaa 1 Tacrra| wwrzos00 [sme| stseoree ooao Jw] "e | Pros 1 worres | smo corms | oer| smo |swem| [amen| am |oo| we maw | on | we | [socrron | nceron | sw |rssasn| www | 0 | we | 44 " ste Page 14101248 56 6 lumtpiciaal Serviceis} Prcinrteead:ted15v0it2h12A0n1a0ty2f:3R4e.p0o0rtPeMr IRC Summary Aniyte Peak ame Praa2 [orsass CleExpWR | Ro Conte | tzrazn| s|s wo| topo | ves TLoewwasm|| 00 ||wwe[|owmweonw||wweo[n| S_1acPFaA 1202 | swe | No |womgsss| te Page 142.0 245 57 LS CS olumu bia services Created with Analy.st7 Reporter Printed: 15/02/2010 2:34:00 PM Quantitative Peak Review K1000968-002 : : F4 ow bg g- A o: T. Lo- :Wo] 5 oe Rb aER 2130P1E69A.T00a Baseline Missed | 21137C0-1P7F2B0A08 cBaseline Missed | Ba2s6e3lPi,En0Pe2e1A9M1i0sDsaed | B3a11s35C0e-/PloF2HM7iXi0Asna0seed --Suonmees apa | ow ty ak = az oJl i=z) |cl = Afi - haI 2ey Ber | s) 299.0P1F8B0.S010a 4108300/-1P0F3H0S0a 313P0H2Y6A901Da 31135C-.P0F2HX7DA0a e oBaselineoa Missed | oBasehlienyeoyMissed || oBaseine Missed | 7Baselin0egG22Maissed ES = i i | = ll = 363P,0F/H1p6A9.10 Da cBaseline Missed | 311530C1-2P7F0H0XDAa Baseline Missed | 2P99F.0H/8S0.01Da cBaselinecMissed | o B4a0s1e38l0i01n-e0Po3F0HMSiDsased - | | | = - Il | I ul SN IE WN 4s03108/100370 s0a isSe0pATf0o0A0a || ssta50i4cTP00r0o8 51155004p7F000ADa cBaselivec Missed | oBaseinecMissed | cBaselinecMissed | oBaseline o Missed O Before O After Page 14301245 58 K Aonlaalymtbiicaal Services PrCinrteeda:te15w0it2h12A0n1a0ly25:3.4R8.e0po0rtPeMr | ne. Toms| hates| Tred g ] -- = fon Ratio Confirmation : | E 2) < K1000968-002 Ci = 2B1as3e0lP1iF1nBe6A9c20Mi0sased | B2a6se3Pl0Fi2nPe1E9A0M2i0sased | o2B0as6e.Pli0Fn9Ee9S02MDisased| c B3a1s3ePl.i0nH1e1c9A2.M0i0sased Wrong Peak Wrong Peak Wrong Peak Wrong Peak = 7 L ~ o Ll Sen ea bd I Tips a wl 363P,0F1H3p1A9.02 Ds 39P9.F0H9G9S02Da 5S1_51034C7P0F0D0Aa NA Baseline Missed Baseline c Missed Baseline c Missed Baseline o Missed NE FFBWAroanndg PPFePakeA da nol have aWuraolnyginPgeaokn Fansiions Wrong Peak Wrong Peak 0 Before 0 After Page 144 of 245 59 a8 ACnaollyutmibciaal Services CrweithAanalytpsot Reepordter Printed: 14/02/2010 6:41:00 PM PDraotgaecFtile T02a08s100PSraemapulPsLroensg wit RIenssutlrutmTeanbtlNeame__ A0P2I 0508010 0Samponegs, [[SAcaaumiesittNioanmDeate |2i1c2o0u1a0ee2a.o2s554 At AceqcuitsotniVonalMetho1d|7P3FCKinetexLdoangm [SianjmepcltieonTVyopleume[5] [Di[uWeiioonwFiaocvtoourmeJ7o0o0 || RReosueltPseakSummary Rate Pron woeron| wesw| oman| o i Gare Mm Pron 1 Pra PrOoA 1 [prea woeron | awa [owgse| Tacerum| sods | areon| 15CPrOA| 10s | moon| cern| tos |oware| 0 | wa | we | sas wor | me | eee | o oem Y wNeo J 0 | wa | me | &0 ere Ll Page 16201242 60 Pn LS Roeservices: iretain slnlMr Weswmay eprorn es Fomorron frruas [[orvosearma sorros ronz s-10e5700 crm [pros [Froon2 rei ne rr | reoens|[| awnwee |woows ||CaEwRamI|eiwene| [w | wwa w|m ve ewe | wn | [maw| wo [Tw [owem| we | |Camaas|m| awames|| wvow ||ommeem|| wmwe] sas| mw |wo|mmam| owe| 0 | - som| ean|w |ower | vw | | wen | moo w |w we | mJoewreen |[| w~e | asa| am | mew [w| r we | owes | B sma | ws | we | omom| .w poes 1n202 61 8 SAnoatluymtibciaalServices Created with Analyps1t1Reporter Printed: 140212010 6:41:00 PM Quantitative Peak Review z 32 # oT |cl Ed A = iZ=| K1000968-003 TE fL=o A o4B1a3s0el/Pi1Fn6Oe8A.01Mi0sased | 411730C3-7P2FO0A08 Baseline cMissed | 463.0P1F41N9A.0T 0a Baseline cMissed | 46153.C0-1P4F2N3DA.a0 Baseline Missed HY. ag o= ey A": a Ii- 1i2 aIJ hana tLfo ll A iL rit We ne 499P.F0O60S01 0a cBasolinecMssed | 501330C/.8P0.F0OSDa cBaselneoMised | 513P0F4D6A9T002 oBaselnecMissed | 51153004-7P0F0OADa Baseline o Missed 3 "havc MdeIse] 7 | i=| ars i- A LI 1 J J I 563P0F/U5R1A901 0a c Baseline Missed | oB51a63s5Ce.0-l1nP2eF70cU.n0MAi0sased | oBa5s00e.lP0i/F8nO0e0ScDM1iassed | c Ba5s01e33l,i0Cn/-e8P0oF.0OMSDisased " - [tt lin eg a I Ll Zh i1 1] giers nBreeen] d RF Hz2lfilinnnngedYam)a] nA e 6130P/F5D6OA901 Da cBaselinecMssed | 611530C/-1P6F9D00A0a cBaselneoMissed | 663.P0E/6T1A9.10 0a oBaselinecMissed | 61135C0-/PF1D6OD9Aa0 Baseline o Missed 3 | Fi af ening] | 713.P0F8T6G9A.1Da 61153C0-/P1F6D9O.0A0a Baseline o Missed| c Baselineo Missed 0 Before O After Page 164of262 62 4 lamba $ Satya services- Created wih Analy p1o2 rter Printed: 1402120106:41:00 PM fon Ratio Confirmation T = K1000968-003 = - E [ TL [zi a 3 I- d | iA| eB [a | lp We 413.0P1F3O69A.20 Da Baseline Missed | 463P01E2N1A920Da Baseline c Missed | 499.P0F/9O9S.02Da Baseline Missed | 513P.F01D22A609a0 Baselineo Missed Wiong Peak Wrong Peak Wong Peak = Wiong Peak EE 2 ; - i HE Se Lue| hen Ely no, 563P,0F1U2R69A.02 Da CBaselinec Missed | 599.P0F1O99S.20 Da oBaselinecMssed | 613P0F/D1O69A02 0a oBaselineoMissed | 663.P0F/1T6A9.20 0a oBaseineo Missed | Wrong Peak Wrong Peak Wrong Peak < Wong Peak | 71P3F0T/e1A629D0a BWasreolinnge.PMeiasksed 0 Before OJ After Page 165 of 262 63 5 Goamia AnalyticalServices Peo atanalpi.1S3epnorer RwDoesnuntTabe GE oooanmeDtP oasmampesS aronsaintids mrumentName_ Abro10p [[cSaAcauqumtieistNoiaonnmeeatteh|Tw2r0o2m0a1e0eTr6-81467 08 SaTDmeipcolaennTFyoapsetmare [[ U 100 n5t] o|| njecionvir Results Summary WeitagVohlrutmre [000] - Tame" |wnme[saa [RENEE] ava ses Preeat | woprwa| sEtoEw [EaTmEa)|EmEew I |om| Ne | raat reat | ores | com| woe smo [[asssmeem||w wn | |w oaom r]| prea | cera| sms [smeay| tens | aoiAl Pre wore | woe nem| ww | om | we saormis | sceron| so [ova| meme | om |we| [somrroonr||rvecoeerro | sso| escen| swe | rw - 4h4o!0 &eT% 2 ste Pag14501245 64 [4`AnalmybtiicaalServices IRC Summary Picnri:os18t02i/2n01i0 2.3g40o0eFIr [Pras2 oraz ra wee| wm No | osT040) we | mom [we | vo [| wrwaem||=ew A 65 8 SAnoalluymtibciaal Services BQueantaitratieve PPeeaskRReeview = m 3 bo-Ss 126 = 3 = be ee] 213P0/F1B6A910 0a 211730C1-7PF2B0A08 cBasolinec Missed| oBaselne oMissed 5 iEl3 350 I| 263P0E1P2e1A901 Da | Baseline Missed p15 PriCnrteeadt:ed15w/i0t2h/A2n0a1l0y2s:t3R4e:p0o0rPteMr K1000968-003 =5 io.. Cl 311530C1-2P7F0H0KA0a | o Baseline Missed =| ores Cpe Bo 2690/8002 -- oBausealinnego pMeissed 3 -3t i i worfis TLR 4030/1030 Da img Baseline c Missed | k= | | pra Shere TL 313012690 Da bsg | Baselinoe Missed L] aorta er] 315012700 Da Baserlienye Missed = IEl1 -=| oBa3s6e3Pl0iF/nH1eD6AM9i01sDsaed | bag pea cB31a1s35eCl0-i2Pe7oF0MH0iAs0saed | cBa3s09Pe.iR0nH/eX2cS00M1iDsased | woe {woes 4013800/-1P0F3H0SDa BasWeolinnegoeMaissed } ~| | i. |] i. = Fo 4S03_.108/010-3P.F0H0Sa cBaseineolissed | 51135C0-4P7F0O0A0a cBaseineoMissed | 5S1_51.30C4.7F0F.D0Aa Baseline Missed | 0 Before O After 511530C4-7P0F0OADa Baseline Missed Page 147 of 245 66 4 SAnoalluymtibciaal Services- Created vith Analyps1t6Reporter Printed: 1510212010 2:34 0 PM e fon Rae tEioeCeo-- nfoirm-- ation ------------ KT1r00o0e e968-0e 03ese ee ee e [ | =-E iE f126 E s|1[m sme m| |o|hseeli fo=HdAYeni | ten 213.0P1r6g9a.02 0a Baseline c Missed | 263,P0E2P19o.R020a Baseline c Missed | 209P.0r1e9s8.?00a Baseline oMissed | 313P.0F11H9.200a Baseline o Missed Wrong Peak S=I Wrong Peak == Wrong Peak =i Wrong Peak x LT AE Re i =) i. Ti otakde 36J3.o0315.0 0a 399.01l90.sDa 51i3.n0c47o0n.00a a oBasWerloinegMPiesasked | BaseWliionnegMPiesasked | Bas0eWlrionnegoPMeiasksed | BasWerloinnego PMeiasksed NB PFBA and PFPA G6 nol have qualiying Ton Vamsions 0 Before 0 After Page 148 of 245 67 8CSolautmbiiea services: PriCnrteeadted14w1i0t2h1A20n10a6tp:411R7e.p0o0rPtMer OPraotjaecFtile Result Table c0E22v00a86n11s00S5PaSrmapmolpeclseLrsoLCnogsngabwif Instrument Name__API 5000 [SAacqmuipsitNioanmDeate |TK2i109200010061%2030510 AM `Acquisition Method| PFCKinetex_doanmg S[ampTle Teypeei[[5oUnnVkaamomwen|| [Dilution Factor [100 | Results Summary bron Analyte Peak || womror | we for sos vornw | zoo | womros| eon [isto| Analyte RT we |tow| Calc. Conc: w [|zowawsye||0 wwe ||owma| | wwo | (PrEmATs oT3eCrPFmDoA| [19m79o00 | [00o05w.1s4)|0 wNnA] | wNoe] ore ed Page 166of 262 68 4 Solambia AnalyticalServices- RSCummary Pr Lr I PrCinrteead:te1d4w/i0t2h/2A0n10a6s.4R1ep0o0rPtAeAr ad [srezman [aC mase||aw wmna||ww weo|wwom|| ww e] [msomn Josmnoaw|| ma+n||wwee|ooommew||wn|] [rss Lomo | + | we|ooo | [pros Toman || ve |wmem| 69 8 Soma Analytical Services" Created with Analysi1R9eporter Printed: 14/02120106:41.00PM QuantitativePeak Review K1000968-004 - -3) rd z |7 | rd [E=H: oF ol -~ =- i=3 -- i= 413P0/F1O6A910 0a Baseline Missed | 41173.C0-3P7F2O0A0a Baseline cMissed | 463.P0F4N19A.T0 0a oBaselineoMissed | 461630C1-4P2F30NADa Baselineo Missed -o! f 3 " | Fw=ffret A : Saesed J =| 499P.F0O60S01 Da Baseline u Missed | 50133.C0/-8P0F.0OSDa cBaselnecMissed | 513P01F4D6A910 Da oBaselineo Missed | 511530C4-7P0F0OA0a oBaseine o Missed T 3 o ord q " Toe zfr ok {i1= iFermgguignn) i3 563.P0F/U5R19A.10 0a U Baselines Missed | 51635C0-/P27F0U0NADa Baseline oMissed | 599.0P/R8O0S.01 0a oBaseline Missed | 5103C0-0PF.GDS0a cBaseline c Missed =Lp] ' FS girm dedl ) A| 6130P/F5D6O9A01 Da Baseline Missed | 61135C0-1P1F6D900ADa Baseline cMissed | 663.P0E/6T1A9.0 Da oBaselinecMissed | 61135C0-/PF1D6OD9Aa0 oBaseine c Missed L71 ]w ipairifey1 eh 713.P0F8T6e9A.1Da Baseline c Missed | 61135C0-/PF1D6O9DA0a Baseline o Missed 0 Before O After Page 168 of262 70 olumbia AnalyticalServices" PriCnrteead:ted14v/i0t2h:A2n0a1l0f6s:P4R1e:p0o0rtPeAr dei . Lc lon Ratio > = Confirmation = = K1000968-004 | =i A | C4B1a3s.e0lP3iR6nO9eA.c2Mi0s8sed | 462.0P2E1N5A.008 Baseline o Missed | 499.P0E9G5S.?00a Baseline oMissed | 513P.F0O2A6290.0a Sassi o Missed -Wiang Peak Wiong Peak = Wrong Peak Wrong Peak a 3 of J E 3eer s|a5SL Al ibMonnOeVIrEE |[[Slap 1ute] TER TR) oB5a6s3eP0iFn2Ue6Ao9M02iDssaed | Ba5s0e9lP.i0Fn1eO95S.M20i0sased | Ba6s1e3Pl0iF/nO1eG6c9AM02i0ssed | B6a5s3e.Pl0i1n6Fe9.0T2Mi0sased Wrong Peak Wrong Peak Wrong Peak Wiang Peak B7as1ePl3iR0nTe1ce62AM9i0s0ased WongPeak DO Before OJ After Page 169 of 262 n 6 Samba AnalyticalServices PaCnrteaa:ted15w0it2h/2A0n1a0ly2t1R3e4p0o0rtPeIr PDraotgaeeFtile FG2a0r8s10PSaomRpalRePssrhCoEr wit RInessturlutmTeanbtleName AP0I205s0{000SampesShorediadh E `AcquisitioT n Date |2E /8/201Y 0 11:23.40 AM |ATcjqouciisotinoVnial tiod|Prounioxshardom RReasueltPsekSummary rSaemcpolenTVyopteame [ [U5 ni] on| |DViigohtniFoavcottoarms[1[00 606]| od Sie Gore Frastro|mwonrs||ssonmo [[asmmaom |[swws|| ooww | z Torro Tacrra| ssisz0 | 530630| tates oz | me PFHpA 1 13C-PFHxA| 4515200 | 6.22 (6.23) 26357 0.09 <4 No S_180-PFHS | 13C-PFDA| 4189100 | 6.31(6.31) | | S_13C-PFDA 13C-PFDA 4189100 | 7.64 (7.65) 3062600 4189100 oss | No | 1.00 No 4Tu pre sl Page 14301245 72 4SolumblS,ervices" IRC Summary Printed: 15/02/2010 2:34:00 PM frreapsere ew [oprarcam [sermon [mDemo||w mweosa|| wm woo |[owweaen|| vvee | mem| mow |we| swem| w Za [mooxemn||owmm ||w we|w owe ||v|e |ssa |wm| wesion| we] 73 5 Golambis AnalyticalServices" PrCintedr: 15ie0t2h1Aa2n0a10lty2t:3Ee4b:p0o0rdtPeMr - Ts Quantitative Peak = Review 7 i -i a= 21p30r1a1690 0a 211730C1-7F2E0A00 cBasedlainngeopMeissed |oBaselinegMissed Y Ss K1000968-004 if ase =x | 2p63r0p2e1A9t008 311530C2P7F0I0XA0a | :oBasbeiinoegcMeiassed | cSalsaegoiMpienasseed i- | i Z| I eB] EL or] Be x 26p6.r0e/8s0.i0 0a 40o30p11i03s0 Da | 313P.0R12A80T.0 0a 511530c27p0F0A0a oBaseine c Missed | oBaseiingecMssed | oBaiselginesc Missed | oBaselningec Missed a Be L= 33 : = ol i: 36P3r,r01i1p69A.10 0a 31s5c02o70r0n0a | 39p0.r0i8n00]0a 40138001-1p0F3i0isDa BaselciMinsseed | BaselinecMissed | oBaselnecMssed | Baseline Missed | z1l [Li = I iz4 = = B4so0s_3e10l81n01e-0cF3F0MHi0Ssased | oBa51s1e35lC0i-n4eP7Fo0O0MAi0sased | oB5aS1s_5e1.i30nC4e.7cP0F0MDi0Asased | o B5a1s51e.l30iC4n-e7Po0F.O0MAiDsased O Before O After Page 1510 265 74 8 lAnualmybtiicaal ServicesTM Created with Analyd2Ae4porter Printed: 15/02/20102.3400PM fon Ratio Confirmation -- 7 || 1 [= 1 K1000968-004 = = as bo=l aps f=T | --| = Ld 2130P/F1E6A920 Da BaseliMinsseed | 263P0F2PE1A9200a BaseloMiisnseed | 209.P0/R9E9S.0? Da 31P30H/1A219D0a Baseline Missed | oBaselo Miisnseed Wrong Peak Wiong Peak Wrong Peak Wrong Peak Tz = 7 : STOR | en : fi) Tips seie a J= 363.P0F1H3D1A.2Da BaselcMiisnseed | 309P.0F/H99A.S0 2Da Baseline Missed | 5S1_31.30C47P0F0D0Aa Baselc iMinsseed | NA ocBaseciMinsseed Wong Peak Wrong Peak Wrong Peak c Wrong Peak NB. PFBA and PFPeA do not have qualifying fon ransitons. O Before O After Page 152of245 75 3AnGaloytmicaal Services- PriCntedr: 14we1i0h21Aa2n0s1h0tp6E.R4ee1p0o0rdPerM PDraotjaeFcitle GEv2a0n8'1s0P0rSoajemcptsePsFLoCnsg.vi InRessturlutmTeanbtleName A0P2I0851000S0amplesLong1db> [[[SAcaamuiesiNtoanmbaete | 2K1i9c2o0o1s0ee7-2a045050 AM E SampleE Type A[cquiwstioen Mecthod[|t3P5FoCnentesvLodanimg ar[|DiwleitgonntFoavcotomrme[[700000 -- || Results Summary natsPeak Tae AY ie Ean ron vworron | mem |1mosn| mew |vom| we | pros ncros| some |2masy| wns Front rs | ome| 0 wo |me| Prowi | oem| ene [aman| om |o|m we | Pros | woeros | sen ane| am |oom| we xryn ZX" L 11kle Page 170 01 242 76 oa \nalytical Services" Sao es Created with Analy Afporter `RC Summary "arate peak ame foeoun [soma [swam| www Got Expy| to ons | we|omen|e | sooron prumnz [oascrmom onmien] | smaw|m|a wm |oo wamm| C wweo||w w0ma||om wme ||mowmoemm | w|e men|w Tow T|ommew| >= | 77 7 SAnoalluymtibciaalServices p27 PriCnrteead:ted14w/i0h2/A2n0a1l0y6s:t4R1e.p0o0rPteMr Quantitative Peak Review =7 ry rg = " | K1000968-005 EE 1 ol 2 i i- I- "gin goon) elas Wane good a 4130P/F1O69A.10 0a 41173.C0-3P7F2O0A08 463P0E4N1A90T Da cBaselinec Missed | Baseline Missed | Baseline: Missed | 4661.30C4-2P3F.0NADa Baseline c Missed g2 iy A z-l |AlstTRnel]! oA Tl A pppoed wef 499.P0F/8O0S.01Da 1530C0-/8P0F0OSDa 513P0F4D6A901 Da lcBaaseelineecsMissed | ooBasg elineyoMissed | oBasewloimnec Missed | oR 511530C4-7P0F0OADa -Baselinngeac Missed i ne | pr I Lobes Ld A 63.P0/F5U19R.A0 1 Da 5615.30C/2-7P0.F0URADa 509.P0R/8O0S.01 0a 501330C/8-0P.F0OSDa --Baseliineac Miassed | BaselitneiucMeissed | TBaseli0n0e0oPMessed | Baso elineg o Missed 3 = iS=hl2ei sogeins NWiAerd]Jo2] 3 | f3h]Addngadn dehesff xf wl | 6130P/F5D6A901 Da 61135C0-/1P6F9D.O0ADa 6630P/F6T1A8T0 0a 61135C0-/PF1D60D9A0a Baselinec Missed | Baseline cMissed | Baseline cMissed | Baseline o Missed = And Fo EE 713P,F0T6e6A910 0a 611530C/-1P6F9D.o0A0a Baseline o Missed | c Baseline c Missed O Before O After Page 17201 262 78 8CSoolaumsbeira vices Created vith Analy!0.R2e8porter Printed: 141022010 6:41:00 PM lon Ratio Confirmation K1000968-005 [i - 138 IELA |i -| -heme |EI= RIe RCe | -=e) ne nt 41B3a0Ps3Fe6OA9l20Mii0snaseed | 4B6as2e0lPi2nF1eN9A.M20is0sed | B4a99s,P0eF9Ol9So.2iM0i0nsseed| oB5a1sP3e0F2Ool62AMii90sn0saeed Wrong Peak Wrong Peak Wrong Peak = Wiong Peak ui -l Lz sl JD hoOsR teEd||boogee y =STfhhA aiif"|iEZR he L epiYA B56o3P.0sU12Te6A9c.lM?0in0ssaeed | B5a99Ps.r0e1o9osl9.M2i0i0snaseed | o B61a3P.s0F/e1D6cAl9.?M0ii0snaseed| oBa6s6e3lP0i1nE1eT69ZM0i0sased Wrong Peak Wrong Peak Wiong Peak WrongPeak 3 ' B7a1sP30Fe1Tl1eo62iAMi90ns0aseed WrongPeak O Before 0 After Page 17301262 79 5 olmbia AnalyticalServices- Created with Anabs2t9Reporter Printed: 15/02/2010 2:34:00 PM Project Data File Evan's ProjecsPFCs 020810\SamplesShor if InRessturlutmTenatleName__ A0P20I851000S0amplesShortedit ab [SampleName Kio00968-005 [[AAccaquuiissiittiioonnDMaettehod||2P1F9C7K2n0e1t0e1x1S:h3o3r:t12dAalm Injection Vial [25 7 [InjectionVolume T6 SDialmuptlieonTFyapcetor |WeighttoVolume[000 Results Summary [Rnaiyte Peak Faiyie RT LT Name [ stone [aw | (ExpRT) | AnalyteAre Gee cone ng/mL) | Modified? PFHpA 1 1ICPFHAA| 4853600 | 621623)| 31533 HPoFHS 1 180PFHs | 3167200| 631632)| 33280 SIBOPFHS | 13CPFDA|441380|0 631631| 3167200 081 1 [sisceron [ rscrron| anseoo [7409[ ssimo0 | 10 | No No No wm | +l? FJuoste Pa153gof2e45 80 AnalyticalServices CrveithAanantSepordes `RCSWmwary Tonaparomrame [eran| men | moana| SH rns | Roocontim|s ws fon Perez sworn [aman [am | we |omen |e soem| wan |we|mom| ve |ame |aso| wo |mew|v] 81 6 AGnualmytbiicaal Services PrCinrteead:ted15w1i0t2h1A2n0a1R0s2t:R3e4p:0o0rtPeAr Quantitative Peak Review =B i 7 ra = [| - a | TFy a] ase Tk K1000968-005 oT f s 1 3 2B1as3e0lP/iFn1eB6A9M01iDsased | 21137C0-1P7F2E0A0 oBaseino Missed | o2B6a3s,sP0iF2nP1ee9c.AM01i0sased | B3a11s35Ce0-P2loF7HMiKi0DAsn0saeed iy ro bag i presi 209.0/800 Da 40w3o01r0d30s08 || 313p0e2d69i008 3115021c00 Da cBaseiinneg Missed | ~oBacsealngecMissed | | oBaCsleianboceMsissed | oBagseyolMiisnseed A : =3 I== =3 3 L nl 1 1 ns 363P0F1H1p6A901 0a "Baselineu Missed | 13135C.0-2P70F.H0A0a oBaselinec Missed | 309P.E0H/A8S0010a oBasainec Missed | 40138001-1P0F3H0SDa oBaselinec Missed ia ec Cong fea ewan tng ea -3 = E = Ll = El S_180-FFHS 13C-PFOA S_13C-FDA 13C-PFOA cB40a3.s0/1o0c3l.M0iiDsnaseed | uB5a1s5e.l0i/n4o70c.M0iDssaed |i oB5a1s5e.l0/i4e7c0M.0isDsaed | B5a15s.0e/47l0o.iM0iDnsaseed O Before O After Page 155 of 245, 8 5AnGaoluytmibciaalService fon Ratio Confirmation --% = PrCinrteeadt:ed15w1i0t2h1A20n1a0l2y:3A4p:0o0rtPeMr K1000968-005 | = = [Ce oh he | ie 2130P/F1B6A920 0a 2P63F0P12e1A920 Da 20P9F.0E/9S92.00a 31P3R0H1A1Z000a _ BasWerlionnegoPMeiasksed | BasWerlionnegcPMeiasksed | BaseWlrionneg PMeiasksed | BasWerloinnegoPMeiaslsed ez El= x. | 4 i ooep | Tenapsrdeie gin } ol 3p63r01i3A1920 0a 30p9.r0/i99s.020a 51Ss510a4C7F0F0oDRa NA BaseWlrionnegcPMeiasksed | BasWerlionneg PMeiasksed | Bas=eWlrionneg:PMeiasksed | BasWerloinneg:PMeiasksed NE PBA and PFPeA do nol have Quallyng on ransiions 0 Before O After Page 156 of245 8 AnalyticalServicesTM [[AcSqauimsietNioanmbaete || 2Ri2o0o1o0s61%2406824 ANT I SampleType [`Acqunisitijon Meethocd[|2Pt6FChoinentexVtdoangim al|DiwluetiointoFgavcothlourtme[T1o0o0 Results Summary -- || PFOS 1 13C-PFOS | 6481000 | 2.41(2.53) 54778 0094 | No Pru | wo|rwarrm |uamman| swe I) M Front | rsceroon| tos [omen| Prat |woeron| own [oma| 0 | wa | we | Ze Aatv 21H 84 Lees Analytical Services `CSOMWQY Roo Created with Analyst. Rporter [eon Prinz wor | mo | omeor| we maw| ms | we|wom| f[rseormon owe [forproeosr: Tovmoos||0 mam | wmm |oomamn||| Tomas| 0 |w[amon|=| wean| wm | te 2- amos | some| wm |omom|e | . 85 5 Solumbia Analytical Services Quantitative Peak Review vi : =7 = bad Map A ol PrCinrteead:ted14w/i0t2h/A2n0a1R0r6s:t4R1e.p0o0rtPeMr K1000968-006 Tg iA 413.P0F1O60A.01 0a oBaseine Missed | 41137C.-0P37F2O0A0a cBaseline a Missed | 463P0E4N1A301 Da oBaselinec Missed | 4681.30C4-2P3F.N0ADa Baselineo Missed i digg ea ATHY. - bicug pea 13 i Jcf A a paS r SHl 499P.0r/O8S001 Da uBaseine oMissed | 51033C0-8P0F0OSDa oBaselie oMissed | 513P0F4D6A90 Da oBaselinec Missed | 511530C4-7P0F0OADa co Baseline Missed 3 = a oe Douche 3 "2 = 563P.0F5U1N9.A1 Da cBaseline c Missed | 15635C,-01P2F7U00nADa Baseline cMissed | 599.P0R/8O0S.01Da oBaselinecMissed | 501330C1-8P0F0OSDa Basen Missed = 7 3 Po 2 I El aE 613P.0F/D5O69A.10 Da GBaselnec Missed | 611530C/-16P9F.D0OA0a oBaselinec Missed | 6630P/F6T19A.10 0a oBaselinec Missed | 611530C/-1P6F9D00ADa Baseline o Missed 7130PF6T6e9A01 Da 61153.C0-/P1FD6O90A.a0 c Baseline Missed | Baseline o Missed O Before O After 86 Page 176 of 262 LSCRooluumsbeiarvices Created with Anlyhp3R6eporter Printed: 14/02/2010 6:41.00 PM lon Ratio Confirmation K1000968-006 [2 Ll EN a =- La14A 0 |i==lhppa|=i71 f Fa:holed, SMVeA Ba1s3P0a1Fn3O8Ao82M.i0s0eaed | B4a6se3lP0iFn2Ne1Ao52M0i0s8sea| 4B9as9eP0iFn2eO5So02M0is8sed| c B5a1se3Pi.nFe0Oo22A6M90is.sed Wong Peak = Wiong Pea Wong Pea Wiong Poa i zriP astiE lio Ba5se6lP3iF0nU2eN6oA6v2.i0n0sed | =Wong Poa 2 bool Rn it, B7Wa1s3oePl0Fni1nT1gee65AP.2Me0ia0skased 2 2a|[= oBa5s9e5PiR0nOe9S520Mi0s8sed | rong Peak 2t relEy N |-]emeditsieofle 0B6a1s5eP0iFn1De1O8AM9i20s0s8ed| c a663sP0/eF16oi8T2.M0ni0saseed =Wong Peak Wiong Peak O Before OJ After Page 177 of 262 87 4 SAnoalluymtibciaalServices- Created with Analys3t7Reporter Printed: 15/02/2010 2:34.00 PM Project warts ProjecisPrCs DReastualFtiTleable 0022008811008iSaampmlpelsesshSohroterdiitffcb Instrument Name __ AP)5000 [sampleName Tiro00668-006 [AAccqquuiissiittiioonnDMaettehod||2P1F87C2K0n1e0te1x1.S4h2o.r45tdAaMm SDaimlptloenTFyapcteor [100] InjectionVial J7 26 [WeightioVolume [ooo | rr | Results Summary a[RT i|GE | | er PRIS 1 180PFHS | 3265500| 6.31632) | 120210 [stops | 1acpron | so [e31@an| sesso | 011 No oss |we| +owa [PSarusasie Page 157 of 245 88 Logon Analytical Services PCireedte1w5i0n33A0n10a3t:3B6.o00 PrA CT IRC Summary [pronz F[orronszs Pepa Cid Tagan | see No | te000| ves 5 mam| wm || v wee| ve cae| wi | Ne | mse| we Page 15001245 89 AnGaollyutmibciaal Services Created with Analpys3t9Reporter Printed 1510212010 3.3400 PM -- Quantitative Peak a Review =5 == HA i 21p3r01a1i65i00a 21w7c0e17f2s0n08 CBaselnec Missed | cBaseinochissed = as 4 or :-boca Ae] E-l = sw K1000968-006 ECol ae i=o {oh | 263e0r2e1n5t00 311530C7P2F7A0D0a | oBasoinoe Missed | Basel i viesed RE= Ea IE= Shp I T 2 ee i =ol| o2Ba0s5eP0iFn6Bo0oSM01i0ssed | oB0as31e08i07n-0ePc3FM0HiS0sased ||| oB3aP1seF3lH0nX2eAo9M10ss0ed | uB3a1s1e35iC0r-2ePsF7mH0eAD0saed zl ne reg Bln = 3] olan Lol 3 = [W ft - Fe metodo] JU NY PFHpA 1 13C-PFHixA { PRHXS 1 180-PFHS. m Ba3s6e3l.i0L n/e169.M0iDsased | B3a1sG5e.li01o270.M0iDsa saed 1| c3o99.0gm/80.ee0 Dat | cd403m.0i110ns3.rh0sDian lL -I ==~| Ibo |=| eA Ar A Jnl A. oB4aSs1_o31l80n01e-0cPM3FiH0sSs0ea | oB5a11s3e5Cl0.n4Po7Fc0MO0iA0s2sed || oB5aS1s_o31i03n4Co-7oP0F0MDi0As0sed | o B5a1s15e30iC4n-7eP0oF0OMAiDsased 0 Before O After Page 159.01 245 20 2CAnoalluymtibciaalServices- CrweithAanatlHeepordter Printed: 15/02/20102:34:00 PM fon Ratio Confirmation K1000968-006 Hi --3 iw | (3=7 se " + 5= ho |2 ee: 2130P/F1B6A920Da Baseline oMissed| 263P0F2P1E9A020a oBaselineoMissed | 209P.0F1B9S3.200a Baseline Missed | 31P3R01H12A00a Baselinec Missed Wrong Peak Wrong Peak Wong Peak Wrong Peak - 622 "| hr 2a i =F emai mem] a 36P3E.H0O3A1290.a 309P.0E/99S.02Da 5s1_51.30C4P7F0D.0A0a NA oBasWerlonnegcPMeiasksed | BasWeilionnegMPiesasked | BaseWlionnegoPMeiasksed | BasWerlionnego PMeiasksed NE PFBA and PFPeA do nol have qualiying fon ransiions. O Before 0 After Page 160 of 245, 91 AnalyticalServices Created with Anal Heporer [[AScaqmuipslietiNoanmDeate |K2i9c7o2o0s1e0e10265757 All SjaemcptlieonTVypoelume [5 | `wAceqcutisointiVoanlMetho[d|2|P7FWCKneeteixLgdoanmghttoDilVutioonFamctoer [[100000 || moneResults Summary | oe RE |min| i | | [ora orma | zee | owas| 0 vost | worros| sms |2s| aswsy| oem Friar | oro |wa [ome | 0| wa wl 4,04 oy 92 AnalyticalServices CrweithAanalty eRepodrter RCSUMMAry Toners [enn| en won| Sg | Rogie [oraz Deva | | wo| owom| w [ores Loman|wom |w|wwmme | A ons w= rose Gia | mw |oom| we [rromz Tomas | om | wo |mem| w 93 ACY olum. bia F-- PrCinrteead:ted14w/i0t2h/A2n0a1i0f6s:4R1e:p0o0rtPeMr Quantitative Peak Review ~ =7 = K1000968-007 T= F Conf es eB] 413.P0F1O60A.01 0a 41137C0-5P7F2O0A00 G Baseline Missed | Baseline c Missed T " am A| A Lo 236 Fl i i lente] 463P0/E4N1A910 Da | cBaselinec Missed | | iT ="lataEWVeir] BA 4681.30C/-42P3F.N0A0a c Baseline c Missed T| 53 499P.F0O8S00 0a 50133.00/-8P0F.0GSDa 513.P0F14O6A9.10 0a 511530C4.7P0F0DA0a Baseline c Missed | Baseline Missed | oBaselnocMissed | Baseline o Missed "A kid 2= | i a. Focl A - E | 7 563.P01F5U1R9A.T0 Da 51635C0-/P2F70U0RADa 509.0P/F8O0S.01Da 50133,C0-P1F8O0DS.a0 CBaseline Missed | Baseline oMissed | oBaselinenMissed | cBasciine c Missed - NE rip niNAL I= bor nif lpg fT 6130P1F5DO6A901 Da Baseline Missed | 6151.30C/-16P9F.D0OA0a Baseline cMissed | 6630P/F6T1A9T0 Da Baseline Missed | 61135C0-/P1F6D9OD.Aa0 oBaseine o Missed 3z FEz Lyrrmansmdet =ere Ae Ba7s1e3Pl.iF0nT6e6E9A.1Mi0sased| o B6a1s1e53lC0i-n/eP1oF6D8MOi.0As0ased 0 Before O After Page 180.01 242 94 Columbia LO Esservices CrweithAanalytpsttRseepordter Printed: 1410212010 6:41.00PAA `lon Ratio Confirmation K1000968-007 [A | "| - |P| ieast||= |/ isd| et | _Ba4s1e3lP.i0Fn3Oe8Ao92.Mi0sased | cB4a6s3eP0lFn2Ne1Ac920Mi0sased | oBa4s99eP.l0Fn1O9e8Sc.2M0i0sased | Ba5se1l3Pi.nF0e2Oo62AM9i.0s0ased ~ Virong Peak Wrong Peak Wrong Peak Wrong Peak -| i} ! 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Wrong Peak O Before 0 After NA Baseline c Missed Wrong Peak Page 164 of265 99 [K Golambia AnalyticalServices PrGintedr: 1w4ei0t2h2Aan0a1i0fts6i:4eB1.e6p0odrPelr DFartoraeFeitle Gvaaoss1PoonRSAaSmEpRlCsTLoinfg RinessturlutmTeanbtleName __AP01205080t00Sampiesto0ngh [[SAacqmupistietNioanmbeate ||2Ki6c2oo0s1e0e-1a:c03s:35 All S[ampilenTypeec[[ t5 oUnnvi ouomne|| [mie[c2P6FtClneo texLonngdavr il[O[uWteiiognntFtaocvtoorume[[700000 | | RReastsulPtesakSummary Haar Sic Soe . orm| ammo | 23sen| asses ros voceros | swan ww | aso =x error| memo [s| w wme| ow |we| [Fro| vniorrtoos| mre|srewsy| mz oon | no Pra 1 TicrooR| ravi | 521619| sez oir No Fras | woeroos| mw [omar| 0 |wa | we | at 5 Zr ns Page 18201242 100 [Se AnalyticalServices: md Created with AnasReporter RCSummary Trnagareare = ferecnreeo [wenn| we Fg| vam| wee | we |oem| ve 1 saz|ww | Wo | ome| v.es Prumz sacrum rou z [sncproon eras Towam| 0| me |wom| - we "enon [0 ram| a ol wean| moo |we|wo|ownm| Do|m moa |wn| mow| vw | 101 8 CRoloumbiia services: PriCnrteeadt:ed14w1i0l2h1A2n0a1l0yps5t.451R1.e0po0rtPeMr Quantitative Peak Review =7 =I Ho iot y 3 o i3EE K1000968-008 = iol = Ba4s1e3lP0i/Fn1eO6Ac910MiDsased | ony Ba4s11e3l7Ci.-n0Pe57FM2Oi0As0saed | tig cB4a6s3e.Pl0iE4n1Ne9A.o1MiDsased | c~o Bo4a6s6g1e.3l0eiC/n-4ee2P3cFa.N0MAisDsased Lluf i7 i a _- =l|o ' L 1 A [hsp pi i : A Bas4e9l9P.i0Rn/eO8S0c01M0isased | oBa50s13e3.i0C/n-8oP0cF.0OMSsDsaed | Ba5s1e3l,Pi0Fn4eD69Ao.M10i0ssaed | Ba5se11l53i0Cn4-e7Pc0F0OMAiDsased = cl = Ei I 410 7 Tine sgh] A [wl ant - | | LA (B56a3P,s0F1U5eR1A9lc.M10iiDsnaseed | Ba5s6e15l30iC/n-2eP7FM0U0iRsADsaed| oBa5s0e9pl.ir0nO8eS0c0M1iDsased | oB50a133,s0C1-e8P0olF.0MOiiSDsnaseed i tomes i my ioTw 2|: i i= ceif: hp odd UL errno Ul Ro c B5a1s3eP.l0Fi1n3De8A9c.10Mi0sased | oB6a1s153.e0Ci1-n1P6eF3c.O00MAi0sased | o6B6as3e0PlF6iTn1Ae8Ao0M1iDsased | B6a11se35lCi0-n/ePF1oD6MOD9iAs0ased -- a dg a FoiA i L afi T one B= F ne B7a1s3e.lP0iE1nTe8e6cA910Mi0sased | Ba6se11l35iC0n-e/PF1oO60M9iA0s0ased 0 Before O After Page 184of 262 102 8 ASnaollytuicmal Services- Greated with Analyspt5R2eporter Printed: 1410212010 6:41:00 PM fon Ratio Confirmation K1000968-008 io E| Z| "f | aii i EE --J GoAE a | ht c4B1a3s.e0lPi1Fn3Oe6A9c.20Mi0sased | Ba4s6el3Pi0En2eN1A9o2M0i0sased | Bas4e99l.Pi0Rn1Oe99Sc.20MiDsased | oBa5s1e3l.Pi0Fn2eD6Ao920M0isased Wrong Peak <Wrong Peak Wrong Peak Wrong Peak == Lol| 25 =- := a. spe | [i =Tap i=Je S-- 563P,0U12T69A.20 Da 59P6F.0O19S9.20 Da 613P0O11C6A920 Da 663.P0/E16T9.A20 Da BaseWlrionnegoPMeiasksed | BaseWlrionneg PMeiasksed | c BasWelrionnegcPMeiasksed | BaseWloinneg PMeiasksed | d= ,indseliden, B7a1s3eP.l0Ei/nT1e6E9A.20MiDsased Wrong Peak [Before OJ After Page 185 of 242 103 4AnSaloyltiucamlServices Created with Analyps5t3Reporter Printed 1510212010 2:34.00 PM PDraotjaecFtie E02v0a8n1s0\PSarmopRleesPSrhoerstwi InRessturlutmTeanbtleName __A0P2I0851000S0amplesShortedit ab [SampleName iooose36e8 ZT [A[cAqcuqiuisiisttiisoonnDHaeetterocd|212t/86220o0101n5v7PiMa__r_|Sw_Daiimes_piglohen_tTtFya|vpcotelourme[6 100 5]| Results Summary p[Airnoeasss Peak INEST BwTorn Anais RY [mam] won | CaltoeeMCone a = [ roar r | oa rs|[st wwes [s r[wmoumm|| ww wwe |aw| wT [prvenr[|soomrer[ewmna] "wm | om wo [swore | acorn | so wow | ow | we | sriceron | woeron| mo | esen| emo | iw | we | Rae "otpiL, Page 165 of 245 104 Koss Analytical Services coCrneasted withAnais Heporter Rosmmay vagaries repr)|wa [5Gen ees| [[orrroesnz [emrmona oom m|eowwrn| wo | omweoml| vo l [masmw||wowemem||[wom| mvemmm|| = ] nor 105 PASCAnoalluymtibciaalServices Created with Anah5s.t55Reporter Printed: 15/02/2010 2:34:00 PM E is | = Quantitative Peak ReviT ew E SI = By K1000968-008 AoA] eld WL 213.P0r1o69n.]0 0a oBaseinec Missed | 21137.C0.11P7F2.B0A0a oBaselne Missed | 263P0p21a9]0 08 oBaselineoMissed | 31135C0P/F2T7xD0A0a Baseline Massed ion hy og a 7 ang =] fF ~ ll J Il s2e 05P.r0ra8s00eDa] s 40w30b o/1P0F30s] 0 | e313pe 02r6A 9a0 0ae W 3115300.2P7A F0F0hnDa oBaseine Missed | oBaselnoo Missed | oBaselneoMssed | oBaseling Missed 1 - M[Fo i : | ii] o3B6as3eP0iF1nH6ep9AM01i0sased | oB15a31sC5el-0nP2oF1oH0MX0iA0s0sed || Ba3se9lP0iHn8Ye0SM01i0s8sed | Ba4s0e13l80i01n-e1P0F3MH0iS0s8sed - = Lx = il il J} | ou 2 | lL A cB4aS0s_e31i08n10e0-o3FMF0iHs0Ssaed | oBsasi1e53l0Cn4-e7PcF0MO0iA0ssaed || oB5aSs1_e51l30nC4e.c7PM0FiD0sA0sed | 51135C0-P4F7O0AD0a Baselineo Missed O Before O After Page 167of 245 106 4AnaollyutmibciaalServices Created with Analypst.5R8eporter Printed: 15/02/2010 2:34:00 PM fon Ratio Confirmation a LoRTw I b \1 =CI K1000968-008 i=!zy = 7| ioe f Loh 2130P1F6E9A20 0a 2630P1F2P16e.A 20a 209.0P/F9E9.S02 Da 31P3F0/H1A12D90a C BasWerlionneg PMeiasksed | Bas<eWlrionneg PMeiasksed | B=asWerlionnegoPMeiasksed | BaseWlrionnegoPMeiasksed CT en E7 [ ja hp io =A ef po 363P.0F/H3O1A9.02 0a 309P.0F/H99X.S0 2Da $S1_51.30C47P0F0DDAa uBaseline o Missed | Baseline a Missed | Baseline o Missed | Wrong Peak Wrong Peak Wrong Peak NB. PFBA and PFPA do nol have qualiying ion iransiions. mpi NA Baselineu Missed Wrong Peak O Before O After Page 168 of 245 107 4ACnoalluytmibciaalServices Created with Analf6Reporter Printed: 14/02/2010 6:41:00 PM FDraotgaeFeitle cTaasisSParmopRlRePrsCLonvig InRessturlutmTeanbtleName__ AGP2I0851000S0amplestong 0b [[SAecqmupislietNioanmbeate ||--2W7i6G2_o0o1s0_ee101_16088_AM _[iSmampelecTypte i[o5 nVorame| `Acquisition Method| PFCkinetexLdoanmg [DilutionFactor [100 | njectionVial {25 | WeightoVonume [000 | | ne FRersyueltPseaSk ummary [we A[rEaT [vere | SiSciceoe | a: rox worron | azo | ere| mwa | iew |wo| Prat wor | zm |zmam| awe |om | wa e | Prost wcrros | swe |zm@w| veo | zw |wo| Teron we| 335039| tow wow |wo| pros wceros| soomm om|ui0 o| wa ~ 40 eTLe we Page 186 01 262 108 Ee RCSummary cnt [fcowrms [we oewans|| amew n|w|owww e||_e| [croomses [aswvaam||wwwne ||ow ||omwaenw|| eve]| [rors Tomo |0m omer| wm] R [em l | i em |n] e en|m | [[rcoomcsoon earmo || en || ve o|oemomn| | ] - 109 4 Solumbia Analytical Services p.59 PrCinrteeadt:ed14w/i0h2/A2n0a1l0ys6t:4R1e.p0o0rtPeMr Quantitative Peak Review K1000968-009 To = TT 3 TI zm Ei+ A ibo. A iE4] i =| A Le BaeNT BC 413P0/F1O6A901 0a 41137C.-0P37F2O0A0a 463P0E4N1A901 0a 4681.30C14-2P3F.N0ADa cBasellnuegceMissed | --oBWauseglianpeceMaissed | E oBase-- lineoMissed | Baselinetianc Mieassed 3 cl = | ==! iot I== as | i=4 499.P0F/8O0S.0TDa 15033C.0-/P80F.O0 SDa 513P01F4D6A901 Da 511530C4-7P0F.O0ADa i Baselie ne cMssed | oBasclinWeocMnigssed | oBnalseinecMissed | lcoBpaseine c Missed zl - 2 ot Hiri " At cl = i Te] 563P0F/U5R1A901 Da 56153.C0-1P27F0U0RADa 509P.F0D80S01Da 501330C/P8F0.OSDa wBaseWinne cMissed | Basehliine oMissed | roBaasedlinieciMissed | Sc BaAseliAneo TMissed - iZi | 1i=zzl -ii3 ern] ii===] | | 613.0P/F5D6O0A.01Da 611530C1-1P6F8D0OAa 6630P1F6T1A9010a 61153.0C/-1P6F9.D0OADa oBaselne Missed | cBaselinecMssed | oBaselinecMssed | Baseline Missed 71P3F0T/6e6A901 Da 611530C/-1P6F9D0OA0a Baseline o Missed| c Baselineo Missed O Before O After 10 Page 188 of 262 LS SSoluombeiaservices: PriCnrteead:ted14w1i0t2h12A0n1a0l'yp6s.:t46R10e:p0o0rPteMr fon Ratio Confirmation K1000968-009 =f we [IE=N Lc5 lo5 izEIN-- Fo fas A =~ fTjpSD 4B1as3e0lP%iF6nOe0A.c20Mi0sased | Ba46s3e.lP0iF2n1eN5Ac.20Mi0sased | Bas4e99lP.i0Fn/Oe99So.20MDiassed | B5as1e3lPi.Fn0DecA226MD0isa.sed Wiong Peak Wiong Peak Wong Peak Wiong Peak ===| ==3= i I2=1 [ ===Ea| mies| 22 Thetis| halen < B5a6s3ePl0Fi1nU2eT6o9A0M2iDsased | Bas5e0l9P.i0Fn1eO99S.20MiDsased | c B6a1s3P.e0iF/nD1e6O9cA.20MiDsased | Ba6s6e3l.Pi0F/n1eT6A9.20MiDsased Wrong Peak Wiong Peak Wiong Peak Wrong Peak B7a1s3ePl0Fi/nT1eE6cA902MiDsased Wiong Peak O Before OJ After Page 189 of 242 m 5 Golambia Analytical Services Created with Analfi6C1Reporter Printed: 15/02/2010 2:34:00PM Project Data File E0v2a0r8t1s0iPSaOmRplCePsSFhCorSt wif InRsesturlutmTeanbtleName __A0P2!08510000amplesShoredi. rab ETT I (iiectonviar----T22P/5r9C/--i2i0--1n0e--e1s2--:S1h1[o:r2w4dPaimMsignt[iDSioawmivpeloenFtTaycupteomre 1[ 00 ta]| Results Summary natyis Peak Fnsite RT Cae Conc IE wo wo | ow ~ PFOA 1 PRHPAY P[Fswso1re 13CPFHAA | 5508000| 530631)| | cera| ssa | 621620)| |[ T1secoerrrouns[|asnrswrom [soar| 588490 ow | wm | wos |ose| wresasn ||13 ow s|[we| Aae [ 2ust Page 169 of 265 112 LSCoSluumbiaservices: IRC Summary PrCinrteeadt:ed15w/i0t2h1A2n0a1l0ys2pt:.36R42e:p0o0rtPeMr Preaz I 'orpenz [raz [prrpa2 s_1ac-pFeA | s_13c-PFHXA [saan | 2020 359360) No 1.00(1.00) ves | No 1000100) | ves sown| ma | we | ooo 21022 |sesso| No | 332003 ves | 120020 | soo | No |z2ee(3ss| Ne | 5.30 (5.30) 5588000 No 9.50 (13.06) No. | Pa170gof2e45 13 4 olumbia Analytical Services- p.63 PrCinrteead:ted15i/t0h22A0na1l0ys2:t3R4e.p0o0rtPeMr Quantitative Peak Review = = Ca "-i we E=lJ Bed] Br PFBAT 13C-PFBA K1000968-008 =3 =5 bo ias =|| A Cen] WL - | PEPE1 13C-PFHXA 7-B2a1s3e.l0i/n1e69c.0MzaiDsased E I | s oBa21s7ey .i0i/n1e72M.i0p sDsaedaI| n c2B6a3s.ey 0l/i2n1e9c.0MiDsased | oc | B3a1se5l.i0ne/Wa2ngo7M0Di.eas0ased 7i fo = pb] 299.P0r/a80s.T0 0a -BaselineogaPeMaissed | : i i i ony 363P.0F/H1p69A.10 0a uBaseine c Missed | "| ib]-| eB] 4013800-1P0F3ii0S08 | 313P.F0H2A6A901 Da oBaselineoMissed |EoBase elinecMissed | i | i1 1 {+l en - hp 311530C/2-7P0F0H0XAa 39P9F.H08I010 Da oBaselinec Missed | oBaselneoMissed fo w|l Ae 311530C2P7F0F0XA0a | c=o BaselineEoeMnissed oi-l wl lr = = 403108/100-3P.0FHSDa | Baselineo Missed bd~1 := |= i3 zl z 4S63_.108/010-3P.F0HDSa 511530C4-7PF0D0A08 cBaselie Missed | Baseline Missed | == Lo= = fz |= zl || 5s1i5.s0c4p70r.o00aa 511530C4-7P0F0OADa | oBaseineoMissed | Baseline c Missed O Before O After Page 171 of 265 14 LE Columbia orice PriCnrteead:ted15w1i0t2h1A2n0a1l0ysp2t36R44e0p0ortPeMr fon Ratio Confirmation | E i- h T 126 F a=f = [14AM | B=5de|i Ba2s1e3l.Pi0Fn1B6e9A.20Mi0sased | 2B6a3seP0lEi2nP1eE9A0M20isased | Wrong Peak o Wrong Peat = = i= i o 3 J e Ji K1000968-009 2= 1 =i o A i ~t!t ld----[ J le i SR 2B9as9e,lP0iFn9Be9S.20M0issed | c B3a1se3PlF0inH/eX1A192Mi.0s0ased a Wrong Peak Wrong Peak T = Popernite oBa36s3eP.i0Fn1He31p9AM.i02sDsaed | Bas3e9lP5i.Fn0He9Y9oS0M2iDsased | Ba$sS1e_5l.1i0n34eC70Po.FM0iD0sAsaed | NA Baseline Missed NB PFBWAraonnag PPFePaekA do nol have aWuraolnyginPgeaiokn Tansions. Wrong Peak Wrong Peak 0 Before 0 After Page 17201245 1s [4 Columbia AnalyticalServices Created with Analyst Reporter Printed: 14/02/2010 6:41:00 PM [[AScaamupilsietoNnabmaet--sTRio210902001608611760E520 [r`AeccqutiosintvioinaMetho[d|3P0FCKnetestdoonmg Results Summary TSnajmepclteonTVyopeume |U [ nk5 oo] vn| [|DWietitghotnFaVcotourme[[1o0o0 || Pros worros|se|zmas | wwe | ire " Frnt | cern| oe [swan| wa |ow| [eros cros|sa|mseei | sw | oon | [roms | cores| immo [omen| 0 | wa | we ,Pe. 7 ue 116 4Somes Analytical Services oCtmrawheitlhAaenrato: eRiepddos Resammay Er [PsFrOaAc.2prom [srrz [[psrcosezros Pronz C 1.35(1.s 36)|ss 1o6515m0a 0 | wm Noo || 214238) swam | YES | [zvieeew||s wesa||m wfeo||oommmeam|| ve 2m3a2s8| san | wo |om|awwe=s| [oma | 0 | mw |owe | |prum2 [omuoo[0 | mw [owom[wm | [pros Fsromce r a) [rere ee oem [| eanrwmoasn| am | twoo ||omwaomm | [we | [sem| we | wo|owom| we | [sme [as | wo [owes| wo age 1910202 nz PASACnoalluytmibciaalServices" Created with Analys6t7Reporter Printed: 14/02/20106:41:00 PM = Quantitative Peak = Review Tw = Ta K1000968-010 - ol Ri Zl ol - - Le el de eA Lo Me fT A 413P0r1O6R9T0 0a 41137C0-3P7F2O0A00 463P.0E4N1A3T. 0a 4661.30C42P3F.N0ADa cBaselinec Missed | oBaselinoo Missed | Baseline oMissed | Baseline o Missed = J = A= : t- = = do mM | hep Pea] mL 459p.r0o30S0T0a 15303C0-1P8F0G0SDa 51P3.r01O46R9.T0 0a 511530C4-7P0F.O0ADa oBaselne o Missed | Baseline Missed | oBaselinec Missed | o Baseline o Missed al age ~| 33 Lo- "J 5a tl RUA re] 136-pFUnA Sees] PrOST ee130FGS Ba563s.0e151l9cM.i0is0nsaeed | cB5a6s5e.0i2n7e0c.0Ms0saed | oBa5s9s9l.i0n8e0c0MDisased | Ba50s3e.0lo80MiDa.sna0seed jii: | F=e i ish h3 o f=F Frog gel o elit eel el i. 61P3F.0O15O6A5.10 0a 5115.30C1-1P69F.B0o0Aa 663.P0E61T9.S0 0a 511530C/-16P9F.B0oA0a oBaseinec Mssed | oBaseinecMssed | oBaselineoMssed | Baseline o Missed | dhedd 2 713P.E06T6O9R.T0 0a 61153.C0-1F6B3oA.00a Baselinec Missed | Baselineo Missed 0 Before O After Page 192 0f 242 18 8 RColoumabima services PrCinrieeda.te14w1i0t2h1A2n0a1l0ys6p:.4Rb1e0po0rtPeMr fon Ratio Confirmation K1000868-010 i = = J] E E E B [-2 ole i t|E i:10Y I==tn | B4a1s3e.l0Pi3Fn6Oe9A.c20MiDsased | Ba4se6l3Pi0Fn2Ne1A9c20Mi0sased | oBa4s99e.Pl0Rn1e9O8S.?MDiassed | Ba5se1l3Pi,Fn0eO2Ao629Mi0.s0sed = Wrong Peak Wrong Peak Wrong Peak < Wrong Peak | 5 a 5 dss | ction | Lhe oncomminal ELSEJ Ra Wh hoiG o Bhi o B5a6s3eP.lF0in2Ue6R9cA.0M2i0sased | Ba5s9e9Pli,Fn0De9So92.M0is0sed | oB6a1s3eP0lF1nD1eO6c9A02Mi0sased | Ba6s6e3l,Pi0F1nT1e6Ic3A.20Mi0sased | Wrong Peak Wrong Peak Wrong Peak Wrong Peak E dr thls B7a1s3eP.l0Fi1nTe6E9oA.20Mi0sased Wrong Peak O Before OJ After Page 13 of 262 110 LS CS olumB bia services: p69 PriCnrteead:ted15i/t0h2/A2n0a1l0y2s:t34R:e0p0orPteMr Project Data File Ewan's ProjectsPFCs 020810\SamplesShort wif InRessturlutmTeanbtleName __ A0P2!0851000S0ampiesShortedit db [[SAcaqmupislietNioanmbeate | 7i9G7020051608152720057 PAE `Acquisition Method| PFCkinelexShdoarmt [injectionVial 30 STanmjpelcteoTnyVpoelume [5] | WeighttoVolumeJoo | Results Summary nai Peak Fnaiyie RY Ge Gane 13CPFHK|A 5771500 | 356360)| 1309700 252 No pros 180PFHS | 3272200 [425(426) | to0s80 | oss | No == | 13cpra| smiso0| 53030| 1801500 2 | wn | PrHpA 1 opr| smis0 [e216| ase0 | ise | ne | PERS 1 1soprHs| S220 [631630| esa |es| No | S180PFHS | 13CPFDA | 4561000 | 631631)| 3212200 081 No we [2224 2s Page 173 of 245 120 Analytical Services RCSwmmary ran Ci |sm w|a we | rom| ve res Prone mm| wn = emi | ww |ow | owe| ve [ememin * Tomow |_| 121 4AnSaollyutmibciaalServices- Created with Analpy.s7t1Reporter Printed: 15/0212010 2:34.00 PM Quantitative Peak Review = 7% T K1000968-010 =3 5 z = f ve] i. eA di A dl Rb A c2B1a3so0Pi1Fn6eBc8AM01is0saed | oB2a7s10a3i1Cn-7gP2oF0BM0Ass0ed ||| oB2a6si3PiE0nP2eE1oA9M01i0s8sed | o3a1135Cs0-P2oF7iiHX0s0A0esad "ina ea mya a BY :| . oo= 7 eA de b-= Ld] dL |a. | S ! L 20P9.r0/8s0.T0 0a uBaseline Missed | 403w.o0p10i3R.0s0a | 313.e0r2m6a9l0Da 311350P02F7A00a Baseline Missed | Baseline: Missed | oBaseine o Missed ong ea To = tics ea wane 7 " [= 3 il Ci i- - If -y 6 Ba3sP6e3Fl.iH0n/p1eA69c.10MiDsased | oB3as11e35lC0i-2nP7eF0cHM0XiA0ssaed | | oBa5s99eP.iR0nH/e8X0SM.0i1sDased | Ba4s0e1l38i00n1-e0P3F0AMSiDsased Mang ea Mong ea ny : a ~ iJ iJ x -- a i ol uL 4S0_3108/01-0P3F0HDSa Baseline Missed | 511530C4-7P0F.O0A0a | cBaselieoMissed | $s13c.0h47o00n0a oBaseinecMissed | 511530C4-7P0F0OADa Baseline o Missed 0 Before O After Page 175 of 245 122 5AnoalluymtibciaalServices" PriCnrteead:ted15w0i2th12A0n1a0ly2t3F4b:p0o0rPteMr Ton Ratio Confirmation K1000968-010 7% 3% . Er T | |2 El z E=o| la [-sh 2130P/1r6a9?0 Da 263.0P1E2P1E8R.0 0a 299P.0F1E99S.02 Da 313P0F11H90202 BaseWlrionnegcPMeiasksed | BasWerloinneg PMeiasksed | BaseWlrionneg PMeiasksed| c BasWeliionnegoPMeiasksed er 7 " a| - 4el | Terapia 363P.0F/H31p0A.02 Da 399P.R0/H9X9S.02Da Baseline c Missed | Baseline Missed | 5S1_5.1034C70P.F0ODAa Baseline oMissed | NA Baselineo Missed Wong Peak Wrong Peak Wrong Peak Wrong Peak NB PFBA and PFPEA G6 nol have qualifying fon ramsiions 0 Before 0 After Page 176 of 245, 123 PASColumbia AnalyticalServices Created with Analyst Reporter Printed: 14/02/2010 6:41:00 PM [[SAacqmupilsietNioanmDaet--eTRic2o17G2a0010801276:778 A TSnajmepclieoTnyVpoerume (AcquinsitieonHecthad[t|sPtFoCAnnetevxdtoimn ar[Di[vliteoignhFtatcotvoorwm[e 0J 0 oo]| Results Summary pro crron| am[vera | reemn| sso 0 FPFrNA o1 st| worros 13C-PFNA | sso 2166900 | [amas| 2.36 (2.42) womo 71582 | wan0.312 |wNoo|b rons noeron | moe wna | 0 | wa | [orunar | vorrom| sam |amaon| wm Ww] ro | errow| [omen| 5 | wm | w| LC 77 124 [i almbia Analytical Services PCrreeadted1w4it1h0A3n2an010Re6p4or1te3r EC RCSUMMER TC sl -- om ~ ereseTrowam|| rweoswm|e[m|woaamonm| |i=e a roe Tome]owomen| - rsoomeoarr TTeaemmmema[| wmweew[|oommeen| Tn| ~] wo ome| Tr [w | wo m |m w| wom| = Page 16501242 125 8 Smbia Analytical Services Created with Analyps.t75Reporter Printed: 14/02/20106:41:00 PM Quantitative Peak Review TT = TT f |= t Fo T EE of A K1000968-011 7 i. Fo 413P0F1O6A0.100a GBaselinec Missed | 41173.C0-3P7F2O0A0a cBaseinecMissed | 463P0E4N1A501 0a oBaselnecMissed | agg shi Vues i2= iLl i iFs i4 - v. aL Nia 499P.F0/O8S001 Da oBaselineo Missed | 5031.30/C8-0.P0FOS0a cBaseinecMssed | 513,P0F4O69A.10 0a oBaselnecMissed | 4681.30C4-2P3F.N0A0a Baseltiuneg Mipsensed 1| 1 511530C4-7P0F0DADa Baselinec Missed T.| ow zl = -| 3oo | : Aero] "| 3 563P,0E/U5N19A.01 Da cBaselinec Missed | 51635C.0-/P27F0U.R0 A0a oBaselinecMissed | 599.P0F/O80S.01 0a Baseline Missed | 50133.0C/.8P0F.0OSDa Baseline c Missed tion ea iy ions oe lta =ondEn aire if elo [Zil ae! x I . 613.0P/F5D69A.10 Da Baseline c Missed | 611530C/-1P69F.D00ADa Baseline cMissed | 6630P/ET6I1A80 Da cBaselinec Missed | 61135C0-/PF1O609DA0a oBaseine o Missed oh = cts EA 2) 713.0P/E8T6e9A.10 Da 61153.C0-/P1F6Do9A.0a0 Baseline Missed| cBaselo Miisnseed 0 Before O After Page 196 of 262 126 8 lama AnalyticalServices" Created with Anal7R6eporter Printed: 14102120106:41:00 PM E Ta [LEI fon Ratio CFolnfirmation | - | I K1000968-011 po Lo I = olf N 4130P1F3O6A920 Baseline c M iDsase d | 463P0E/2N1A920 Da cBaselinec Missed | 499P.F0O0S920 Da c Baseline oMissed | 513.P0F26O92A00a c Baseline Missed Wiong Peak Wrong Peak Wrong Peak Wrong Peak a|nnalltstirs|lzoLl ax erveenalelodetdy | le 28 | 1 "3eEgMgESEL | Ii=nnPW i 2 563P02U6T9A02 0a 599.P0F9D9S02Da 6130P/F1D6G9A02Da 663P.F0T/I1A6290.0a BaWsreonlgoPMeiasksed | BaseWlrionnegPoeMaisksed | BaWserloinnegPoMeiasksed | BasWerlionnegcPMeiasksed 71P3E.T0E1A629D.a B<asWerlionnegPeMaisksed 0 Before 0 After Page 197 of 242 127 3 Solumbia AnalyticalServices Created with Analyps7t7Reporter Printed: 15/022010 234.00 PM PDraotjaecFitle E0v2a0n8'1s0\PSraomjpecltessShRoCrst wif InRessturlutmTeanbtlNeame __A0P2I0851000S0amplesshortdit db [S`aAcmapuliseitNiaonmDeate |T2/R9I7o2000180881.2G.13T0.32 PI `Acauisition Method|PFCkinetexSdhoarm [injectionVia J31 = [TSjaemcplteonTVyopetame [5] DilutionFactor |WeighttoVolume [ooo | Results Summary `AAnnaaliyyi Peak isname [sara| TAnaTiSyiReTRT | nae aren | CGaatleeCoGonne Modified? PFBAT cere | artooo 12020| meso | ise |Ne| [PFPea 1aCPFH| 5115000 |359060)| 3136300 640 No PRES 1 180PFHS | 3208500 | 425626)| 2690400 23 No PFHcA 1 13cprH | 5115000 | 530631)| 957200 m2 | we | [ Pepa 1 CPA| 5115000 | 622623)| 721300 [ow| PFHAS 1 180-PFHS | 3288500 | 631632) No [s_13cProa | 13ceron e465)| 121500 wo [ow| & Jo on eer Sse Page 177 of 245 128 8 Sumi AnalyticalServices PrCinrteead:ted1w5ith/A0na2y2/i32R4e:0p0o01rPt0Mer RCSummary Araepestane | RT(EoRT)| Aes | moans|SHEN|Reoenim:| reruns Ssocen|sew| wo | moe| ves prasz sam | ew | i ee an| [sracern 060 wo | mcm| w 129 5 Soumbia AnalyticalServices Greated vith Analyps.t79Reporter Printed: 15/02/20102:34.00 PM Quantitative PeakReview K1000868-011 -- 7 Eg Ed =5 3 3 | - F = F=f a of A A J A 2130/P1F6B9A.01 0a 21173.C0-1P7F2B0A0a 263P0E2P1e9A01 0a 31135C-0P2F7HX00A0a Baseline0gMissed | Baselinea Missede | oBaselinegceMiossed | Baselitangeec Missed 3-: 1 266.P0E/8B0S.01 Da cBaseline o Missed i=|1. 4031.8001-0P3F.H0S0a Baseline u Missed ioo2ll, 8 313P0H26A901 0a | Baseline o Missed 4 a==oy 311530C2-7P0F0HADa Baseline c Missed Eo =zl fIi d= Hl2 363.P0R/1H6D9.A0 | 0a 311530C2-7P0F0HADa | 399P.F0H/I8S001Da 403108/100-3P.0FHSDa Baselwionneg: MPeiassed | SBasaelisneioMissed | oBaselimnyco Missed | --ccoBvaangselineec aMissed =| 1 1 |CLf =zl [xol 4S0_3.108/01-0P3F0H0Sa 511530C1-7PF0O0A0a | 5s15..0c1p47r0o0 n0a 511530C/-4P7F00OADa cBaseline Missed | Baseline oMissed | o Baseline Missed | Baseline o Missed 0 Before O After Page 179 of 245 130 8AnSaolyltiucamlServices" PrCinrteead:te1d5w/it0h2A1n2a0i1B0i2B:3p4:o0r0 tPeMr fon Ratio Confirmation K1000968-011 = EE 7 = j- | <i o | Zi |[I . 23 6 4J =d | p 213.0P/1F6E9A.02 0a BaseWlrionneg PMeiasksed | i-- | boo i iL 2630P/F2P1E8A020a 209.P0R19E9S.0? Da BaseWlrionnegoPMeiasksed | BasWeliionneg PMeiasksed | 4h e 7 e --- ---- F of aL a 31P30R1H1G92A008 o BasWelrionnegoPMeiasksed Diets sdukte 36P3F.0H1p31A9.02 Da 309P.F0R/H99A.S02Da 5S1_51034C7P0F0D0A2 NA BaseWlrionnegcPMeiasksed | BaseWlrionneg PMeaiks.sed | BaseWlrionneg PMeiasksed | BaWsreloinnegoPMeiasksed NB. PFBA and PFPeA do not have qualifying ion transitions. O Before OI After Page 180of 245 131 4 Solumbia AnalyticalServices- Created with Analyps.t61Reporter Printed: 14/02/20106:41:00 PM Project RDeastualFtilTeable Instrument Name E0v2a0n8'1s0P0rioSjaemcptlsePsFLCosng iff A0P2I0851000S0ampesLong rab [S`aAcpautiesitiNoanmDeate T| r2r9a7m200o1s0s10:3732.53 A Sample Type [Unknown| Acquisition Method| PFCKneiexLdoanmg Dilution Facter [100 | Injection Vial Js 2 WeightioVolume [000 | Results Summary [Tarnati Peak [sone [om[RAnEaiyEieTRT] mvanenes| GGaEteCGoEneTT wouter | PFOA 1 sosion [142038|saca| s osu No PENA 1 nce| eis [23804| 2st 0125 No PFS 1 13CPFOS | 5022700| 2.42259) No PFDA1 13C.PFOA 337030| 1198 0075 No +[pros | 13cpros | sozzroo| ooocer0 owe [Tw] A ef? Lue! 0 Page 198of242 132 nalytical Services omni RCSUmOary Created vith AnalyB BBporter |[| I Eg = saceros |zea| mmm | v me | swam | we Ta TaTe T ror Jame ww |owew| w. 5rscrron "muse | prea wo | owes | | 133 5 umbia AnalyticalServices Created with Analpys8t3Reporter Printed: 14/02/2010 6:41.00 PM Quantitative Peak Review 5 ra on = LC | = i Tee Bed AC 41P3F0/O16A9.01 Da 41137C.-0P37F2O0A0a Baseltiinea Miesa sed | BasA elinYe oMissed K1000968-012 = = Er Lo as 2A el A IF Aer BR | 463.P0E41N9A.0T 0a cBaselinec Missed | 4681.30C4-2P3F.0NADa Baseline o Missed <1 chong pe is A i A i3 i1 499.P0r12O0S.01 Da oBaseine Missed | 50133.0C/-8P0.F0OSDa oBaselinec Missed | 513.P01F4D6A9.10 0a oBaselinec Missed | 511530C1-4P70F0OADa Baselineo Missed 3 Coa wai,T k Fel 1 | = cz ol ipntpeney] 563P0F/U5R1A910 Da 56153C0-2P7F0U0RA0a CBaseline Missed| oBaslinecMissed | 509P.0F/O8S001Da oBaselnecMissed | 50133.0C/-8P0F.0OSDa Baselines Missed oink --cWonapea Ta wasn i[ i ebotnf i ==Z|| 1 Ih8,egros shoi afan ivnfbl=32) _ 613.0P1F5D6O9.A010a 6151.30C/1-6P9F.B00ADa cBasetiunoecMissed | a Baseline oMissed | ooff ist al a ye i 663.P0F6T19A.100a cBaWanselinec Missed | 61153C0-/P1F6D90D.Aa0 oBaseine c Miassed 713.PE0T6E9A01 0a Baseline c Missed| 61153.C0-/P1F6D09aA.0 o Baseline c Missed O Before O After Page 200 of 262 134 PAYColumobt ia T---- PCrreeadted14wi0th2A/na2l0y'1p:4o01R:te0ga0rtoerh lon Ratio Confirmation K1000968-012 =wt. 142 4| Loou f Fl=! be EWE 2 1 | - a he a e oBa1sWe3Pii0oFn3nOe8gA8o2.Pve0ia0et8ed | oB4a6so3Pl0En2eN1Ao820Mi0s0sed = Wiong Pea | 4BW9asr0ePlo3iFnn9OegS0cP20Meia0sksed| B5a1se3lP0iFn2e8Dc92A0Mi0s0sed 5 Wiong Pea oi = -l -. PI | am| Theyengabte|SNENT Ba5s6eW3lPi0iFo1nUn2eNg8A9P.2Meia0skased | oBaW5s9eol9Fin0Dng9eS9o2P0Me0ia8sksed | B6Wa1soe3Pl0Fni1nDge6O9AP02Meia0skased|o B6wa6soe3Plni0nF/ge1cT2p6Me6ias0ksed | AR | B7a1se3Pl0Fin1Te6e0A20Mi0s8sed Wong Peat 0 Before OJ After Page 201 of 262 135 LCE olumR biaservices Created with Analys8t5Reporter Printed: 15/02/2010 2:34:00 PM Project Data File E02v0a8n1'0s\PSraojmepcliessPShFoCrst wif InRsesturlutmTeanbtleName __0A2P0I85100080ampiesShortedit db [SampleName |Kioooees-072 [AAeacuqisuiionsHDieatttheiood|n|2P15F7C2K07m0et12e:x40S:h07doaPrmtM [injectionVotame [5] IE`Sample Type WeighttoVolume [000 | Results Summary - A[rnaiai Peak [svame| sama | TAnaRiyNteTRT aayenes | iCcaeColne Modified? PFH 1 1cPRca | seo [530630| veo | ote | me | S_160-PFHS | 13C-PFDA| 4777100 | 631(631|) 3497100 083 No SIICPFOA | 13CRFOA|aTTr|Tieeoqees | arrioo 1.00 No x ZF . 20051 Pa181gof2e45 136 AnalyticalServices Created vith Analy Harter RCS4mmary reama e CC r)|a d me m | we | = mam| vieid| [perenz Co|mwew |swoe| wom| ve [erm mom|ww | we[omen|e | 137 [3 Columbia AnalyticalServices* Created with Anaifps.t6R7eporter Printed: 15/02/20102:34:00 PM Quantitative Peak Review =]-- LoSI i= i ] Le ih L K1000968-012 , 5% i | m21P2e 0r/1i66]e 0 0ae 27v0e1eA 7f2dn00 L | 263p0r51A e5.a000 L 51153002700F0ADa oBaselinecMissed | oBsselneoMssed | oBaseinecMissed | cSaseoiMinsseed =I = = bd] io | i. a EA E296P0ra8s0000 = vw 4ep--0w30o110r30ea0a w | | _ w 513pp 0e28d0m i0 0a] wl 51153002p7i00TA0a oBasellnienciMaissed | oBaselnccMissed | cBascinorc gMissed| a oBaseln o missed =bool i| i|e i== 3P63r.0i/1p650 0a BaselineeoeMissed 511530c2.7p0F0TA0a 39p90r2s00108 Baasleliincee"Missed || c Base=lineFo Missed 4013500.1pF0i3i0s 0 = Baseline - Miassed i i. i. i. 3 " Nn . oBS4a_6st3e0ai1n00o3o.MH0iss0saed | oB5a1s15e3l00n4.e7pc0FM50iAsbsaed | $s7153.0c4.7F000Aba cBaselneoMissed | 511530407F0D0Aba oBaselne o Missed O Before O After Page 18301245 138 Columbia 4 Analytical Services" PrCinrteead:ted15wi0t2h2A0n1al0ys2:P3R4E.b0o0rtPeAr ee Tong Ratio Con-- fimrameatieoen e------ K1T 00096o 8-- -012creeps -- F111 J i= --ee 359. +| |= | _3 o2B1as3Pe0lF/iBn1e6A9o2M0iDsased | B2a6s3e.l0Pi1rn2Pe1e8A.M02i0ssaed | 209.p0r1e99s.20 Da oBaselinecMissed | 313P0R1H1IA92008 oBasceMiisnseed Wrong Peak Wrong Peak Wrong Peak 5 Wrong Peak TF = r [Bm IJ i ls = --r - - ipo: %; tL -- hr Tip dite. 363P.0R1H3G1A9.02 Da 3P09F.0H/9X9.S0 2Da 5S75_.10134C7F0.F0D0Aa BaWserloinnegPMeiasksed BasWerlionnegoPMeiasksed BWasreloinnegcPMeiasksed NB. FFBA and PFPeA do net have auallyng on ransfions. 0 Before OJ After NA BaWserloinnegPoeMaisksed. Page 184 of 245 139 Solumbia AnalyticalServices PrCerde.te14w0it2h/A20n1a0py58a.94R1e.po0rPtehr FDraotaeFtile ResunTasle Eoza0r8tsonPSraomRplceRsPLConTg wi o30s10samesLaanhg Instrument Name__ 4%5000 [[AScqauimseitNioanmveate | K2i0o2o0o1o0es1a471527 A `AceqcutiisointiVoinlMethod[|3P5FCKnetexLdoanmg TSnajmcptiloeTnyVpoelume |[ Unk5 no] wn| | DwieluitgihontFoaVcatourme [oso] EiRweysulPtesakSum[miaroyneme| sams | TAGaERiEr] -- anapenms | Gmaeceoe Pront | wwoe|rseomen [ome| 0 | wa | we | [Prost Taceros| wa | oe| a wo | [Frrext | cero| ows [omer] 0| wa "o 3i0 cc" 0 2th Pogo 20201202 140 Columbia LS Sonim services: CrweitAanalty Reepordter Printed: 14/02/2010 6 41:00 PM RC summary Vamos [freo:mer raz ose [rrmonn| wes [wouter] Ge Exp| Ro Canis [ow | wo |[owoman |= e Cm|aowmm| wm | owem| | 2mam| wz |o we |me | m we | (cooser vmwan||owws w |w[|ommmeon ||| e srreri [muon| we|w|omam| w-m | 141 PASCAnoalluymtibciaalServices Create wih Anap.sotReporter Printed: 14/02/20106:41:00 PM Quantiative PeakReview iooosesois :3 2 hao iaikADE3R "; -l| SI | 4 Loo LA El aheres iHRC uBs4s1o3iP0no1e8ic9Mi0i0s0sed | 4117a08p7F2o0A00 Baseline oMssed | o4B6a3s0oP4ie1nne8ic.M0i0ss0ed | oB4a6s1e8ic.n0eP4sMA2i5s0.sa ed ne mv - 2 mr =7 iL = ER | ai de| bis id 0 | Ca49s9e0rs0o0soiM0ii0ns0soed | ca5s01i33n.0.0op5cF0M50sS0saed| Ga5s1a3Pi0rn4eo65Rc.M0i0sased | Ba5s1h15i30n4Cg7Po0F0aAsDaed 3 pile EC P oB=3 Ld Foekaang 563P0r5u15000 cBassinecMissed | Ba5s0e15l.3i0np5er7o0nM0As0saed | cBa5s6Pe8ri.on0e0s0o10i0o8sed| oBa5s10d33i0n0.e0p0MF0Ga0Sc0ed li ts daa iano -| . le zl hemlet 2 HE = zpe i Fi Wan cB6a1sPs3ri0on50e6Ro8M0ss0ed | oG6as11a53i00n1Pe6FoB3Mo0sA0sed | B6a6s3h0iP0nEg1T8oA0mi0s0sed | B5a11s35ic0n.g/pF1oBp6oh90Ao0ased jLi ode 4ol | B7a1s3Pi0en6rg8ec0TM0s0ced| o B5a11s53i0cn1.g1p6F5BMo0in0s0sed O Before 0 After Pago 204 or 242 142 LSCoSluambiia services: PriCnrteead:ted14wi/t0h2A1n20a1l0py'56R2ep41:o00rtPeMr fon Ratio Confirmation |= = FX J ~K1000968-013 a _ a. [ Ba4s1e3l.Pi0F1n3Oe6A0M.2i0s0saed | Ba4s6Pe3lF0i7nN2eA192M0isDsaed | cB49a9.P0sF/O9e9Sc.02iMiDnsaseed | Wrong Peak Wrong Peak Wrong Peak t 3i hro iLl"aidPh |Lla"eN miTs | Cite | MOME | Ba563sP.0Fe1U2R6lo9A.iM20insDsaeed | Bas5e09l.Pi0/nF9e9O.S0 M2i0s8sed | B6aP13sF0De/1Ol6oA8iM20i0nssaeed | Wong Peak Wrong Peak Wong Peak 3 hog 713P.F0T/E1A6200.0a BaWseiloinnegPoeMaisksed O Before 0 After B5a1s3P0eF26lO9o2AMi0is0nsaeed Wong Peak p|] ipet RAT B6a63s.P0e/F16lo9A.2iM0iDsnsaeed Wiong Peak Page 205 of 262 143 3 Solambia AnalyticalServices* PCrradte 15i0t3h2n01052.h933R4e6s0sor FDroamFet ResulTable E ocza0oeartr 0osaammppr lieessssnhowonineasbt instrumentName __AP15000 [[ASRccaaamuueiirsttNooannmDMeaett--ehTord|i|oP2o2Fo0Cs1ke0eEt1o2er4x5a3s5hdoaPirm Cectonviar 58 I ET -- [wI Weignttovaatume [ KRo-- oo] RARenlsetupletsskSum|mawry e[nen T[RETET mavens | oee lCore | eater Pron 1 ce |sor e |sa me | rare [Pret soerks |a |enem| sem [sworrns sermon | | vaceron | worn | sssom0 | sot ean | wom | Tesasy| svzzom sow | om "o ow wo ow | wm | iw |we| xpe E25te age 16501245 144 OSAnalmytiicnalServices PrinCrteeadt;ed15w1i0t2h1A2n0a1l0yb2i:3S4:p0o0rPteMr IRC Summary mre rn|mtn S| ores: Co|w 0a| m we [wow| w | raz To|mmwe| mo | omew| v.e | [Peeeror mom| om | wo |[oowmaem|| ves 145 LS CS olumB bia services: Created with Analpys.t95Reporter Printed: 15/02/2010 2.3400 PM Quantitative Peak Review = T = % -a 3cl " a il 2130P1F6B9A.01 0a GBaseline c Missed | 211730C1-7PF2B0A08 cBaselieoMissed TT --waigeen K1000968-013 : = 3 fL x= es iAl Sed | 263.P0F2P1e9A.01 0a Baseline Missed | 31135C0-P2F7HI0DA0a Baselineo Missed uae cng ca 5 i= Tegan doe Be 209P0ra/s8000 40s3o0p1f0r3i0s02 Baseline Missed| oBaselineo Missed E | heeded A || 313P0R2A60T000 31153C0-2P7F0H0xADa | oBaseinecMissed | BaseloMiisnseed Lo - . 623 = EN = 631 i.| i== 1 in :~ Geo prHgh BeedlceAi P|E eesA f1h s0.pis Ba3s6e3l,i01n1e69c.M0i0sased | oBa3s1e5l0i2n7e0cM0i0sased | oBa3s99e.l0i/n80e.o0MDsased | Ba4s0e3l0i/n1e0o30MiDsased xo ng mang wf | fa |= on | il | Ah A lA 4S0_3108101-0P3F0H0Sa 51135C0-4P7F0O0ADa BaselciMinsseed | oBaselinec Missed | | 5s15c04h7o00n02 511530C4-7P0F0OADa Baseline Missed | Baseline Missed 0 Before O After Pa187gof2e45 146 Columbia PAYev P-- PriCnrteead:te1d5v1i0t2h1A2n01a0ly2:3B4E0p0orPteAr fon Ratio Confirmation pr ; K1000968-013 = = =i rer |joT C o eLms| Ba2s1e3lP0i1nF1eB6Ac920Mi0sased | B2a6se3lP0i2Fn1eP9A0M20is8sed | wWrn ong Peak - Wrong Peak g o M-y k | A = a Theptinenn| Bas2e0l9P.i0Fn1Ee9S8o2.M0i0sased | = Wrong Peak |: 2EA, Slee = B3a1se3PlF0inH1eI1oA90M2i0s8sed Wrong Peak Pepsi B36a3P.sF0H3eP1cl9AM.i2i0snaseed | Ba29s9P0Fe/H90lIc.S0iM2i0nsaseed | B5aS1_5s1.3e0C4lP7c0FMi0iDs0nAsaeed | NA Baselc Miisnseed | | Wrong Peak Wrong Peak Wrong Peak Wong Peak NB. PFBA and PFPeA do not have qualifying ion transitions. O Before OJ After Page 186of 265 147 A Columbia Analytical Services" Crested with Analpys9t7Reporter Printed: 14/02/2010 6:41:00 PM RPeDrsaotujalectFtilTeable EG02w20a0sn81'0100P\rSSoaajmempcptlsee\ssPttFoConscgngbif instoument Name API 5000 [SampleName Kiooooee014 Tnjecion Volume `AAccqquuiissiittiioonnDMaettehod||2P/F6/C2H01n0e1t:e48x:0t2doAanMrg. Sample Type [DilutionFactor [100 [niec[5tonviat|WeigtoVotume [000 BT | ie ARresausltPseakSummary | vie [REafHe RT|mie| ocare eCone | [Pront rn Tico | azoTan0 | 1403| or|amo[meen | taser oss wa | ome | Prost | vomros|sm|zeesy| ews | ee || wenn No 0 Prom | cers| nan [omuss| 0| wa | [rar | noeroos| naan [ome | 0| wa 0 Print| morro| ree [ower] 0 | wa | ow | A "ored o Page206 of 262 148 Columbia FAYsv FR-- PrCorveeda.ted14wi1h0A55a01B0416R.e6p0ortPoetr hd RCSummary wseerron [ern aman|w|oww woww|| Lomein |ww| Tome] | foames prumz Treiwoowm ||wvmw|noommse || n|| . Towam | 0 | w perez wom |] Page 207 ot 242 149 4SAonlaluymtbiciaalServicesTM Created with Analyps.t99Reporter Printed: 14/0212010 6:41:00PM Quantitative Peak Review : ro 77 ~ = K1000968-014 Tz : i FJ A io fa A BR VNI heme) TL - 413P0/F1O6A910 0a Baseline cMissed | 41137C0-5P7F2O0A00 Baseline cMissed | 463P0E4N1A91002 oBaselnecMissed | 4681.30C4-2P3F.0NADa oBaseine Missed T= 240 =3 240 po2 C 4 Ha - [= i= i A J RA heen LR 499P.0R/O6S0010a 50133,0C1-8P0F.0OSDa cBaseline c Missed| cBaselieoMissed | 513P,F0O46A9100a oBaselinec Missed | 511530C4-7P0F0OADa cBaseline o Missed bm HE aa ions ol 418 ol Jeo F =| 3 Eo i3 ha 563P0F/U5R1A901 0a cBaselinec Missed | 51635C0-/P2F7U0R0ADa oBaselnecMissed | 599.P0/F80O.0S1 Da oBaselneoMissed | 50133.0C/-8P0.F0GSDa Baseine o Missed Wines lio ze Wag pea: copes 3 PSShs an 2 faagpoaE ft |2 = Fe2 lMhe omit e = 613P.0F/D56O9A.01 0a Baseline: Missed | 611530C/-16P9F.D00A0a 663P0/T6A1901 Da Baseline Missed | oBaselinec Missed | 611530C/-1P6F9O00ADa Basie o Missed 7130P/F6T6e9A01 Da 61153C.-0P1F6D80.AD0a Baseline o Missed | Baseline o Missed 0 Before O After 150 Page 208 of262 4 lumi Analytical Services Created ith Analy!1R0ep0orter Printed: 14/02/2010 6:41:00 PM fon Ratio Confirmation = TT = K1000968-014. 3 7 l= FsBE = ien (J Ji R =- lt 413.P0F3O6A9.20 0a 463P0F2NA120 0a 499.P0F19O9S.20 Da 51P3F02O26A900a BWasoelninge cPMeiasksed | BaseWlrionneg PMeiasksed | BaseWlrionneg PMeiasksed| c BasWelrionnegoPMeiasksed - = =| ttn | 7 ET NE i pone 2 | 416 ALE | NMEA 563P,0F1U26N9A.02 Da 50P9.F0D19S9.20 Da 613P0F1D6O9A020a 663P0F/1T269D0a _ BasWelrionnegPMeaiks.sed | BaseWlrionnegMPiesasked | cBasWerlionnegcPMeiasksed | o BasWerloinneg;PMeiasksed ] To 713.P0F/1T69e.A20Da BasWerloinnegPMeiasksed O Before 0 After Page 209of242 151 5 Some AnalyticalServices rsEop7r.101 a bhe ryrmeyn EEoraassseee : s toni [SAacmqpuilseitNiaonmDeate | 2i/a6o/2o0s16051527.5%9.12 PI `Acquisition Method| PFCKnetexSdhaarm TE ST ample TE ype DilutionFactor -- [ -- [U1 nk0n0 ow] n| Ei ReSsults Sum|mwary e a r[SrE pen | wSwESe esr prt wos | se|srmor[aase| em [owns | smo [mum| wen | wa | o ne | sons | acon | smo[sem| www | ashe | PFHpA 1 13C-PFHXA 5453900 | 6.22 (6.23) 82017 033 [woroersms | Terorrosr|| swrnen T[osmvmie]n| wmms || avwe o |s_13cPFDA | 13cFDA| 4274300| 76465)| 4270 | 100 | Ne x0 AY reACrS e pas ets 152 column & cenvcar rA esna aS0is t2ec IRC Summary omaatperealstis [rronz [preeesn rraaz rn [rrmesz Soren sco | e ty n | wn es ) woumer|Calc So)(Exp) MRM|Ratio =Confirms. mam| wm | re | mam | ve aso(tm3.o60) || amwmoo || wwoe ||ooown(a1.o0w0)n| [vevse Coes| sew | | aww| ves cmon|m|w wo | owew| ve | owom|so| wo | wow | ve | Tam | wom | we | semos| swe| sew | wo | wma| vw w | oe ors 153 7 Colmbia AnalyticalServices" PGrraeted1w5it0h 8An2ap0y.a1100R3e3po5rt4er rr Quantitative Peak Review 7 wa Ts K1000968-014 - [| BE] Cl aueb21i3eP0rs1o6do0l0i0s0seede|] 2oBrasowocinrmefogbNnismsed|||[ oBaasboeimrneeoI odominusecd | | c S51aIso5cs0a37Fs0v6i0m0se d 3[ i i7 | co2m6pm8ri5en8s5e0o0M0sd | co1m0eo5i7pn0ei5ov0si0s0ed || oS51w3po05re8o0i5m0ent | o5o155oc0p2.F7i0i6an0s0ed I| "a|l 4 i' =|= Cbo56a3Pr s0e1eg5i5oe V0ii0nsa] sa | o oB3a1swo5l5A no2o7c0vr6im0] sned|| e oBa3c55epih 0en3ews0s0muased | PLB(a0Tis5noe5A ps5ie0ss0sa i | i3 |= ol JCo3Em5iR0nE0Aoh00 J| oco5m1eo5ir6nA 4eio7ot0i0nu0s0ed | | coB5wls7s2oc0i4nie7A oo0m0na0w0ed |boS5aa 1sss5i5nc4e7c0is0ix u0caed O Before O After Page 1910245 154 8 Solum Analytical Services- Created with Analysi10Re4porter Printed: 1510212010 2:34:00 PM fon Ratio Confirmation 3 : rd po Im - i "4 1d K1000968-014 = bo) a Ec afts El a sp 2130P1F1E6A920Da 2630P/F2P1e9A20Da 2090P/F8E9.S02Da BasWerloinnegcPMeiasksed | BaseWlrionnegoPMeiasksed | BaseWlrionneg PMeiasksed | 3wi 622 Ll == " 4iA | ul ed p5al 31P3H0/Y1A12D9a0 BasWeliionnego PMeiasksed Tide 363P.0E1H31p9A.20 Da 399P.0F19H9S.02Da 5S1_5.1034C7P0F0D0Aa BasWelrionnegoPMeiasksed BasWelrionnegoPMeiasksed BasWelrionnegcPMeiasksed NB PFBA and PFPeA do nol have Qualiying fon ansiions NA Ba=sWelrionnegoPMeiasksed 0 Before 0 After Page 162 of 245 155 5AnSaollyatmitciaalServices PiCrnedate14w0i2t/2A0na1l0y8ps..t411R0e5p6o0rPteUr PrDoatjaecFtile Result Table Gcv22a00r8e11s00S0PaSomaRpmiapelRsePtsoRLnCognEg00vi Instrument Name API 5000 [a ASAeccenraiaiisinmonsbaeatds]2v42e01g0e1.5s6 5o 70 SampleTyvpoe uasa [ E-- E 00] [armor[mo HReisyualPtosokSummary [io so| m ow ART| pare mven| CHE Cone |e [snrorsr scarrroonn [[ssmonm TTaow||m5 awaoswns| rwem | wo orn rscmum| ras [s|rmww| aww | ror sermon| oo Tamu] 5| wm | we] rar Teves | woeTomam] wT Ae Eatr e Page 21001262 156 oO Columbia AnalyticalServices- Printed: 14/02/2010 6:41:00 PM RCSummary [ros [vw [wwe | wo | mam| | Toma orTeTT o o] Pros 2 pros 2a| [sam| m ws | wew |o omew n||owem| erro w 157 4ACnoalluytmibciaalServices Created with Anal}10R7eporter Printed: 14/02/20106:41:00 PM : TT Quantitative Peak SR Review z |= 3 A A n 2 BA = B 7 K1000968-015 = - 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PFBA and PFPeA do nol have quallying on transitions 0 Before OJ After Page 196 of 245 163 PASColumbia Analytical Services" CanarapoitSsnt Printed: 14/02/2010 6:41:00 PM J Rmameaomnas S CSmaemsR aompensoint sors [[SAacqmupilsietNioanmbaete |2R7i2o0oG1a00261670647A STampE le Type E-- S `AjceqcutiisointiVoinalMethod|[[3P%FCwKinWelexeLonig dagm nttoDilvutioon Famctoer [000] a Results Summary er war war | coerroan|| smeaom za | wwww || oowms | |wwee|| ros norros| sw |zwas| wom |ten| mw | [Preuonnst [root | mom aw [oJamssaaomn||[ 0 waew |oa m | | w | [Pereosm1 | worroos| swoww [[wsomwes|| wom |om | wo | rear | vorroos| wm [owe] 0 | wa | we | ww Jower| 0 | wa | we EReo Ce- , 164 Analytical Services Create with AnalHfeporter RCSummary pers |nvr] swore |vm |maa me|m we | men |v | corm |amas| mmm | me | wemoen |v ores |amas |sw | ne | enas |v [rome [arscrroon Ferraz wi vmaasse|| wmrw || wwoe||oowmoemm|| w | [soem| [smem| sa we | we| omom| |w |omem | w 165 LS CSoloumbiia services: PrCinrteead:ted14w/i0t2h/A2n0a1l0yp6s.:t141R1e5.p0o0rPteMr Quantitative Peak Ed 9d c4B1a3sPe0l/Fi1On6eA9c10Mi0sased tip Review rd Ef ||A | Ba4s1e1l73i0Cn3-e7Pc2FO0MAi0s8sed Wgpe K1000968-016 = m7 = Et lol231a | 463P0/E4N1A901 Da 46183.C0-1P8F2N3AD.a0 | BBaaseline cMissed | BaselionnegcpeMaissed : | = | g3l oc a i, [ "2hp even ll IL | GBa4s99eP.l0Fn1e6O0S.01MiDsased | cBa15s03e3Cl,0i-/nP8e0Fc.G0MSiDsased | oBa51s3e.lP0i/Fn4De69Ac.10MiDsased | 5151034C7-0.P0FOADa Baseline o Missed Sanpe nun ae lige . z crfse= = cl foLo se h a. fd cBa5s6e3Pl0iF1nU5eR1AC901MiDsased | oBa6s15.e30lC/2i-7eP0.Fc0UMNiAsDsaed | cBa5s0e9.Pl0iR/n8Oe0Sc.0M1iDsased | B5a013s03/iC8n.0.Po0FOMSiDsased J | eran) 2 3 2 | Bunion J cB6a1s3eP.l0Fi1Dn56Oe9cA.0M1i0sased | B16a13s5eC0l-i/nP1eF6c9DM0oiA0ssaed | cB6a6s3e.Pl0iF5n1Te9Ac.1MiDsased | co B6a1s15e30lC/i-1ne6P9F.D0M0iADsased 7 a = [ ea a ie te A= B7a1s3eP.l0Fi/Tn6ee69A.01Mi0sased | B6a1s1e35lCi0-n/ePF1oD6MO09iAsa0sed 0 Before O After Page 216 of 262 166 4 Golam Analytical Services- paCnrieeda:ted14v/i0t2h/A20n10a6t.4K1p.0o0rtPeAr fon Ratio Confirmation 1 1.38 == io oi K1000968-016 = =| [=xl 4 oox! | 412P0F3O6A920 0a Baseline Missed | oB4as6e3Pl0Fi2Ne1A920Mi0s8sed | oBa4s0e9Pl.iE0nG9eS9c.20M0isased | c B5a1se2Pl.iFn0e2O6A9Mi0.s0ased _ WrongPeak Wrong Peak =Wiong Peak Wrong Peak - = | -i . 3] i id = |- ET h Ba5s6e2lP0iF1nU2eR6cA90M2iDsased | Bas5e95lP.i0Fn9Oe9S0o2DMiassed | oBa6s1e3Pl0Fi/On1eG6oA9M20i0ssaed | Ba6s6e3lP0i/En1eT69I.2A0Mi0sased Wrong Pea Wrong Peak Wiong Peak Wrong Peak _ B7as1ePl3Fi0nTe1eA62M9i0s0ased Wong Peak 0 Before 0 After Page 217 of 242 167 PASColumbia AnalyticalServices Greated with Analys1t1R7eparter Printed: 15/02/2010 2:34:00 PM PDRraoetjsaeucnFtiTlaeble Eo0wz2a00nB'stsioP0irSosjaaemcmtpps\lePesFsCsssh.howoinrite>d instrument Name__ Ap! 3000 [[AScAacaquumiisseiittNiooannmbWeaettheod || 2KFr5Fo2Co0oH1sn06e81i01e766x2S0hdoarr TSiarmepclteonTVypoetre [5] [DionFactor [100] [iie[c35tonvar|Wagmttovolums Joos Ar--RerosanuiltPsekS[umtmaorwymorreen ||saaomas[RT|RairIaeaFnr|]w svurenms||m GoaOesCGonEe|[weaver || Frnt | scemon| amam [ssa| mew| om | soci | worms| seen mam| man | oz |we| [pear [acer| sie [sa| ewozm n| om w [perms 1 Toorrrs| a7e400 | 631630| 1026900 I no | [smoems | taceron| soso |ost@s|n soon | open|wa|crasoan| om woo | | om 1m | ne | eZ 2Lu 205 Pa157gore245 168 4AGnaoltyutmibciaalServices PrCinrteeadt:ed15w1i0t2h1n20a10n2i:3R4e:p0o0rPtAer nei] es | | RCSummary ron ram| ww | we | wom| vw | sremien owen||mwwm||we owomm||evwnw|] Pa198gof2e45 169 LSCo5l0um0b0i8a services Quantitative Peak Review wt 127 d! 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