Document 10eGqpkYK2ZJ1pnN32dqvDYGm

U-50 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES EPIDIDYMID ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) TESTES ORG/TBW ORG/BRN (X 1000) (X 1) GROUP I - 0 PPM 1031 1032 1033 1035 1037 1039 1041 1043 1045 1047 1048 1052 1054 1056 1057 511.1 494.6 570.8 530.6 413.6 446.6 404.6 451.8 491.2 447.7 413.7 470.3 504.3 454.8 480.3 1.5015 1.4652 1.6422 1.3356 1.3697 .8429 1.2828 1.3140 1.6937 1.3248 1.3384 1.6338 1.3814 1.5093 1,5060 2.94 2.96 2.88 2.52 3.31 1.89 3.17 2.91 3.45 2.96 3.24 3.47 2.74 3.32 3.14 7.04 6.63 7.31 5.76 6.84 3.59 6.68 5.82 7.74 6.24 6.13 8.18 6.61 7.07 6.88 3.921 3.689 3.521 3.330 3.100 1.813 2.925 3.322 3.445 3.933 3.293 3.190 2.741 3.749 3.259 7.67 7.46 6.17 6.28 7.50 4.06 7.23 7.35 7.01 8.78 7.96 6.78 5.44 8.24 6.79 1.84 1.67 1.57 1.44 1.55 .77 1.52 1.47 1.57 1.85 1.51 1.60 1.31 1.76 1.49 MEAN S.D. N MIN. MAX. 472.4 46.3 15 404.6 570.8 1.4094 .2039 15 .8429 1.6937 2.99 .40 15 1.89 3.47 6.57 1,05 15 3.59 8.18 3.282 .529 15 1.813 3.933 6.98 1.17 15 4.06 8.78 1.53 .26 15 .77 1.85 BFG 003113 U-51 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES THYMUS ORG/TBW ORG/BRN (X 10000) (X 10) GROUP I - 0 PPM 1031 1032 1033 1035 1037 1039 1041 1043 1045 1047 1048 1052 1054 1056 1057 511.1 494.6 570.8 530.6 413.6 446,6 404.6 451.8 491.2 447.7 413.7 470.3 504.3 454.8 480.3 .234 .181 .317 .245 .281 .158 .261 .271 .290 .287 .248 .230 .246 .276 .182 4.58 3.66 5.55 4.62 6.79 3.54 6.45 6.00 5.90 6.41 5.99 4.89 4.88 6.07 3.79 1.10 .82 1.41 1.06 1.40 .67 1.36 1.20 1.32 1.35 1.14 1.15 1.18 1.29 .83 MEAN S.D. N MIN. MAX. 472.4 46.3 15 404.6 570.8 .247 .045 15 .158 .317 5.28 1.08 15 3.54 6.79 1.15 .23 15 .67 1.41 BFG 003114 U-52 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO IS) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) ADRENALS ORG/TBW ORG/BRN 1[X 10000) (X 100) GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 2.041 2.289 2.355 2.374 2.321 2.245 2.174 2.115 2.265 2.236 2.378 2.225 2.053 2.237 2.314 4.51 3.51 4.82 3.86 4.32 5.03 5.37 4.47 4.87 4.38 4.57 4.44 5.39 4.60 4.21 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0755 .0892 .0883 .0692 .0559 .0405 .0505 .0459 .0597 .0623 .0948 .0711 c .0664 .0601 1.67 1.37 1.81 1.13 1.04 .91 1.25 .97 1.28 1.22 1.82 1.42 1.36 1.09 3.70 3.90 3.75 2.91 2.41 1.80 2.32 2.17 2.64 2.79 3.99 3.20 2.97 2.60 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 2.241 .107 15 2.041 2.378 4.56 .50 15 3.51 5.39 1.00 .00 15 1.00 1.00 .0664 .0163 14 .0405 .0948 1.31 .29 14 .91 1.82 2.94 .68 14 1.80 3.99 BFG 003115 U-53 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (6) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000} (X 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100} (X 1} GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 3.948 4.974 4.574 5.149 4.555 3.948 3.034 4.069 4.381 4.027 4.407 3.929 3.186 4.727 4.889 8.72 7.62 9.36 8.38 8.47 8.85 7.49 8.60 9.42 7.90 8.47 7.84 8.36 9.71 8.89 1.93 2.17 1.94 2.17 1.96 1.76 1.40 1.92 1.93 1.80 1.85 1.77 1.55 2.11 2.11 11.936 20.812 13.240 19.094 16.053 13.403 12.781 13.900 14.077 16.505 16.450 14.403 10.950 14.303 18.177 2.64 3.19 2.71 3.11 2.99 3.01 3.16 2.94 3.03 3.24 3.16 2.87 2.87 2.94 3.30 5.85 9.09 5.62 8.04 6.92 5.97 5.88 6.57 6.22 7.38 6.92 6.47 5.33 6.39 7.86 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 4.253 .609 15 3.034 5.149 8.54 .65 15 7.49 9.71 1.89 .22 15 1.40 2.17 15.072 2.742 15 10.950 20.812 3.01 .19 15 2.64 3.30 6.70 1.03 15 5.33 9.09 BFG 003116 U-54 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) PROSTATE ORG/TBW ORG/BRN (X 1000) (X 10) GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 1.560 2.073 2.016 1.967 1.980 1.510 1.538 1.806 1.814 1.574 1.953 1.619 1.382 2.042 2.250 3.45 3.18 4.13 3.20 3.68 3.39 3.80 3.81 3.90 3.09 3.76 3.23 3.63 4.20 4.09 7.64 9.06 8.56 8.29 8.53 6.73 7.07 8.54 8.01 7.04 8.21 7.28 6.73 9.13 9.72 .866 1.435 .868 1.085 .758 .897 .728 .596 .967 .408 1.050 .732 .989 .627 1.91 2.20 1.78 1.77 1.41 2.01 1.80 1.26 2.08 .80 2.02 1.46 2.59 1.29 4.24 6.27 3.69 4.57 3.27 4.00 3.35 2.82 4.27 1.82 4.42 3.29 4.82 2.80 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 1.806 .258 15 1.382 2.250 3.63 .37 15 3.09 4.20 8.04 .93 15 6.73 9.72 .858 .251 14 .408 1.435 1.74 .46 14 .80 2.59 3.83 1.08 14 1.82 6.27 BFG 003117 U-55 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES SEMIN VESI ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) SPLEEN ORG/TBW ORG/BRN i[X 1000) (X 10) GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 2.1472 2.1508 2.4449 2.5329 1.6337 1.5075 1.9104 2.4999 2.7441 2.8180 2.9327 1.9890 .9535 2.9977 2.9209 4.74 3.30 5.00 4.12 3.04 3.38 4.72 5.28 5.90 5.53 5.64 3.97 2.50 6.16 5.31 1.05 .94 1.04 1.07 .70 .67 .88 1.18 1.21 1.26 1.23 .89 .46 1.34 1.26 .735 1.130 .766 .770 .794 .568 .617 .845 .673 .586 .704 .675 .746 .889 1.334 1.62 1.73 1.57 1.25 1.48 1.27 1.52 1.78 1.45 1.15 1.35 1.35 1.96 1.83 2.43 3.60 4.94 3.25 3.24 3.42 2.53 2.84 4.00 2.97 2.62 2.96 3.03 3.63 3.97 5.76 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 2.2789 .5992 15 .9535 2.9977 4.57 1.13 15 2.50 6.16 1.01 .25 15 .46 1.34 .789 .204 15 .568 1.334 1.58 .33 15 1.15 2.43 3.52 .88 15 2.53 5.76 BFG 003118 U-56 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES EPIDIDYMID ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) TESTES ORG/TBW ORG/BRN (X 1000) (X i: GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 1.5752 1.3679 1.7404 1.5357 1.3614 1.4678 1.3757 1.4488 1.6135 1.4306 1.6206 1.2787 1.2908 1.7032 1.5068 3.48 2.10 3.56 2.50 2.53 3.29 3.40 3.06 3.47 2.81 3.12 2.55 3.39 3.50 2.74 7.72 5.98 7.39 6.47 5.87 6.54 6.33 6.85 7.12 6.40 6.81 5.75 6.29 7.61 6.51 3.428 3.353 3.795 3.831 3.401 3.494 3.135 3.461 3.299 3.746 3.585 3.118 2.888 3.551 3.112 7.57 5.14 7.77 6.24 6.33 7.83 7.74 7.31 7.10 7.35 6.89 6.22 7.58 7.30 5.66 1.68 1.46 1.61 1.61 1.47 1.56 1.44 1.64 1.46 1.68 1.51 1.40 1.41 1.59 1.34 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 1.4878 .1426 15 1.2787 1.7404 3.03 .46 15 2.10 3.56 6.64 .61 15 5.75 7.72 3.413 .272 15 2.888 3.831 6.93 .83 15 5.14 7.83 1.52 .11 15 1.34 1.68 BFG 003119 U-57 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES THYMUS ORG/TBW ORG/BRN (X 10000) (X 10) GROUP II - 10 PPM 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2056 452.7 652.4 488.6 614.4 537.7 446.0 405.1 473.4 464.9 510.0 520.1 501.1 381.2 486.6 550.1 .190 .284 .283 .355 .338 .208 .212 .243 .257 .199 .379 .445 .313 .360 .378 4.20 4.35 5.79 5.78 6.29 4.66 5.23 5.13 5.53 3.90 7.29 8.88 8.21 7.40 6.87 .93 1.24 1.20 1.50 1.46 .93 .98 1.15 1.13 .89 1.59 2.00 1.52 1.61 1.63 MEAN S.D. N MIN. MAX. 499.0 71.3 15 381.2 652.4 .296 .078 15 .190 .445 5.97 1.50 15 3.90 8.88 1.32 .33 15 .89 2.00 BFG 003120 U-58 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (GJ (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000} (X 1} WT. (GJ ADRENALS ORG/TBW ORG/BRN I[X 10000) (X 100) GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 2.214 2.284 2.042 2.111 2.309 2.308 2.207 2.335 2.179 2.129 2.260 2.223 2.157 2.128 2.241 3.82 4.18 4.71 4.59 4.65 4.58 4.97 4.65 4.43 4.10 4.75 4.65 4.21 3.88 4.41 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0465 .0672 .0409 .0608 .0672 .0755 .0573 .0691 .0647 .0721 .0634 .0714 .0633 .0702 .0600 .80 1.23 .94 1.32 1.35 1.50 1.29 1.38 1.32 1.39 1.33 1.49 1.24 1.28 1.18 2.10 2.94 2.00 2.88 2.91 3.27 2.60 2.96 2.97 3.39 2.81 3.21 2.93 3.30 2.68 MEAN S.D. N MIN. MAX. 500.0 39.5 15 433.2 580.1 2.208 .084 15 2.042 2.335 4.44 .33 15 3.82 4.97 1.00 .00 15 1.00 1.00 .0633 .0094 15 .0409 .0755 1.27 .19 15 .80 1.50 2.86 .40 15 2.00 3.39 BFG 003121 U--59 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (GJ (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100) (X 1) GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 4.426 4.139 3.706 3.676 4.128 3.978 3.887 4.057 4.132 4.159 4.780 4.443 4.900 5.311 4.017 7.63 7.58 8.55 8.00 8.31 7.90 8.75 8.09 8.41 8.02 10.05 9.29 9.56 9.69 7.90 2.00 1.81 1.81 1.74 1.79 1.72 1.76 1.74 1.90 1.95 2.12 2.00 2.27 2.50 1.79 19.282 16.360 13.984 12.790 16.399 16.560 14.132 14.625 19.275 18.319 17.538 16.455 20.482 18.421 14.657 3.32 2.99 3.23 2.78 3.30 3.29 3.18 2.92 3.92 3.53 3.69 3.44 4.00 3.36 2.88 8.71 7.16 6.85 6.06 7.10 7.18 6.40 6.26 8.85 8.60 7.76 7.40 9.50 8.66 6.54 MEAN S.D. N MIN. MAX. 500.0 39.5 15 433.2 580.1 4.249 .453 15 3.676 5.311 8.51 .79 15 7.58 10.05 1.93 .22 15 1.72 2.50 16.619 2.265 15 12.790 20.482 3.32 .36 15 2.78 4.00 7.54 1.08 15 6.06 9.50 BFG 003122 U-60 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) PROSTATE ORG/TBW ORG/BRN (X 1000) (X 10) GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 1.686 2.303 1.623 1.894 1.890 1.588 1.606 2.134 1.736 2.073 1.847 1.817 1.808 1.830 1.823 2.91 4.22 3.75 4.12 3.80 3.15 3.61 4.25 3.53 3.99 3.88 3.80 3.53 3.34 3.59 7.62 10.08 7.95 8.97 8.19 6.88 7.28 9.14 7.97 9.74 8.17 8.17 8.38 8.60 8.13 .551 .602 .554 1.184 .613 .793 .787 .887 .847 1.423 .822 1.128 .817 1.043 .793 .95 1.10 1.28 2.58 1.23 1.57 1.77 1.77 1.72 2.74 1.73 2.36 1.59 1.90 1.56 2.49 2.64 2.71 5.61 2.65 3.44 3.57 3.80 3.89 6.68 3.64 5.07 3.79 4.90 3.54 MEAN S.D. N MIN. MAX, 500.0 39.5 15 433.2 580.1 1.844 .200 15 1.588 2.303 3.70 .38 15 2.91 4.25 8.35 .86 15 6.88 10.08 .856 .248 15 .551 1.423 1.72 .51 15 .95 2.74 3.89 1.20 15 2,49 6.68 BFG 003123 U-61 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES SEMIN VESI ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) SPLEEN ORG/TBW ORG/BRN 1[X 1000) (X 10) GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 2.8737 1.4407 2.5208 2.2408 2.2838 2.0022 1.9718 2.3692 2.5255 3.0409 2.7585 2.3833 2.3363 2.6049 1.7142 4.95 2.64 5.82 4.87 4.60 3.97 4.44 4.72 5.14 5.86 5.80 4,98 4.56 4.75 3.37 1.30 .63 1.23 1.06 .99 .87 .89 1.01 1.16 1.43 1.22 1.07 1.08 1.22 .76 1.129 1.546 .677 .791 .782 .919 .761 .777 .882 .883 .801 .792 .915 .980 .882 1.95 2.83 1.56 1.72 1.57 1.82 1.71 1.55 1.79 1.70 1.68 1.66 1.79 1.79 1.73 5.10 6.77 3.32 3.75 3.39 3.98 3.45 3.33 4.05 4.15 3.54 3.56 4.24 4.61 3.94 MEAN S.D. N MIN. MAX. 500.0 39.5 15 433.2 580.1 2.3378 .4271 15 1.4407 3.0409 4.70 .88 15 2.64 5.86 1.06 .21 15 .63 1.43 .901 .209 15 .677 1.546 1.79 .31 15 1.55 2.83 4.08 .90 15 3.32 6.77 BFG 003124 U-62 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (6) (G) INDIVIDUAL VALUES EPIDIDYMID ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) TESTES ORG/TBW ORG/BRN (X 1000) (X 1 GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 1.2965 1.4290 1.1813 1.4550 1.4460 1.2608 1.1497 1.4530 1.5672 1.5310 1.4678 1.3673 1.6734 1.4861 1.4098 2.23 2.62 2.73 3.17 2.91 2.50 2.59 2.90 3.19 2.95 3.08 2.86 3.27 2.71 2.77 5.86 6.26 5.79 6.89 6.26 5.46 5.21 6.22 7.19 7.19 6,49 6.15 7.76 6.98 6.29 3.158 3.328 3.057 3.506 3.044 3.259 2.963 3.373 3.393 3.607 3.756 3.898 4.143 4.060 3.412 5.44 6.09 7.06 7.63 6.13 6.47 6.67 6.72 6.90 6.95 7.89 8.15 8.09 7.41 6.71 1.43 1.46 1.50 1.66 1.32 1.41 1.34 1.44 1.56 1.69 1.66 1.75 1.92 1.91 1.52 MEAN S.D. N MIN. MAX. 500.0 39.5 15 433,2 580.1 1.4116 .1415 15 1.1497 1.6734 2.83 .28 15 2.23 3.27 6.40 .70 15 5.21 7.76 3.464 .366 15 2.963 4.143 6.95 .78 15 5.44 8.15 1.57 .19 15 2.32 1.92 BFG 003125 U-63 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES THYMUS ORG/TBW ORG/BRN (X 10000) (X 10) GROUP III - 100 PPM 3031 3032 3033 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 580.1 546.3 433.2 459.7 496.8 503.8 444.4 501.7 491.6 518.9 475.8 478.1 512.3 548.2 508.4 .271 .276 .192 .207 .262 .290 .334 .377 .261 .217 .170 .242 .229 .318 .370 4.67 5.05 4.43 4.50 5.27 5.76 7.52 7.51 5.31 4.18 3.57 5.06 4.47 5.80 7.28 1.22 1.21 .94 .98 1.13 1.26 1.51 1.61 1.20 1.02 .75 1.09 1.06 1.49 1.65 MEAN S.D. N MIN. MAX. 500.0 39.5 15 433.2 580.1 .268 .062 15 .170 .377 5.36 1.22 15 3.57 7.52 1.21 .26 15 .75 1.65 BFG 003126 U-64 96-4080 APPENDIX U (CQNT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000) (X I) WT. (G) ADRENALS ORG/TBW ORG/BRN 1[X 10000) (X 100) GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 2.275 2.440 2.119 2.192 2.295 2.099 2.226 2.106 2.106 2.291 2.299 1.945 2.329 2.218 2.108 4.18 4.91 3.77 3.81 4.61 4.30 4.60 4.26 4.36 4.71 4.47 3.97 4.78 4.79 4.33 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 b .0522 .0917 .0589 .0683 .0806 .0572 .0501 .0769 .0648 .0792 .0649 .0733 .0769 .0630 1.05 1.63 1.02 1.37 1.65 1.18 1.01 1.59 1.33 1.54 1.32 1.50 1.66 1.29 2.14 4.33 2.69 2.98 3.84 2.57 2.38 3.65 2.83 3.44 3.34 3.15 3.47 2.99 MEAN S.D. N MIN. MAX. 503.6 31.8 15 462.9 575.2 2.203 .124 15 1.945 2.440 4.39 .35 15 3.77 4.91 1,00 .00 15 1.00 1.00 .0684 .0119 14 .0501 .0917 1.37 .24 14 1.01 1.66 3.13 .60 14 2.14 4.33 BFG 003127 U-65 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100) (X 1 GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 4.446 3.999 4.336 4.657 4.451 4.081 4.047 4.679 4.073 4.265 4.775 3.910 4.466 3.944 3.413 8.16 8.05 7.72 8.10 8.94 8.36 8.37 9.46 8.44 8.76 9.28 7.97 9.17 8.52 7.01 1.95 1.64 2.05 2.12 1.94 1.94 1.82 2.22 1.93 1.86 2.08 2.01 1.92 1.78 1.62 18.645 16.533 18.976 19.946 16.646 15.341 16.077 17.479 17.951 17.023 17.708 15.797 16.620 16.346 14.109 3.42 3.33 3.38 3.47 3.34 3.14 3.33 3.53 3.72 3.50 3.44 3.22 3.41 3.53 2.90 8.20 6.78 8.96 9.10 7.25 7.31 7.22 8.30 8.52 7.43 7.70 8.12 7.14 7.37 6.69 MEAN S.D. N MIN. MAX. 503.6 31.8 15 462.9 575.2 4.236 .361 15 3.413 4.775 8.42 .64 15 7.01 9.46 1.93 .17 15 1.62 2.22 17,013 1.494 15 14.109 19.946 3.38 .19 15 2.90 3.72 7.74 .75 15 6.69 9.10 BFG 003128 U-66 96-4080 APPENDIX U (CONI.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) PROSTATE ORG/TBW ORG/BRN (X 1000) (X 10) GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 1.874 2.139 2.220 2.132 1.834 1.915 1.770 2.000 2.105 1.842 1.597 1.595 1.784 1.589 1.450 3.44 4.30 3.95 3.71 3.68 3.92 3.66 4.04 4.36 3.79 3.10 3.25 3.66 3.43 2.98 8.24 8.77 10.48 9.73 7.99 9.12 7.95 9.50 10.00 8.04 6.95 8.20 7.66 7.16 6.88 1.003 .425 1.082 1.220 .881 .993 .558 .728 1.100 .767 1.058 .882 .639 1.021 1.019 1.84 .86 1.93 2.12 1.77 2.03 1.15 1.47 2.28 1.58 2.06 1.80 1.31 2.21 2.09 4.41 1.74 5.11 5.57 3.84 4.73 2.51 3.46 5.22 3.35 4.60 4.53 2.74 4.60 4.83 MEAN S.D. N MIN. MAX. 503,6 31.8 15 462.9 575.2 1.856 .233 15 1.450 2.220 3.69 .40 15 2.98 4.36 8.44 1.12 15 6.88 10.48 .892 .225 15 .425 1.220 1.77 .41 15 .86 2.28 4.08 1.11 15 1.74 5.57 003129 U-67 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES SEMIN VESI ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) SPLEEN ORG/TBW ORG/BRN (X 1000) (X 10) GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 3.1406 2.5453 2.6035 2.0727 1.5318 1.6065 1.9450 2.4959 1.9460 2.1381 1.8817 2.3152 2.4456 1.2807 1.4616 5.76 5.12 4.64 3.60 3.08 3.29 4.02 5.04 4.03 4.39 3.66 4.72 5.02 2.77 3.00 1.38 1.04 1.23 .95 .67 .77 .87 1.19 .92 .93 .82 1.19 1.05 .58 .69 .969 1.273 .949 .951 1.342 .847 .808 1.620 .927 1.074 .874 .865 .827 .755 .725 1.78 2.56 1.69 1.65 2.70 1.73 1.67 3.27 1.92 2.21 1.70 1.76 1.70 1.63 1.49 4.26 5.22 4.48 4.34 5.85 4.04 3.63 7.69 4.40 4.69 3.80 4.45 3.55 3.40 3.44 MEAN S.D. N MIN. MAX. 503.6 31.8 15 462.9 575.2 2.0940 .5071 15 1.2807 3.1406 4.14 .90 15 2.77 5.76 .95 .23 15 .58 1.38 .987 .246 15 .725 1.620 1.96 .50 15 1.49 3.27 4.48 1.11 15 3.40 7.69 BFG 003130 U-68 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES EPIDIDYMID ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) TESTES ORG/TBW ORG/BRN (X 1000) (x i; GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 1.4564 1.2880 1.6885 1.3653 1.4459 1.5775 1.4360 .6551 1.6071 1.4006 1.3446 1.4926 1.2744 1.5443 1.2914 2.67 2.59 3.01 2.37 2.90 3.23 2.97 1.32 3.33 2.88 2.61 3.04 2.62 3.34 2.65 6.40 5.28 7.97 6.23 6.30 7.52 6.45 3.11 7.63 6.11 5.85 7.67 5.47 6.96 6.13 3.372 3.060 3.460 3.509 3.306 3.461 3.141 1.714 3.275 3.128 3.324 3.304 4.430 3.487 3.519 6.19 6.16 6.16 6.10 6.64 7.09 6.50 3.46 6.78 6.43 6.46 6.74 9.09 7.53 7.22 1.48 1.25 1.63 1.60 1.44 1.65 1.41 .81 1.56 1.37 1.45 1.70 1.90 1.57 1.67 MEAN S.D. N MIN. MAX. 503.6 31.8 15 462.9 575.2 1.3912 .2378 15 .6551 1.6885 2.77 .49 15 1.32 3.34 6.34 1.21 15 3.11 7.97 3.299 .540 15 1.714 4.430 6.57 1.15 15 3.46 9.09 1.50 .25 15 .81 1.90 BFG 003131 U-69 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - MALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES THYMUS ORG/TBW ORG/BRN 1;x ioooo) (X io) GROUP IV - 1100 PPM 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 544.8 497.0 561.4 575.2 497.8 488.4 483.5 494.8 482.7 486.6 514.7 490.5 487.2 462.9 487.2 .433 .215 .415 .358 .314 .294 .269 .519 .422 .183 .320 .115 .246 .269 .153 7.95 4.33 7.39 6.22 6.31 6.02 5.56 10.49 8.74 3.76 6.22 2.34 5.05 5.81 3.14 1.90 .88 1.96 1.63 1.37 1.40 1.21 2.46 2.00 .80 1.39 .59 1.06 1.21 .73 MEAN S.D. N MIN. MAX. 503.6 31.8 15 462.9 575.2 .302 .113 15 .115 .519 5.96 2.14 15 2.34 10.49 1.37 .54 15 .59 2.46 bfg 003132 U-70 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) ADRENALS ORG/TBW ORG/BRN (X 10000) (X 100) GROUP I - 0 PPM 1531 1533 1538 1540 1541 1543 1551 1553 1555 1557 1558 1563 1568 1574 1578 260.3 303.4 306.4 281.1 234.8 198.9 320.4 323.8 277.1 266.8 280.1 257.6 261.5 273.9 265.4 2.184 2.068 2.059 1.831 2.169 2.194 2.230 2.120 1.957 2.090 2.069 1.994 2.062 2.014 1.957 8.39 6.82 6.72 6.51 9.24 11.03 6.96 6.55 7.06 7.83 7.39 7.74 7.89 7.35 7.37 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0719 .0749 .0592 .0610 .0631 .0785 .0660 .0902 .0557 .0686 .0877 .0651 .0826 .0739 .0756 2.76 2.47 1.93 2.17 2.69 3.95 2.06 2.79 2.01 2.57 3.13 2.53 3.16 2.70 2.85 3.29 3.62 2.88 3.33 2.91 3.58 2.96 4.25 2.85 3.28 4.24 3.26 4.01 3.67 3.86 MEAN S.D. N MIN. MAX. 274.1 32.2 15 198.9 323.8 2.067 .106 15 1.831 2.230 7.66 1.19 15 6.51 11.03 1.00 .00 15 1.00 1.00 .0716 .0103 15 .0557 .0902 2.65 .52 15 1.93 3.95 3.47 .48 15 2.85 4.25 BFG 003133 U-71 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) LIVER ORG/TBW ORG/BRN {X 100) (X 1 GROUP I - 0 PPM 1531 1533 1538 1540 1541 1543 1551 1553 1555 1557 1558 1563 1568 1574 1578 260.3 303.4 306.4 281.1 234.8 198.9 320.4 323.8 277.1 266.8 280.1 257.6 261.5 273.9 265.4 2.551 2.774 2.555 2.577 2.055 2.520 2.601 3.011 2.368 2.384 2.344 2.048 2.047 2.269 2.282 9.80 9.14 8.34 9.17 8.75 12.67 8.12 9.30 8.55 8.94 8.37 7.95 7.83 6.28 8.60 1.17 1.34 1.24 1.41 .95 1.15 1.17 1.42 1.21 1.14 1.13 1.03 .99 1.13 1.17 10.671 7.963 12.722 10.118 6.948 10.622 9.317 11.159 9.344 10.102 9.076 8.117 10.011 9.136 8.534 4.10 2.62 4.15 3.60 2.96 5.34 2.91 3.45 3.37 3.79 3.24 3.15 3.83 3.34 3.22 4.89 3.85 6.18 5.53 3.20 4.84 4.18 5.26 4.77 4.83 4.39 4.07 4.85 4.54 4.36 MEAN S.D. N MIN. MAX. 274.1 32.2 15 198.9 323.8 2.426 .272 15 2.047 3.011 8.92 1.17 15 7.83 12.67 1.18 .14 15 .95 1.42 9.589 1.433 15 6.948 12.722 3.54 .66 15 2.62 5.34 4.65 .71 15 3.20 6.18 BFG 003134 U-72 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) OVARIES ORG/TBW ORG/BRN (X 10000) (X 100) GROUP I - 0 PPM 1531 1533 1538 1540 1541 1543 1551 1553 1555 1557 1558 1563 1568 1574 1578 260.3 303.4 306.4 281.1 234.8 198.9 320.4 323.8 277.1 266.8 280.1 257.6 261.5 273.9 265.4 1.541 1.243 1.267 a 1.229 1.449 1.335 1.494 1.231 1.298 1.293 1.147 1.388 1.230 1.194 5.92 4.10 4.14 - 5.23 7.29 4.17 4.61 4.44 4.87 4.62 4.45 5.31 4.49 4.50 7.06 6.01 6.15 - 5.67 6.60 5.99 7.05 6.29 6.21 6.25 5.75 6.73 6.11 6.10 .1353 .1042 .0901 .1328 .0714 .1271 .1134 .1406 .0968 .1170 .1140 .0687 .1219 .0978 .0842 5,20 3.43 2.94 4.72 3.04 6.39 3.54 4.34 3.49 4.39 4.07 2.67 4.66 3.57 3.17 6.20 5.04 4.38 7.25 3.29 5.79 5.09 6.63 4.95 5.60 5.51 3.45 5.91 4.86 4.30 MEAN S.D. N MIN. MAX. 274.1 32.2 15 198.9 323.8 1.310 .117 14 1.147 1.541 4.87 .86 14 4.10 7.29 6.28 .43 14 5.67 7.06 .1077 .0226 15 .0687 .1406 3.98 .99 15 2.67 6.39 5.22 1.10 15 3.29 7.25 BFG 003135 U-73 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES SPLEEN ORG/TBW ORG/BRN (X 1000) 10) WT. (G) THYMUS ORG/TBW ORG/BRN (X 10000) (X 10) GROUP I - 0 PPM 1531 1533 1538 1540 1541 1543 1551 1553 1555 1557 1558 1563 1568 1574 1578 260.3 303.4 306.4 281.1 234.8 198.9 320.4 323.8 277.1 266.8 280.1 257.6 261.5 273.9 265.4 .547 .614 .565 .504 .535 .538 .561 .642 .486 .689 .538 .394 .959 .608 .505 2.10 2.02 1.84 1.79 2.28 2.70 1.75 1.98 1.75 2.58 1.92 1.53 3.67 2.22 1.90 2.50 2.97 2.74 2.75 2.47 2.45 2.52 3.03 2.48 3.30 2.60 1.98 4.65 3.02 2.58 .196 .188 .238 .458 .161 .236 .323 .266 .162 .329 .180 .174 .344 ,190 .295 7.53 6.20 7.77 16.29 6.86 11.87 10.08 8.21 5.85 12.33 6.43 6.75 13.15 6.94 11.12 .90 .91 1.16 2.50 .74 1.08 1.45 1.25 .83 1.57 .87 .87 1.67 .94 1.51 MEAN S.D. N MIN. MAX. 274.1 32.2 15 198.9 323.8 .579 .126 15 .394 .959 2.14 .53 15 1.53 3.67 2.80 .60 15 1.98 4.65 .249 .086 15 .161 .458 9.16 3.14 15 5.85 16.29 1.22 .47 15 .74 2.50 BFG 003136 U-74 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES UTERUS ORG/TBW ORG/BRN (X 1000) (X 10) GROUP I - 0 PPM 1531 1533 1538 1540 1541 1543 1551 1553 1555 1557 1558 1563 1568 1574 1578 260.3 303.4 306.4 281.1 234.8 198.9 320.4 323.8 277.1 266.8 280.1 257.6 261.5 273.9 265.4 .929 .630 .573 .772 .995 .584 .743 1.131 .661 .595 .795 .656 .607 .484 .677 3.57 2.08 1.87 2.75 4.24 2.94 2.32 3.49 2.39 2.23 2.84 2.55 2.32 1.77 2.55 4.25 3.05 2.78 4.22 4.59 2.66 3.33 5.33 3.38 2.85 3.84 3.29 2.94 2.40 3.46 MEAN S.D. N MIN. MAX. 274.1 32.2 15 198.9 323.8 .722 .177 15 .484 1.131 2.66 .68 15 1.77 4.24 3.49 .81 15 2.40 5.33 BFG 003137 U-75 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) ADRENALS ORG/TBW ORG/BRN ![X 10000) (x ioo; GROUP II - 10 PPM 2532 2533 2536 2538 2540 2543 2544 2546 2550 2552 2553 2554 2558 2569 2575 295.5 288.3 302.9 279.7 285.7 295.6 268.6 302.7 253.5 266.5 292.4 296.2 282.4 272.6 276.6 2.014 1.971 2.227 2.061 2.038 2.056 2.234 2.270 2.007 1.880 2.077 2.146 2.027 1.857 2.048 6.82 6.84 7.35 7.37 7.13 6.96 8.32 7.50 7.92 7.05 7.10 7.25 7.18 6.81 7.40 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0713 .0752 .0867 .0773 .0572 .0699 .0662 .0377 .0767 .0853 .0713 .0799 .0744 .0671 .0820 2.41 2.61 2.86 2.76 2.00 2.36 2.46 1.25 3.03 3.20 2.44 2.70 2.63 2.46 2.96 3.54 3.82 3.89 3.75 2.81 3.40 2.96 1.66 3.82 4.54 3.43 3.72 3.67 3.61 4.00 MEAN S.D. N MIN. MAX. 283.9 14.4 15 253.5 302.9 2.061 .119 15 1.857 2.270 7.27 .41 15 6.81 8.32 1.00 .00 15 1.00 1.00 .0719 .0122 15 .0377 .0867 2.54 .47 15 1.25 3.20 3.51 .66 15 1.66 4.54 BFG 003138 U-76 APPENDIX U (CONT.) 96-4080 VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000) 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100) (X 1) GROUP II - 10 PPM 2532 2533 2536 2538 2540 2543 2544 2546 2550 2552 2553 2554 2558 2569 2575 295.5 288.3 302.9 279.7 285.7 295.6 268.6 302.7 253.5 266.5 292.4 296.2 282.4 272.6 276.6 2.379 2.466 2.218 2.503 2.795 2.563 2.634 2.599 2.082 2.201 2.481 2.498 2.380 2.421 2.465 8.05 8.55 7.32 8.95 9.78 8.67 9.81 8.59 8.21 8.26 8.48 8.43 8.43 8.88 8.91 1.18 1.25 1.00 1.21 1.37 1.25 1.18 1.14 1.04 1.17 1.19 1.16 1.17 1.30 1.20 9.115 10.796 8.901 9.407 7.960 9.393 10.303 9.656 8.107 7.843 10.312 9.418 9.273 11.346 11.351 3.08 3.74 2.94 3.36 2.79 3.18 3.84 3.19 3.20 2.94 3.53 3.18 3.28 4.16 4.10 4.53 5.48 4.00 4.56 3.91 4.57 4.61 4.25 4.04 4.17 4.96 4.39 4.57 6.11 5.54 MEAN S.D. N MIN. MAX. 283.9 14.4 15 253.5 302.9 2.446 .181 15 2.082 2.795 8.62 .62 15 7.32 9.81 1.19 .09 15 1.00 1.37 9.545 1.117 15 7.843 11.351 3.37 .42 15 2.79 4.16 4.65 .63 15 3.91 6.11 BFG 003i: U-77 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) OVARIES ORG/TBW ORG/BRN i[X 10000) (X 100) GROUP II - 10 PPM 2532 2533 2536 2538 2540 2543 2544 2546 2550 2552 2553 2554 2558 2569 2575 295.5 288.3 302.9 279.7 285.7 295.6 268.6 302.7 253.5 266.5 292.4 296.2 282.4 272.6 276.6 1.371 1.355 1.352 1.443 1.286 1.395 1.369 1.487 1.058 1.390 1.539 1.403 1.382 1.242 1.458 4.64 4.70 4.46 5.16 4.50 4.72 5.10 4.91 4.17 5.22 5.26 4.74 4.89 4.56 5.27 6.81 6.87 6.07 7.00 6.31 6.79 6.13 6.55 5.27 7.39 7.41 6.54 6.82 6.69 7.12 .0972 .0872 .1395 .0990 .0840 .0655 .1335 .1050 .0813 .0676 .1059 .1198 .0791 .0968 .0894 3.29 3.02 4.61 3.54 2.94 2.22 4.97 3.47 3.21 2.54 3.62 4.04 2.80 3.55 3.23 4.83 4.42 6.26 4.80 4.12 3.19 5.98 4.63 4.05 3.60 5.10 5.58 3.90 5.21 4.37 MEAN S.D. N MIN. MAX. 283.9 14.4 15 253.5 302.9 1.369 .113 15 1.058 1.539 4.82 .33 15 4.17 5,27 6.65 .55 15 5.27 7.41 .0967 .0216 15 .0655 .1395 3.40 .73 15 2.22 4.97 4.67 .86 15 3.19 6.26 BFG 003140 U-78 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES SPLEEN ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) THYMUS ORG/TBW ORG/BRN (X 10000) (X 10) GROUP II - 10 PPM 2532 2533 2536 2538 2540 2543 2544 2546 2550 2552 2553 2554 2558 2569 2575 295.5 288.3 302.9 279.7 285.7 295.6 268.6 302.7 253.5 266.5 292.4 296.2 282.4 272.6 276,6 .453 .432 .611 .499 .502 .620 .491 .546 .438 .607 .550 .560 .573 .675 .510 1.53 1.50 2.02 1.78 1.76 2.10 1.83 1.80 1,73 2.28 1.88 1.89 2.03 2.48 1.84 2.25 2.19 2.74 2.42 2.46 3.02 2.20 2.41 2.18 3.23 2.65 2.61 2.83 3.63 2.49 .257 .224 .184 .169 .209 .168 .200 .295 .261 .208 .177 .248 .195 .201 .262 8.70 7.77 6.07 6.04 7.32 5.68 7.45 9.75 10.30 7.80 6.05 8.37 6.91 7.37 9.47 1.28 1.14 .83 .82 1.03 .82 .90 1.30 1.30 1.11 .85 1.16 .96 1.08 1.28 MEAN S.D. N MIN. MAX. 283.9 14.4 15 253.5 302.9 .538 .072 15 .432 .675 1.90 .26 15 1.50 2.48 2.62 .42 15 2.18 3.63 .217 .039 15 .168 .295 7.67 1.43 15 5.68 10.30 1.06 .19 15 .82 1.30 BFG 003141 U--79 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES UTERUS ORG/TBW ORG/BRN (X 1000) (X 10) GROUP II - 10 PPM 2532 2533 2536 2538 2540 2543 2544 2546 2550 2552 2553 2554 2558 2569 2575 295.5 288.3 302.9 279.7 285.7 295.6 268.6 302.7 253.5 266.5 292.4 296.2 282.4 272.6 276.6 .599 .614 .680 .852 1.249 .589 .651 .650 .643 .446 .553 .700 1.300 .422 .959 2.03 2.13 2.24 3.05 4.37 1.99 2.42 2.15 2.54 1.67 1.89 2.36 4.60 1.55 3.47 2.97 3.12 3.05 4.13 6.13 2.86 2.91 2.86 3.20 2.37 2.66 3.26 6.41 2.27 4.68 MEAN S.D. N MIN. MAX. 283.9 14.4 15 253.5 302.9 .727 .259 15 .422 1.300 2.56 .92 15 1.55 4.60 3.53 1.27 15 2.27 6.41 BFG 003142 U-80 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) ADRENALS ORG/TBW ORG/BRN 1[X 10000) (X 100) GROUP III - 100 PPM 3531 3532 3533 3534 3535 3536 3541 3543 3555 3556 3557 3559 3560 3562 3564 292.7 286.5 261.5 275.6 282.0 275.6 260.4 282.3 282.0 240.3 270.4 329.2 325.2 320.2 306,7 1.958 1.984 1.523 1.871 2.152 2.086 1.904 2.038 2.053 1.862 2.048 2.238 2.088 2.146 2.166 6.69 6.92 5.82 6.79 7.63 7.57 7.31 7.22 7.28 7.75 7.57 6.80 6.42 6.70 7.06 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0786 .0889 .0730 .0702 .0696 .0671 .0577 .0849 .0510 .0490 .0828 .0882 .0869 .0709 .0848 2.69 3.10 2.79 2.55 2.47 2.43 2.22 3.01 1.81 2.04 3.06 2.68 2.67 2.21 2.76 4.01 4.48 4.79 3.75 3.23 3.22 3.03 4.17 2.48 2.63 4.04 3.94 4.16 3.30 3.92 MEAN S.D. N MIN. MAX. 286.0 25.2 15 240.3 329.2 2.008 .174 15 1.523 2.238 7.04 .52 15 5.82 7.75 1.00 .00 15 1.00 1.00 .0736 .0132 15 .0490 .0889 2.57 .38 15 1.81 3.10 3.68 .67 15 2.48 4.79 BFG 003143 U-81 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN {X 1000) (X 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100) (X i; GROUP III - 100 PPM 3531 3532 3533 3534 3535 3536 3541 3543 3555 3556 3557 3559 3560 3562 3564 292.7 286.5 261.5 275.6 282.0 275.6 260.4 282.3 282.0 240.3 270.4 329.2 325.2 320.2 306.7 2.394 2.694 2.230 2.274 2.919 2.473 2.253 2.597 2.613 2.372 2.190 2.928 2.501 2.821 2.660 8.18 9.40 8.53 8.25 10.35 8.97 8.65 9.20 9.27 9.87 8.10 8.89 7.69 8.81 8.67 1.22 1.36 1.46 1.22 1.36 1.19 1.18 1.27 1.27 1.27 1.07 1.31 1.20 1.31 1.23 9.171 9.482 9.621 9.614 12.573 9.917 9.557 10.982 9.449 10.386 8.173 10.264 12.007 9.870 12.663 3.13 3.31 3.68 3.49 4.46 3.60 3.67 3.89 3.35 4.32 3.02 3.12 3.69 3.08 4.13 4.68 4.78 6.32 5.14 5.84 4.75 5.02 5.39 4.60 5.58 3.99 4.59 5.75 4.60 5.85 MEAN S.D. N MIN. MAX. 286.0 25.2 15 240.3 329.2 2.528 .246 15 2.190 2.928 8.86 .70 15 7.69 10.35 1.26 .09 15 1.07 1.46 10.249 1.285 15 8.173 12.663 3.60 .45 15 3.02 4.46 5.13 .64 15 3.99 6.32 BFG 003144 U-82 APPENDIX U (CONT.) 96-4080 VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (6) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) OVARIES ORG/TBW ORG/BRN (X 10000) (X 100) GROUP III - 100 PPM 3531 3532 3533 3534 3535 3536 3541 3543 3555 3556 3557 3559 3560 3562 3564 292,7 286.5 261.5 275.6 282.0 275.6 260.4 282.3 282.0 240.3 270.4 329.2 325.2 320.2 306.7 1.260 1.292 1.193 1.310 1.329 1.287 1.254 1.214 1.405 1.178 1.329 1.578 1.422 1.887 1.419 4.30 4.51 4.56 4.75 4.71 4.67 4.82 4.30 4.98 4.90 4.91 4.79 4.37 5.89 4.63 6.44 6.51 7.83 7.00 6.18 6.17 6.59 5.96 6.84 6.33 6.49 7.05 6.81 8.79 6.55 .1133 .1223 .0589 .1114 .1127 .1214 .0994 .1390 .0926 .0866 .0668 .1070 .1122 .0883 .0968 3.87 4.27 2.25 4.04 4.00 4.40 3.82 4.92 3.28 3.60 2.47 3.25 3.45 2.76 3.16 5.79 6.16 3.87 5.95 5.24 5.82 5.22 6.82 4.51 4.65 3.26 4.78 5.37 4.11 4.47 MEAN S.D. N MIN. MAX. 286.0 25.2 15 240.3 329.2 1.357 .180 15 1.178 1.887 4.74 .38 15 4.30 5.89 6.77 .72 15 5.96 8.79 .1019 .0211 15 .0589 .1390 3.57 .73 15 2.25 4.92 5.07 .96 15 3.26 6.82 BFG 003145 U-83 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES INDIVIDUAL VALUES TERMINAL SPLEEN THYMUS AN BODY WT. WT. ORG/TBW ORG/BRN WT. ORG/TBW ORG/BRN NO (G) (G) (X 1000) (X 10) (G) 1[X 10000) (X 10) GROUP III - 100 PPM 3531 3532 3533 3534 3535 3536 3541 3543 3555 3556 3557 3559 3560 3562 3564 292.7 286.5 261.5 275.6 282,0 275.6 260.4 282.3 282.0 240.3 270.4 329.2 325.2 320.2 306.7 .602 .656 .424 .571 .501 .502 .473 .672 .552 .560 .459 .564 .744 .684 .599 2.06 2.29 1.62 2.07 1.78 1.82 1.82 2.38 1.96 2.33 1.70 1.71 2.29 2.14 1.95 3.07 3.31 2.78 3.05 2.33 2.41 2.48 3.30 2.69 3.01 2.24 2.52 3.56 3.19 2.77 .234 .222 .337 .291 .261 .201 .266 .228 .254 .236 .344 .377 .224 .266 .236 7.99 7.75 12.89 10.56 9.26 7.29 10.22 8.08 9.01 9.82 12.72 11.45 6.89 8.31 7.69 1.20 1.12 2.21 1.56 1.21 .96 1.40 1.12 1.24 1.27 1.68 1.68 1.07 1.24 1.09 MEAN S.D. N MIN. MAX. 286.0 25.2 15 240.3 329.2 .571 .091 15 .424 .744 1.99 .25 15 1.62 2.38 2.85 .40 15 2.24 3.56 .265 .051 15 .201 .377 9.33 1.91 15 6.89 12.89 1.34 .33 15 .96 2.21 BFG 003146 U-84 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES UTERUS ORG/TBW ORG/BRN (X 1000) (X 10) GROUP III - 100 PPM 3531 3532 3533 3534 3535 3536 3541 3543 3555 3556 3557 3559 3560 3562 3564 292.7 286.5 261.5 275.6 282.0 275.6 260.4 282.3 282.0 240.3 270.4 329.2 325.2 320.2 306.7 .678 .854 .711 .570 .617 .584 .859 1.089 .531 .762 .945 .626 .587 .549 .633 2.32 2.98 2.72 2.07 2.19 2.12 3.30 3.86 1.88 3.17 3.49 1.90 1.81 1.71 2.06 3.46 4.30 4.67 3.05 2.87 2.80 4.51 5.34 2.59 4.09 4.61 2.80 2.81 2.56 2.92 MEAN S.D. N MIN. MAX. 286.0 25.2 15 240.3 329.2 .706 .164 15 .531 1.089 2.51 .69 15 1.71 3.86 3.56 .93 15 2.56 5.34 BFG 003147 U-85 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES BRAIN ORG/TBW ORG/BRN (X 1000} (X 1) WT. (G) ADRENALS ORG/TBW ORG/BRN 1[X 10000) (X 100) GROUP IV - 1100 PPM 4531 4538 4545 4546 4549 4555 4556 4557 4558 4560 4562 4563 4566 4574 4577 305.1 303.5 231.2 268.3 316.2 276.9 281.0 293.0 293.6 324.7 270.1 243.4 305.0 254.5 228.5 2.227 2.013 1.838 2.034 2.100 1.974 1.978 2.029 2.151 2.039 2.208 1.914 2.065 1.920 1.663 7.30 6.63 7.95 7.58 6.64 7.13 7.04 6.92 7.33 6.28 8.17 7.86 6.77 7.54 7.28 1.00 1.00 1.00 1.00 1.00 1.00 3.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 .0791 .0738 .0600 .0763 .0722 .0729 .0707 .0731 .0768 .0920 .0662 .0720 .0867 .0661 .0656 2.59 2.43 2.60 2.84 2.28 2.63 2.52 2.49 2.62 2.83 2.45 2.96 2.84 2.60 2.87 3.55 3.67 3.26 3.75 3.44 3.69 3.57 3.60 3.57 4.51 3.00 3.76 4.20 3.44 3.94 MEAN S.D. N MIN. MAX. 279.7 30.2 15 228.5 324.7 2.010 .144 15 1.663 2.227 7.23 .54 15 6.28 8.17 1.00 .00 15 1.00 1.00 .0736 .0082 15 .0600 .0920 2.64 .19 15 2.28 2.96 3.66 .36 15 3.00 4.51 BFG 003148 U-86 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES KIDNEYS ORG/TBW ORG/BRN (X 1000) (X 1) WT. (G) LIVER ORG/TBW ORG/BRN (X 100) (X 1 GROUP IV - 1100 PPM 4531 4538 4545 4546 4549 4555 4556 4557 4558 4560 4562 4563 4566 4574 4577 305.1 303.5 231.2 268.3 316.2 276.9 281.0 293.0 293.6 324.7 270.1 243.4 305.0 254.5 228.5 2.628 2.792 2.323 2.427 2.901 2.354 2.405 2.532 2.262 2.917 2.287 2.005 2.378 2.275 2.391 8.61 9.20 10.05 9.05 9.17 8.50 8.56 8.64 7.70 8.98 8.47 8.24 7.80 8.94 10.46 1.18 1.39 1.26 1.19 1.38 1.19 1.22 1.25 1.05 1.43 1.04 1.05 1.15 1.18 1.44 11.930 11.307 8.836 11.437 10.844 10.025 11.194 10.555 9.652 12.037 9.248 8.352 10.397 9.663 10.853 3.91 3.73 3.82 4.26 3.43 3.62 3.98 3.60 3.29 3.71 3.42 3.43 3.41 3.80 4.75 5.36 5.62 4.81 5.62 5.16 5.08 5.66 5.20 4.49 5.90 4.19 4.36 5.03 5.03 6.53 MEAN S.D. N MIN. MAX. 279.7 30.2 15 228.5 324.7 2.458 .254 15 2.005 2.917 8.83 .74 15 7.70 10.46 1.23 .13 15 1.04 1.44 10.422 1.108 15 8.352 12.037 3.74 .38 15 3.29 4.75 5.20 .62 15 4.19 6.53 BFG 003149 U-87 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES LUNGS ORG/TBW ORG/BRN (X 1000) 10) WT. (G) OVARIES ORG/TBW ORG/BRN (X 10000) (X 100) GROUP IV - 1100 PPM 4531 4538 4545 4546 4549 4555 4556 4557 4558 4560 4562 4563 4566 4574 4577 305.1 303.5 231.2 268.3 316.2 276.9 281.0 293.0 293.6 324.7 270.1 243.4 305.0 254.5 228.5 1.353 1.597 1.375 1.239 1.507 1.255 1.288 1.470 1.295 1.330 1.576 1.319 1.381 1.251 1.272 4.43 5.26 5.95 4.62 4.77 4.53 4.58 5.02 4.41 4.10 5.83 5.42 4.53 4.92 5.57 6.08 7.93 7.48 6.09 7.18 6.36 6.51 7.24 6.02 6.52 7.14 6.89 6.69 6.52 7.65 .1000 .1090 .0736 .1075 .1646 .0984 .1147 .1012 .0959 .0464 .1221 .0662 .1179 .0950 .1010 3.28 3.59 3.18 4.01 5.21 3.55 4.08 3.45 3.27 1.43 4.52 2.72 3.87 3.73 4.42 4.49 5.41 4.00 5.29 7.84 4.98 5.80 4.99 4.46 2.28 5.53 3.46 5.71 4.95 6.07 MEAN S.D. N MIN. MAX. 279.7 30.2 15 228.5 324.7 1.367 .118 15 1.239 1.597 4.93 .56 15 4.10 5.95 6.82 .60 15 6.02 7.93 .1009 .0268 15 .0464 .1646 3.62 .87 15 1.43 5.21 5.02 1.26 15 2.28 7.84 BFG 003150 U-88 APPENDIX U (CONT.) 96-4080 VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO <G) (G) INDIVIDUAL VALUES SPLEEN ORG/TBW ORG/BRN (X 1000) (X 10) WT. (G) THYMUS ORG/TBW ORG/BRN 1[X 10000) (X 10) GROUP IV - 1100 PPM 4531 4538 4545 4546 4549 4555 4556 4557 4558 4560 4562 4563 4566 4574 4577 305.1 303.5 231.2 268.3 316.2 276.9 281.0 293.0 293.6 324.7 270.1 243.4 305.0 254.5 228.5 .632 .594 .469 .588 .718 .501 .552 .656 .708 .641 .674 .570 .665 .505 .582 2.07 1.96 2.03 2.19 2.27 1.81 1.96 2.24 2.41 1.97 2.50 2.34 2.18 1.98 2.55 2.84 2.95 2.55 2.89 3.42 2.54 2.79 3.23 3.29 3.14 3.05 2.98 3.22 2.63 3.50 .362 .180 .176 .164 .234 .323 .175 .245 .234 .244 .301 .302 .193 .223 .162 11.86 5.93 7.61 6.11 7.40 11.66 6.23 8.36 7.97 7.51 11.14 12.41 6.33 8.76 7.09 1.63 .89 .96 .81 1.11 1.64 .88 1.21 1.09 1.20 1.36 1.58 .93 1.16 .97 MEAN S.D. N MIN. MAX. 279.7 30.2 15 228.5 324.7 .604 .076 15 .469 .718 2.16 .22 15 1.81 2.55 3.00 .30 15 2.54 3.50 .235 .063 15 .162 .362 8.43 2.25 15 5.93 12.41 1.16 .28 15 .81 1.64 BFG 003151 U-89 96-4080 APPENDIX U (CONT.) VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS TERMINAL ORGAN AND BODY WEIGHTS, ORGAN/BODY WEIGHT AND ORGAN/BRAIN WEIGHT RATIOS TERMINAL SACRIFICE - P2 GENERATION - FEMALES TERMINAL AN BODY WT. WT. NO (G) (G) INDIVIDUAL VALUES UTERUS ORG/TBW ORG/BRN (X 1000) (X 10) GROUP IV - 1100 PPM 4531 4538 4545 4546 4549 4555 4556 4557 4558 4560 4562 4563 4566 4574 4577 305.1 303.5 231.2 268.3 316.2 276.9 282.0 293.0 293.6 324.7 270.1 243.4 305.0 254.5 228.5 .612 .551 .351 .635 .775 .612 .627 .596 .651 .856 1.138 .741 .842 .620 .696 2.01 1.82 1.52 2.37 2.45 2.21 2.23 2.03 2.22 2.64 4.21 3.04 2.76 2.44 3.05 2.75 2.74 1.91 3.12 3.69 3.10 3.17 2.94 3.03 4.20 5.15 3.87 4.08 3.23 4.19 MEAN S.D. N MIN. MAX. 279.7 30.2 15 228.5 324.7 .687 .175 15 .351 1.138 2.47 .64 15 1.52 4.21 3.41 .79 15 1.91 5.15 003152 bfg APPENDIX V BFG 003153 Huntingdon Life Sciences Reproduction Study 96-4080 Page 1 Draft Final Report Terminal Organ and Body Weights and Organ/Body Weight Ratios - Terminal Sacrifice - Pups Appendix V Key to Abbreviations TBW ORG/TBW General = - Terminal Body Weight Organ/Terminal Body Weight Ratio Due to technician error, greater than 15 pups were processed in some groups. BFG 003154 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Male Pups Page 2 Female No. Terminal Pup Body No. Weigh* <g) Adrenal Weight (8) Adrenal/ TBW (XI000) Brain Weight <E) Brain/ TBW (XI00) Group 1 - 0 ppm 1501 2 1505 4 1506 2 1508 3 1510 3 1514 7 1516 2 1517 3 1518 3 1519 1 1520 2 1521 8 1522 3 1524 7 1525 3 1528 2 1529 5 62.3 54.2 58.3 58.2 48.9 58.5 58.3 45.0 46.2 57.0 45.7 50.0 62.6 61.3 45.8 70.2 54.9 0.0223 0.0183 0.0185 0.0188 0.0227 0.0201 0.0144 0.0100 0.0181 0.0271 0.0141 0,0187 0.0234 0.0155 0.0078 0.0214 0.0173 0.3579 0.3376 0.3173 0.3230 0.4642 0.3436 0.2470 0.2222 0.3918 0.4754 0.3085 0.3740 0.3738 0.2529 0.1703 0.3048 0.3151 1.4305 1.4801 1.4328 1.5695 1.2965 1.5871 1.4860 1.4647 1,5207 1.4836 1.5613 1.4805 1.6183 1.6386 1.4689 1.6558 1,5050 2.2961 2.7308 2.4576 2.6967 2.6513 2.7130 2.5489 3.2549 3.2916 2.6028 3.4164 2.9610 2.5851 2.6731 3.2072 2.3587 2.7413 Kidneys Weight (8) 0.8362 0.7630 0.9100 0.8690 0.7664 0.8837 0.7333 0.6273 0.7210 0.7691 0.6812 0.7139 0.9168 0.8907 0.7255 1.0384 0.7750 Kidneys/ TBW (XI00) (g) Liver Weight (g) 1.3422 1.4077 I.S609 1.4931 1.5673 1.5106 1.2578 1.3940 1.5606 1.3493 1.4906 1.4278 1.4645 1.4530 1.5841 1.4792 1.4117 2.6186 2.1530 2.9605 2.6056 2.3539 2.8784 2.6093 1.8964 2.0633 2.2307 2.7290 2.2357 2.9369 2.7975 2.1364 3.2573 2.3862 Liver/ TBW (xlOO) 4.2032 3.9723 5.0780 4.4770 4.8137 4.9203 4.4756 4.2142 4.4660 3.9135 5.9716 4.4714 4.6915 4.5636 4.6646 46400 4.3464 Spleen Weight (g) Spleen^ TBW (xlOO) Testes Weight (g> Testes/ TBW (xlOO) Tliymus Weight (g) Thymus/ TBW (xlOO) 0.3014 0.3663 0.3571 0.2924 0.4134 0.2967 0.3024 0.2768 0.2288 0.3815 0.2402 0.2580 0.3888 0.3002 0.281! 0.3817 0.3129 0.4838 0.6758 0.6125 0.5024 0.8454 0.5072 0.5187 0.6151 0.4952 0.6693 0.5256 0.5160 0.6211 0.4897 0.6138 0.5437 0.5699 0.3310 0.2510 0.2652 0.3146 0.2651 0.3083 0.2651 0.2105 0.2395 0.2753 0.2309 0.2757 0.3319 0.3096 0.1769 0.4046 0,2693 0.5313 0.4631 0.4549 0.5405 0.5421 0.5270 0.4547 0.4678 0.5184 0.4830 0.5053 0.5514 0.5302 0.5051 0.3862 0.5764 0.4905 0.2342 0.2112 0.2008 0.2202 0.1881 0.2330 0.2381 0.1986 0.1511 0.2045 0.1694 02093 0.2832 0.2545 0.2291 0.2693 0.2000 0.3759 0.3897 0.3444 0.3784 0.3847 0.3983 0.4084 0.4413 0.3271 0.3588 0.3707 0.4186 0.4524 0.4152 0.5002 0.3836 0.3643 BFG 003155 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Male Pups Page 3 Terminal Femule Pup Body Adrenol No. Nu. Weight Weight (g> <S> Adrenal/ TBW (X1000) Brain Weight <g) Group II 2503 2504 2506 2510 2515 2516 2518 2522 2523 2524 2525 2527 2528 2530 2531 10 ppm 4 2 9 1 11 2 3 12 4 2 3 4 6 5 7 54.0 60.9 62.6 59.2 54.9 58.7 64.3 50.6 55.5 59.3 47,0 50.4 61.0 51.7 61.0 0.0188 0.0177 0.0106 0.0302 0.0203 0.0266 0.0227 0,0117 0.0187 0.0181 0.0226 0.0339 0.0189 0.0288 0.0162 0.3481 0.2906 0.1693 0.5101 0.3698 0.4532 0.3530 0.2312 0.3369 0.3052 0.4809 0.6726 0.3098 0-5571 0.2656 1.5498 I.SI18 1.5454 1.5528 1.4896 1.5605 1.5390 1.4909 1.4718 1.4510 1.4758 1.5107 1.5862 1.5416 1.5903 Brain/ TBW (X100) 2.8700 2.4824 2.4687 2.6230 2.7133 2.6584 2.3935 2.9464 2.6519 2.4469 3.1400 2.9974 2.6003 2.9818 2.6070 Kidneys Weight (e) 0.7778 0.8484 0.9084 0.9026 0,8032 0.8158 0.9364 0.7291 0.7502 0.8135 0.7411 0.7057 0.9052 0.6910 0.8601 Kidneys/ TBW (XI00) <g) Liver Weight (g) 1.4404 1.3931 1.4511 1.5247 1.4030 1.3898 1.4563 1.4409 1.3517 1.3718 1.5768 1.4002 1.4839 1.3366 1.4100 2.1145 2.5660 3.1826 2.7993 2.4118 2.7395 2.9362 2.2227 2.4552 2.7424 2.1621 2.3223 2.8987 2.3562 2.4501 Liver/ TBW (xlOO) 3.9157 4.2135 5.0840 4.7285 4.3931 4.6670 4.5664 4.3927 4.4238 4.6246 4.6002 4.6077 4.7520 4.5574 4.0166 Spleen Weight (g) Spleen/ TBW (xlOO) 0.2900 0.3422 0.3063 0.2637 0.3405 0.4099 0.2563 0.2942 0.2645 0.2863 0.1874 0.2573 0.3301 0.2560 0.3745 0.5370 0.5619 0.4893 0.4454 0.6202 0.6983 0.3986 0.5814 0.4766 0.4828 0.3987 0.5105 0.5411 0.4952 0.6139 Testes Weight <g) Testes/ TBW (xlOO) Thymus Weight (e) Thymus/ TBW (xlOO) 0.2328 0.2694 0.3826 0.3181 0.2419 0.2949 0.3099 0.2805 0.3590 0.3773 0.2496 0.2503 0.3087 0.2818 0.2896 0.4311 0.4424 0.6112 0.5373 0.4406 0.5024 0.4820 0.5543 0.6468 0.6363 0.5311 0.4966 0.5061 0.5451 0.4748 0.2127 0.2634 0.2480 0.1772 0.2475 0.2483 0.1897 0.1883 0.1875 0.2894 0.1729 0.1958 0.2521 0.2107 0.2972 0.3939 0.4325 0.3962 0.2993 0.4508 0.4230 0.2950 0.3721 0.3378 0.4880 0.3679 0.3885 0.4133 0.4075 0.4872 BFG 003156 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Male Pups Page 4 Terminal Female Pup Body No. No. Weight <g) Adrcnul Weight (g) Adrenal/ TBW (XI00) Drain Weight (8) Brain/ TBW (XI00) roup III - 100 ppm 3502 1 59.7 3506 2 60.4 3507 2 39.4 3509 6 66.3 3511 69.2 3512 4 70.8 3515 1 48.1 3516 3 63.3 3517 3 61.7 3518 2 56.3 3519 5 70.0 3521 7 56.3 3523 6 46.1 3524 2 72.5 3528 7 60.0 0.0135 0.0194 0.0127 0.0092 0.0166 0.0183 0.0164 0.0187 0.0197 0.0177 0.0209 0.0246 0.0142 0.0181 0.0263 0.2261 0.3212 0.3223 0.1388 0.2399 0.2585 0.3410 0.2954 0.3193 0.3144 0.2986 0.4369 0.3080 0.2497 0.4383 1.4267 1.5227 1.3371 1.6463 1.6121 1 6549 1.5013 1.6836 1.6016 1.5216 1.5913 1.6126 1.5632 1.7474 1.4738 2.3898 2 5210 3.3937 2 4831 2 3296 2.3374 3.1212 2.6597 2.5958 2.7027 2.2733 2.8643 3.3909 2.4102 2.4563 Kidneys Weight (g) 0.8595 0.8980 0 6083 0.9211 0.9222 0.9981 0.7617 0.8848 0.8861 0.7788 1.1382 0.7860 0.6695 0.9890 08686 Kidneys/ TBW (XI00) (S) Liver Weight (g) 1.4397 1.4868 l 5439 1.3893 1 3327 1.4097 1.5*36 1.3978 1.4361 1.3833 1.6260 1.3961 1.4523 1.3641 1.4477 2.6355 3.1553 1.7052 3.1098 3.3301 3.2219 2.3497 3.2332 2.6983 2.3090 3.5341 2.3950 1.6902 3.9753 2.6058 Liver/ TBW (xlOO) 4.4146 5.2240 4.3279 4.6905 4 8123 4.5507 4.8850 5.1077 4.3733 4.1012 5.0487 4.2540 3.6664 5.4832 4.3430 Spleen Weight (R) Spleen/ TBW (xlOO) Testes Weight (S) Testes/ TBW (xlOO) Thymus Weight (*) Thymus/ TBW (xlOO) 0.3567 0.3382 0.2842 0.3293 0.3563 0.3422 0.3064 0.4026 0,3077 0.3374 0.3442 0.2997 0.2616 0.2854 0.3644 0.5975 0.5599 0.7213 0.4967 0.5149 0.4833 0.6370 0.6360 0,4987 0.5993 0.4917 0.5323 0.5675 0.3937 0.6073 0.3570 0.3440 0.1531 0.351* 0.4199 0.3613 0.2436 0.2773 0.3647 0.2637 0.4025 0.2447 0.2184 0.46*6 0.3552 0.5980 0.5695 0.38*6 0.5306 0.6068 0.5103 0.5064 0.4381 0.5911 0.4684 0.5750 0.4346 0.4738 0.6463 0.5920 0.2255 0.2395 0 1951 0.2932 0.3021 0.3229 0.2064 0.2282 0.3160 0.2534 03328 0.2172 0.2017 0.3163 0.2365 0.3777 0.3965 0.4952 0.4422 0.4366 0.4561 0.4291 0.3605 0.5122 0.4501 0.4754 0.3858 0.4375 0.4363 0.3942 BFG 003157 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Male Pups Page 5 Terminal Female Pup Body No. No. Weight (S) Adrenal Weight (s) Adrenal/ TBW (X100) Brain Weight (e) Brain/ TBW (XI00) Group IV - 1100 ppm 4501 2 62.7 4502 2 56.6 4503 2 38.3 4504 2 55.9 4506 9 54.0 4509 3 60.8 4511 5 57.1 4512 2 72,5 4515 2 56.0 4518 6 64.2 4519 5 47.1 4521 4 76.3 4522 l 50.9 4524 1 65.7 4528 2 51.5 4529 3 33.7 4530 5 50.2 0.0176 0.0134 0.0150 0.018.3 0.0155 0.0279 0.0202 0.0305 0.0247 0.0227 0.0131 0.0373 0.0173 0.0254 0.0190 0.0192 0.0182 0.2X07 0.2367 03916 0.3274 0 2X70 0.4589 03538 0.4207 0.4411 0.3536 0.2781 0.4889 0.3399 0.3866 0.3689 0.5697 0.3625 1.6097 1.5286 1.3623 1.4380 1.6007 1.6784 1.6106 1.7145 1.5930 1.5887 1.5202 1.7400 1.3701 1.5238 1.4940 1.3667 1.5558 2.5673 2.7007 3.5569 2 5725 2.9643 2.7605 2.8207 2.3648 2.8446 2.4746 3.2276 2.2805 2.6917 2.3193 2.9010 4.0555 3.0992 Kidneys Weight (g) 0.8700 08132 0 5233 0.8413 0 8754 0.8527 0.8011 1.1625 0.7839 0.9646 0,6757 1.1036 0.7216 0.9741 0.7683 0.5120 0.7649 Kidneys/ TBW (XtOO) <g) Liver Weight (g) 1.3876 1.4367 1.3663 1.5050 1 6211 1.4025 1.4030 1.6034 1.3998 1.5025 1.4346 1.4464 1.4177 1.4826 1.4918 1.5193 1.5237 2.7832 2.8104 1 3766 2.8006 2.5741 2.8924 2.5014 3.2616 2.3558 3.3276 1.9845 3.9687 2.2481 3.2112 2.1060 1.2345 2.2144 Liver/ TBW (xlOO) 4.4389 4.9654 3.5943 5.0100 4.7669 4.7572 4.3807 4.4988 4.2068 5.1832 4.2134 5.2014 4.4167 4.8877 4.0893 3.6632 4.4112 Spleen Weight (S) Spleen/ TBW (XlOO) Testes Weight (e) Testes/ TBW (xlOO) Thymus Weight (g) Thymus/ TBW (xlOO) 0.4045 0.3360 0 1724 0 2339 03357 0.4063 0.3320 0.3991 0.2206 0.3390 0.2655 0.3846 0.3217 0.3677 0.2893 0.1763 0.2795 0.6451 0.5936 0.4501 0.4184 0.6217 0 6683 0.5814 0.5505 0.3939 0.5280 0.5637 0.5041 0.6320 0.5597 0.5617 0.5231 0.5568 0.3122 0.2522 0.1892 0.2598 0.2160 0.3583 0.2760 0.3976 0.3483 0.3470 0.2306 0.3938 0.2231 0.3382 0.2394 0.1138 0.2433 0.4979 0.4456 0.4940 0.4648 0.4000 0.5893 0.4834 0.5484 0.6220 0.5405 0.4896 0.5161 0.4383 0.5148 0.4649 0.3377 0.4847 0.3970 0.2687 0.1877 0.2249 1.9555 0.2615 0.2394 0.2410 0.2287 0.2881 0.1716 0.2563 0.1843 0.2298 0.2082 0.1500 0.2231 0.6332 0.4747 0.4901 0.4023 3.6213 0.4301 0.4193 0.3324 0.4084 0.4488 0.3643 0.3359 0.3621 0.3498 0.4043 0.4451 0.4444 BFG 003158 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Female Pups Page 6 Terminal Female Pup Body Adrenal No. No. Weight Weight (s> (g) Adrenal/ TBW (X1000) Drain Weight (g) Brain/ TBW (XlOO) Group 1 0 ppm IS01 3 1505 7 1500 13 1508 7 1510 10 1513 4 1514 14 1516 12 1517 10 1518 11 1519 9 1520 9 1521 14 1522 9 1524 8 1525 14 1528 5 1529 7 57.5 45.1 58.7 55.6 42.6 59.7 57.2 42.4 50.2 42.0 49.7 48.2 42.3 55.6 56.4 48.6 57.0 48.9 0.0186 0.0160 0.0233 0.0185 0.0129 0.0150 00244 0.0211 0.0161 0.0183 0.0241 0.0192 0.0104 0.0101 0.0143 0.0125 0.0200 0.0134 0.3235 0.3548 0.3969 0.3327 0.3028 0.2513 0.4266 0.4976 0.3207 0.4357 0.4849 0.3983 0.2459 0.1817 0.2535 0.2572 0.3509 0.2740 1.4092 14118 1.4080 1.4502 1.2906 1.4646 1.4830 1.4631 1.5817 1.3767 1.3857 1.4414 1.4642 1.5965 1.6360 1.4760 1.6248 1.4691 2.4508 3.1304 2.3986 2.6083 3.0296 2.4533 2.5927 3.4507 3.1508 3.2779 2.7881 2.9905 3.4615 2.8714 2.9007 3.0370 2.8505 3.0043 Kidneys Weight (g) 0.8546 0.7364 0.9002 0.8612 0.6549 0.8508 0.8758 0.6032 0.7119 0.6485 0.6580 0.7300 0.6748 0.8152 0.9048 0.8474 0.8605 0.6406 Kidneys/ TBW (X100) (g) Liver Weight (8) 1.4863 1.6328 1.5336 1.5489 1.5373 1.4251 1.5311 1.4226 1.4181 1.5440 1 3239 1.5145 1.5953 1.4662 1.6043 1.7436 1.5096 1.3100 2.5134 2.1767 2.9315 2.7498 1.9900 2.2876 3.0669 1.8530 2.3659 1.8108 2.4982 2.1068 2.1657 2.4240 2.681] 2.4675 2.7833 1.9712 Liver/ TBW (xlOO) 4.3711 4.8264 4.9940 4.9457 4.6714 3.8318 5.3617 4.3703 4.7129 4.3114 5.0266 4.3710 5.1199 4.3597 4.7537 5.0772 4.8830 4.0311 Ovaries Weight (g) Ovaries/ TBW (xlOO) Spleen Weight (g) Spleen/ TBW (XlOO) Thymus Weight (g) Thymus/ TBW (xlOO) 0.0213 0.0253 0.0479 0.0300 0.0176 0.0144 0.0186 0.0209 0.0193 0.0117 0.0183 0.0157 0.0170 0.0220 0.0193 0.0186 0.0217 0.0281 0.0370 0.0561 0.0816 0.0540 0.0413 0.0241 0.0325 0.0493 0.0384 0.0279 0.0368 0.0326 0.0402 0.0396 0.0342 0.0383 0.0381 0.0575 0.3074 0.2624 0.3700 0.2784 0.3235 0.2677 0.5648 0.2558 0.3374 0.2107 0.2591 0.2144 0.2376 0.3038 0.2890 0.3447 0.2963 0.2080 0.5346 0.5818 0.6303 0.5007 0.7594 0.4484 0.9874 0.6033 0.6721 0.5017 0.5213 0.4448 0.5617 0.5464 0 5124 0.7093 0.5198 0.4254 0.2747 0.2142 0.2342 0.1461 0.2246 0.2717 0.2986 0.1998 0.2287 0.0153 0.2135 0.2165 0.1496 0.3118 0.2798 0.2749 0.2661 0.2217 0.4777 0.4749 0.3990 0.2628 0.5272 0.4551 0.5220 0.4712 0.4556 0.0369 0.4296 0.4492 0.3537 0.5608 0.4961 0.5656 0.4668 0.4534 BFG 003159 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Female Pups Page 7 Female No. Terminal Pup Body No. Weight (g) Adrenal Weight (g) Adrenal/ TBW (X1000) Drain Weight (e) Brain/ TBW (XI00) Group II 2503 2504 2506 2510 2515 2516 2518 2522 2523 2524 2525 2527 2528 2530 2531 10 ppm 7 8 10 10 13 6 6 13 12 7 11 6 8 13 12 54.8 44.6 57.9 57.6 43.5 53.1 66.8 50.4 49.4 53.3 45.8 62.6 57.1 53.7 59.5 0.0096 0.0129 0.0158 0.0199 0.0170 0.0190 0.0281 0.0063 0.0149 0.0121 0.0236 0.0357 0.0203 0.0131 0.0158 0.1752 0.2892 0.2729 0.3455 0.3908 0.3578 0.4207 0.1250 0.3016 0.2270 0.5153 0.5703 0.3555 0.2439 0.2655 1.3425 1.3615 1.6082 1.4463 1.5552 1.4293 1.5321 1.4919 1.3834 1.3892 1.2930 1.5885 1.4376 1.5359 1.5191 2.4498 3.0527 2.7775 2.5109 3.5752 2.6917 2.2936 2.9601 2.8004 2.6064 2.8231 2.5375 2.5177 2.8601 2.5531 Kidneys Weight (8) 0.8323 0.7127 0.8916 0.9028 0.6433 0.7421 0.9400 0.7391 0.6557 0.7296 0.6794 0.9825 0.8914 0.8376 0.8515 Kidneys/ TBW (XI00) (8) Liver Weight (8) 1.5188 1.5980 1.5399 1.5674 1.4789 1.3976 1.4072 1.4665 1.3273 1.3689 1.4834 1.5695 1.5611 1.5598 1.4311 2.6008 1 8458 3.2997 ' 2.7478 1.8668 2.3362 3.5616 2.3690 1.9216 2.3714 2.0743 3.0526 2.8528 2.5064 2.5569 Liver/ TBW (xlOO) 4.7460 4.1386 5.6990 4.7705 4.2915 4.3996 5.3317 4.7004 3.8899 4.4492 4.5290 4.8764 4.9961 4.6674 4.2973 Ovaries Weight (8) Ovaries/ TBW (xlOO) Spleen Weight (8) Spleen/ TBW (XlOO) Thymus Weight (8) Thymus/ TBW (xlOO) 0.0189 0.0037 0.0224 0.0389 0.0155 0.0213 0.0344 0.0175 0.0141 0.0217 0.0196 0.0231 0.0387 0.0203 0.0230 0.0345 0.0083 0.0387 0.0675 0.0356 0.0401 0.0515 0.0347 0.0285 0.0407 0.0428 0.0369 0.0678 0.0378 0.0387 0.3608 0.3181 0.2562 0.2994 0,3032 0.2784 0.3289 0.2819 0.2587 0.2510 0.1951 0.3020 0.2650 0.2594 0,3167 0.6584 0,7132 0.4425 0.5198 0.6970 0.5243 0.4924 0.5593 0.5237 0,4709 0.4260 0.4824 0.4641 0.4831 0.5323 0.2772 0.1839 0.2653 0.2324 0.1957 0,2341 0.2455 0.2217 0.2102 0.2978 0.2030 0.2752 0.2626 0.2307 0.2806 0.5058 0.4123 0,4582 0.4035 0.4499 0.4409 0.3675 0.4399 0.4255 0.5587 0.4432 0.4396 0.4599 0.4296 0.4716 BFG 003160 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - FI Female Pups Page Female Pup No. No, Terminal Body Weight (fi) Adrenal Weight (S) Adrenal/ TBW (X1000) Brain Weight <g) Brain/ TBW (XI00) Llroup III -100 ppm 3502 14 55.6 3506 13 50.2 3507 10 41.2 3509 10 53.9 3511 8 61.1 3512 7 63.0 3515 9 54.0 3516 10 56.6 3517 fl 50.7 3518 14 57.5 3519 7 62.9 3521 8 60.6 3523 9 59.5 3524 8 64.9 3528 13 55.6 0.0153 0.0365 0.0194 0.0187 0.0147 0.0127 0.0171 0.0139 0.0106 0.0200 0.0175 0.0351 0.0201 0.0150 0.0058 0.2752 0.7271 0.4709 0.3469 0.2406 0.2016 0.3167 0.2456 0.2091 0.3478 0.2782 0.5792 0.3378 0.2311 0.1043 1.5336 1.4328 1.3277 1.5638 1,4778 1.5848 1.4964 1.5660 1.5328 1.5180 1.5449 1.5717 1.5730 1.6362 1.5782 2.7583 2.8542 3.2226 2.9013 2.4187 2.5156 2.7711 2.76 6 8 3.0233 2.6400 2.4561 2,5936 2.6437 2.5211 2.8385 Kidneys Weight <g> 0.7950 0.7360 0.6382 0.7980 0.7924 0.8695 0.7936 0.7637 0.6975 0.7494 1.0843 0.8433 0.8621 0.9319 0.8641 Kidneys/ TBW (X100) (e) Liver Weight (g) 1.4299 1.4661 1.5490 1.4805 1.2969 1.3802 1.4696 1.3493 1.3757 1.3033 1.7238 1.3916 1.4489 1.4359 1.5541 2.6815 2.6635 1.7363 2.7005 2.9106 2.9656 2.7168 3,1270 2.7311 2.4714 3.1425 2.5540 2.5920 3.5279 2.3337 Liver/ TBW (x100) Ovaries Weight (g) Ovaries/ TBW (xlOO) Spleen Weight (fi) Spleen/ TBW (XlOO) Thymus Weight (E) Thymus/ TBW (xlOO) 4.8228 5.3058 4.2143 5.0102 4.7637 4.7073 5.0311 5.5247 53868 4.2981 4.9960 4.2145 4.3563 5.4359 4.1973 0.0325 0.0225 0.0175 0.0222 0.0279 0.0103 0.0206 0.0236 0.0159 0.0258 0.0193 0.0265 0.0206 0.0201 0.0179 0.0585 0.0448 0.0425 0.0412 0.0457 0.0163 0.0381 0.0417 0.0314 0.0449 0.0307 0.0437 0.0346 0.0310 0.0322 0.2897 0.2117 0.2648 0.2554 0.2134 0.3870 0.2996 0.3494 0.2222 0.3335 0.2908 0.3669 0.3331 0.2161 0.3750 0.5210 0.4217 0.6427 0.4738 0.3493 0.6143 0.5548 0.6173 0.4383 0.S800 0.4623 0.6054 0.5598 0,3330 0.6745 0.2398 0.2280 0.2259 0.2375 0.1928 0.3108 0.2570 0.2692 0.2351 0.2379 0.3150 0.2994 0.2779 0.2972 0.2387 04313 0.4542 0.5483 0.4406 0.3155 0.4933 0.4759 0.4756 0.4637 0.4137 0.5008 0.4941 0.4671 0.4579 0.4293 Terminal Organ and Body Weights and Organ/Body Weight Ratios o> <0o0)> CL 33 CL G> CO E0) u_ oo r-- Wo<c c E <LJa> O O09 CGD> (0fAj) c mo >os w co 0 o' o> -a I cs aa). 1 CC Terminal ; Thymus/ 0.6400 | 0.4251 | | 0.4835 | | 0.4131 | | 0.3856 | | 0.4188 1 f 0.4010 | | 0.3330 | i 0.4028 | 1 91 CO & S3 oo' HJ 3 1 u3 Xo ?2 9 dd 90 n d cins NTs !Cr*rS SO *T 99d 1 d <*0 cON' d vOn 9 9cs O* r* f*i d o ?: d 9V r*> CCCCSSSs a On d X d o d o v d 90 va X ao 9ccss V> X 9oo 2 dddd ddddddddo9od Spleen/ Ovaries/ 5 S3 o o E- * s *VE5L 1 3 1 > cd H j E; m I X 9> *s 3 c s 03 oo HX j i i ; X x dn o9 in O9C9S' e^r~i 9^r VA S s<n sS NT NOnS CS s n on <OnN d on Or*si in NOT Os i? in cs r~ 9 Vv O<mnn r9m~ 9 ddddddd oddddd Oo' NX cn Xn m r ocs isn rh oXirnA d d Os d ao o. Ppci ome cs m**> On rcs- o d d t*i <ranns d cs voa d WVN dodddodddd dddddd n VNo 9 9 con o o do d fS d O <N md O OWfS1' o do d o 0.0402 0.0214 0.0096 0.0290 cmrsn omcn TT Op*-' ia C199 ceeses c0mn0 ra~o cs ao m fn v<an 999 o9 9 9 9o dod dd d d dddd cs 9 CS o nin o o 9" cs cs cos 5 cs cs s 1 p* 9CS o cs cs o d d d d o' dod oo V N vOOn IA NO d d X d d m cn acso SoOe r r- X Cn d X IA IT X o cs 9cn- m9r-' 9rccns dm X m d p" 9mr~- WN wi d rf iri tr d 9- d 9 * > 3 u 4l WM o' ca H o K S' s -o *6X 1 3 s 9CS 9 ao o o X d dd 00 o d 9n va rcsc~ NCOS so X cn d va dm ON o 9 oOn X XNVO no x PI ocs CS <N rn cs d cs ri d fT> d r% d j dom d -- [ ao -- ;o CS V; j c<nn O' o* wv% X in N d 9 9 9NS m V <n o va va ?n d in v 'O m d cs 9 9 p'l 9 o* Vni n 1 1 pW*l On d On NO Os d 90 es in o o o X sa in x c*oe 9NSn r- m 9 9 9 9 9 O P- 9CS" o i9n o n 9 Oee d sa 9 9 oddddd d 9Od dd Liver/ Kidneys/ Adrenal/ s 5 oo 3SX 1 u3 > x X Os 90 <N N X o d t 'C vc r* r9cs c~ o m m sa o d <n d Cs 9CeeS oe fs 9- 9 9 fs 9 m en CN 1A d Vl d 00 r> Q ? On O d X d d f^i cs cn cs d d cs CS CS d d cn r"i 00 V ocn rt*) n cs 00 c^ tn 9 X d X m d m m md dvs \D Os \a ea9eo- VX d dNO d On dn v<an o rcn- dX edn din d oopcs 00 90 5? Os ors cs cs n 9 *CTS morl d n 9 cs 0ccns0 CS CnS <n 9tn- 99- 9 9ccns p~ c9s nond n cs in o ddddddddddddddd (o o o ix ) | " s u3 ss < sxa o o VO O o o NS Os o <n Ooos SO o o o ddo o d d O cr~s 9 mcs r 9 9 m 9CS 9 m cs o 90 O od d d ddd ddod o d o >1 It 9 1 3 & S al Bui ai ! b x d I a. *n X r- n cs n o sa V% Kin S3 d in d d in in va 9 9 d Vi 9 9 dd 0 d 9 Cs 90 cs cn r- vs cs r- en ts cs 9 00 > & 1 V> ** n o v> * fon vh 9- o icn Os 9 m 9- IA d n IA V> X Vi 9 m 9- cs m 9 CCSS m 9 9 CS m 9 SO CnS 9 On (S m BFG 003162 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Male Pups Page 10 Terminal Female Pup Body Adrenal No. No. Weight Weight (0 (8> Adrenal/ TBW (X1000) Bruin Weight <g> Brain/ TBW (XI00) Group I - Oppm 1535 9 1537 4 1538 5 1540 2 1542 7 1543 4 1551 3 1553 6 1558 2 1561 1 1565 3 1570 5 1572 7 1578 3 1580 1 47.9 23.4 46.2 46.9 40.6 39.2 40.8 31.5 36.6 38.7 42.8 45.4 47.8 41.4 38.1 0.0180 0.0073 0.0138 0.0116 0.0168 0.0134 0.0150 0.0132 0.0156 0.0143 0.0201 0.0141 0.0206 0.0123 0.0133 0.3758 0.3120 0.2987 0.2473 0.4138 0.3418 0.3676 0.4190 0.4262 0.3695 0.4696 0.3106 0 4310 0.2971 0.3491 1.5380 1.3373 1.5687 1.5415 1.5671 1.5102 1.5191 1.3866 1.4489 1.5714 1.4407 1.6119 1.5101 1.4167 1.5221 3.2109 5.7150 3.3955 3.2868 3.8599 3.8526 3.7233 4.4019 3.9587 4.0605 3.3661 3.5504 3.1592 3.4220 3.9950 Kidneys Weight (e) 0.8221 0.3730 0.6909 0.7215 0.5408 0.5297 0.6602 0.4295 0.5359 0.5602 0.6333 0.6258 0.6804 0.5809 0.5968 Kidneys/ TBW (XI00) (E) 1.7163 1.5940 1.4955 1.5384 1.3320 1.3513 1.6181 1.3635 1.4642 1.4475 1.4797 1.3784 1.4234 1.4031 1.5664 Liver Weight (e) 2.6870 0.9669 2.1872 2.4812 1.6145 1.2803 1,8760 1.2141 1 6136 1.6716 1.9363 1.8290 1.8616 1.6201 1.7342 Liver/ TBW (xlOO) 5.6096 4.1321 4.7342 5.2904 3.9766 3.2661 4.5980 3.8543 4.4087 4.3194 4.5241 4.0286 3.8946 3.9133 4.5517 Spleen Weight (E) Spleen/ TBW (xlOO) Testes Weight (8) Testes/ TBW (xlOO) Thymus Weight (> Thymus/ TBW (xlOO) 0.2220 0.0552 0.2493 0.1836 0.1458 0.0902 0,1447 0.1303 0.1465 0.3313 0.1692 0.1723 0.2014 0.1559 0.1040 0.4635 0.2359 0.5396 0.3915 0.3591 0.2301 0.3547 0.4137 0.4003 0.8561 0.3953 0.3795 0.4213 0.3766 0.2730 0.2163 0.0833 0.1995 0.1818 0.1806 0.1481 0.1884 0.1190 0.1608 0.1687 0.1978 0.2104 0.2055 0.1574 0.1449 0.4516 0.3560 0.4318 0.3876 0.4448 0.3778 0.4618 0.3778 0.4393 0.4359 0.4621 0.4634 0.4299 0.3802 0.3803 0.2591 0.0733 1.21 SO 0.1991 0.1909 0.1070 0,1878 0.1572 0.1217 0.1367 0.1328 0.1730 0.2598 0.1388 0.1027 0.5409 0,3132 2.6299 0.4245 0.4702 0.2730 0.4603 0.4990 0.3325 0.3532 0,3103 0.3811 0.5435 0.3353 0.2696 BFG 003163 Terminal Organ and Body Weights and Organ/Body Weight Ratios 43 03 0CO - V) 3Q. a. a> CO CM o CO CO cco E H03 oe .2&' "R = . o W C Q. 3 03 X E Terminal A d re n a l/ 1 (X I000) I B ra in / K id n e y s / L iv e r/ ! S p le e n / T e ste s/ Thym us/ 0 .3 3 5 3 1 | 0 .3 1 4 1 I | 0 .3 3 7 5 1 i 0 .3 4 3 1 | ; 0 .3 7 9 5 | | 0 .4 0 2 7 I | 0 .2 8 7 G \ S a b- X s 1 'B s 1 o Hx 52 n us 1 H i S' X s 41 41 "Sc I* 1 u PS s 90 PI CS PT ri n Ov <s pi r- vs Pi (T) d do V -flOn 90 r* cs PS cs dd 06 so vs PS 90 <T oc 00 sO PS r* 90 OS Vi 'T 90 VN cs ii r~ CS oodd fl- r~ SO SO v> CS CS r NO o 90 NO PS VO CS 00 cr cs o Cl Vi cs OS 90 fl fl 'T 2 *r cs p*l Pi PI m d o do d dodddd X 90 r so 90 NO ps 5r-* PN r- r* cs SO PS cs PS PS 8 SO o r- PS v> p*i PS n 00 pH PH o d o dd o dd d * d d o T pi 90 r- Cs 90 Vi oc PN Os O' 96 P* S" PI pi CN T r*i PS 90 PS P^ cs n fi c*> a pi 90 s- o odoooo d cs v% p*i Cn o 'T o o PI r^i n Pi r- PS s0 00 On Os 90 00 ~ VN NO 00 fl o CN cs cs O cs PS d o' o O d o d d d o E X h> 4t > u ti 3w S' a u HX PS 00 5 cs A PS r- cs v% r> O' 90 P^ sp fl ee v> r*- cs On SO 00 90 r- o\ cs <s 90 2 f> V PI Os 90 v% 00 06 NO n o m *T PS V p^ p*i fl- fl1 VS a- fl* PS CS a Os cs pn 00 Cs PS PI rl oc o p"> PS o PS S' s Os VN n cs cs p^ Cs X cv fl- 96 90 cs 90 O (N PS PS oc cs On PS r- \Q VN m o trj PS cs 96 'C 06 NO ON PS a cs PS <s BO VS 00 BO m V in cs PO CS cs r*i jj u 4 M *s * s % 1 M es ! VN n PI On 9- P^ cs m o P^ o V> v go NO o fl- VO v> V| cs m Os o 90 o r-. P-5 cs PS PS m SO V| Pi VS so VS o v> NO do o o O PS C" m PS r- P^J pi Ml r- v> oc r- V~1 ON cs o NO V| os SO oc cs V O' cs Vi r 06 cs en cs v> 00 PS PS pn v CS PS pi pi ri A ri tn ri pn PS cS pn pi ri pi vi vi p* Os vs 1 PS SO vs VS NO 06 96 NO p^ cn NO PS 90 p^i o Cs V Vi 00 Vi CS Vi VI h* fi vj cn VN PI PN VI Vi m S go cs Vl r* m fll cn a sO V"i PS in V> 00 9i cs r*- e PS PS v> Cl m v> CS 90 cs PI A en pn cn cs n m cs cs ddd d d s *40 * o cs 00 W *o V*l cn fl- r~ 90 v-> CS r* cs cs cs os oa o Oo d dd d ddd 1 Cs V a. z a 1Z CS C-i 90 so flse S X A n PS p' P- *i K PS H CS Vi pn fl- V> >r Cl p^ fl- fl- S' s a. c. - - VI 00 - r* - PS VO CN PS Pi PS PI 3w O cs tr f*> ITS PS V> PS Pi io PS vs PS -<r Ti CS 90 VN CS Vi VN PS cs v> v\ PS V Vi Vi rs Vi Vi Vi cs On Vi vs PS n w PS in es Vi rVi PS O BFG 003164 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Male Pups Page 12 Terminal Female Pup No. No. Body Weight Adrenal Weight (e) (g> Adrenal/ TBW (X1000) Brain Weight (E) Brain/ TBW (X100) roup Hi - 100 ppm 3533 2 50.2 3534 2 44.5 3536 2 46.9 3537 1 35.9 3538 1 43.4 3543 2 41.5 3545 2 44.8 3547 1 41.4 3549 7 34.8 3551 1 37.2 3555 5 49.2 3557 7 41.5 3564 2 32.5 3565 5 27.9 3568 4 28.4 0.0160 0.0142 0.0140 0.0218 0.0153 0.0140 0.0176 0.0155 0.0120 0.0125 0.0203 0.0173 0.0148 0.0101 0.0118 0.3187 0.3191 0.2985 0.6072 0.3525 0.3373 03929 0.3744 0.3448 0.3360 0.4126 0.4169 0.4554 0.3620 0.4155 1.4966 1.4291 1.5796 1.4427 1.4846 1.5036 1.3923 1.4533 1.3271 1 3769 1.3758 1.4079 1.3842 1.4800 1.3761 2.9813 3.2115 3.3680 4.0187 3.4207 3.6231 3,1078 3,5104 3.8135 3.7013 2.7963 3.3925 4.2591 5.3047 4.8454 Kidneys Weight <e) 0.7526 0.6262 0.6831 0.5069 0.5431 0.6118 0.6196 0.6191 0.4574 0.5483 0.7023 0.5622 0.4770 0.4235 0.3958 Kidneys/ TBW (X100) <e) Liver Weight (e) 1.4992 1.4072 1.4565 1.4120 1.2514 1.4742 1.3830 1.4954 1.3144 1.4739 1.4274 1.3547 1.4677 1.5179 1.3937 2.2327 1.9026 2.2119 1.4007 1.7575 1.8664 1.9J4J 1.7517 1.3172 1 5159 2.1714 1 6676 1.3800 1.2377 1.0161 Liver/ TBW (xIOO) 4.4476 4.2755 4.7162 3.9017 4.0495 4.4973 4.2725 4.2312 3.7851 4.0750 4.4134 4.0183 4.2462 4.4362 3.5778 Spleen Weight (t) Spleen/ TBW (xIOO) Testes Weight (e) Testes/ TBW (xIOO) Thymus Weight (e) Thymus/ TBW (xIOO) 0.2280 0.1912 0.1976 0.0875 0.1750 0.1289 0.1854 0.1527 0.1107 0.1328 0.2092 0.1237 0.1245 0.0907 0.1078 0.4542 0.4297 0.4213 0.2437 0.4032 0.3106 0.4J38 0.3688 0.3181 0.3570 0.4252 0.2981 0.3831 0.3251 0.3796 0.2114 0.1784 0.1924 0.1646 0.1779 0.2007 0.2099 0.1909 0.1570 0.1669 0.1862 0.1544 0.1534 0.1214 0.0928 0.4211 0.4009 0.4102 0.4585 0.4099 0.4836 0.4685 0.4611 0.4511 0.4487 0.3785 0.3720 0.4720 0.4351 0.3268 0.2752 0.2008 0.1790 0.1987 0.1986 0.1983 0.1387 0.1641 0.0983 0.1565 0.1726 0.1486 0.1335 0.0865 0.1668 0.5482 0.4512 0.3817 0.5535 0.4576 0.4778 0.3096 0.3964 0.2825 0.4207 0.3508 0.3581 0.4108 0.3100 0 5873 BFG 003165 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Male Pups Page 13 Terminal Female Pup Body No. No. Weight Adrenal Weight (E> <e) Adrenal/ TBW (XI000) Brain Weight () Brain/ TBW (XI00) Group IV - 1100 ppm 4531 7 43.7 4535 4542 4548 4551 4554 4555 4556 4557 4564 4566 4568 4575 4577 4579 2 7 1 9 2 3 1 5 6 8 2 4 6 3 41.4 53.7 44.9 34.1 42.4 52.9 43.2 42.7 35.5 37.9 30.9 37.1 32.9 44.1 0.0155 0.0100 0.0179 0.0130 0.0150 0.0182 0.0170 0.0098 0.0138 0.0134 0.0144 0.0167 0.0133 0.0102 0.0180 0.3547 0.2415 0.3333 0,2895 0.4399 0.4292 0.3214 0.2269 0.3700 0.4338 0.3799 0.540S 0.3585 0.3100 0.4082 1.5198 1.5192 1.6129 1.4517 1.5325 1.4215 1.5621 1.4643 1.5038 1.3777 1.3927 1.1827 1.5263 1.3549 1.5408 3.4778 3.6696 3.0035 3.2332 4.4941 3.3526 2.9529 3.3896 3 5218 3.8808 3.6747 3.8275 4.1140 4.1182 3.4939 Kidneys Weight (8) 0.5930 0.5705 0.7566 0.5676 0.5030 0.5843 0.6742 0.5913 0.6098 0.5545 0.4841 0.4364 0.6171 0.4935 0.6255 Kidneys/ TBW (XI00) (E) 1.3570 1.3780 1.4089 1 2641 1.4751 1.3781 1.2745 1.3688 1.4281 1.5620 1.2773 1.4123 1.6633 1.5000 1.4184 Liver Weight (E) 1.9245 1.7620 2.5416 1.8943 1.2053 1.7323 2.2573 2.1617 1.8778 1.7072 1.4774 1.2177 1.5326 1.2452 2.0171 Liver/ TBW (xlOO) 4.4039 4.2560 4.7330 4.2189 3.5346 4.0856 4.2671 5.0039 4.3977 4.8090 3.8982 3.9408 4.1310 3.7848 4.5739 Spleen Weight (b) Spleen/ TBW (XlOO) Testes Weight (e) Testes/ TBW (XlOO) Thymus Weight (E) Thymus/ TBW (xlOO) 0.2013 0.1495 0.3308 0.1668 0.1034 0.1447 0.1720 0.2231 0.1960 0.1410 0.1389 0.1014 0 1518 0.1000 0.2614 0.4606 0.3611 0.6160 0.3715 0.3032 0.3413 03251 0.5164 0.4590 0.3972 0.3665 0.3282 0.4092 03040 0.5927 0 1839 0.1660 0.2113 0.1880 0.1212 0.1872 01952 0.1872 0.1767 0.1428 0.1239 0.1310 0.1585 0.1196 0.1640 0.4208 0.4010 0.3935 0.4187 0.3554 0.4415 0.3690 0.4333 0.4138 0.4023 0.3269 0.4239 0.4272 0.3635 0.3719 0.1817 0.1572 0.1825 0.1730 0.1159 0 1397 0.2250 0.1198 0.1270 0.1208 O.I359 0.1050 0.1436 0.1541 0.1512 0.4158 0.3797 0.3399 0.3853 0.3399 0.3295 0.4253 0.2773 0,2974 0,3403 0.4113 0.3398 0.3871 0.4684 0.3429 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Female Pups Page 14 Terminal Female Pup Body No. No. Weight (g) Adrenal Weight (8) Adrenal/ TBW (X1000) Brain Weight (E) Brain/ TBW (X100) Group 1 - 0 ppm 1535 15 1537 9 1538 10 1540 7 1542 14 1543 8 1551 16 1553 14 1558 6 1561 14 1565 12 1570 14 1572 11 1578 10 1580 4 48.2 24.2 43.4 43.0 37.5 43.6 40.3 32.3 37.2 32.9 45.2 42.1 47.8 45.8 43,2 0.0127 0.0077 0.0169 0.0100 0.0146 0.0149 0.0166 0.0098 0.0139 0.0129 0.0167 0.0138 0.0188 00138 0.0177 0.2635 0.3182 0 3894 0.2326 0.3893 0.3417 0.4119 0.3034 0.3737 0.3921 0.3695 0.3278 0.3933 0.3013 0.4097 1.5278 1.1128 1.4808 1.4529 1.4446 J.519I 1.4206 1.4079 1.4435 1.4692 1.4816 1.4687 1.4670 1.5145 1.5746 3 1697 4 59X3 3 412CJ 3 37KX 3.X523 3 4842 3.5251 4.3588 3.8804 4.4657 3.2779 3.4886 3.0690 3.3068 3.6449 Kidneys Weight (g) 0.7273 0.3748 0.6607 0.6160 0 495X 0.6903 0.6005 0.4536 0.5857 0.5472 0.6339 0.7045 0.7443 0.6201 0.7158 Kidneys/ TBW (XI00) (S) Liver Weight (g) 1.5089 1.5488 1.5224 1 4326 1.3221 1.5833 1.4901 1.4043 1.5745 1.6632 1.4024 1.6734 1.5571 1.3539 1.6569 2.4504 0.9628 2.0097 1.7664 1.4380 2.0102 1.7639 1.4268 1.5834 1.5208 1.8858 2.1447 2.2165 1.9303 2.3735 Liver/ TBW (xlOO) Ovaries Weight (g) Ovaries/ TBW (xlOO) Spleen Weight (g) Spleen/ TBW (xlOO) Thymus Weight (g) Thymus/ TBW (xlOO) 5.0838 3.9785 4.6306 4.1079 3 8347 4.6106 4.3769 4.4173 4.2565 4.6225 4.1721 5.0943 4.6370 4.2146 5.4942 0.0173 0.0037 0.0139 0 0151 0.0170 0.0113 0.0147 0.0116 0.0137 0.0120 0.0227 0.0109 0.0175 0.0186 0.0179 0.0359 0.0153 0.0320 0.0351 0.0453 0.0259 0.0365 0.0359 0.0368 0.0365 0.0502 0.0259 0.0366 0.0406 0.0414 0.2335 0.0777 0.2580 0.1948 0.1726 0.1979 0.1913 0.1224 0 1115 0.1301 0.2217 0.2067 0.2143 0.0778 0.1600 0.4844 0.3211 0.5945 0.4530 0.4603 0.4539 0.4747 0.3789 0.2997 0.3954 0.4905 0.4910 0,4483 0.1699 0.3704 0.1971 0.0913 0.2105 0.1878 0.1973 0.1419 0.1662 0.1458 0.1513 0.1178 0.2028 0.1664 0.2247 0.1825 0.1455 0.4089 0.3773 0.4850 0.4367 0.5261 0.3255 0.4124 0.4514 0.4067 0.3581 0.4487 0.3952 0.4701 0.3985 0.3368 BFG 003167 Terminal Organ and Body Weights and Organ/Body Weight Ratios aOco) CL </) D3. cl ce Ea> CliM. Woco CO E L0_) oooo CO 05 t0ocn5 .o2 -S' CO H 6w Li c eO .-Q2 "O -3o --e 2cL 3 4) X S pleen/ 1 i 0.3767 j 35 1 co H o o M 3 | P U 5 o a H s S% *3 MS* Of c =5 S' 5 cc H x o 5 2* 3 > c* 1 & CO o' o 6- 1. u3 J * 0881 0 90 O' IN O' pn pn m p- pn p- o VI in IN n p- rs p ip O' T n O <n pn pn pn ip IP tn r o' e> d d d d o d m C\ w es SO o fn 00 m ffs n- s m rs 90 ipp vs oe o 'O 90 m vs oc n 99 pn 90 90 m IN oo 9dd dd d9 VpOn cs N VP SO CN IN rs en n 00 o r90 pIN O' in 00 00 m tn 00 pn V> rs n VI ^r N r> n pn rn pn m OddddOd dd o> p~ ee Ch o r- rs m *r PN M o o so ip \S <n o pIN 00 i? pn 90 r- vs ip O 90 SS o in PN pn d 9 o' d d d d d d d d l j r^* *o m n m rs pj rs 99 o !^ s r* m w nr rs m rs rs m rm 0 rs m rs 2 pn s P *T IP O o * d d d d 2 i rs rs m *o Z2 'O m o o '* o Pv o oo o oo id d d d d d ' i m r~ | r* in -- o tn rs in 00 5 vP ! O' \5 IN ! v> Cs Nic|0 -- -- *P -- cSS- O' 3990 s pn rs 00 pn s r* 00 tn r* : j ip ^ rn fi r*i sr 1 -i2 n;-- -- ! rs "MIM'-I!t\?: or-'. m|X jh pn -- ; ] in ^ in n* n i im o ^ IN in SO VI O' w 06 90 00 O r-fl- m o. 00 IN O' pn 00 pn rs; cs IN,-;- - rs Kidneys/ & CC H o' o "G m : r* rn i X I ^ X 90 n rs 00 pn rn i -- ! pn 1 NO ^ fN i N 1 -- n*. 3* *r\ n n m rs 09 pv%n 00 m i pn ! ^ <*: n pn V\ rs pn pn sr s 9 JU *5 G w' ** S' o 1m f- X 1 Of ea > m 1 H l OC ' m nio'n1* x x x ^ r*. p* p' O' IN T 90 rs 99 PN S3 ;' -- j ^ O o O' 00 pn VI V V VP P* |d!dj,,d| o o d o o' 11 V I IN I r, i n ! O fs 1 1 o 1 -- p> tn rs 00 rs vs VO m rs 1 Cn -- i i m rs pn IN oc *T j ^ ; O | ^ O' cs in cs p- cs cn | m j | pn pn ip H rn pn pn pn IN _ l:ll VO VI [ (N i P- * n IN o rs O' O' C"5 -- IN O' PN 00 o 00 m ** [C - 1 X 1 VI Viviin1 V m fn o *r IN r^ $ 00 pn VI TT o pn pn i' m oc ^r HM -i X nip'ic t"-1 m t^* ] m C^- rs o pn o rs 90 sO *** m pn r- v-i v-> IN ' ! P~. cn r|m n pn m tn 90 rs rs o:o;o |o o d d d d d Adrenal/ Ti e i 2 Of 1 u f *3 a& e. 3 6 a> Z * 6 sZ 90 pn N cs m P- j i M r*i 1 O : vi O ;OIo m o o in m - O' PI IN O ip o <n pn d idid d d o o d d d d o 1; !i 00 O' -imlC m n V 00 O' ip pi | d 1 r>i nl m m j | ^ rl ri o>` in m cn ip Os IP VP i m| o K ec 1 ! ^ * : - pi V 00 - 1 Jp W 1 -o x O ph pn m 1& f-*! v> pn V* m ^Itf TT m i m | in im n : <n v% n in 1 n n in in n in CS (S rs N N N rs i rs rs rs j rs rs rs rs rs Terminal | 0.3978 | 0031^8 Huntingdon Life Sciences 96-4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Female Pups Page 16 Terminal Female Pup Body Adrenal No. No. Weight Weight is) (S) Adrenal/ TBW (X1000) Brain Weight () Brain/ TBW (XI00) Group (II 100 ppm 3533 13 47.7 3534 8 45.0 3536 7 44.6 3537 9 35.1 3538 9 39.7 3543 4 42.1 3545 10 47.9 3547 10 43.7 3549 9 43.0 3551 6 34.5 3555 12 39.4 3557 7 41.5 3564 13 22.6 3565 11 43.2 3368 6 33.8 0.0120 0.0155 0.0093 0.0168 0.0170 0.0120 0.0198 0.0(85 0.0111 0.0134 0.0138 0.0198 0.0099 0.0156 0.0131 0.2516 0.3444 0.2085 0.4786 0.4282 0.2850 0.4134 0.4233 0.2581 0.3884 0.3503 0.4771 0.4381 0.3621 0.3876 1.4362 1.4438 1.4236 1.3083 1.4068 1.4326 1.4133 1.4085 1.3746 1.2747 1.2721 1.4944 1.2146 1.4636 1.3664 3.0109 3.2084 3.1919 3.7274 3.5436 3.4029 2.9505 3.2231 3.1967 3.6948 3.2287 3.6010 5.3743 3.3880 4.0426 Kidneys Weight (fi) 0.7903 0.6100 0.6953 0.5681 0.5733 0.6394 0.6638 0.5757 0.6318 0.4702 0.6067 0.5470 0.3563 0.6922 0.5058 Kidneys/ TBW (X100) (r) 1.6568 1.3556 1.5590 1.6185 1.4441 1.5188 1.3858 1.3174 1.4693 1.3629 1.5398 1.3181 1.5765 1.6023 1.4964 Liver Weight is) 2.2751 2.0296 2.0246 1.3778 1.7292 1.8845 1.9031 1.7507 1.8746 1.5040 1.7715 1.5781 1.0042 2.1045 1.2519 Liver/ TBW (xlOO) 4.7696 4.5102 4.5395 3.9254 4.3557 4.4762 3.9731 4.0062 4.3595 4.3594 4.4962 3.8027 4.4434 4.8715 3.7038 Ovaries Weight (e) Ovaries/ TBW (XlOO) Spleen Weight is) J Spleen/ TBW (xlOO) Thymus Weight is) Thymus/ TBW (xlOO) 0.0157 0.0135 0.0084 0.0019 0.0087 0.0140 0.0233 0.0154 0.0144 0.0134 0.0162 0.0134 0.0079 0.0050 0.0107 0.0329 0.0300 0.0188 0.0054 0.0219 0.0333 0.0486 0.0352 0.0335 0.0388 0 0411 0.0323 0.0350 0.0116 0.0317 0.2432 0.2264 0.1859 0.1329 0.1502 0.1392 0.1625 0.1268 0.2081 0.1213 0.1507 0.1505 0.0693 0.1412 0.1021 0.5099 0.5031 0.4168 0.3786 0.3783 0.3306 0.3392 0.2902 0.4840 0.3516 0.3825 0.3627 0.3066 0.3269 0.3021 0.2664 0.1678 0.1758 0.1667 0.1649 0.1850 0.1551 0.1667 0.2304 0.1695 0.1862 0.2037 0.0968 0.2525 0.1673 0.5585 0.3729 0.3942 0.4749 0.4154 0.4394 0.3238 0.3815 0.5358 0.4913 0.4726 0.4908 0.4283 0.5845 0.4950 BFG 003169 Huntingdon Life Sciences 96*4080 Reproduction Study Appendix V Terminal Organ and Body Weights and Organ/Body Weight Ratios Terminal Sacrifice - F2 Female Pups Page 17 Female No. Terminal Pup Body No. Weiglil (g) Adrenal Weight (b) Adrenal/ TBW (X1000) Bruin Weight <g> Brain/ TBW (XI00) Group IV -1100 ppm 4531 9 44.1 4535 10 46.6 4542 9 50.9 4548 9 43.2 4549 2 21.7 4551 11 36.1 4554 6 44.4 4555 13 44.6 4556 12 46.1 4557 12 41.9 4564 12 46.0 4566 12 35.9 4568 7 40.5 4575 9 42.4 4577 11 26.4 4579 11 47.6 0.0129 0.0188 0.0230 0.0163 0.0108 0.0147 0.0155 0.0162 0.0109 0.0203 0.0224 0.0137 0.0176 0.0139 0.0070 0.0155 0.2925 0.4034 0.4519 0.3773 0.4977 0.4072 0.3491 0.3632 0.2364 0.4845 0.4870 0.3816 0.4346 0.3278 0.2652 0.3256 1.5231 1.4749 1.5945 1.4308 1.2359 1.2722 1.4812 1.4443 1.2891 1.4311 1.4769 1.3753 1.4628 1.5011 1.2844 1.5439 3.4537 3.1650 3.1326 3.3120 5.6954 3.5241 3.3360 3.2383 2.7963 3.4155 3.2107 3.8309 3.6119 3.5403 4.8652 3.2435 Kidneys Weight (e) 0.7115 0.6518 0.7634 0.6542 0.3327 0.5201 0.7282 0.6115 0.6770 0.5932 0.6552 0.5128 0.6305 0.6553 0.4040 0.6793 Kidneys/ TBW (X100) <g) Liver Weight (g) 1.6)34 1.3987 1.4998 1.5144 1.5332 1.4407 1.6401 1.3711 1.4685 1.4158 1.4243 1.4284 1.5568 1.5455 1.5303 1.4271 1.9081 2.2046 2.1955 2.0272 0.8532 1.4235 2.1211 2.0122 2.4884 1.8800 2.1163 1.4185 1.7056 1.9915 1.0004 2.1238 Liver/ TBW (xlOO) Ovaries Weight (E) Ovaries/ TBW (xlOO) Spleen Weight (g) Spleen/ TBW (xlOO) Thymus Weight (e) Thymus/ TBW (xlOO) 4.3268 4.7309 4.3134 4.6926 3.9318 3.9432 4.7773 4.5117 5.3978 4.4869 4.6007 3.9513 4.2114 4.6969 3.7894 4.4618 0.0098 0.0152 0.0205 0.0169 0.0140 0.0180 0.0105 0.0166 0.0139 0.0210 0.0185 0.0141 0.0215 0.0230 0.0042 0.0191 0.0222 0.0326 0.0403 0.0391 00645 0.0499 0.0236 0.0372 0.0302 0.0501 0.0402 0.0393 0.0531 0.0542 0.0159 0.0401 0.1977 0.1948 0.2375 0.2004 0.0611 0.1058 0.1631 0.1648 0.1965 0.1733 0.2225 0.1630 0.1455 0.1758 0.0780 0.2504 0.4483 0.4180 0.4666 0.4639 0.2816 0.2931 0.3673 0.3695 0.4262 0.4136 0.4837 0.4540 0.3593 0.4146 0.2955 0.5261 0.2350 0.2284 0.1779 0.1625 0.0652 0.1237 0.1962 0.1926 0.2123 0.2237 0.2405 0.1440 0.1345 0 1708 0.1225 0.1867 0.5329 0.4901 0.3495 0.3762 0.3005 0.3427 0.4419 0.4318 0.4605 0.5339 0.5228 0.4011 0.3321 0.4028 0.4640 0.3922 BFG 003170 APPENDIX W BFG 003171 Pathology Associates International A Company of Science Applications International Corporation An EmptoyBfrOwntd Company APPENDIX W SPERM ANALYSIS REPORT FOR VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS HLS STUDY NUMBER: 96-4080 PREPARED FOR HUNTINGDON LIFE SCIENCES (HLS) METTLERS ROAD EAST MILLSTONE, NJ 08875-2360 PREPARED BY PATHOLOGY ASSOCIATES INTERNATIONAL. (PAI) 15 WORMAN'S MILL COURT, SUITE I FREDERICK, MD 21701 BFG 003172 15 Worman's Mill Court, Suite I Frederick, Maryland 21701 (301) 663-1644 (301) 663-8994 FAX Draft Report HLS Study No.: 96-4080 TABLE OF CONTENTS Section Page No. I. QUALITY ASSURANCE STATEMENT ................................................................................. 4 II. MATERIALS AND METHODS ......................................................................................................... 5 A. Sample Collection .................................................................................................... B. Sperm Motility Evaluation ............................................................................ C. Total Sperm Count Determination.......................................................... D. Sperm Morphology Evaluation ...................................................................... E. Statistical Analyses ........................................................................................ 5 5 5 6 6 III. RESULTS ............................................................................................................................................. 6 A. Sperm Motility .......................................................................................................... B. Total Sperm Count ................................................................................................. C. Sperm Morphology .................................................................................................... 6 6 7 IV. DISCUSSION AND CONCLUSIONS ....................................................................................... 7 V. REFERENCES .................................................................................................................................... 7 2 BFG 003173 Draft Report HLS Study No.: 96-4080 INDEX OF TABLES AND APPENDICES Table Page No. 1. Summary of Px Sperm Analysis Parameters .................................................. 8 2. Summary of P2 Sperm Analysis Parameters .................................................. 9 Appendix Page No. A. Individual P2 Sperm Motility and Total Count Data ................... 10 B. Individual P2 Sperm Motility and Total Count Data.................... 12 C. Individual Px Sperm Morphology Data ......................................................... 14 D. Individual P2 Sperm Morphology Data............................................................. 18 3 BFG 003174 Pathology Associates International A Company of Science Applications International Corporation An Employee-Owned Company Sperm Analysis Report Vinyl Chloride Combined Inhalation Two-Generation Reproduction and Developmental Toxicity Study in CD Rats HLS Study Number: 96-4080 QUALITY ASSURANCE STATEMENT This sperm analysis project has been inspected and audited by the PA1 Quality Assurance Unit (QAU) as required by the Good Laboratory Practice (GLP) regulations promulgated by the U.S. Food and Drug Administration (FDA), Environmental Protection Agency (EPA) and the Organization for Economic Co operation and Development (OECD). The sperm analysis report is an accurate reflection of the recorded data. The following table is a record of the inspections/audits performed and reported by the QAU. Date of Inspection 05/09/97 11/24,25/97 11/24,25/97 Phase inspected Date Findings Reported to Management/ Study Teratoloqist Sperm Motility Study Data and Supporting Documentation Draft Sperm Analysis Report 05/09/97 11/25/97 11/25/97 Sharon E. Abel Quality Assurance Specialist Date 4 BFG 003175 I . RESERVED FOR QUALITY ASSURANCE STATEMENT 4 BFG 003176 Draft Report HLS Study No.: 95-4080 Vinyl Chloride Combined Inhalation Two-Generation Reproduction and Developmental Toxicity Study in CD Rats II. MATERIALS AND METHODS A. Sample Collection After the last Fx and F2 litters were delivered, the first 15 surviving P1 and P2 males, respectively, were euthanized by carbon dioxide asphyxiation followed by exsanguination. The P1 males were sacrificed on April 28-29, 1997, and the P2 males were sacrificed on September 15-16, 1997. For all animals, the abdominal cavity was opened and the reproductive organs exposed. For motility assessment, the right vas deferens was dissected away from the testis and immediately placed in a petri dish containing 10 ml of a solution consisting of 1% Bovine Serum Albumin dissolved in Phosphate Buffered Saline. The solution was prewarmed to a temperature of approximately 38C. A minimum 3 minute period was allowed for the sperm to swim out. The right epididymis was then removed and placed on dry ice. The frozen epididymides were then transferred to Pathology Associates International, Frederick, MD. and stored frozen at -70C or lower until evaluation for total sperm count. B. Sperm Motility Evaluation Following the swim out period, a sperm sample was obtained using a 100 ^im deep cannula. The cannula was immediately loaded into the prewarmed stage of the Hamilton Thorne IVOS automated sperm analyzer. Five fields were automatically selected by the analyzer and each motion image was recorded and stored on an optical disk. The images were subsequently analyzed and the percent motility determined for each animal. C. Total Sperm Count Determination Each frozen epididymis was removed from the freezer, thawed and the caudal section was trimmed and weighed. The cauda epididymis was homogenized and the suspension was transferred to a plastic test tube and vortexed. A 100 \il sample was transferred to a vial containing a dye which uniquely stains the head of the sperm. A sample of the stained sperm was placed into a 20 jam deep glass slide which was loaded into the analyzer. Twenty fields were automatically selected by the analyzer for each animal and total sperm counts determined. The counts were reported adjusted for caudal epididymal weight. 5 BFG 003177 Draft Report HLS Study No.: 96-4080 D. Sperm Morphology Evaluation Two Eosin stained slides were prepared for each animal from the caudal epididymis total count preparation. The slides were evaluated and a minimum of 200 sperm cells/animal were examined for morphological development. E. Statistical Analyses The means and standard deviations for the sperm motility, total count and sperm morphology data were calculated and compared across groups using the Kruskal-Wallis nonparametric ANOVA test. If a significant effect occurred {p<0.05), the Wilcoxon (MannWhitney U) test was used for pair-wise comparisons of each treated group to the control group. Statistical analyses were performed using an IBMTM compatible computer with SAS computer programs (SAS/STAT User's Guide, 1989). III. RESULTS A. Sperm Motility Table 1 (Pj_ Summary Data) Table 2 (P2 Summary Data) Appendix A (P1 Individual Appendix B (P2 Individual Data) Data) No apparent treatment-related effects were observed for the sperm motility data in either the P. or P2 males. Group mean values were comparable between the study groups. Group mean values ranged from 88.5% to 96.5% and 89.3% to 97.3% for the Pa and P2 males, respectively. No evidence of reduced motility due to treatment with Vinyl Chloride was observed in either generation. B. Total Sperm Count Table 1 (Px Summary Data) Table 2 (P2 Summary Data) Appendix A (Pi Individual Appendix B (P2 Individual Data) Data) The number of sperm/gram of cauda epididymis was comparable between the study groups. Mean values ranged from 819.9 to 947.2 and 850.1 to 1063.9 million sperm/gram for the P1 and P2 males, 6 BFG 003178 respectively. No treatment-related differences were observed. Draft Report HLS Study No.: 96-4080 C. Sperm Morphology Table 1 (Pi Summary Data) Table 2 (P2 Summary Data) Appendix C {Px Individual Appendix D (P2 Individual Data) Data) A low incidence of head/tail abnormalities was observed for animals in all treatment groups. Group mean values ranged from 0.03 to 5.13 and 0.07 to 0.27 percent abnormal sperm for the Px and P2 males, respectively. No treatment related differences were observed. IV.DISCUSSION AND CONCLUSIONS Mean percent motility, total sperm count and morphology were not affected by treatment with Vinyl Chloride in either generation at dosage levels of 0, 10, 100 and 1100 ppm. No biologically meaningful differences were observed between the study groups. __________________________________________ Michael D. Mercieca, B.S. Reproductive Toxicologist Pathology Associates International Date: V. REFERENCES SAS Institute Inc., SAS/STAT User's Guide, Version 6, Fourth Edition, Cary, NC:SAS Institute Inc., 1989. Vol. 2 p. 1195-1210. 7 BFG 003179 HLS STUDY NO.: 96-4080 TABLE 1 VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS SUMMARY OF Pt SPERM ANALYSIS PARAMETERS MOTILITY (PERCENT) Group: 12 3 Level: VINYL CHLORIDE (PPM) 0 10 100 Mean SD N 91.5 11.4 15 88.5 24.9 15 NONE SIGNIFICANTLY DIFFERENT FROM CONTROL 96.5 2.9 15 4 1100 91.4 14.9 14 TOTAL SPERM COUNT (MILLION SPERM/GRAM) Group: 12 3 4 Level: VINYL CHLORIDE (PPM) 0 10 100 1100 Mean SD N 826.5 197.9 15 947.2 313.8 15 NONE SIGNIFICANTLY DIFFERENT FROM CONTROL. 872.2 222.2 16 819.9 313.5 15 SPERM MORPHOLOGY (PERCENT ABNORMAL) Group: 12 3 4 Level: VINYL CHLORIDE (PPM) 0 10 100 1100 Mean SD N 0.03 0.13 15 0.23 0.50 15 5.13 19.70 16 0.86 2.65 14 MEAN AND STANDARD DEVIATIONS WERE CALCULATED USING THE TOTAL NUMBER OF ABNORMAL SPERM AS A PERCENTAGE OF THE NUMBER OF SPERM EXAMINED. NONE SIGNIFICANTLY DIFFERENT FROM CONTROL. 8 BFG 003180 HLS STUDY NO.: 96-4080 TABLE 2 VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS SUMMARY OF P2 SPERM ANALYSIS PARAMETERS MOTILITY (PERCENT) Group: 1 Level: VINYL CHLORIDE (PPM) 0 23 10 100 Mean SD N 96.2 2.3 13 97.3 1.9 15 NONE SIGNIFICANTLY DIFFERENT FROM CONTROL 94.5 9.0 15 4 1100 89.3 17.8 13 TOTAL SPERM COUNT (MILLION SPERM/GRAM) Group: 1 Level: VINYL CHLORIDE (PPM) 0 23 4 10 100 1100 Mean SD N 1063.9 231.1 15 1053.1 340.1 15 NONE SIGNIFICANTLY DIFFERENT FROM CONTROL. 850.1 223.2 15 1025.4 396.1 15 SPERM MORPHOLOGY (PERCENT ABNORMAL) Group: 1 Level: VINYL CHLORIDE (PPM) 0 23 4 10 100 1100 Mean SD N 0.07 0.18 14 0.27 0.46 15 0.20 0.41 15 0.23 0.65 15 MEAN AND STANDARD DEVIATIONS WERE CALCULATED USING THE TOTAL NUMBER OF ABNORMAL SPERM AS A PERCENTAGE OF THE NUMBER OF SPERM EXAMINED. NONE SIGNIFICANTLY DIFFERENT FROM CONTROL. 9 BFG 003181 WT.fi STUDY NO. : 96-4080 APPENDIX A VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL Pj, SPERM MOTILITY AND TOTAL COUNT DATA Group 1: 0 PPM (VINYL CHLORIDE) Animal No. 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1023 1027 % Motility 94 89 98 74 97 97 94 90 96 97 57 98 94 99 98 Total Count {million sperm/gram) 759.8 1004.1 678.5 1048.8 626.8 921.4 729.0 904.2 123S.4 1033.4 844.2 479.4 651.3 732.8 748.5 Group 2: 10 PPM (VINYL CHLORIDE) 2001 2002 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2020 97 98 88 96 97 83 97 97 96 88 100* 98 0a 98 94 a=ONLY 4 SPERM PRESENT FOR MOTILITY EVALUATION. 784.6 1254.1 529.4 1025.9 942.2 821.5 1753.4 718.1 752.1 903.3 1085.3 658.3 640.0 1276.4 1062.8 10 003182 HLS STUDY NO.: 96-4080 APPENDIX A VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL Px SPERM MOTILITY AND TOTAL COUNT DATA Group 3: 100 PPM (VINYL CHLORIDE) Animal No. % Motility Total Count (million sperm/gram) 3001 3002 3003 3004 3005 3006 3007 3008 3009 3010 3014 3020 3022 3026 3029 3030 94 97 95 99 88 98 99 98 99 96 96 98 99 97 95 a a=NO SPERM PRESENT FOR MOTILITY EVALUATION. 961.0 1091.8 790.7 1105.7 654.2 1009.8 646.4 1179.0 531.5 869.6 574.6 908.7 1136.4 731.1 1123.5 641.7 Group 4: 1100 PPM (VINYL CHLORIDE) 4001 4002 4003 4004 4005 4006 4007 4008 4009 4010 4011 4012 4013 4014 4027 79 99 95 93 95 94 98 a 93 98 99 98 43b 98 98 a=NO SPERM PRESENT FOR MOTILITY EVALUATION. b=ONLY 7 SPERM PRESENT FOR MOTILITY EVALUATION. 782.7 1310.1 981.7 764.3 719.4 1015.2 671.9 154.3 1028.5 1094.8 603.3 723.2 451.8 1325.0 657.9 II BFG 003183 HLS STUDY NO.: 96-4080 APPENDIX B VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL P2 SPERM MOTILITY AND TOTAL COUNT DATA Group 1: 0 PPM (VINYL CHLORIDE) Animal No. % Motility Total Count (million sperm/gram) 1031 1032 1033 1035 1037 1039 1041 1043 1045 1047 1048 1058 1068 1071 1078 94 92 97 95 98 a 93 95 97 98 100 a 96 97 98 841.5 1247.1 1065.9 1033.9 1161.7 400.5 1077.0 1360.7 1295.9 1148.5 930,7 1148.8 920.8 1164.1 1160.9 a=NO SPERM PRESENT FOR ANALYSIS. Group 2: 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2066 10 PPM (VINYL CHLORIDE) 98 99 99 96 94 99 99 98 97 95 99 95 94 99 98 770.2 1182.8 759.8 1198.1 1492.2 806.6 972.0 1034.1 1434.0 1152.8 820.5 754.0 1851.3 978.3 590.5 12 BFG 003184 KLS STUDY NO.: 96-4080 APPENDIX B VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL P2 SPERM MOTILITY AND TOTAL COUNT DATA Group 3: 100 PPM (VINYL CHLORIDE) Animal No. % Motility Total Count (million sperm/gram) 3031 3032 303 3 3034 3035 3037 3039 3041 3042 3043 3045 3046 3047 3048 3049 99 98 63a 93 96 100 94 99 98 95 99 96 93 99 95 740.5 425.6 870.3 763.7 698.5 769.9 1015.7 993.1 1191.4 699.8 847.2 747.7 1364.6 850.0 772.8 a=ONLY 7 SPERM PRESENT FOR MOTILITY EVALUATION. Group 4: 1100 PPM (VINYL CHLORIDE) 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 94 96 98 94 98 98 a a 97 100 33b 90 97 84 82 a=NO SPERM PRESENT FOR ANALYSIS. Q=ONLY 12 SPERM PRESENT FOR MOTILITY EVALUATION. 1208.5 1370.2 1120.1 1099.2 907.6 710.0 654.0 315.6 1406.3 1148.2 606.5 765.7 1660.2 1654.2 754.4 13 BFG 003185 HLS STUDY NO.: 96-4080 APPENDIX C VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS GROUP 1: 0 PPM (VINYL CHLORIDE) Animal No. Normal Amorphous 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1023 1027 200 200 200 200 200 200 200 200 200 199 200 200 200 200 200 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 INDIVIDUAL p! SPERM MORPHOLOGY DATA Small 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Enlarged 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Tail- Coiled Bent Double 000 00 0 00 0 00 0 00 0 00 0 00 0 000 00 0 000 000 000 000 000 000 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003186 14 HLS STUDY NO.: 96-40B0 APPENDIX C VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL Pj SPERM MORPHOLOGY DATA GROUP 2: 10 PPM (VINYL CHLORIDE) Animal No. 2001 2002 2003 2004 2005 2006 2007 2008 2009 2010 2011 2012 2013 2014 2020 Normal 200 200 200 198 200 197 200 200 200 198 200 200 200 200 200 -------- H e a d---------------------- Amorphous Small Enlarged 0 00 0 00 0 00 2 00 0 00 3 00 0 00 0 00 0 00 2 00 0 00 0 00 0 00 0 00 0 00 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 -Tail- Coiled Bent Double 000 00 0 000 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 00 0 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 % c L8XS00 15 HLS STUDY NO.: 96-4080 APPENDIX C VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL PL SPERM MORPHOLOGY DATA GROUP 3: 100 PPM (VINYL CHLORIDE) Animal No. Normal --------H e a d---------------------- Amorphous Small Enlarged Double -Tail- Coiled Bent Double 3001 3002 3003 3004 3005 3006 3007 3008 3009 3010 3014 3020 3022 3026 3029 3030 200 200 199 200 200 200 200 200 199 199 200 200 200 200 197 42 0 0 0 0 0 0 0 0 1 0 0 0 0 0 1 158 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 00 0 10 0 00 0 00 0 000 00 0 00 0 00 0 01 0 000 000 000 00 0 02 0 00 0 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003188 16 HLS STUDY NO.: 96-4080 APPENDIX C VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL SPERM MORPHOLOGY DATA GROUP 4: 1100 PPM (VINYL CHLORIDE) Animal No. Normal -------- H e a d-------- v.............. Amorphous Small Enlarged 4001 4002 4003 4004 4005 4006 4007 4008 4009 4010 4011 4012 4013 4014 4027 200 200 200 198 200 199 200 a 200 200 200 199 b 180 200 200 0 00 0 00 0 00 2 00 0 00 0 00 0 00 0 00 0 00 0 00 1 00 20 0 0 0 00 0 00 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 -Tail- Coiled Bent Double 000 000 0 00 000 000 010 000 000 000 000 000 000 000 000 a=Too few cells (less then 200) to evaluate. b=Excessive fragmentation. Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003189 17 HLS STUDY NO.: 96-4080 APPENDIX D VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL P2 SPERM MORPHOLOGY DATA GROUP 1: 0 PPM (VINYL CHLORIDE) Animal No. Normal Amorphous Small Enlarged Double Coiled 1031 200 1032 200 1033 200 1035 200 1037 200 1039 a 1041 200 1043 199 1045 199 1047 200 1048 200 1058 200 1068 200 1071 200 1078 200 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 1 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 a=Too few cells (less then 200) to evaluate. Bent 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003190 18 HLS STUDY NO.: 96-4080 APPENDIX D VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS GROUP 2: 10 PPM (VINYL CHLORIDE) Animal NO. Normal Amorphous 2031 2033 2034 2036 2037 2038 2040 2042 2044 2046 2048 2050 2052 2054 2066 200 200 199 200 198 200 200 199 200 200 200 200 199 197 200 0 0 1 0 0 0 0 1 0 0 0 0 1 3 0 INDIVIDUAL P2 SPERM MORPHOLOGY DATA Small 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Enlarged 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Coiled 0 0 0 0 2 0 0 0 0 0 0 0 0 0 0 Bent 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Double 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003191 19 u<n & ooooooooooooooo 4-> o ooooooooooooooo u H Ca> ns CQ ooooooooooooooo ooooooooooooooo V IN Y L CHLORIDE COMBINED IN H A LA TIO N TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL T O X IC IT Y STUDY IN CD RATS ooooooooooooooo T<3u cn d ooooooooooooooo rH ac ooooooooooooooo 0D01 JS a HiHrOOOOOOOOHOOO o A o CD o M > V> <J\ OOOr-OOOOOOOCTiOOO OOiffi^OOOOOOOfflOOO o (NrlHHNNDMNNNriflMfl o * n cH/i ns E2 H Z OOOOOOOOOOOOOOO BFG 003192 HLS STUDY NO.: 96-4080 APPENDIX D VINYL CHLORIDE COMBINED INHALATION TWO-GENERATION REPRODUCTION AND DEVELOPMENTAL TOXICITY STUDY IN CD RATS INDIVIDUAL P2 SPERM MORPHOLOGY DATA GROUP 4: 1100 PPM {VINYL CHLORIDE) Animal No. Normal Amorphous -------- H e a d---------------------- Small Enlarged Double -Tail- Coiled Bent Double 4031 4033 4035 4037 4039 4041 4043 4045 4046 4047 4049 4050 4052 4054 4056 200 200 195 200 200 200 200 200 200 199 200 200 199 200 200 0 00 0 0 00 0 2 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 0 00 0 1 00 0 0 00 0 0 00 0 1 00 0 0 00 0 0 00 0 000 0 00 2 10 0 00 000 0 00 000 000 000 000 000 0 00 000 0 00 000 Other 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 BFG 003193 21 APPENDIX X BFG 003194 Huntingdon Life Sciences Reproduction Study 96-4080 Page 1 Draft Final Report Inhalation Report Appendix X 1. INTRODUCTION.................................................................................................. 2 2. MATERIAL AND METHODS 2.1. Husbandry During Exposure Periods......................................................................2 2.2. Test Material Preparation....................................................................................... 3 2.3. Test Material Administration and Chamber Operation........................................... 3 2.4. Exposure Chamber Sampling.................................................................................. 5 EXPOSURE GENERATION SYSTEM...................................................................................... 7 EQUIPMENT LIST........................................................................................................................ 8 MIRAN AMBIENT AIR ANALYZER Procedure and Methodology...................................................................................10 Miran Ambient Air Analyzer Setup....................................................................... 13 Calibration Curve - Groups II and III.................................................................... M Calibration Curve - Group IV................................................................................15 SUMMARY OF DISTRIBUTION TRIAL SAMPLES.............................................................16 CUMULATIVE EXPOSURE RECORD....................................................................................17 IN-CHAMBER OBSERVATIONS.............................................................................................62 BFG 003195 Huntingdon Life Sciences Reproduction Study 96-4080 Page 2 Draft Final Report inhalation Report Appendix X 1. INTRODUCTION This appendix presents the methodology for exposure atmosphere generation, monitoring and results. 2. MATERIAL AND METHODS 2.1. HUSBANDRY DURING EXPOSURE PERIODS 2.1.1. HOUSING Animals were individually housed in stainless steel, wire mesh cages within a 6m3 stainless steel and glass whole-body exposure chamber. The placement of the animals in the whole-body exposure cages was rotated at each exposure to ensure uniform exposure of the animals. A description of the animal rotation is included in the raw data. 2.1.2. FOOD None was provided during exposure. 2.1.3. WATER Water was available without restriction via an automated watering system (Elizabethtown Water Company, Westfield, New Jersey). 2.1.4. ENVIRONMENTAL CONDITIONS Chamber temperature and relative humidity were recorded every half-hour during exposure and maintained, to the maximum extent possible, within the ranges presented below. Temperature Desired: Actual: 20 to24C 16 to28C Relative Humidity Desired: Actual: 40 to60% 29 to79% BFG 003196 Huntingdon Life Sciences Reproduction Study 96-4080 Page 3 Draft Final Report inhalation Report 2.2. TEST MATERIAL PREPARATION The test material was used as received. Appendix X 2.3. TEST MATERIAL ADMINISTRATION AND CHAMBER OPERATION 2.3.1. ROUTE OF ADMINISTRATION Inhalation, whole body. 2.3.2. ROUTE JUSTIFICATION The inhalation route is one of the potential routes of human exposure to this test material. 2.3.3. EXPOSURE LEVELS 10, 100 and 1100 ppm 2.3.4. FREQUENCY OF EXPOSURES 6 hours per day. 2.3.5. DURATION Animals were exposed 2.3.6. DATES OF EXPOSURES Pi Generation: 7 January 1997 to 5 June 1997 Fi Generation: 20 May 1997 to 3 October 1997 2.3.7. PRE-STUDY TRIALS Trials were performed, prior to the start of the study, to evaluate the optimal set of conditions and equipment to generate a stable atmosphere at the targeted exposure levels. BFG 003197 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 4 Draft Final Report Inhalation Report Appendix X 2.3.8. CHAMBER OPERATION The exposure chambers were operated dynamically under slight negative pressure at a minimum airflow rate of 1200 liters per minute (Lpm), This flow rate was calculated to provide one complete air change every 5.0 minutes and a 99% equilibrium time (T99) of 23 minutes. This chamber size and airflow rate was considered adequate to maintain the animal loading factor below 5% and oxygen above 19%. The chamber was exhausted through a system consisting of a coarse filter, a HEPA filter and a MOCO fume incinerator (on days when the fume incinerator was not functioning, a charcoal filter was used along with the coarse filter and HEPA filter). 2.3.9. EXPOSURE PROCEDURE Group I: House supply air was fed through the turret of a 6m3 glass and stainless steel whole-body exposure chamber, at a rate of 1329 Lpm, with a static pressure of-0.15 in. H2O. The airflow and static pressure were maintained at these settings throughout the 360 minute exposures. The animals remained in the chamber for a minimum of 30 minutes following the exposures to allow the chamber to clear at the same airflow rate used during exposures. Groups H through IV: House supply air was fed through the turret of a 6m3 glass and stainless steel whole-body exposure chamber at flow rates of 1267 Lpm, 1257 Lpm and 1239 Lpm for Groups II, III and IV, respectively. The airflow and static pressure were maintained at these settings throughout the 360 minute exposures. The test material was delivered from a compressed gas cylinder via Vi' tubing to a Scott Specialty Gases regulator (equipped with inlet and outlet backpressure gauges). From the regulator, the test material flowed to a purge/vent system, which was attached to the inlet side of an electronic solenoid valve. The electronic solenoid valve was intended to shut-off the test material flow if electrical power or bfg 003198 Huntingdon Life Sciences Reproduction Study 96-4080 Page 5 Draft Final Report Inhalation Report Appendix X chamber airflow was interrupted. The outlet of the solenoid valve was attached to a stainless steel cross union, from which 14" tubing branched to the three generation flowmeters. The test material exited the flowmeters via V" tubing at flow rates of 12.36 mL/min, 128.3 mL/min and 1312 mL/min for Groups II, III and IV respectively, and was directed into the turret of each of the 6m3 exposure chambers, where it mixed with the house supply air. The generation system from the regulator through the flowmeters, was contained within a separate 6m3 glass and stainless steel chamber. This containment chamber was exhausted through the in-house filtering system, which consisted of a charcoal filter, a coarse filter and a HEPA filter. All animals remained in the chamber for a minimum of 30 minutes at the end of each exposure to allow for clearing of the chamber. During this time, the chamber operated at the same airflow rate as during the exposure. Refer to Diagram and equipment list (pages 7-9 of Appendix X) for equipment details. 2.4. EXPOSURE CHAMBER SAMPLING 2.4.1. CHAMBER SAMPLING (ER) Measurements of airborne concentrations of the test material were made using a MIRAN Ambient Air analyzer equipped with a strip chart recorder. The test atmosphere samples were drawn hourly during the exposures through a filter or a Drierite drying tube (Groups I and II only) and then through the MIRANT and measurements were recorded. Samples were drawn through a filter attached to 14" tubing, and into the inlet of the MIRAN. A vacuum pump was used to pull the chamber air through the MIRANT. The pump was exhausted into the exhaust pipe of the 6m3 exposure chamber, via 14" plastic tubing. The exposure levels were determined by comparison of the measured absorbance to a calibrated response curve constructed using the same instrument settings. BFG 003199 Huntingdon Life Sciences Reproduction Study 96-4080 Page 6 Draft Final Report inhalation Report Appendix X Refer to pages 10-15 of Appendix X equipment details. 2.4.2. CHAMBER SAMPLING (GC) GC (gas chromatography) sampling was performed twice during this study on one day per week with approximately two weeks between analysis. GC analyses of the chamber atmospheres were performed along with the IR (Miran infrared spectrophotometer) analyses in each exposure group at each hourly interval. The procedure for sampling is included in Appendix Z. 2.4.3. PARTICLE SIZE DISTRIBUTION ANALYSIS Particle size distribution measurements were performed once weekly from the chambers and room air using a TSI Aerodynamic Particle Sizer. The samples were drawn for 20 seconds at a flowrate of 5 Ipm. A computer was used to program the system to the appropriate settings prior to sampling. The mass median aerodynamic diameter, geometric standard deviation and Total Mass Concentration were calculated by the computer and printed out. 2.4.4. NOMINAL CONCENTRATION To calculate the nominal concentrations (ppm), the flow of test material and air through the chamber was monitored using appropriate calibrated equipment. The test material (liters) consumed during the exposure was then divided by the total volume of air (liters) passing through the chamber [volumetric flow rate (L) X total exposure time (min)] X 106pl/L. BFG 003200 Huntingdon Life Sciences Reproduction Study______ 97-4080 Page 7 Draft Final Report Exposure Generation System Appendix X PresaureSwtch NOTE: The generation system, ercmtnQ the carprcsscd gas vfftda was housed a SnPeapoang chamber. BFG 003201 Huntingdon Life Sciences Reproduction Study______ 96-4080 Page 8 Draft Final Report Equipment List Appendix X Exposure Chamber Haiford 6000 liter glass and stainless steel chamber. Compound Reservoir Compressed gas cylinder (Sponsor supplied Ton cylinder) Flowmeters Gilmont Flowmeter/Micrometer, size micro (range 0-100% of scale), size 11 (range 0250 mL/min), size 12 (range 0-2000 mL/min), Gilmont Industries, Inc. The flowmeters were calibrated prestudy with a Gilibrator (range 1-250 cc), P/N D800287, SN6675-2 with a sensor block P/N D800290 or with a Gilibrator (range 20 cc-6 Lpm), P/N D800286, SN 569-S with a flow cell P/N A800266; Gilian Instrument Corp. Dwyer, 0-20 Lpm. Pressure/Vacuum Gauge(s) Dwyer Magnehelic gauge, 0 - 2 in. and a 0 + 1 in. (center zero) 0-30 in. Hg Gast vacuum gauge Regulator(s) Scott Specialty Gases regulator (equipped with a 0-100 psi inlet backpressure gauge and a 0-100 psi outlet backpressure gauge) MG Industries stainless steel Purge/Vent System Solenoid Valves Allenair *6 electronic solenoid valve Pressure Switch Dwyer Instruments Inc. (ID# 1950-0). Connector Stainless steel cross union. Tubing BFG 003202 Huntingdon Life Sciences Reproduction Study______ 96-4080 Page 9 Draft Final Report Equipment List Appendix X Size 14" plastic (American Scientific Products). Size VS" plastic (Baxter Scientific Products. Size 14" and 14" Teflon. Size Vi" stainless steel. Filters PALL Corp. (HC9020F UP4H) filter PTI Tecnologies (B129327044) filter Vacuum Pumps Thomas Industries Inc., Model 707CM 50. Air Analyzer Wilks, MIRAN 1A Ambient Air Analyzer with a Fisher Recordall Series 5000, Model D5117-SAQ and a Micronta LCD Benchtop Digital Multimeter No. 22-195. Particle Sizer/Analyzer TSI Aerodynamic Particle Sizer, Model 3310A, and a DELL computer (model #A86P125) equipped with an Epson LQ-578+ Dot matrix printer Thermometer and Humidity Gauge Springfield Precision Instruments, Temperature/Humidity gauges calibrated before use with a Fischer Digitial Hygrometer/Thermometer. Chamber Air-flow Gauge Dwyer Magnehelic gauge, 0-2 in. H2O; calibrated prestudy with a Sierra Acumass Flowmeter (model 730-N8-2) with a Sierra Instruments Digital meter (model 831-N2). Chamber Static Pressure Gauge Dwyer Magnehelic gauge, 0-+ 1 in. H2O (center zero); calibrated prestudy with a Dwyer Mark II Manometer (model 25). BFG 003203 Huntingdon Life Sciences Reproduction Study 96-4080 Page 10 Draft Final Report Inhalation Report Appendix X Miran Ambient Air Analyzer Procedure and Methodology Procedure Hourly samples for determination of the levels of exposure to Vinyl Chloride were analyzed for Groups I-IV, using a MIRAN Ambient Air Analyzer equipped with a strip chart recorder and multimeter. The test atmospheres were drawn continuously through a glass fiber filter in a filter holder, and then through 1/4" Teflon tubing to the inlet of the Miran. A vacuum gauge was connected to the outlet of the Miran. The gauge was connected, via 1/4" Teflon tubing, to a flowmeter equipped with a metering valve. A pump was used to pull chamber air through the Miran. When the Mran cell was considered equilibrated, the pump was turned off and the absorbance was read off the multimeter. The absorbances and flowmeter settings were recorded. The pump was exhausted into the in-house filtering system consisting of a coarse and HEPA filters and activated charcoal. The exposure levels were determined by comparison of the measured absorbance to a calibrated response curve (see pages 14 and 15 of Appendix N) constructed using the same instrument settings. Settings. The instrument settings for the unit are summarized below: wavelength, microns pathlength, dial setting slit width, mm range, absorbance response, seconds gain chart speed, cm/min chart volts 11.1 (Groups I, II, III); 10.9 (Group IV) 11.5 (Groups I, II, III); 4.48 (Group IV) 1 0.25A (Groups I, II, III); 1A (Group IV) 1 High 1 1 BFG 003204 Huntingdon Life Sciences Reproduction Study 96-4080 Page 11 Draft Final Report Inhalation Report Appendix X Calibrations. The MIRAN was turned on and allowed to warm up for approximately 20 minutes. The cell was flushed with room air for approximately one minute. The loop (5.64 Liters) was closed, the unit was zeroed and the injection series was performed as shown below. The resultant data was plotted to obtain separate calibration curves for Groups I and II, for Group IH and for Group IV. Groups I, II and HI: Iniection Volume (HL) 28 56 140 280 560 850 Calculated Concentration* (ppm) 5.0a 9.9a 25"'b 50a'b 99b IS lb ABSORBANCE Observer I Observer 2 Average 0.0313 0.0600 0.2160 0.350 0.599 0.833 0.0321 0.0610 0.2265 0.357 0.645 0.923 0.0317 0.0605 0.2213 0.354 0.622 0.878 Group IV: ABSORBANCE Iniection Volume Calculated Concentration* Observer 1 Observer 2 Average (HL) (ppm) 560 99 0.0680 0.0666 0.0673 2800 496 0.312 0.306 0.309 4500 798 0.472 0.464 0.468 6200 1099 0.626 0.612 0.619 7500 1330 0.730 0.731 0.731 "ppm = Volume of Vinyl Chloride(jjL) / Volume of Air (L) * These concentrations were used to prepare the calibration curve for Groups I and II. b These concentrations were used to prepare the calibration curve for Group III. BFG 003205 Huntingdon Life Sciences Reproduction Study 96-4080 Page 12 Draft Final Report Inhalation Report Appendix X Calibration Checks. A three-point calibration check of the MTRAN* was performed for each trial/exposure day prior to sampling the chambers as shown below: INJECTION VOLUME (ML) 56 560 6200 CALCULATED CONCENTRATION (ppm) 9.9 99 1099 EXPECTED ABSORBANCE READING (v) 0.0605 0.622 0.619 ACCEPTABLE ABSORBANCE RANGE (v) 0.0514-0.0696 0.529- 0.715 0.526-0.712 Injections were made with a 100 \XL Precision Sampling Corp. syringe, a 1000 pL Hamilton syringe or a 10 mL Hamilton syringe (model 1001 and 1010). The absorbance was recorded after each injection. The absorbance must be within 15% of the original calibrations series. If any of the absorbance values fell outside the 15% range, the injection was rechecked as follows: the volume for the value that was out of range was reinjected twice. The two closer pair of the three injections were averaged and the results compared with the original curve. If the value of the average was outside the 15% range, the Study Director or Inhalation Toxicologist decided if a new graph was to be prepared. Significant Figures. Sample concentrations and daily means were reported to two significant figures. bfg 003206 Huntingdon Life Sciences Reproduction Study 96-4080 Inhalation Report Miran Ambient Analyzer Setup Page 13 Draft Final Report Appendix X Prom chamber 1 Strip Chart Recorder BFG 003207 Huntingdon Life Sciences Reproduction Study 96-4080 Inhalation Report Calibration Curve - Groups I and II 40.0 -r 35.0 30.0 Faa 25.0 0 20.0 e V 15.0 S V 10.0 -295.82x* + 178.4x R1 - 0.9989 5.0 - 0.0 0.0000 Calibration Curve - Group III Page 14 Draft Final Report Appendix X BFG 003208 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 15 Draft Final Report Inhalation Report Calibration Curve - Group IV Appendix X 1400 1200 - - y - -301.17x4 + 133.59x3 + 616.48x2 + 1415.5x R2 0.9997 1000 - Eaa eo 800 - oceuco 600 400 -- Coefficients 200 - 0.0000 0.1000 0.2000 0.3000 0.4000 0.5000 0.6000 0.7000 0.8000 Absorbance (Volts) BFG 003209 Huntingdon Life Sciences Reproduction Study 96-4080 Page 16 Draft Final Report Inhalation Report Appendix X GROUPn 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 GROUPm 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec % 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 GROUP IV 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec % 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 23 Dec 96 SUMMARY OF DISTRIBUTION TRIAL SAMPLES ANALYTICAL (JR) RATIO SAMPLE PORT CONCENTRATION DISTRIBUTION PATENUMBERLD.(PPM)SAMPLE/H-1 223 H-l 223 H-4 223 H-6 223 H-7 224 H-l 224 H-9 224 H-I2 224 H-14 225 H-l 225 H-15 225 H-17 10 11 1.10 10 1.00 11 1.10 11 11 1.00 11 1.00 11 1.00 11 10 0.91 11 1.00 322 H-l 322 H-4 322 H-6 323 H-l 323 H-12 323 H-14 324 H-l 324 H-15 324 H-17 325 H-l 325 H-7 325 H-9 100 110 1.10 100 1.00 100 100 1.00 100 1.00 100 97 0.97 95 0.97 100 100 1.00 100 1.00 422 H-l 422 H-4 422 H-6 423 H-l 423 H-12 423 H-14 423 H-7 424 H-l 424 H-9 424 H-5 425 H-l 425 H-17 1100 1100 1100 1100 1100 1100 1100 1100 1100 1200 1100 1100 - 1.00 1.00 - 1.00 1.00 1.00 - 1.00 1.09 - 1.00 003210 Huntingdon Life Sciences Reproduction Study 97-4080 Page 17 Draft Final Report Cumulative Exposure Records Preface Appendix X Footnotes: Bold values indicate GC confirmation of IR sample. bDue to equipment problems, GC sample was not taken. c Sample taken before a leak in the sample line or a fitting was repaired. dDue to equipment problems, Miran sample was not taken. "Due to elevated chamber humidity, a valid Miran sample could not be taken. fDue to equipment problems, accurate temperature readings could not be taken. g A second exposure (4-hours) was run on this date to expose animals that were erroneously not loaded in the morning. h Sample not taken due to technician error. `Mean and SD of all individual IR samples. JMean and SD of all individual GC samples. <LOQ = Less than the limits of quantification. BFG 003211 Huntingdon Life Sciences Reproduction Study 96-4080 Page 18 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 2 3 4 Date 7-Jan-97 8-Jan-97 9-Jan-97 10-Jan-97 13-Jan-97 14-Jan-97 15-Jan-97 16-Jan-97 17-Jan-97 20-Jan-97 21-Jan-97 22-Jan-97 23-Jan-97 24-Jan-97 27-Jan-97 28-Jan-97 29-Jan-97 30-Jan-97 31-Jan-97 3-Feb-97 Exposure Number Mean (ppm) 1 0.0 2 0.0 3 00/0.90 4 0.0 5 0.0 6 0.0 7 0.0 8 0.0 9 0.0/0.099 10 0.0 11 0.0 12 0.0 13 o.o/o.o 14 00 15 0.0 16 0.0 17 0.0 18 0.0/0.0 19 0.0 20 0.0 0.0 0.0 0.0/1.2 0.0 0.0 0.0 0.0 0.0 0.0/0.593' 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 Miran (IR)' Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0/1.2 0.0 b 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o 0.0 0.0 o.o/o.o* 0.0 0.0 0.0 o.o/o.o' 0.0 0.0 0.0 00/0.0' 0.0 0.0 0.0 0.0 0.0 O.O/O.O 0.0 0.0 0.0 o.o/o.o 0.0 0.0 d 0 0/0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0/1.2 0.0 0.0 0.0 0.0 00 o.o/o.o 0.0 0.0 d o.o/o.o 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 d o.o/o.o 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m3) 3.114 1.714 5.41B-04 1.812 2.271 1.29E-03 3.798 2.192 2.00E-03 7.101 2.014 1.19E-03 Chamber Environment Mean Temoerature Humiditv (C) 22 22 23 22 23 (%) 41 39 42 49 48 22 41 22 40 23 53 22 42 22 39 22 38 23 40 23 42 22 34 22 34 22 45 21 34 20 32 20 37 21 40 003212 Huntingdon Life Sciences Reproduction Study 96-4080 Page 19 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 5 6 7 a Date 4-Feb-97 5-Feb-97 6-Feb-97 7-Feb-97 10-Feb-97 11-Feb-97 12-Feb-97 13-Feb-97 14-Feb-97 17-Feb-97 18-Feb-97 19-Feb-97 20-Feb-97 21-Feb-97 24-Feb-97 25-Feb-97 26-Feb-97 27-Feb-97 28-Feb-97 3-Mar-97 Exposure Number 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 Mean (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 Mlran (IR)* Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 o.o/o.o 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m3) 6.641 2.072 3.42E-04 2.851 2.128 2.58E-03 2.843 1.878 1.37E-03 0.9951 1.945 4.46E-03 Chamber Environment Mean Temoerature Humidity CC) (%) 21 39 20 39 22 39 22 41 21 41 21 42 21 35 21 33 20 47 21 40 21 41 22 39 22 40 22 47 22 39 22 41 22 46 25 62 23 50 21 48 BFG 003213 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 20 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitorinq Results Appendix X Week 9 to II 12 Date 4-Mar-97 5-Mar-97 6-Mar-97 7-Mar-97 IO-Mar-97 11-Mar-97 !2-Mar-97 13-Mar-97 M-Mar-97 17-Mar-97 18-Mar-97 19-Mar-97 20-Mar-97 21-Mar-97 22-Mar-97 2 3-Mar-97 24-Mar-97 25-Mar-97 26-Mar-97 27-Mar-97 28-Mar-97 29-Mar-97 30-Mar-97 31-Mar-97 Exposure Number 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 Mean (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 Miran <IR)a Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 o.o/o.o 0.0 e 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o e 0.0 0.0 0.0 e 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o e 0.0 0.0 0.0 e 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 e 0.0 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m3) 0.9153 1.314 9.97E-03 1.740 1.847 1.81E-03 1.218 1.509 2.40E-03 1.748 1.922 1.89E-03 Chamber Environment Mean Temoerature Humidity CC) 21 (%) 49 21 50 21 54 21 39 20 53 19 54 19 51 19 46 19 54 19 51 19 52 20 55 20 58 20 57 20 61 16 50 21 48 22 46 21 51 21 51 21 47 21 53 21 49 20 64 BFG 003214 Huntingdon Life Sciences Reproduction Study 96-4080 Page 21 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 13 14 15 Date 1-Apr-97 2-Apr-97 3-Apr-97 4-Apr-97 5-Apr-97 6-Apr-97 7-Apr-97 8-Apr-97 9-Apr-97 10-Apr-97 11 -Apr-97 12-Apr-97 13-Apr-97 14-Apr-97 15-Apr-97 16-Apr-97 l7-Apr-97 18-Apr-97 19-Apr-97 20-Apr-97 21-Apr-97 Exposure Number 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 Mean (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0,0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 <LOQ 0.0 Miran (UR)" Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0 0/0.0 0,0 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 Particle Size Determinations MMAD OSD TMC (pm) (mg/m3) 2.633 1.794 3.96E-03 1.257 1.365 5.28E-04 2.025 2.16) 2.45E-03 Chamber Environment Mean TemnerBture Humiditv CC) (%) 20 54 18 49 20 53 19 55 19 55 19 58 22 63 22 54 21 48 21 52 20 48 20 54 20 62 20 36 20 42 22 44 21 46 20 44 20 43 21 43 22 42 BFG 003215 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 22 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 16 17 18 Date 22-Apr-97 23-Apr-97 24-Apr-97 25-Apr-97 26-Apr-97 27-Apr-97 28-Apr-97 29-Apr-97 30-Apr-97 1-May-97 2-May-97 3-May-97 4-May-97 5-May-97 6-May-97 7-May-97 8-May-97 9-May-97 lO-May-97 11-May-97 12-May-97 Exposure Number 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103 104 105 106 Mean (ppm) 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0/0.0 00 0.0 0,0 0.0 0.0 0.0 o.o/o.o 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 Mlran (IR)* Individual (ppm) 0.0 0.0 0.0 0.0 o.o/o.o 00/<LOQ 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 00 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m5) 0.769 1.710 7.48E-03 1.175 2.57 1.73E-03 8.335 1.59 5.67E-03 Chamber Environment Mean Temperplpre Humiditv CC) (%) 22 46 20 46 20 45 21 44 20 40 21 36 24 54 22 42 22 54 25 50 22 38 25 55 23 43 20 37 21 44 19 36 19 42 19 51 21 55 22 46 21 50 BFG 003216 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 23 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 19 20 21 22 Date 13-May-97 M-May-97 15-Mav-97 16-May-97 17-May-97 18-May-97 ] 9-May-97 20-May-97 21-May-97 22-May-97 23-May-97 26-May-97 27-May-97 28-May-97 29-May-97 30-May-97 2-Jun-97 3-Jun-97 4-Jun-97 5-Jun-97 6-Juii-97 9-Jun-97 Exposure Number 107 108 109 no 1)1 112 113 114 115 116 117 120 121 122 123 124 125 126 127 128 129 130 Mean (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 O.O/O.O 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.Q 0.0 0.0 0.0 0.0 Mfran (!R)" Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m3) 1.278 2.58 2.63E-03 1.949 2.74 1.81E-03 2.058 2.53 1.36E-03 1.796 2.34 1.39E-03 Chamber Environment Mean Temperature Humiditv (C) <%) 20 54 19 58 19 55 21 50 19 57 21 51 20 62 19 62 18 55 19 49 20 52 f 63 20 49 20 47 20 47 20 56 22 62 22 58 22 54 22 52 21 59 22 53 BFG 003217 Huntingdon Life Sciences Reproduction Study 96-4080 Page 24 Draft Hngl Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 23 24 25 26 Date 10-Jun-97 1 l-Jun-97 12-Jun-97 13-Jun-97 16-Jun-97 17-Jun-97 l S-Jun-97 19-Jun-97 20-Jun-97 23-Jun-97 24-Jun-97 25-Jun-97 26-Jun-97 27-Jun-97 30-Jun-97 l-Jul-97 2-Jul-97 3-Jul-97 4-Jul-97 7-Jul-97 Exposure Number 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 150 Mean (ppm) 0.0 0.0 0.0 0,0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0,0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 Mi ran (IR)" Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0,0 0.0 0.0 0.0 0.0 0.0/0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 Particle Size Determinations MMAD OSD TMC (pm) (mg/m5) 1.100 2.01 1.52E-03 0.990 1.62 8.00E-03 0.665 1.32 5.22E-03 1,513 2.41 2.93E-03 Chamber Environment Mean Temperature (C) 22 Humidity (%) 55 24 54 22 58 21 58 22 51 21 58 22 56 22 60 22 57 23 60 23 63 23 66 23 68 22 65 23 63 24 63 24 67 23 67 23 65 23 64 bFG 003218 LO x X T3 C CL a. < o </) 8i a a 3C oCO V> w oo o a. .ts I CD ^i 05 s ~ '5 . 11 ou a o c w"o I c .2 -g U 05 |1 3 X cd a Q. O a. 3 OW o os oso t-- s<5 c-- OWN' IsNn fWsN i/NC IsNo Tso 7sO wi \0 ^ in 3m sr i-**. in -- cs -- f| -- -- <N in v n pi in in n IN N fS N IN N IN N (N N M N IN N IN N N IN IN M IN IN sa OsO' ? W I*NT qrIN 'T o 5 d d d d d 5 O odd d d d d o' d S 5 d d d d 5 d ddd dd d d d d dd 5 odd d d d d d i * 5 e dddod d d d d d d d d d c w--\ Ii/N*> mI'Ni urnf mmii ici r- moo vOi' ic r oo -- c r* f~ a r. t* Os rs r- r t" Os r*> pOs- tO**s r> t 3 3333 3 3 3 3 3 3 3 3 oo oo ao e 3 3 3= -- mi sc r~ OfNs m --C*N <:-<:< - IN Pi N V r in 00 IN m BFG 003219 Mean Humiditv (% ) 21 22 22 21 22 22 21 21 21 21 21 21 20 22 23 62 23 54 23 66 23 69 21 65 23 65 23 64 23 73 P article Size D e te rm in a tio n s MMAD GSD (pm) 1.488 1,74 9.70E-04 I 0.823 2.40 i 8S g, g'oc ^ <0 c S3 O x x TD C CL Q. < s Ea >o \n 'O ov co- t*~ fpi- e'Oo Voi >o N9O o frS- Or-- to*t B? bd Akw E xQll oW U |f H J, g J3 JS JS 0*0 00 00 00 0 0 /0 0 00 00 00 00 00 00 00 00 00 00 0*0 00 00 00 0*0/00 00 00 00 00 00 00 00 00 00 00 *o to oo o I? oCO CO CoO wo LoxU. .cOti ii03 .it sco ^ s oo S Individual (ppm) 00 00 0*0 0 0 0*0 0*0 0*0 0*0 0*0 0 0 0*0 0*0 00 00 0*0 0*0 00 0*0 0*0 0*0 00 00 O'O 0*0/00 0*0 00 00 00 00 00 00 00 00 00 00 0*0 0*0 0*0 00 0*0 0*0 0*0 0*0 0*0 00 0*0/00 0*0 0*0 00 00 00 00 00 00 00 00 00 00 0*0 00 00 00 00 00 0*0 00 00 0*0/00 0*0 00 00 00 00 00 00 00 00 00 00 00 0*0 0*0 00 0*0 0*0 00 00 0*0 00 0*0/00 0*0 00 00 00 00 00 00 00 00 00 Mean (ppm) I ! ! | 0*0 0*0 00 0*0/00 0*0 0*0 0*0 00 00 00 00 00 00 00 V) oc `3 to ^ C0| '-I c co .2* o y g-i S 2 cc 3 X cn E QOl. O Q. 3O 5 a ti 567891011- Exposure Number Aug-97 173 Aug-97 174 Aug-97 175 Aug-97 176 Aug-97 177 Aug-97 178 Aug-97 179 ooooooo o' 0000009 187 187 188 189 190 191 192 193 OOC - 9rs9 mOS 90 u90r oW CP* rO*n rO-n r^- fO*n ^ e^tr-r-r-r-r-r- ftfl 3 MQ S3 QA 3 Q3j Q9A BA 3 Q3f daosBn'eao&soosoesfi&sOBsO <<: <:<:<: <f Nw^ Is oc S'a,o-Nw?m rs m BFG 003220 Huntingdon Life Sciences Reproduction Study 96-4080 Page 27 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 34 35 36 Date 26-Aug-97 27-Aug-97 28-Aug-97 29-Aug-97 30-Aug-97 31 -Aug-97 1-Sep-97 2-Sep-97 3-Sep-97 4-Sep-97 5-Sep-97 6-Sep-97 7-Sep-97 8-Sep-97 9-Sep-97 10-Sep-97 11-Sep-97 12-Sep-97 13-Sep-97 14-Sep-97 15-Sep-97 Exposure Number 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 2)1 212 213 214 Mean (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mi ran (IR)" Individual (ppm) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0,0 0,0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 o.o/o.o 0.0 0.0 0.0 0,0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Particle Size Determinations MMAD GSD TMC (pm) (mg/m3) 1.363 2.47 6.17E-03 3.302 3.21 1.22E-03 0.821 1.33 6.78E-03 Chamber Environment Mean TemDerature Humidity (C) (%) 24 73 24 74 24 79 24 72 23 71 23 74 23 79 22 74 22 62 22 58 22 60 22 65 23 67 24 69 24 71 24 68 25 76 24 71 23 67 23 63 24 61 BFG 003221 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 28 Draft Final Report Group 1 - 0 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 37 38 39 Dale 16-Scp-97 17-Scp-97 18-Sep-97 19-Sep-97 20-Sep-97 21-Sep-97 22-Sep-97 23-Sep-97 24-Sep-97 25-Sep-97 26-Sep-97 27-Sep-97 28-Sep-97 29-Sep-97 30-Sep-97 1-Oct-97 2-Oct-97 3-Oct-97 Eiposure Number 218 219 220 221 222 223 224 225 226 227 228 229 230 231 232 233 234 235 Mean (ppm) 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0,0 0,0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Mlran <IR)* Individual (ppm) 0.0 0.0 0.0/0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0/0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 00/0.0 0.0 0,0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 Panicle Size Determinations MMAD GSD TMC (pm) (mg/m3) 1.014 3.81 2.01E-03 1.573 1.90 6.13E-04 1.605 1.77 4.85E-04 Chamber Environment Mean Temnerature Humidity CC) 23 23 23 24 <*) 59 62 64 64 24 69 24 50 21 47 21 54 20 50 20 48 21 55 20 49 21 55 23 66 22 58 20 56 20 49 25 48 BFG 003222 Mean: SD: 0.00 1 0.00 0.036 0.197 2.1 2.0 4.6E-03 1.8 - 7.7E-03 22 1.6 55 11 Huntingdon Life Sciences Reproduction Study 96-4080 Page 29 Draft finaL Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitoring Results Week 1 2 3 4 Date 7-Jan-97 8-Jan-97 9-Jan-97 10-Jan-97 13-Jan-97 14-Jan-97 15-Jan-97 16-ian-97 17-Jan-97 20*Jan*97 21-Jan-97 22-Jan-97 23-Jan-97 24-Jan-97 27-Jan-97 28-Jan-97 29-Jan-97 30-Jan-97 31-Jan-97 3*Feb-97 Exposure Number Nominal (ppm) 1 9.8 2 9.8 3 9.8 4 9.8 5 9.8 6 9.8 7 9.8 8 9.8 9 9.4 10 9.8 11 9.7 12 9.8 13 98 14 9.8 15 9.8 16 9.8 17 9.8 18 9.8 19 9.8 20 9.8 Mean (ppm) 10 97 9.5/14 10 10 9.7 10 10 9.5/7.6 10 12 12 11/14 11 10 11 11 11/12 11 11 Chamber Concentration 11 9.2 9.4 b 9.3 10 9.3 11 9.6 7.2/0.95* 11 12 10 12/14 11 8.8 10 11 11/11 11 9.6 Mlran (IR)a Individual (ppm) 11 11 9.9 9.8 9.7 11 9.3/14 9.2/13 9.7/14 9.9 9.4 11 10 10 10 9.9 10 10 9.9 10 10 11 10 10 8.0/2.7* 11/2.9* 11/13 11 9.7 10 11 12 10 14 11 d 11/14 11/14 11/13 11 11 11 11 11 10 11 11 11 11 11 10 12/13 11/13 11/13 11 11 11 12 n II 9.1 9.0 10/13 II 10 9.6 10 10 10/12 10 13 d 11/13 11 11 H 10 11/10 11 11 Appendix X 8.2 9.4 9,2/14 10 11 9.6 10 10 10/14 11 12 d 11/13 11 11 n 10 10/12 u li Particle Size Chamber Environment Determinations MMAD OSD TMC (pm) (mg/m3) 1.755 1.887 2.21E-04 2.152 2.555 1.29E-03 1.654 2.049 1.31E-03 Mean Temperature Humidity TO (%) 21 42 22 42 22 42 22 42 22 42 22 42 22 42 22 42 22 42 22 33 24 33 22 41 25 42 25 35 24 36 1.616 1.647 1.72E-04 24 25 24 27 25 45 35 35 29 38 BFG 003223 2co toili S'* c 00 Q X x 'c$ o. Q. < O CoO I CO o> U0O5) c u w >o coj cOo ' g-Oj -a 3 CD X AC Cl o Cl 3 O 11 41 10 38 12/1 32 1 2 44 11 35 12 10 1 2 /1 11 11 *s 2 w H 2 ?! c>i ^ v~i n T V 2X sm fit! 2 5~ vi in ri X ^w w^ <s \o m in ^ <T o y-i o ^^ *T vs ao VS Vs g (N N N M (S N N <S N N N M N M N N N c oil OH _ y -`g& A g Vi Ji J5 a 2 E 2 z. B i 0. g l/*l O OJ o >0 -- oo o -- f*S 99 W F gj r oo <*4 -- ^6 rs r~- cn r O 00 -- -- ri r- rm <N SO o -- ci -- W1 f> -- -- -- o o -- ^ <S -- o -- o -- -- -- o c; -- <s T <s -- -- o -- -- <s -- N O ? N N nM -- -- -- -- c-o 0 -- 0 -- 0 - is C N s- "" 6 t: : a 'Is 2 *n OO -- O -- O - C N N -- -- o -- -- r* -- -- -- <-n 8 --- . s u It 01 U Z\ 01 4* T r*> js 2 Z Z Z Z a .e u T -- C* <-* O O o -- c: -- ^ -- o -- ^ N ---- -- . 3 --~^O 2: 3 * O - C N - -- -- o -- o CN -- -- -^ rS ---- | oo go oo oo oc 90 00 00 00 00 00 ooo lS O'* O' O' O' Ov s O' O' O' O' fl\ Oi " - 2 9 * L. 4> -C & M &a Z Q .9 8 * - n w <r ^ s oo o' o " N m v m so r** oo Os o (N <S (S fS (N fN IN (N N n n tn t*> r~> r- r- r- r- r- r- r~ r- r- f" r- r~ r- r- r- ffi ffi o\ o< ^ J> A J> J> -6 JL J> -i JL A M J> Ji M Ji J> J> i t* Cl. U. Uh U. Urn b. u. u. u. u. u, h. b. u. ^ v o r* -- <N fn rr r* oo -- rr O C* 06 ` mMMNM r- 00 BFG 003224 Huntingdon Life Sciences Reproduction Study 96-4080 Page 31 Draft Final Report Group II - 10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 9 10 11 12 Date 4-Mar-97 5-Mar-97 6-Mar-97 7-Mar-97 10'Mar-97 11 -Mar-97 12-Mot-97 13-Mar-97 14-Mar-97 17-Mar-97 18-Mar-97 19-Mar-97 20-Mar-97 21-Mar-97 22-Mar-97 23-Mar-97 24-Mar-97 25-Mar-97 26-Mar-97 27-Mar-97 28-Mar-97 29-Mar-97 30-Mar-97 31-Mar-97 Exposure Number Nominal (ppm) 41 10 42 10 43 10 44 9.8 45 9.8 46 9.8 47 9.8 48 9.8 49 9.8 50 9.8 51 9.8 52 9.8 53 9.8 54 9.8 55 9.8 56 9.8 57 9.8 58 9.8 59 9.8 60 9.8 61 9.1 62 8.1 63 7.9 64 8.1 Mean (ppm) 12 12 11 11 11 11 11 11/9.1 11 9.7 10 10 10 (0 10 11 11 12 12 11/10 12 11 9.1 II 12 14 10 11 10 10 10 13/9.1 10 9.1 10 to 8.2 10 II 10 10 n 12 11/9.7 11 14 8.7 12 Chamber Concentration 12 12 11 11 11 11 10 13/8,8 11 9.9 10 10 10 9.9 10 11 8.8 12 12 11/11 12 II 8.9 12 Mi ran (lR)a Individual (ppm) 12 12 12 12 11 11 11 II 12 12 11 11 11 II 12/9.2 98/8.6 10 10 10 9.9 10 10 10 10 10 It 10 10 10 10 11 11 10 12 12 12 12 12 11/9.7 12/11 12 13 10 10 9.1 9.2 11 10 12 12 11 11 11 11 II 9.6/9.1 10 9.4 10 9.9 11 10 10 11 12 12 13 12/11 11 10 8.9 10 13 12 11 11 11 11 12 10/9.7 12 10 10 10 10 11 10 11 13 12 13 11/10 11 9.3 9.5 11 Particle Slie Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m5) 0.9201 1.428 9.9 IE-03 1.429 1.622 1.28E-03 1.334 1.527 2.52E-03 16.95 2.588 7.27E-03 Mean (C) 25 25 25 24 24 25 25 25 25 25 25 24 24 24 25 25 23 22 20 21 22 21 21 20 (%) 51 55 45 43 60 56 54 38 41 35 39 40 44 40 46 36 34 60 44 35 38 44 44 54 BFG 003225 BFG 003226 l cc 3X iOL. < SMea U t- t^-- r^- r* r** ^r~ ^ra tbl tba. tbL. *&1. &ll kaL <.<,<<.<.<.< - N if 1^1 ^ Is -J c c3 o o ll aa. o 3a. o coan ca> 2 V> Week Date ; 8-Apr-97 1 9-Apr-97 10-Apr-97 -- <N V o e* 00 -- 1!. C<L. bu <. < <: < <; k kk k <: <; <. < il CL 1Q!. . iOi. il CL r*' rC-ft r-~ rO-* rO-' r-s r- r- Number Nominal (ppm) 65 8.8 66 8.7 67 9.2 68 9.2 69 9.2 70 9.2 71 1 9.2 72 9.2 73 9.2 74 9.2 75 1 9.2 76 | 8.2 77 1 7.8 78 9.2 79 1 9.2 80 I 9.2 81 92 82 9.2 83 9.2 84 8.5 85 10 -- -- O O -- fN <N 0 C-* 0 0 0 -- Mean (ppm) 12 11 12/12 11 II 9.3 ll 1 11 1 11 l 11/11 1 1! 10 1 9.9 9.9 11 11 12 _^ _ fi <s 0 -- 0 --* JR W NO-O-O- Ahw. > '55iij= &IS uc 2 5 8se U eC IS = ew Xc UJ Q <1o o> g f3 3 C_ OC a. O 00 0 (N (S (N " - a 0 - in m 12 11 12/12 11 9.6 12 (0 10 II 11 12 11 I 12/12 12 11 8.0 i 11 12 to 9.8 10 10 11 12 -- -- --. Q> ^ Os *+{ 11 10 12 to 9.6 10 11 12 11 12/12 11 11 9.3 11 -- -- 0 0 0 -- <-* 11 9.9 12 10 10 10 10 12 12 12/12 11 9.7 9.4 11 2 c tc 1i a-V5) TO i0s Zl 01 01 01 0E II II * a. l <S I5 o^ S St t/1 X X `S ca> o. Cl < OSD 12 10 12 10 9.2 9.7 10 II 11 12/12 11 11 9.7 12 I2.57E-03 2.643 1.837 1 1 1 1 | 1.259 1.499 5.91E-04 1.116 1.445 1.21E-03 20 18 19 20 19 20 22 21 20 20 21 21 22 20 21 21 21 21 21 22 21 o 51 48 50 1 50 51 54 54 c m Bd .b4sA< 2 31 Sj Q s Q c-*-T> 5sT 0f*0N Nn 90 (V*1 Sf'O-. r4 S O^O O' O O 5 5 a4 Se Huntingdon Life Sciences Reproduction Siudv-------- 96-4080 Page 33 Draft Final Report Group II - 10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 16 17 18 Date 22-Apr-97 23-Apr-97 24-Apr-97 25-Apr-97 26-Apr-97 27-Apr-97 28-Apr-97 29-Apr-97 30-Apr-97 1-May-97 2-May-97 3-May-97 4-May-97 5-May-97 6-May-97 7-May-97 8-May-97 9-May-97 IO-May-97 11-May-97 12-May-97 Exposure Number Nominal (ppm) 86 9.8 87 9.8 88 9.6 89 9.6 90 10 91 10 92 9.5 93 9.8 94 9.6 95 9.5 96 9.5 97 9.5 98 9.5 99 9.5 100 9.6 101 9.1 102 9.1 103 9.4 104 10 105 10 106 9.1 Mean (ppm) 12 11 12/10 12 II 9.9 12 11 11 11 11 11 11 10 12 10 11/12 11 11 11 11 11 II I2/II 11 11 10 12 11 11 13 11 11 11 11 12 10 11/12 11 11 11 11 Chamber Concentration 12 12 12/11 12 11 9.7 13 II 11 11 12 12 12 10 12 11 10/12 12 11 10 12 Miran (IK) Individual (ppm) 12 12 11 11 12/11 11/9.4 12 12 11 12 10 9,6 13 12 n 10 10 11 ii II u 10 n 12 12 9.8 10 10 12 12 10 10 10/U 11/12 12 11 10 11 11 I! 11 10 II 11 11/9.4 12 11 10 11 10 U 11 It 11 11 11 11 10 11/12 II 11 10 11 II II 11/9.9 II 12 10 II 10 11 11 10 11 11 10 It 10 11/12 11 12 10 11 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 0.775 1.710 7.88E-03 Mean Temperature Humiditv m <%) 22 43 20 42 20 41 20 41 20 40 20 45 22 59 1.241 2.12 2.07E-03 1.862 2.75 8.26E-04 23 23 24 23 24 23 21 20 20 20 20 21 21 22 43 44 49 35 53 42 34 49 30 32 48 43 40 42 B FG 003227 Huntingdon Life Sciences Reproduction Study 96-4080 Page 34 Draft Final Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week Date Exposure Number Nominal (ppm) 19 l3-Mav-97 107 9.1 !4-May-97 15-May-97 108 109 8.8 8.7 !6-May-97 no 9.1 17-Mav-97 111 9.5 l8-May-97 112 9.5 19-May-97 113 9,1 20 20-May-97 114 9.1 21-May-97 115 9.1 22-May-97 116 8.8 23-May-97 117 8.5 26-May-97 118 8.9 21 27-May-97 119 8.5 28-May-97 120 8.5 29-Mav-97 121 8.5 30-May-97 122 8.5 2-Jun-97 123 8.5 22 3-Jun-97 124 8.5 4-Jun-97 125 8.5 5-Jun-97 126 8.5 6-Jun-97 127 8.5 9-Jun-97 128 8.5 Mean (ppm) 11 11 12 11 11 10 11 11 11 12/11 11 11 11 10 9.8 I! 11 12/10 to 10 10 11 11 12 11 12 n u n 10 ii 11/12 10 9.7 10 10 9.5 10 11 12/10 10 10 10 11 Chamber Concentration 11 11 12 11 10 10 11 II II 12/12 II II 11 11 10 It 10 12/9.8 10 10 11 11 Miran (IR) Individual (ppm) 12 II 11 12 11 12 11 11 10 11 10 8.0 12 11 11 10 11 12 12/12 11/10 11 10 11 11 II 10 10 10 10 10 II 11 II 12 12/11 10 M/9.4 10 10 10 10 9.4 12 11 II 11 12 11 10 11 12 11 M 11/11 11 12 11 10 10 It 11 12/9.6 9.7 to 10 12 II 11 12 10 11 9.9 11 10 11 12/11 10 12 10 10 9.3 10 11 12/10 10 10 10 II Particle She Chamber Environment Determinations MMAD OSD TMC (pm) (mg/m3) 11.024 5.27 7.38E-03 Mean Temperature Humidity CC) (%) 22 43 21 45 20 47 22 39 22 40 22 38 23 54 1.397 1.83 4.17E-04 20 21 20 21 f 54 40 37 39 56 1.458 1.84 8.12E-04 21 21 20 20 21 43 48 47 54 61 1.250 2.01 8.61E-04 21 21 20 19 21 55 46 49 50 55 BFG 003228 Huntingdon Life Sciences Reproduction Study 96-4080 Page 35 Draft Final Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 23 24 25 26 Date IO-Jun-97 11 -Jun-97 12-Jun-97 H-Jun-97 !6-Jun-97 17-Jun-97 18-Jun-97 19-Jun-97 20-Jun-97 23-Jun-97 24-Jun-97 25-Jun-97 26-Jun-97 27-Jun-97 30-Jun-97 l-Jul-97 2-Jul-97 3-Jul-97 4-Jul-97 7-Jul-97 Exposure Number Nominal (ppm) 129 8.5 130 8.5 131 8.5 132 8.5 133 8.5 134 8.5 135 8.5 136 8.5 137 8.5 138 8 5 139 8.5 140 8.5 141 8.5 142 8.5 143 8.5 144 8.5 145 8.5 146 8.5 147 8.9 148 8.5 Mean (ppm) 12 10 10 10 11 12/11 11 10 11 10 10 9.7 10 9.9 9.7 10 10/11 11 9.8 10 10 10 10 10 10 11/10 10 12 11 10 10 9.8 9.8 9.7 8.6 10 10/10 10 9.7 8.9 Chamber Concentration Miran (IR)1 Individual (ppm) 12 12 12 11 10 10 11 11 10 11 10 10 11 11 II 11/9.9 II 10 II 10 ll/ll 11 9.7 10 10 12/11 11 10 11 9.9 II 10 10 10 10 10 10 10 10 10 9.9 10 10 10 10 10 11/11 11 10 10 10 10/11 10 9.2 10 11 11/11 10 to 10 ]] 10 10 10 II 12/11 II 10 11 11 10 8.2 10 10 10 10 10/10 11 10 10 12 10 10 11 10 12/11 II 10 11 10 10 10 10 9.5 9.7 10 10/12 11 10 11 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m5) 1.089 2.16 I.60E-03 1.028 1.67 9.70E-03 0.668 1.34 5.51E-03 1.227 1.74 1.09E-03 Mean Temperature Humiditv (C) (%) 21 54 23 52 21 56 21 56 21 50 20 56 21 56 2) 60 21 56 22 56 22 61 22 64 23 67 21 62 22 60 23 60 22 64 21 75 21 60 22 60 BFG 003229 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 36 Draft Final Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitorina Results Appendix X Week 27 28 29 30 Date 8-Ju)-97 9-Jul-97 10-Jul-97 ll-Jul-97 14-Jul-97 15-Jul-97 16-Jul-97 17-Jul-97 18-Jul-97 2I-M-97 22-Jul-97 23-JuI-97 24-Jul-97 25-Jul-97 28-Jul-97 29-JuI-97 30-Jul-97 3!-Jul-97 1-Aug-97 2-Aug-97 3-Aug-97 4-Aug-97 Exposure Number Nominal (ppm) 149 8.5 150 8.9 151 8.9 152 8.9 153 8.9 154 8.9 155 8.9 156 8.9 157 8.9 158 8.9 159 8.9 160 8.9 161 8.9 162 8.9 163 8.9 164 8.5 165 8.5 166 8.5 167 8.5 168 8.9 169 8.9 170 8.9 Mean (ppm) 10 11 10 10 9.8 10 10/8.9 9.9 10 9.8 10 to 10 10 9.6 10 10 9.8 98/9.9 9.9 9.7 10 10 10 11 10 80 10 10/8.4 9.6 9.6 8.6 10 9.6 10 8.8 8.8 10 10 10 9.7/10 8.4 8.5 10 Chamber Concentration Miran (>* Individual (ppm) 10 10 10 11 11 11 11 10 10 10 10 II 11 10 10 10 10 10 10/8.9 10/9.6 10/8.7 10 10 9.7 10 10 10 10 10 10 10 10 10 II 10 10 10 10 10 10 10 11 9.5 9.4 10 10 9.9 10 10 10 10 10 10 10 96/9.7 10/10 10/10 11 10 10 9.5 10 10 10 10 10 II 11 10 11 10 11 10/9.3 10 11 10 10 10 10 10 9.7 9.8 10 9.4 10/10 10 10 10 10 10 10 10 10 10 9.8/8.4 10 10 10 10 10 9.8 10 10 10 10 9.3 9.6Z9.5 10 10 10 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 0.718 1.22 1.61E-02 Mean TgmEsrehgs Humidity ro (%) 25 67 26 68 23 68 25 63 26 70 0.662 1.95 2.31E-02 23 22 22 20 21 70 76 70 68 73 1.147 1.61 7.31E-04 21 21 20 20 21 74 72 70 71 61 1.678 2.17 5.47E-04 20 23 24 21 21 22 22 55 47 54 56 61 61 63 003230 a CO a> CO ooaacs -a a Q X c a. Q. < "O B] o 4g 83 OC O CoO <) g 0o9 c. UQXi. cc a 'C i53 E3 U <- to cu <n^ M *c -tSt cS -S51 c3 _ X cc a. Q. O a o3 a Particle Size Chamber Environment Mean Temnerahire Humidity 21 60 1.393 2.24 7.54E-04 22 62 21 64 21 63 21 68 21 72 21 65 c <o <o >o r- v 21 21 22 21 2! 0.767 22 21 uo (mg/m3) M M AD GSD TMC s .c 15 oi 1 e 1 r** .c 1 <0 (pm) rs 0 0 5^;"^ ---- ffs o O' I -- 0 0 0 300 -- 04 3 ~ P*; '> , *'1 -- 10 10 10 10 10 10 10 to 10 10 10 7.1 9.7 10 10 10 9.4 10/10 9.9 9.6 9.4 10 10 to 9.0 12 9.7 10 9.4 10 10 10 10 9.4 10 10 (0 1) 10 10 torn 9.9 10 9.7 10 J | w cC 8s s <2 I jua<0 E Individual (ppm) 10 10 10 10 01 98 01 01 01 01 01 00-000 0 10 11 11 11 to 10/11 10 9.7 9.0 to 10 10 10 10 9.5 9.8 10 OOOO^.f".-- ^ r*: o -- ooo - - O' "* ? 30 " -- -- -- <3 O' -- Exposure Number BO I 8. sa -o ^ -- -- O' O' O' !I *-i Vi v*i O' */> 06 06 60 CO 00 09 0Q zw IS> Vk */ WV O' O' V"l ao ao ed oe ac go ee p6- oO>' O w Nss W oe 'T r-- t-- r-~ r-~ r~- c~ t~- r- St. t-t-'.r'.r-r-r- ^ ^ ^ ^ O' 1 5oo 3 o> 3 ac 55 aco do 3 SP <<<<<> 32 } 5 O' OC 3 5 v> \o r oc O' " .. P4 O' O' O' O' O' S' O' 9> C> O0 06 OD 0006 W >aoat>o0eoeflcococo S 3 S 3 3 3 3^333333 <. <. < <. <: <: *:<<:<<<<: f*1 4T -P' 00 O' os o <s fn v wi Date 185 ; 8.5 9.9 185 ; 8.9 10 186 ; 8.5 10 187 i 8.5 10 188 8.5 10 189 1 8,9 9.2 190 8.9 10 191 i 85 9.9 171 to 172 10 i 173 10 | 174 10 1 175 10 ! 176 9 . 7 1 177 10 32 Week BFG 003231 22 56 23 54 22 68 22 73 20 70 22 65 22 61 22 66 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 38 Prgft Final Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 34 35 36 Date 26-Aug-97 27-Aug-97 28-Aug-97 29-Aug-97 30-Aug-97 3 l-Aug-97 1-Sep-97 2-Sep-97 3-Sep-97 4-Sep-97 5-Sep-97 6-Sep-97 7-Sep-97 8-Scp-97 9-Sep-97 10-Sep-97 11-Sep-97 12-Sep-97 13-Sep-97 14-Sep-97 !5-Sep-97 Exposure Number Nominal (ppm) 192 8.5 193 8.5 194 8.5 195 8.5 196 8.9 197 8.9 198 8.9 199 8.5 200 8.5 201 8.5 202 8.5 203 8.3 204 8,2 205 8.5 206 8.5 207 8.5 208 8.5 209 8.5 210 8.9 211 8.9 212 8.5 Mean (ppm) 10 10 10 9.9 10 10 10 9.9 10/9.8 9.9 10 10 9.6 10 10 9.8 10 10 9.9 10 10 10 10 9.7 10 10 10 11 10 10/9.7 9.6 10 12 9.7 10 10 10 10 10 9.4 10 10 Chamber Concentration 10 10 10 10 10 10 11 10 10/9.6 10 10 11 9.8 11 II 10 10 11 10 10 10 Miran (IR) Individual (ppm) 10 10 10 10 10 10 10 10 10 10 9.8 10 10 12 10 9.5 10/9.9 10/10 10 10 10 10 9.4 11 8.7 9.4 9.0 10 10 10 8.9 10 10 10 10 10 10 10 10 11 10 10 10 10 10 9.5 10 to 9.1 10 10/10 10 10 9.1 11 10 10 10 10 11 10 9.6 10 10 10 10 10 10 10 9.8 10 10/9.7 10 10 7.6 8.8 10 10 10 11 10 10 10 10 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 0.776 2.11 2.70E-03 1.551 2.48 6.25E-04 0.796 1.34 6.98E-03 Mean ISiPRgstMS Humiditv (C) (%) 21 69 22 69 23 79 22 71 21 71 21 72 22 73 21 76 21 60 21 52 21 58 22 65 22 71 22 68 23 67 22 66 23 76 23 74 22 67 22 61 22 61 BFG 003232 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 39 Draft Final Report Group 11-10 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 37 38 39 Date 16-Sep-97 l7-Sep-97 18-Sep-97 19-Sep-97 20-Sep-97 21-Sep-97 22-Sep-97 23-Sep-97 24-Sep-97 25-Sep-97 26-Sep-97 27-Sep-97 28-Sep-97 29-Sep-97 30-Sep-97 1 -Oct-97 2-Oct-97 3-Oct-97 Exposure Number Nominal (ppm) 218 8.5 219 8.5 220 8.5 221 8.5 222 8.9 223 8.9 224 8.5 225 8.5 226 8.5 227 8.5 228 8.9 229 8.9 230 8.9 231 8.5 232 8.5 233 8.9 234 8.9 235 9.1 Mean (ppm) 10 10/8.7 9,9 99 9.3 9.4 10 9.8 9.9 9.9 10 10 10 10 10 10 10 10 10 10/7.4 9.6 9.3 92 9.6 10 9.6 9.2 10 10 10 9.7 10 10 10 9.8 10 Chamber Concentration 10 10/8.9 10 9.8 9.5 9.0 10 10 10 10 10 11 9.3 10 10 10 10 10 Mlran (tR)* Individual (ppm) 10 10 10/9.1 9.6/9.2 10 10 10 10 9.8 8.5 9.3 9.4 10 10 10 9.3 10 10 10 10 10 10 9.4 9.4 11 11 10 10 10 10 10 10 10 11 10 9.9 10 11/8.5 10 10 9.2 9.7 10 10 10 10 10 It 10 10 10 10 11 10 10 10/8.8 10 10 9.5 9.4 10 10 10 9.6 10 10 9.3 10 10 10 10 10 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m5) 0.870 1.71 2.27E-03 1.918 2.10 6.70E-04 Mean Temperature Humidity re) (V.) 21 62 22 63 22 64 23 67 22 72 22 51 20 43 20 57 19 43 18 47 20 59 19 49 20 57 22 65 1.622 1.98 5.36E-04 21 19 19 23 58 54 45 51 BFG 003233 Mean: SD: 9.08 0.58 10.5 1 0.85 10.9 i 2.2 2.0 1.9 4.0E-03 3.0 - 5.8E-03 22 1.8 52 12 Huntingdon Life Sciences Reproduction Study 96-4080 Page 40 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week I 2 3 4 Date 7-Jan-97 8-Jan-97 9-Jan-97 l0-Jan-97 13*Jan-97 14-Jan-97 15-Jan-97 16-Jan-97 l7-Jan-97 20-Jan-97 21-Jan-97 22-Jan-97 23-Jan-97 24-Jan-97 27-Jan-97 28-Jan-97 29-Jan-97 30-Jan-97 3l-Jan-97 3-Feb-97 Exposure Number Nominal (ppm) 94 2 94 3 94 4 94 5 94 6 94 7 94 8 94 9 95 10 94 11 94 12 94 13 94 14 94 15 94 16 94 17 94 18 94 19 94 20 94 Mean (ppm) 97 100 99/110 98 110 110 98 96 100/63 100 110 110 110/100 99 100 99 100 110/130 100 too Chamber Concentration Miran (IR' a Individual (ppm) 95 95 100 96 99 110 100 no 99 96/110 100/110 100/110 97 97 99 95 110 110 no 97 no 100 100 no 93 94 93 no 94 93 96 96 110/50* 90/90* 110/93* 93/0.0* 100 100 no no 100 110 no 100 110 no no d 110/120 100/75* 100/65* 110/120 100 98 100 99 100 100 100 100 100 100 100 97 100 100 100 100 110/140 100/120 110/130 110/130 110 100 100 100 100 100 no 100 Particle Size Chamber Environment 94 100 100/110 too 100 no 100 98 100/37* 100 no 100 110/120 100 100 100 99 110/130 100 100 100 100 100/120 100 no no 100 96 100/110 100 no 100 110/120 98 100 98 110 100/130 100 100 Determinations MMAD GSD TMC (Mm) (mg/m3) 7.015 2.056 1.06E-03 3.727 2.495 1.94E-03 1.356 1.487 1.48E-03 3.273 1.856 4.27E-04 Mean Temoerature Humiditv <C) <%) 21 40 20 40 20 41 21 42 22 48 23 40 22 39 23 57 22 40 22 40 20 39 21 43 20 46 20 44 20 42 20 47 21 44 20 45 20 44 21 44 BFG 003234 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 41 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 5 6 7 8 Date 4-Feb-97 S-Feb-97 6-Feb-97 7-Feb-97 IO-Fcb-97 11 -Feb-97 l2-Feb-97 13-Feb-97 I4-Feb-97 17-Feb-97 I8-Feb-97 19-Feb-97 20-Feb-97 21-Feb-97 24-Feb-97 25-Feb-97 26-Feb-97 27-Feb-97 28-Feb-97 3-Mar-97 Exposure Number Nominal (ppm) 21 91 22 94 23 94 24 94 25 94 26 94 27 94 28 94 29 94 30 94 31 94 32 97 33 100 34 100 35 100 36 100 37 100 38 100 39 100 40 100 Mean (ppm) 98 100 110 MO 100 100 100 100/120 100 100 no no no ioo 100 100 100 110/130 100 no Chamber Concentration Minin (IR) individual (ppm) 100 97 100 100 93 100 100 no 110 no 100 too 98 no 120 120 98 100 99 100 100 100 100 100 95 100 100 100 99/(20 95 100/120 100/120 100/120 96 97 no 96 99 100 100 no no no no 100 110 100 110 no no 100 100 no 100 100 100 no 100 100 100 100 100 100 100 100 100 no no 110/130 110/130 110/130 100/130 98 100 100 100 110 no no no 83 110 MO 110 no too 110 110/120 no 100 120 no no 100 100 no 100 110/130 no 110 Particle Size Chamber Environment no no 100 no no no no 100/120 no no no no no 100 no Determinations MMAD OSD TMC (pm) 5.493 1.849 5.93E-04 1.349 2.187 2.55E-03 7.082 2.603 1.29E-03 Mean Temperature Humidity CO {%) 21 44 22 45 20 46 20 46 20 46 20 48 20 41 19 41 20 42 19 41 20 42 21 50 20 44 20 44 20 41 100 100 100/130 100 no 0.9237 1.493 3.84E-03 20 20 23 21 20 40 45 53 45 40 BFG 003235 Huntingdon Life Sciences Reproduction Study 96-4080 Page 42 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 9 10 n 12 Date 4-Mar-97 5-Mar-97 6-Mar-97 7-Mar-97 10-Mar-97 11-Mar-97 12-Mar-97 13-Mar-97 14-Mar-97 17-Mar-97 !8-Mar-97 19-Mar-97 20-Mar-97 21-Mar-97 22-Mar-97 23-Mar-97 24-Mar-97 25-Mar-97 26-Mar-97 27-Mar-97 28-Mar-97 29-Mar-97 30-Mar-97 31-Mar-97 Exposure Number Nominal (ppm) 41 100 42 100 43 100 44 100 45 100 46 100 47 100 48 100 49 100 50 100 51 100 52 100 53 100 54 100 55 100 56 100 57 100 58 too 59 100 60 too 61 100 62 100 63 100 64 100 Mean (ppm) 100 100 99 100 100 100 100 98/95 100 100 100 99 97 no 100 100 99 100 no 110/100 100 100 98 99 Chamber Concentration Miran (IR)ft Individual (ppm) 97 98 no no no 99 100 100 99 98 100 99 100 100 100 98 100 100 100 100 110 no 100 100 no 100 100 99 100/91 92/92 98/93 100/100 100 100 100 100 no 100 no 100 no 100 no 100 100 99 98 100 93 100 100 96 110 92 100 no 100 100 100 98 92 100 95 100 100 96 100 100 100 100 no/ito 100 100 98 99 100 100 110/110 100 no 95 99 100 no n o/ioo 100 100 100 100 100 no 100/100 99 100 100 100 100 100 99 100 100 100 100 100/96 100 100 100 98 97 no 100 100 99 100 no 100/100 100 100 95 95 Particle Size Chamber Environment 100 100 97 100 98 99 100 100/99 98 100 100 100 98 no 100 no 100 no 100 110/100 100 100 100 100 Determinations MMAD OSD TMC (pm) (mg/m3) 0.9302 1.549 1.07E-02 1.396 1.560 1.72E-03 1 240 1.582 3.41E-03 0.9995 1.639 1.11E-03 Mean Temperature Humiditv co (%) 21 44 20 46 21 45 21 44 21 57 22 57 21 56 21 58 21 56 20 53 21 53 20 53 20 53 21 53 22 53 20 54 22 44 22 46 22 45 23 46 24 46 23 46 24 45 21 56 BFG 003236 Huntingdon Life Sciences Reproduction Study 96-4080 Page 43 Draft Final Report Group Id - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week n 14 15 Date 1 -Apr*97 2-Apr-97 3~Apr-97 4-Apr-97 5-Apr*97 6-Apr-97 7-Apr-97 8-Apr-97 9-Apr-97 10-Apt-97 11-Apr-97 12-Apr-97 13-Apr-97 14-Apr-97 15-Apr-97 16-Apr-97 17-Apr-97 18-Apr-97 19-Apr-97 20-Apr-97 21-Apr-97 Exposure Number Nominal (ppm) 65 100 66 100 67 100 68 100 69 100 70 100 71 96 72 97 73 100 74 100 75 100 76 100 77 100 78 100 79 100 80 100 81 100 82 100 83 100 84 100 85 100 Mean (ppm) 100 98 99 100 100 97 110 120 98 no/iio 100 110 no 100 99 100 100 98 100 100 no Chamber Concentration Mlran (IR] Individual (ppm) 100 100 100 100 97 100 98 100 100 98 97 100 100 100 too 100 98 110 no 99 96 100 94 100 85 100 130 130 150 84 87 92 68 70 120 no 110/120 100 no 120 110/120 no no no 110/110 no no no 110/110 97 no 100 100 100 100 100 99 97 too 96 100 no 98 no 99 no no 100 92 99 100 100 99 98 no 110 96 95 100 no 110 no no 120 99 97 100 98 95 94 100 140 no 110/110 100 no 100 110 100 no no 99 110 100 96 Particle Size Chamber Environment Determinations Mean 99 98 100 100 91 99 95 140 no 100/110 100 100 no 100 100 100 100 100 100 no 97 MMAD OSD TMC (pm) (mg/m1) 3.122 1.875 8.66E-03 1.314 1.394 6.10E-04 1.453 2.059 1.67E-03 Temoerature ec) 20 19 19 20 20 22 23 21 20 20 20 20 22 20 20 20 21 21 21 22 22 Humidity (%) 56 60 56 56 57 57 65 61 52 52 52 57 62 32 33 36 37 36 34 34 34 BFG 003237 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 44 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 16 17 18 Date 22-Apr-97 23-Apr-97 24-Apr-97 25-Apr-97 26-Apr-97 27-Apr-97 28-Apr-97 29-Apr-97 30-Apr-97 1-May-97 2-May-97 3-May-97 4-May-97 5-May-97 6-May-97 7-May-97 8-May-97 9-May-97 I0-May-97 11-May-97 12-May-97 Exposure Number Nominal (ppm) 86 100 87 100 88 100 89 100 90 100 91 100 92 100 93 100 94 100 95 100 96 100 97 100 98 100 99 100 100 100 101 97 102 94 103 98 104 100 105 100 106 95 Mean (ppm) 100 110 100/94 110 no 100 no no no 100 100 100 100 no no 120 no/no 100 100 99 no Chamber Concentration Miran (IR] a Individual (ppm) 100 no 110 98 110 no no 100 100/91 100/94 110/94 100/91 no 100 no no no no no no no 100 100 100 no no no 110 no no 100 no no 120 no 120 no no 100 110 100 100 99 100 too 100 97 100 no 100 100 100 100 100 HO 100 no 120 120 no 120 120 120 120 no/no 110/110 120/110 no/no no no 91 no 100 100 100 100 97 99 100 100 120 no 100 100 100 100 110/96 no 100 100 97 100 no 100 100 100 100 no no no 100/100 too 100 98 no Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 3 8I Mean Humidity (%) no 100 100/95 no no 100 no no no 96 100 100 97 no no no 100/100 100 100 98 no 0.805 1.840 8.70E-03 1.485 3.38 2.09E-03 1.698 2.71 6.93E-04 22 20 20 20 20 20 22 22 23 23 22 23 23 22 22 21 22 22 22 22 21 36 37 37 36 35 34 51 46 46 49 44 48 46 37 46 37 39 45 44 41 46 BFG 003238 Huntingdon Life Sciences Reproduction Study 96-4080 Page 45 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week Date 19 13-May-97 l4-May-97 15-May-97 16-May~97 17-May-97 18-May-97 19-May-97 20 20-May-97 21-May-97 22-May-97 23-Mey-97 26-May-97 21 27-May-97 28-May-97 29-May-97 30-May-97 2-Jun-97 22 3-Jun-97 4-Jun-97 5-Jun-97 6-Jun-97 9-Jun-97 Exposure Number Nominal (ppm) 107 94 108 92 109 100 no 100 111 96 112 96 m 100 114 100 ns 100 116 100 117 94 118 100 119 94 120 94 121 94 122 94 123 94 124 94 125 94 126 94 127 94 128 94 Mean (ppm) 100 110 120 110 98 92 100 100 no 110/110 no 100 100 100 110 99 too 100/95 no 99 99 100 Chamber Concentration Mlran (IR) Individual (ppm) no 100 100 100 no no 110 120 no 120 no no no 110 no no 99 98 96 97 91 93 94 90 100 100 100 100 92 100 99 96 no 100 no 110 110/110 no/no 110/110 100/110 no 110 100 no 100 100 100 100 100 98 100 100 100 99 100 no no no no 110 100 96 100 100 no 99 100 100 100/90 100 95/97 no 100/97 no 100/97 no 94 no 100 100 100 97 100 98 no 100 100 100 100 100 120 MO 98 93 100 no 100 110/110 no 98 100 HO no 100 100 110/97 no 91 100 100 100 MO 120 100 98 90 100 100 100 MO/UO 100 100 100 110 100 100 100 100/92 100 98 100 100 Particle Size Chamber Environment Determinations Mean MMAD OSD TMC Temnerature Humiditv (pm) (mg/m3) (C) (%) 20 47 0.873 1.96 1.78E-03 20 20 21 21 21 24 45 48 42 45 43 54 22 56 2.245 2.73 9.53E-04 22 22 22 f 50 48 49 56 1.818 2.48 9.23E-04 21 21 21 20 22 47 46 47 52 56 4.414 3.27 I.72E-03 21 21 21 21 22 53 50 52 52 49 BFG 003239 Huntingdon Life Sciences Reproduction Study_____ 96-4060 Page 46 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 23 24 25 26 Date 10-Jun-97 1 l-Jun-97 12-Jun-97 !3*Jun-97 16-Jun*97 17-Jun-97 18-Jun-97 19-Jun-97 20-Jun-97 23-Jun-97 24-Jun-97 25-Jun-97 26-Jun-97 27-Jun-97 30-Jun-97 l-Jul-97 2-Jul-97 3-Jul-97 4-Jul-97 7-JuI-97 Exposure Number Nominal (ppm) 129 94 130 94 131 94 132 94 133 94 134 94 135 94 136 94 137 94 138 94 139 94 140 94 141 94 142 94 143 94 144 94 145 94 146 94 147 96 148 94 Mean (ppm) 100 98 100 100 100 100/99 97 100 100 100 100 110 97 99 100 98 110/110 100 96 110 Chamber Concentration Mi ran (IR)II Individual (ppm) 100 100 110 100 100 100 96 98 100 1 10 100 97 100 100 100 110 100 97 100 100 98/98 96/97 100/100 100/100 96 96 97 95 100 99 100 100 110 100 100 100 110 no 100 99 97 100 97 no 110 100 110 no 91 100 100 95 91 96 110 100 100 110 100 100 94 93 89 110 110/110 95/100 100/100 100/110 110 110 no 100 90 95 90 98 110 100 no 110 98 100 110 100 100 98/99 100 100 100 100 110 110 98 100 100 100 110/110 89 100 100 Particle Size Chamber Environment no 94 100 100 100 110/100 100 99 100 no Determinations MMAD GSD TMC (pm) (mg/m3) 1.204 2.33 1.49E-03 0.988 1.58 9.86E-03 Mean Temnerature Humiditv CC) <%) 23 50 25 49 22 52 22 52 21 49 21 52 21 52 22 53 22 51 25 58 110 100 0.666 1.35 5.99E-03 100 99 100 25 24 25 23 23 60 61 61 59 61 100 100/100 93 100 100 1.263 1.88 1.I9E-03 23 23 23 22 23 61 63 64 63 63 BFG 003240 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 47 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week Date 27 8-Jul-97 9-Ju!-97 10-Jul-97 II-Jul-97 l4-Jul-97 28 lS-Jul-97 16-Jul-97 I7-Jul-97 18-Jul-97 21-Jul-97 29 22-Jul-97 23-Jul-97 24-Jul-97 25-Jul-97 28-Jul-97 30 29-Jul-97 30-Jul-97 31-Jul-97 1-Aug-97 2-Aug-97 3-Aug-97 4-Aug-97 Exposure Number Nominal (ppm) 149 94 150 96 151 96 152 96 153 96 154 96 155 96 156 96 157 96 158 96 159 96 160 96 161 96 162 96 163 96 164 94 165 94 166 94 167 94 168 96 169 96 170 96 Mean (ppm) 100 95 97 100 96 90 97/100 95 96 95 98 97 99 99 96 98 110 HO 100/100 94 94 93 Chamber Concentration Miran (IR)A Individual (ppm) 100 99 100 100 90 94 99 95 98 99 95 100 100 100 100 100 100 91 100 97 84 89 85 87 98/100 95/100 95/100 97/99 no 98 81 90 96 100 100 100 100 96 100 90 92 100 100 100 100 100 96 92 95 96 100 100 100 94 100 100 95 99 100 94 96 100 100 98 110 110 no 120 no no no no 98/110 99/100 100/100 110/100 91 90 93 93 95 80 97 95 85 86 94 100 99 94 91 100 93 97 100/99 95 91 90 100 95 100 100 96 95 120 no 110/110 98 100 97 Partlcte Size Chamber Environment 100 100 97 100 93 98 98/100 94 91 93 98 97 too 97 94 100 no 98 100/100 98 99 96 Determinations MMAD GSD TMC (pm) (mg/m3) 0.705 1.17 1.50E-02 0.675 2.97 2.47E-02 1.127 1.57 5.82E-04 1.411 1.74 4.76E-04 Mean Temperature Humidity (C) (%) 24 65 25 64 23 63 24 62 26 64 23 65 23 68 22 65 20 63 22 66 20 68 21 66 20 65 21 67 22 64 21 63 24 58 25 60 22 63 22 66 22 67 21 62 BTG 003241 Huntingdon Life Sciences Reproduction Study __ 96-4080 Page 48 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 31 32 33 Date Exposure Number Nominal (ppm) 5-Aug-97 I7J 94 6-Aug-97 172 94 7-Aug'97 173 94 8-Aug-97 174 94 9-Aug-97 l0-Aug-97 11-Aug-97 175 176 177 96 96 94 12-Aug-97 13-Aug-97 M-Aug-97 15-Aug-97 16-Aug-97 178 179 180 181 182 94 94 94 94 96 17-Aug-97 18-Aug-97 183 184 96 94 19-Aug-97 19-Aug-97B 185 185 94 96 20-Aug-97 21-Aug-97 186 187 94 94 22-Aug-97 188 94 23-Aug-97 24-Aug-97 189 190 99 99 25-Aug-97 191 94 Mean (ppm) 100 100 no 100 97 97 100 100 100 100 100/100 88 88 100 no 99 99 no 100 95 92 100 Chamber Concentration Mlran (IR] Individual (ppm) 100 100 too 100 100 100 100 100 no no 100 100 100 100 100 100 91 95 95 98 96 96 98 94 83 100 100 100 100 100 100 100 no 100 100 100 110 110 100 100 100/110 90 83 100/100 91 87 99/100 86 89 98/100 86 90 130 93 98 95 120 120 no 110 100 100 100 94 95 100 100 100 no 110 no 110 no 100 100 too 91 87 99 95 89 94 89 97 100 100 100 110 100 100 110 100 100 99 no 100 100 100 100/100 90 88 100 100 100 100 100 100 90 no Particle Size Chamber Environment 100 100 no 100 100 99 110 100 no 100 110/100 87 91 110 too - Determinations MMAD GSD TMC (pm) (mg/m3) 1.528 1.99 8.36E-04 0.754 1.25 2.20E-02 Mean Temperature Humiditv (C) (%) 22 60 22 63 22 63 21 61 22 64 22 66 22 64 22 62 22 66 22 63 22 62 23 67 22 65 21 63 21 67 23 62 100 h h h 100 100 98 92 100 23 67 22 68 21 68 23 65 23 64 23 69 BFG 003242 Huntingdon Life Sciences Reproduction Study 96-4080 Page 49 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 34 35 36 Date 26-Aug-97 27-Aug-97 28-Aug-97 29-Aug-97 30-Aug-97 31-Aug-97 1-Sep-97 2-Sep-97 3-Sep-97 4-Sep-97 5-Sep-97 6-Sep-97 7-Sep-97 8-Scp-97 9-Sep-97 IO-Sep-97 11 -Scp-97 !2-Sep-97 13-Sep-97 !4-Sep-97 !5-Sep-97 Exposure Number Nominal (ppm) 192 94 193 94 194 94 195 94 196 96 197 96 198 96 199 94 200 94 201 94 202 94 203 96 204 96 205 94 206 94 207 94 208 94 209 94 210 96 211 96 212 94 Mean (ppm) 100 100 110 100 93 100 96 100 100/110 no 100 97 100 97 100 100 110 100 99 96 100 Chamber Concentration Miran (tR) Individual (ppm) 100 no no 91 110 100 100 98 110 no no 100 100 100 too no 91 91 89 90 100 100 100 98 98 95 100 93 100 100/110 too 97 100/110 no no 100/110 no 98 100/110 110 100 100 120 100 92 98 99 100 92 96 100 no 100 95 92 96 110 100 100 97 100 100 100 100 110 no no 100 100 100 100 100 98 99 97 100 100 100 100 90 100 100 100 100 97 97 no no 100 100 90 100 100/110 120 100 96 no 97 100 100 100 100 97 96 100 100 100 no 100 99 100 97 100 98/100 120 100 95 95 100 100 100 100 100 too 90 100 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 0.759 2.01 3.32E-03 1.959 2.41 7.96E-04 0.802 1.27 7.1 IE-03 Mean Temoerature Humiditv CC) (%) 23 69 23 69 24 74 23 69 22 69 22 72 22 73 21 72 20 65 20 61 20 64 20 67 22 69 22 69 22 68 22 69 23 72 22 72 22 68 21 67 22 60 BFG 003243 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 50 Draft Final Report Group III - 100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 37 38 39 Date 16-Scp-97 l7-Sep-97 18-Sep-97 (9-Sep-97 20-Sep-97 21-Sep-97 22-Sep-97 23-Sep-97 24-Sep-97 25-Sep-97 26-Sep-97 27-Sep-97 28-Sep-97 29-Sep-97 30-Sep-97 1-Oct-97 2-Oct-97 3-Ocl-97 Exposure Number Nominal (ppm) 218 94 219 94 220 94 ,221 94 222 96 223 96 224 94 225 94 226 94 227 94 228 96 229 96 230 96 231 94 232 94 233 96 234 96 235 100 Mean (ppm) 100 110/110 110 100 89 91 100 100 100 100 99 94 95 100 100 98 97 110 Chamber Concentration Mlran (IR] m Individual (PPm) 100 100 100 100 100/110 100/100 100/110 110/110 110 no 110 110 100 100 100 97 94 87 90 86 91 87 92 87 HO 100 100 100 100 100 100 99 100 100 100 100 100 100 99 100 87 94 94 100 93 92 93 95 98 93 97 95 98 99 100 100 100 100 100 100 87 95 97 100 92 93 100 100 HO 100 100 100 100 110/110 no 100 88 96 100 100 100 100 100 97 93 100 100 97 99 110 100 110/110 110 no 89 91 100 110 100 110 120 95 95 100 100 110 98 110 Particle Size Chamber Environment Determinations MMAD GSD TMC (pm) (mg/m3) 0.896 2.04 2.58E-03 1.573 1.98 4.67E-04 Mean TemDerature Humiditv (C) (%) 21 6) 22 61 22 62 24 60 22 65 22 52 20 42 20 49 19 44 19 47 20 49 19 46 20 52 23 69 1.308 1.72 2.77E-04 22 21 20 24 66 66 60 61 B FG 003244 Mean: SD: 96.41 2.69 102 1 7.0 105 J 17.5 1.9 2.0 4.1E-03 1.6 - 5.8E-03 22 1.4 54 10 Huntingdon Life Sciences Reproduction Study____ 96-4080 Page 51 Draft_FinaLReoort Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 1 2 3 4 Date 7-Jan-97 8-Jan-97 9-Jan-97 IO-Jnn-97 13-Jan-97 14-Jan-97 15-Jan-97 16-Jan-97 17-Jan-97 20-Jan-97 21-Jan-97 22-Jan-97 23-Jan-97 24-Jan-97 27-Jan-97 28-Jan-97 29-Jan-97 30-Jan-97 31-Jan-97 3-Feb-97 Chamber Concentration Particle Size Chamber Environment Exposure MJran (IR)B Determinations Mean Number Nominal Mean Individual MMAD GSD TMC Temnerature Humidity (ppm) (ppm) (ppm) (Mm) (mg/m3) (*C) <%) 1 noo MOO 1200 MOO MOO 1100 1100 MOO 20 45 2 1100 MOO 1100 MOO 1200 1200 1100 1100 1.544 1.357 2.27E-04 20 3 1100 1200/1100 U00b 1200/1200 1100/760 1200/1200 1200/1100 1100/1200 20 45 45 4 1100 MOO MOO MOO 1100 1100 MOO MOO 20 45 5 1100 MOO 1200 1200 i 100 MOO MOO MOO 20 46 6 1100 MOO MOO MOO MOO MOO 1200 MOO 20 45 7 1100 MOO MOO 1100 noo MOO 1100 MOO 1.227 1.345 7.05E-04 20 39 8 MOO MOO MOO MOO noo MOO MOO 1100 20 42 9 1100 1200/1300 1100/890' 1100/1300 1300/1400 1200/1300 1200/1400 1200/1300 20 42 10 MOO 1200 1200 1200 1200 1200 MOO 1200 21 43 11 1100 1100 noo noo MOO 1200 1200 noo 20 42 12 1100 MOO MOO MOO MOO 1100 1200 1100 1.404 1.837 I.79E-03 21 48 13 1100 1100/1300 1200/1400 1100/1300 1100/1300 1100/1300 1100/1300 1100/1300 14 1100 1100 1100 MOO MOO 1100 MOO MOO 21 52 20 47 15 1100 1100 1100 1100 MOO MOO MOO MOO 20 47 16 MOO MOO 1100 MOO MOO 1100 MOO noo 21 53 17 MOO 1100 MOO MOO 1100 MOO MOO 1100 1.325 1.336 2.37E-04 21 47 18 MOO 1100/1400 1100/1500 1100/1400 1200/1500 1100/1400 1100/1400 1100/1400 19 MOO MOO 1100 MOO MOO 1100 MOO noo 20 53 21 49 20 MOO MOO noo 1100 MOO 1100 1200 1200 21 49 BFG 003245 Huntingdon Life Sciences Reproduction Study 96-4080 Page 52 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 5 6 7 8 Chamber Concentration Particle Size Chamber Environment Date Exposure Miran (IR) i Determinations Mean Number Nominal Mean Individual MMAD GSD TMC Temperature Humidity (ppm) (ppm) (ppm) (pm) (mg/m5) to <%) 4-Feb-97 21 1100 1100 1100 1100 noo noo noo noo 21 51 5-Feb-97 22 1100 1100 1100 1100 noo noo 1200 noo 1.197 1.296 1.50E-04 21 49 6-Feb-97 23 1100 1100 1100 1200 noo 1200 noo noo 20 49 7-Feb-97 24 1100 1100 1100 1100 1100 noo noo noo 21 48 IO-Feb-97 25 1100 1100 1100 1100 noo noo noo 1100 20 45 11-Feb-97 26 1100 1100 1100 1100 noo noo noo noo 20 47 12-Feb-97 27 1100 1100 1100 1100 noo noo noo noo 1.372 2.280 2.94E-03 20 44 13-Feb-97 28 1100 1100/1400 1100/1400 1100/1400 1100/1400 1100/1400 1100/1500 1100/1500 20 39 l4-Fcb-97 17-Feb-97 29 30 1100 1100 1100 1100 1100 1100 1100 1100 noo noo noo 1200 noo 1100 1200 noo 20 48 20 46 18-Feb-97 31 1100 1200 1100 1200 1200 1100 1200 1200 21 48 I9-Feb-97 32 1100 1200 1200 1100 noo 1200 1200 1200 2.322 1.910 9.55E-04 22 58 20-Feb-97 33 1100 1200 1200 1200 noo 1200 1200 1200 20 57 21-Feb-97 34 1100 1200 1200 noo noo 1200 noo 1200 21 57 24-Feb-97 35 1100 1100 1100 noo noo noo noo 1100 21 48 25-Feb-97 36 1100 1100 1100 1100 noo noo noo 1100 20 49 26-Feb-97 37 1100 1200 1100 noo 1200 1200 1200 1200 0,9406 1.844 5.15E-03 20 54 27-Feb-97 38 1100 1200/1500 1200/1500 1200/1500 1200/1500 n oo/i 400 1100/1500 1200/1500 22 62 28-Feb-97 39 1)00 1100 noo 1100 1100 1200 noo noo 20 53 3-Mar-97 40 1100 noo noo noo noo noo noo 1000 20 45 BFG 003246 0032*7 aa.. oo > a. o <3 tn o c -A ~o c .2 oo c IS D x <n IuMAelueuS_l N o- Week (gS iN'ONf'IgN oN^or-t 5522555 go 0 " N w t 2-- 2fsi 225 ^^ 2*n 5si 2r-2 A r- 4A A r^A t-* A t^-. A rO-' ro--* AS (3 Or*'' rO~-' fll CO Or~'- FO'-' c3 SB [-- <3 ^uS3 rOiC**lB' r^A* r* tCOl 0^k61'}s rW-' rO-' Or~' r0-\ *Svi S 3 S s| Date iExposure Number Nominal (ppm) Mean (ppm) Individual (ppm) S--' 22 GSD TMC j (mg/mJ) 0011 i 0011 0011 O tOl oori ! -V ('ST W^ ^'I- W'T 1100 1100 1200 1100 1200 1100 1200 1100 1100 1100 1100 1100 1200 1100 0.9226 1.307 1.02E-02 1100 1100 1200 1100 1100 1100 1100 1100 1100 1100 1(00 1100 1100 1100 1100 1200 1100 1200 1200 1200 1100 0011 0011 0011/0011 0011/0011 0011 0011 00(1 0001 0011 0011 0011 oou 0011 0011 oooi ! oou oou j 0001 I oou oou ; oou oou oou oou oou 0011 oou 0011 0011 0011 0011 001! 46 1100 1 1100 1100 1100 47 1100 1 1100 1100 1100 0011 0011 1100 1100 7.226 2.695 3.32E-03 48 1100/1100 1100/1100 1100/1000 1100/1100 49 1100 j 1100 1100 1100 0011 0011 1200/1200 noo 50 1200 1100 1200 1200 1200 uoo 1100 1200 noo noo 1 1200 ci oou oou oou oou O lOl/OOU oou oou m-rsi/ifmn^v)um'i'oviri-^i g*'o1 9> O> -O N'M nsD 'tO uoo noo noo noo noo 1100 1.234 1.573 1100 noo noo uoo noo noo 1200 noo 1200 1100 1100 1200 uoo 1100 1100 1100 noo noo noo noo 1100 noo 1100 1100 uoo uoo uoo uoo uoo noo 1000 1(00 uoo noo 1100 noo noo 1100 noo uoo noo uoo 1.114 1.678 1.28E-03 1100/1200 1100/1200 uoo uoo 1100/1100 1100/1200 1100/1100 1100/1200 noo noo noo uoo 1100 1100 uoo uoo uoo uoo uoo noo uoo uoo noo 1200 uoo uoo 1100 1100 uoo noo g a I "tdoI* <Ji oCO e o s a r a* *> c: 21 4ft 1 *> i oo V 1 MMJu&iwsB_i X X T3 Ca> CaL. < 1 co t: io a "a a a 20 20 20 20 21 21 21 21 21 21 21 20 20 21 21 21 21 22 22 22 23 23 24 20 f'nT vsol fvii of*'i --^ iTs '*T> f'T*' *2 ? kO oTnT o'T r*%r 'VC< so >n w**>i t*' <vs* *i r* rw* *o d aV ECz Huntingdon Life Sciences Reproduction Study 96-4080 Page 54 Draft Final. Recoct Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 13 14 15 Date I-Apr-97 2-Apr-97 3-Apr-97 4-Apr-97 5-Apr-97 6-Apr-97 7-Apr-97 8-Apr-97 9-Apr-97 10-Apr-97 11-Apr-97 12-Apr-97 13-Apr-97 14-Apr-97 15-Apr-97 16-Apr-97 17-Apr-97 l8-Apr-97 19-Apr-97 20-Apr-97 21 -Apr-97 Exposure Number Nominal (ppm) 65 1100 66 1100 67 1100 68 1100 69 1100 70 1100 71 1100 72 1100 73 1100 74 1100 75 uoo 76 1100 77 1100 78 1100 79 1100 80 1100 81 1100 82 1100 83 1100 84 1100 85 1)00 Chamber Concentration Mlran (1R) 1 Particle Size Determinations Mean Individual MMAD GSD TMC (ppm) (ppm) (pm) (mg/m3) 1100 1100 UOO uoo uoo uoo uoo 1100 1100 UOO uoo uoo uoo uoo 6.444 2.699 8.67E-03 1100 UOO 1100 uoo uoo uoo uoo 1100 UOO 1200 uoo uoo 1100 uoo 1100 1100 1200 uoo uoo uoo 1200 1100 UOO UOO uoo 1100 1100 1200 1100 1100 1200 uoo uoo 1000 uoo 1200 uoo uoo 1200 1200 1200 1200 1200 UOO 1200 uoo 1200 1200 1200 1.218 1.350 4.70E-04 1200/1300 1200/1300 1200/1300 1200/1300 1200/1200 1100/1200 1200/1300 UOO UOO UOO uoo 1200 1200 UOO UOO UOO 1200 uoo uoo uoo uoo UOO UOO UOO 1200 1000 1000 uoo 1100 uoo UOO uoo 1200 1200 uoo 1100 1000 UOO uoo uoo uoo uoo 1100 uoo uoo uoo uoo uoo uoo 1.144 1.528 1.20E-03 uoo 1000 1100 uoo uoo 1200 1200 1100 uoo uoo 1100 1100 uoo 1100 1100 1000 1100 uoo uoo uoo 1100 1100 uoo uoo uoo uoo uoo uoo 1200 1200 1200 uoo uoo uoo 1200 Chamber Environment Mean Temperature Humidity CC) (%) 19 46 18 49 19 50 19 49 19 50 20 55 21 64 20 50 20 50 19 57 20 56 19 59 21 67 20 40 20 43 20 44 21 48 21 47 22 43 23 48 23 46 BFG 003248 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Rage 55 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Chamber Concentration Particle Size Chamber Environment Week Date Exposure Miran (1R)a Determinations Mean Number Nominal Mean Individual MMAD GSD TMC Temoerature Humiditv (ppm) (ppm) (ppm) (Mm) (mg/m3) CC) (%) 16 22-Apr-97 86 1100 1100 1100 MOO MOO MOO MOO 1200 22 48 23-Apr-97 87 1100 1200 1200 1200 1200 MOO MOO 1200 0.925 7.860 1.08E-02 20 50 24-Apr-97 88 1100 1100/1200 1100/1200 1100/1200 MOO/1100 1100/1200 1100/1200 1100/1200 20 50 25-Apr-97 89 1100 1100 1100 MOO MOO MOO MOO 1200 20 48 26-Apr-97 90 1100 1200 1200 1200 1200 1200 1200 1200 21 48 27-Apr-97 91 1100 1100 1100 MOO 1100 1100 1200 1200 20 44 28-Apr-97 92 1100 1200 1200 MOO 1200 1200 1200 1200 23 62 17 29-Apr-97 93 1100 1100 1100 MOO MOO MOO MOO 1200 23 49 30-Apr-97 94 1100 1200 1200 1200 1200 1100 MOO MOO 1.302 3.04 2.12E-03 23 47 1-May-97 95 1100 1100 MOO 1200 1100 1100 MOO 1000 24 53 2-May-97 96 1100 1100 1100 1200 MOO MOO MOO MOO 23 43 3-May-97 97 1100 1100 MOO MOO MOO MOO MOO MOO 24 57 4-May~97 98 1100 1100 1200 1100 1100 MOO MOO MOO 23 44 5-May-97 99 1100 1100 1100 MOO 1200 1100 MOO 1200 21 40 18 6-May-97 100 1100 1100 1000 1100 1000 MOO MOO MOO 21 53 7-May-97 101 1100 1200 1300 1200 MOO 1200 MOO MOO 3.560 2.62 1.1 IE-03 21 41 8-May-97 102 1100 1100/1200 1200/1300 1100/1200 1100/1100 1100/1200 1100/1200 1100/1100 21 43 9-May*97 103 1100 1100 1100 1100 MOO MOO MOO MOO 21 55 10-May-97 104 1100 1100 1100 MOO MOO MOO MOO MOO 21 53 11-May-97 105 1100 MOO MOO MOO MOO MOO 1100 1100 !2-May-97 106 1100 1200 1200 1100 1100 1200 1200 MOO 22 48 22 50 1 BFG 003249 Huntingdon Life Sciences Reproduction Study:___ 96-4080 Page 56 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week Date Exposure Chamber Concentration Miran (1R)a Particle Sire Determinations Chamber Environment Mean Number Nominal Mean Individual MMAD GSD TMC Temperature Humidity (ppm) (ppm) (ppm) (pm) 19 13-Mav-97 107 1100 1100 1100 tioo 1100 1100 MOO MOO (mg/mJ) (*C) 21 (%) 53 14-May-97 108 1100 1100 1100 MOO 1100 MOO 1200 MOO 0.815 1.97 2.33E-03 20 59 15-May-97 109 1100 1100 1000 1100 1000 MOO 1100 MOO 21 58 16-May-97 110 1100 1100 1200 1200 1200 MOO MOO 1000 21 47 17-May-97 111 1100 1100 1100 1100 MOO MOO MOO 1000 18-May-97 112 MOO 1100 MOO MOO MOO MOO 1 100 1000 19-May-97 113 1100 1100 MOO 1100 MOO 1000 MOO MOO 22 51 22 50 22 58 20 20-Mav-97 114 1100 1100 1000 1000 MOO 1000 MOO MOO 20 56 21-May-97 115 1100 1100 1100 1100 1100 MOO MOO 1100 1.361 1.85 4.89E-04 21 45 22-May-97 116 1100 1100/1200 1100/1200 1100/1100 1100/1100 1100/1200 1100/1200 1100/1200 20 41 23-May-97 117 MOO 1100 1100 1100 1100 MOO MOO MOO 26-May-97 118 1100 1100 1000 1100 1100 1100 MOO 1100 20 45 f 59 21 27-May-97 119 MOO 1100 MOO MOO MOO MOO MOO MOO 19 48 28-May-97 120 1100 1100 1100 1100 MOO 1200 1100 MOO 1.562 1.86 7.48E-04 19 45 29-May-97 121 MOO 1100 1100 1100 1100 1100 MOO 1100 19 46 30-May-97 122 1100 1100 1100 MOO MOO MOO MOO 1100 2-Jun-97 123 1100 1100 1200 MOO 1200 MOO 1100 1100 19 55 20 58 22 3-Jan-97 4-Jun-97 5-Jun-97 6-Jun-97 124 125 126 127 1100 1100/1100 1100/1100 1100/1100 1100/1100 1100/1100 1100/1100 1100/1100 1100 1100 1000 1100 MOO 1100 1200 1200 1.328 1.69 7.66E-04 MOO 1100 MOO MOO MOO MOO MOO MOO MOO 1100 1100 1100 MOO 1100 MOO MOO 20 20 20 20 50 44 47 47 9-Jun-97 128 1100 1100 1100 1100 MOO 1100 1100 MOO 21 52 osieoo Huntingdon Life Sciences Reproduction Study 96-4080 Page 57 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 23 24 25 26 Date 10-Jun-97 ll-Jun-97 12-Jun-97 13-Jun-97 !6-Jun-97 l7-Jun-97 I8-Jun-97 19-Jun-97 20-Jun-97 23-Jun-97 24-Jun-97 25-Jun-97 26-Jun-97 27-Jun-97 30-Jun-97 l-Jul-97 2-Jul-97 3-Jul-97 4-Jul-97 7-Jul-97 Chamber Concentration Particle Size Chamber Environment Exposure Miran (IR) Determinations Mean I 6g 1 Number Nominal Mean Individual MMAD GSD TMC Humidify (ppm) (ppm) (ppm) (pm) (mg/m3) (%) 129 1100 1100 noo noo noo 1100 noo noo 21 57 130 1100 1100 noo noo noo noo noo noo 1051 2.08 1.46E-03 23 52 131 1100 1100 1000 1100 1100 noo noo 1000 . 20 60 132 1100 1100 1100 1100 noo 1100 noo noo 20 60 133 1100 1100 1100 1100 noo 1100 1100 noo 21 52 134 1100 1100/1100 1100/1100 1100/1100 1100/1100 noo/itoo noo/iioo 1100/1100 21 55 135 1100 noo 1100 noo 1100 noo noo noo 1.010 1.57 I.05E-02 21 55 136 1100 1100 noo noo noo 1100 1100 noo 21 60 137 1100 1100 noo noo noo noo noo noo 21 56 138 1100 1100 1100 noo noo 1100 1100 noo 22 51 139 noo 1200 1200 1200 noo 1200 noo noo 22 60 140 1100 1200 1200 1200 1200 1200 1200 noo 0.658 1.22 8.76E-03 22 63 141 1100 1100 1100 1100 noo 1200 noo noo 22 65 142 1100 1100 1100 1100 noo 1100 noo noo 21 60 143 1100 1100 1200 noo noo 1100 noo noo 22 59 144 1100 1100 1100 noo noo 1100 noo noo 22 61 145 1100 1100/1200 1100/1200 noo/1200 1100/1200 noo/1200 1100/1200 1100/1200 1.299 2.08 1.40E-03 22 64 146 1100 noo noo noo 1100 1100 noo noo 21 68 147 1100 1100 noo noo noo 1100 noo noo 21 65 148 noo noo noo noo noo 1100 noo noo 21 62 BFG 003251 Huntingdon Life Sciences Reproduction Study_____ 96-4080 Page 58 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 27 28 29 30 Dale 8-Ju!-97 9-Jul-97 10-Jul-97 !I-Jul-97 !4-Jul-97 15-Jul-97 !6-Jul-97 !7-Jul-97 1 S-Jul-97 21-Jul-97 22-Jul-97 23-Jul-97 24-Jul-97 25-Jul-97 28-JuI-97 29-Jul-97 30-Jul-97 31-Jul-97 1-Aug-97 2-Aug-97 3-Aug-97 4-Aug-97 Chamber Concentration Particle Size Chamber Environment Exposure Mlran (IR) Determinations Mean Number Nominal Mean Individual MMAD GSD TMC Temperature Humidity (ppm) (ppm) (ppm) (pm) 149 1100 1100 noo 1100 1100 MOO 1000 noo (mg/m3) (C) 24 <%) 66 150 1100 1200 1200 1200 noo 1200 noo 1200 0.736 1.69 2.2 IE-02 25 67 151 1100 1100 1200 1100 1100 1200 MOO noo 23 67 152 100 1100 noo 1200 1100 1100 1200 noo 153 1100 1200 1200 1200 1200 1100 1200 1200 25 64 26 69 154 1100 1100 1100 1100 1200 1200 noo 1100 22 155 1100 1100/1200 1000/1100 1100/1(00 1100/1200 1200/1200 1100/(200 1100/1100 0.711 7.45 2.90E-02 22 156 1100 1100 1200 noo 1200 noo noo 1100 22 157 1100 1200 1100 1200 1200 1200 noo 1100 20 158 1100 1100 1100 1200 1100 noo 1100 1100 21 71 74 66 68 73 159 1100 1100 1200 110Q 1100 1100 noo 1100 20 160 1100 1100 noo noo 1100 noo 1100 noo 1.323 1.76 8.06E-04 20 161 1100 1100 1100 noo noo noo noo noo 20 162 1100 1100 1100 noo noo 1100 1100 noo 20 163 1100 1100 noo 1100 noo noo noo noo 21 75 73 68 67 61 164 1100 1100 1000 noo noo 1100 1100 1100 21 165 1100 1100 noo 1000 noo noo 1100 1000 2.007 1.87 7.03E-04 23 166 1100 1100 970 noo noo noo noo 1100 23 167 noo 1100/1200 1100/1200 1100/1200 1100/1200 noo/noo 1100/1100 1100/1200 21 168 1100 1100 1100 1100 noo 1100 1100 1100 20 169 1100 1200 1200 1200 1100 noo noo 1200 20 170 1100 noo noo noo noo noo noo noo 20 54 50 57 60 62 68 62 BFG 003252 Huntingdon Life Sciences Renroduction Studv 96-4080 Page 59 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Chamber Concentration Particle Size Chamber Environment Week Date Exposure Miran (IF) i Determinations Mean Number Nominal Mean Individual MMAD GSD TMC Temnerature Humiditv (ppm) (ppm) (ppm) (pm) (mg/m3) co (%) 31 5-Aug-97 171 1100 1100 1000 1000 noo noo noo 1000 20 64 6-Aug-97 172 1100 1100 noo noo noo noo noo 1200 1.502 1,98 8.51E-04 22 62 7-Aug-97 173 1100 1100 noo noo 1100 noo noo noo 21 63 8-Aug-97 174 1100 1100 noo 1100 noo 1100 noo noo 20 64 9-Aug-97 175 1100 noo 1200 noo noo noo noo noo 21 72 1O-Aug-97 176 1100 1100 1200 noo 1100 noo noo 1200 21 74 11 -Aug-97 177 1100 1100 noo 1100 noo noo noo noo 22 64 32 12-Aug-97 178 1100 1100 noo noo noo noo MOO NOO 22 63 13-Aug-97 179 1100 1100 noo noo noo noo noo NOO 0.744 1.21 2.21E-02 22 68 M-Aug-97 180 1100 1100 noo 1100 noo noo NOO NOO 22 63 15-Aug-97 181 1100 1100/1200 1100/1200 1100/1200 1100/1200 1100/1200 1100/1200 1100/1200 22 60 16-Aug-97 182 1100 1100 noo 1100 noo 1000 MOO NOO !7-Aug-97 183 1100 1100 noo noo noo noo 1100 1000 23 70 22 68 lS-Aug-97 184 1100 1100 1200 noo noo noo 1100 1000 19 60 33 !9-Aug-97 185 noo 1200 1200 1200 1200 1200 1100 1100 20 59 19-Aug-97* 185 1100 noo 1100 noo noo noo - - 20 55 20-Aug-97 186 noo 1100 noo noo noo 1100 1100 1100 h h h 20 65 21-Aug-97 187 1100 1100 noo noo noo noo 1100 noo 19 70 22-Aug-97 188 1100 1100 noo noo noo noo noo noo 23-Aug-97 189 1100 1200 noo 1200 1200 1200 1200 1100 24-Aug-97 190 1100 1200 MOO noo 1200 1200 1200 NOO 25-Aug-97 19! 1100 1100 noo noo noo 1100 noo noo 18 73 20 65 20 63 20 68 BFG 003253 Huntingdon Life Sciences Reproduction Study 96-4080 Page 60 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 34 35 36 Date 26-Aug-97 27-Aug-97 28-Aug-97 29-Aug-97 30-Aug-97 31-Aug-97 1-Sep-97 2-Sep-97 3-Sep-97 4-Sep-97 5-Sep-97 6-Sep-97 7-Sep-97 8-Sep-97 9-Sep-97 10-Sep-97 11-Sep-97 12-Sep-97 13-Sep-97 14-Sep-97 15-Scp-97 Chamber Concentration Particle Size Exposure Miran (DR)B Determinations Number Nominal Mean Individual MMAD GSD TMC (ppm) (ppm) (ppm) (pm) (mg/nri*) 192 1100 1100 1100 1100 1200 MOO MOO MOO 193 1100 1100 1100 1100 1200 1100 1100 MOO 0.883 3.13 3.95E-03 194 1100 1200 1200 1200 1200 MOO 1100 1100 195 1100 1100 1200 1100 1100 1100 1100 MOO 196 1100 1100 1100 1100 1100 MOO MOO 1100 197 1100 1100 1100 1100 1100 1100 1100 1100 198 1100 1100 1100 1100 1100 MOO 1000 1000 199 1100 1000 960 1000 1000 MOO MOO 1100 200 1100 1100/1100 1000/1100 1100/1100 1100/1200 1100/1200 1100/1100 iioo/noo 1.380 2.08 5.62E-04 201 1100 1100 1000 1100 1100 MOO MOO 1100 202 1100 1100 1100 1100 1200 MOO MOO MOO 203 1100 1200 1300 1100 1100 1200 MOO 1200 204 1100 1100 1100 1100 1100 MOO 1200 1200 205 1100 1100 1100 1100 1100 1000 MOO 1100 206 1100 1100 1100 1100 1100 1000 MOO MOO 207 1100 1100 1100 1)00 1100 MOO MOO MOO 0.794 1.31 7.21E-03 208 1100 1100 1100 1100 MOO MOO MOO MOO 209 1100 1100 1100 1100 1100 MOO 1100 MOO 210 1100 1100 1100 1100 1100 MOO MOO MOO 211 1100 1100 1100 1100 1100 1100 1000 MOO 212 1100 1100 1100 1100 MOO MOO MOO MOO Chamber Environment Mean Temperature Hiimiditv CC) (%) 20 70 21 69 21 77 21 71 20 69 20 71 21 73 21 73 20 59 20 51 20 56 21 65 22 68 22 68 22 66 22 66 23 76 22 71 22 68 21 62 22 62 BFG 003254 Huntingdon Life Sciences Reproduction Study 96-4080 Page 61 Draft Final Report Group IV - 1100 ppm Cumulative Exposure Record Chamber Monitoring Results Appendix X Week 37 38 39 Date 16-Sep-97 17-Sep-97 I8-Sep-97 19-$ep-97 20-Sep-97 21-Sep-97 22-Sep-97 23-Sep-97 24-Sep-97 25-Sep-97 26-Sep-97 27-Scp-97 28-Sep-97 29-Sep-97 30-Sep-97 1-Oct-97 2-Oct-97 3-Oct-97 Exposure Number Nominal (ppm) 218 1100 219 1100 220 1100 221 1100 222 1100 223 1100 224 1100 225 1100 226 1100 227 1100 228 1100 229 1100 230 1100 231 1100 232 1100 233 1100 234 1100 235 noo Chamber Concentration Particle Size Chamber Environment Mi ran (IR) Determinations Mean Mean Individual MMAD GSD TMC Temperature Humidity (ppm) (ppm) (pm) (mg/m5) CC) (%) 1100 noo 1100 noo 1100 noo noo 21 61 II00/II00 1000/1000 1100/1100 1100/1100 MOO/UO0 1100/1100 1100/1100 0.835 I >00 noo noo noo 1100 1100 1100 1200 1100 noo 1200 1200 1200 1100 1.63 2.27E-03 21 21 23 63 64 67 1100 1100 noo noo 1100 1100 1100 22 71 1100 1000 noo noo 1100 noo 1100 1100 1100 noo 1100 MOO noo noo 22 52 19 46 1100 1000^ noo noo MOO 1000 noo 19 1100 noo noo noo 1100 noo 1100 1.498 1.64 4.01E-04 19 58 45 noo noo 1100 1100 1100 noo noo 1100 noo noo noo 1100 noo 1100 18 49 19 57 1000 1000 1000 1000 1100 1000 1000 18 49 1100 1000 noo noo 1100 noo 1000 1100 noo 1100 1100 noo noo 1100 19 58 20 69 1200 1200 noo noo 1200 1200 noo 20 62 MOO noo noo noo 1100 1100 noo 1.270 1.73 2.75E-04 18 58 noo noo 1100 1100 1100 noo 1200 18 49 noo 1200 1100 1100 1100 1100 1200 22 52 BFG 003255 Mean: SD: 1100 0.00 1112 1-------------- 45 1212 j 135 1.6 2.1 4.5E-03 1.4 - 6.8E-03 21 1.3 56 9.3 Huntingdon Life Sciences Reproduction Study Key to Observations: Few = < 20% Some = 21 - 50% Most = 51 - 99% All 100% 96-4080 In-chamber Observations Preface Page 62 Draft Final Report Appendix X BFG 003256 Huntingdon Life Sciences Reproduction Study 96-4080 Page 63 Draft Final Report in-chamber Observations Appendix X Group Observation Test Days 74 75 76 77 78 79 80 1 - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some II-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some (II-100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some Group Observation Test Days 81 82 83 84 85 86 87 1 - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some II -10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some 111-100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some BFG 003257 Huntingdon Life Sciences Reproduction Study 96-4080 Page 64 Draft Final Report In-chamber Observations Appendix X Group Observation Test Days 88 89 90 91 92 93 94 I - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some II -10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some III -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Some Some Group Observation Test Days 95 96 97 98 99 100 101 I - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Few Few II -10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Few Few III -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Few Few IV- 1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Some Some Some Some Some Few Few 003258 bfg Huntingdon Life Sciences 96-4080 Page 65 In-chamber Observations Appendix X Group Observation Test Days 102 103 104 105 106 107 108 1-0 ppm Within Normal Limits Unobservable Chromodacryorrhea Most Most Most Few Few Few * - Few Most Few - Most Few - Most Few - Most Few - II-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few III -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few Group Observation Test Days 109 110 111 112 113 114 115 I-0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few II-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few III -100 ppm Within Norma! Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV-1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few BFG 003259 Huntingdon Life Sciences Reproduction Study 96-4080 Page 66 Draft Final Report In-chamber Observations Appendix X Group Observation Test Days 116 117 118 119 120 121 122 I - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few If-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few III -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV-1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few Group Observation Test Days 123 124 125 126 127 128 129 I - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Some II-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Some III -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Some IV-1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Some bfg 003260 Huntingdon Life Sciences 96-4080 Page 67 In-chamber Observations Appendix X Group Observation Test Days 130 131 132 133 134 135 136 1-0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few II -10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few 111 -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few Group Observation Test Days 137 138 139 140 141 142 143 1 - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Some Few Few Few 11-10 ppm Within Normal Limits Unobservable Red Nasal Discharge Chromodacryorrhea Dried Red Material Facial Area Labored Breathing Most Few - - - Most Few - - - Most Few - - Most Some Few Few Few Few Most Few - - Most Few - - Most Few - -- III - 100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Some Few Few Few IV- 1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Some Few Few Few BFG 003261 Huntingdon Life Sciences 96-4080 Page 68 In-chamber Observations Appendix X Group Observation Test Days 144 145 146 147 148 149 150 I * 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few 11-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few Hi -100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV -1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few Group Observation Test Days 151 153 154 155 156 157 158 I - 0 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few II-10 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few 111 100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few IV-1100 ppm Within Normal Limits Unobservable Most Most Most Most Most Most Most Few Few Few Few Few Few Few BFG 003262 Huntingdon Life Sciences Reproduction Study 96-4080 Page 69 Draft Final Report In-chamber Observations Appendix X Group Observation Test Days 161 162 163 164 165 168 169 1 - 0 ppm Within Normal Limits Unobservable Most Most All All All All All Few Few - - - - - 11 -10 ppm Within Normal Limits Unobservable Most Most All Ail All All All Few Few - - - - III -100 ppm Within Normal Limits Unobservable Most Most All All All All All Few Few - - - - - IV -1100 ppm Within Normal Limits Unobservable Most Most All All All All All Few Few Group Observation 170 171 Test Days 172 175 176 177 178 1 - 0 ppm 11-10 ppm Within Normal Limits Unobservable Within Normal Limits Unobservable All Ail All All All All All m * "" All All All All All All All - III -100 ppm Within Normal Limits Unobservable All All All All All All All w IV-1100 ppm Within Normal Limits Unobservable All All All All All All All . BFG 003263 Huntingdon Life Sciences 96-4080 Page 70 !n-chamber Observations Appendix X Group Observation Test Days 179 180 183 184 185 186 189 i - 0 ppm Within Normal Limits Unobservable All All All All All All All II -10 ppm Within Normal Limits Unobservable All All All All All All All ... . . - III -100 ppm Within Normal Limits Unobservable All All All All Ail All All ... - - - IV-1100 ppm Within Normal Limits Unobservable All All All All All All All ... . . - Group Observation 190 191 Test Days 192 193 196 197 198 I - 0 ppm Within Normal Limits Unobservable All All All All All All All 11-10 ppm Within Normal Limits Unobservable All All All All All All All ... . . - III -100 ppm Within Normal Limits Unobservable All All All AH All All All ... . - - IV-1100 ppm Within Normal Limits Unobservable All All All All All All AH ... - - - BFG 003264 Huntingdon Life Sciences Reproduction Study 96-4080 Page 71 Draft Final Report Group I - 0 ppm Observation In-chamber Observations Appendix X Test Days 199 200 203 204 205 206 207 Within Normal Limits Unobservable All All All All All All All II -10 ppm Within Normal Limits Unobservable All All All All All All All ... - . - III -100 ppm Within Normal Limits Unobservable All All All All All All All ... . . - IV-1100 ppm Within Normal Limits Unobsenrable All All All All All All All ... . - - Group Observation Test Days 208 209 210 211 212 213 214 l - 0 ppm Within Normal Limits Unobservable All All All All All All All II-10 ppm Within Normal Limits Unobservable All All All All All All All ... . - - 111-100 ppm Within Normal Limits Unobservable All All All All All All All ... - - - IV-1100 ppm Within Normal Limits Unobservable Alt All All All All All All ... - - - BFG 003265 Huntingdon Life Sciences 96-4080 Page 72 Group I - 0 ppm Observation In-chamber Observations Appendix X Test Days 215 216 217 218 219 220 221 Within Normal Limits Unobservable All All All All All All All 11-10 ppm Within Normal Limits Unobservable Ail All All All All All All III -100 ppm Within Normal Limits Unobservable Ail All All All All All Ail IV -1100 ppm Within Normal Limits Unobservable All All Alt All All All Ail - --- Group Observation 222 223 Test Days 224 225 226 227 228 1 - 0 ppm Within Normal Limits Unobservable All All All All All All All 11-10 ppm Within Normal Limits Unobservable All All All All All All All ... - - - III -100 ppm Within Normal Limits Unobservable All All All All All All All - --- IV-1100 ppm Within Normal Limits Unobservable All All All All All All All ... . . - 003266 bfg Huntingdon Life Sciences 96-4080 Page 73 Reproduction StudyDraft Final Report In-chamber Observations Appendix X Group Observation Test Days 229 230 231 232 233 234 235 I - 0 ppm Within Normal Limits Unobservable Chromodacryorrhea Ail Most All Ail All AH All -- - - - -- Few - II- 10 ppm Within Normal Limits Unobservable All All All All All All All -- - - - 111-100 ppm Within Normal Limits Unobservable Chromodacryorrhea Ail Most All All All All All --- - - -- Few - - - IV-1100 ppm Within Normal Limits Unobservable All All All All AH All All -- - - - -- Group Observation Test Days 236 237 238 239 240 241 242 I - 0 ppm Within Normal Limits Unobservable All All AH AH All AH All -- - - - - II -10 ppm Within Normal Limits Unobservable All All All All All AH AH -- - - - -- III -100 ppm Within Normal Limits Unobservable All All All AH All All All -- - - - - IV-1100 ppm Within Normal Limits Unobservable All All All Ail All Ail All .- . - - -. BFG 003267 Huntingdon Life Sciences Reproduction Study______ 96-4080 Page 74 Draft Final Report Group Observation In-chamber Observations Appendix X Test Days 243 244 245 246 247 248 249 I - 0 ppm Within Normal Limits Unobservable All All All All All All All -- II -10 ppm Within Normal Limits Unobservable Chromodacryorrhea Most Most All All All All Ail -- - - - -- Few Few " III -100 ppm Within Normal Limits Unobservable Ail All All All All All All - - - *" " IV-1100 ppm Within Normal Limits Unobservable All All All All All All All -- - - - - - Group Observation Test Days 250 251 252 253 254 255 256 I - 0 ppm Within Normal Limits Unobservable All All All All All All All --- - - - II -10 ppm Within Normal Limits Unobservable All All All All All All All -- " 111-100 ppm Within Normal Limits Unobservable All All All All All All Ail -- - - - - IV - 1100 ppm Within Normal Limits Unobservable All All All All All All All -- - - . -- BFG 003268 Huntingdon Life Sciences Reproduction Study 96-4080 Page 75 Draft Final Report In-chamber Observations Appendix X Group 1 - 0 ppm Observation Within Normal Limits Unobservable 11 -10 ppm Within Normal Limits Unobservable III -100 ppm Within Normal Limits Unobservable IV- 1100 ppm Within Normal Limits Unobservable Group 1 - 0 ppm Observation Within Normal Limits Unobservable Chromodacryorrhea Labored Breathing Gasping 11-10 ppm Within Normal Limits Unobservable Chromodacryorrhea 111 - 100 ppm Within Normal Limits Unobservable IV-1100 ppm Within Normal Limits Unobservable 257 258 259 260 261 262 263 All All All All All All All -- - - - AH Ail All Ail All All Ail -- - - - - - All All AH All All All All -- - - - -- All All All All All All All Test Days 264 265 266 267 268 269 270 Most - Few Few Few Most - Few Few - Most - Few Few - Most - Few Few - Most - Few Few - Most - Few - All - Most Most Most All All Ail All - - -- - - - Few Few Few - - -- All All All All All Ail All -- - - - -- All All All AH All All AH -- - - - -- BFG 003269