Document 10Ngxg3JdvV0ez39qYrJRENZZ
"c `g CODE YE-721-D
" / S/ ( DATE )
lj2j (? < LOT'7
.ENDED BACK
4448* LBS. ( EST WT )
/*&
PROCESSES < > YE-721-D CM)
COMTYP JOB NAME:
APPROVED BY; FWP 11/08/82
01YE721DMH
4eoiiT^
EQUIP KENT
PREP 1
NAME: MOLYBDATE RED
BTAIN FOR S-12 J>TJ)BTAIN FOR S-34 3^V OBTAIN FOR S-38
BTAIN FOR S-40 BTAIN FOR S-44 OBTAIN FOR S-47
USE |
1 ACCT
LBS | N-CODE | LBS
~------- 1 68 | 108-A
600 | 4-A
68 600
120 | 3-A
120
195 | 32-D 350 . I 3-A
195 350
61 | 711-BD
61
351 WEIGH IN : OPTRj&C-,
2
OPTR
MK ___ , T-_____,
35? WEIGH IN; OPTRy^l, MK zc, t -me
3
OPTR
MK ___ , T~,,
Wsu\ i
sSc!
1
10-D 423-D
1509 243
358 -'9\L-Kf?N 10* (500 G> WATER INTO V-358
4 U^>-PUN V-359 INTO V-351 2, PUMP IN V-351
TO 55' (2600 G>
IFT IN N-108-A FROM SI
tfYlR 5 MIN & RECORD; PH~%l 4.<9 JhJ D.0>
| ADJ TO PH 9.8-?.? 2. RECORD: PH_^tgL
| ASSUME 50%
^ ASSUME 66%
I RUN INTO V-35.L. FROM BADGER MOER
U 0PTR_^2^r--> NK_si2.,%3U&
,Mt)MP FROM V-351 TO V-358
| FLUSH V-351 & PUMPING LINES WITH 1000G
>^TER INTO V-358
I ADJ TO 74* (3530 C> AT 67-69*F
CORD: VOLJm.* 4=
F
STIR 5 MIN 6. RECORD: PRZ?.<7.2-7.4> 2,
I G/ML /&2l ._(1.055-1 .058)
I NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
I LIST & ATTACH. TAKE 1 QT SAMPLE.
I 7-D I 33-D
,,I 28-D
SV RUN 20* (996 G) WATER INTO V-^^-- 5 RECORD N-41-D STORAGE TANK TO PUMP^EBOM. CIRCLE ONE: 402 410 411 420 424rC425J
| CHECK WITH CU SUPV: | ^STORAGE TANK MUST CONTAIN AT LEAST 1900
NOV 10198,J GAL: 402=39*. 410=20'. 411=38*, 420-20*
j 424=20* j ^STORAGE TANKMUST HAVE STIRRED AT LEAST
J 20 MIN SINCE LAST ADDITION OR ADJUSTMENT
| ^STORAGE TANK'MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMPLETE,
\ SET METER FOR 300 G & PUMP TO SV
LOT:___ EQUIP | MENT | |
COMTYP JOB NAME: 01YE721DMM PAGE 02
BATE PRINTED 11Z08/82 USE N- |ACCT LBS CODE | LBS
SV
5 CONT
AT APPROX 100 G WHILE CONTINUING TO PUMP,
CHECK PH & DENSITY. RECORD BELOW. IF NOT
IN RANQE, STOP PUMPING & SEE SUPV.
* PH: ML <2^2-3,?)
DENSITY:
G/ML Cl.270-1.328)
IF S-23 OK
N S-22 COMPLETE, RECORD
DENSITY & G/ML ON TRAPPED SAMPLE
ROM END OF S-22 PUMPING.
USING DENSITY FROM S-24, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22.
CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
*#* TABLE #
G/ML SETTING I G/ML SETTING 1 G/ML SETTING 1 I !
1 .270 1.271
1259 1253
i 1.291 1 1.292
1146 1141
1 1.312 1 1.313
1049 1 1045 I
1 1
1 .272 1248 1 1.293 1136 I 1.314 1040 1
1
1.273 1242 1 1.294 1131 1 1 *315 1036
11
1 .274 1236 1 1.295 1126 1 1.316 1032 1 1 1
1.275 1231 I 1.296 1121 1 1 .317 1027
1
1 .276 1225 idjszz:1m) 1 1.318 1023 1
1
1.277 1219 I 1.298 1112 1 1.319 1019
1
1.278 1214 I 1.299 1107 1 1 .320 1015 1 1 1
1.279 1208 I 1.300 1103 1 1 .321 1010 1
t
1.280 1203 J 1.301 1098 1 1.322 1006 I 1 I
1.281 1198 I 1.302 1094 1 1.323 1003
1I
1.282 1193 I 1.303 1089 ! 1.324
999
i
1.283 1187 I 1.304 1084 1 1 .325
995
i1
1.284 1 182 1 1.305 1080 I 1.326
991 1
1
1.285 11 77 f 1.306 1076 1 1.327
987
II
1.286 1171 I 11307 1070 1 1 .328
983 1
1
1
1.287 1166 1 1.308 1066 1 1.329
979
1
1*288 1161 1 1.309 1 061 t 1.330
975 1
1
1
1 .289 1155 I 1.310 1 057 1 1 .331
971
11
1.290 1151 I 1.311 1053 1 1 .332
967
1\
SET METER 6 PUMP
G (RECORD FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
I 130-SECONDS
P*TADJ LEAD NITRATE TO 1 I 247) AT &Z.-69*F
3244
G
(68*-242/245
6 HP
JH2COORRD: ,,h&____ *F & ICE
SUMED (330S/BLQCK) 330X__
2T STIR 5 MIN & RECORD PH:
<2.2-3.7)
I LJ**** USE TITRIMETER TO AI JUST N-41-D PH ****
lJUTS IF NECESSARY ADJ TO PH 3. 0-3.1
ASSUME 667.
& RECORD PH:
ASSUME 507.
TE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING
RECORD : /Zc 20G/ML (1.128-1.129) IF OUT OF SPEC
FILL OUT CHECK LIST 6 ATTACH.
STIR AT 67-69*F FOR S-33. TAKE 1 QT SAMPLE.
41-D 57-A
33-D 7-D
I | 4094 I l_____ , I I -j
I______ I I I
DUP050059714
Lor= .
EQUIP MENT I
COMTYP JOB NAME; 01YE721DMM
/Ml
PA^GE 03
DATE PRINTED:11/0S/82 I USE | N- | USE I LBS | CODE | UBS
SV
5I CONT I
I I I
I
I I
I OBTAIN 1 QT SAMPLES OF S-19 6 S-31 SOLUTIONS
| 6 TITRATE TWICE
I NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
I 9*5-9*9 OR IF THE TWO TITRATIONS DIFFER BY
| MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL
I EQUIPMENT it REPEAT TITRATIONS). DO NOT
I PROCEED IF N-10-D TITRATION IS OUT OF RANGE
I ADJUST V-35S FOR A TITRATION PH OF
I *701____ _
I FROM FINAJ- IN-LINE TITRATION, RECORD LOWEST
I I PH
it ML N-10-D
f.r7o-/,'xO 1
SV WHEN"s-32"flfRAflON"oi<7"sfRlKE~V::38"fHR0'*B6fH'`!
6 UNDERSURFACE SISTRigJJIORS INTO SV IN ,,44M6 MINI
J RECORD: START
TOTAL MIN*
I
I NOTf: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
BUBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER
I L^TOR 15 MINUTES
J&WRTNG S 34, WASH IN V-358^
i^Srn STj^, 2 MIN it RECORD PH_ykJL_< 1 *7-1 *8)
JXS,,,^rr_<MUST BE + 3
I STIR TOTAL OF 15 MIN FROM S-34 it
7 1RECORD: TEMP_ - -_#F <67-73*F>
N-3-A FROM S-3
3 MIN
IN N-32-D FROM S-4
2 MIN
IN LIQUID ALUM USING BADGER METER
I
JXSLIR 3 MIN it FLUSH ALUM LINE WITH WATER
I^J^JUMP IN N-3 FROM S-5
\qgr\ STIR 4 MIN FOR S-49
604
33-D 7-D
115-D
302
390 |
RUN IN HYDROCHLORIC ACID USING WEIGHT &
| CONTROL PANEL
MK
0L% i32
28-D
7 I Jr*
MK___
%|_______ I 28-D
\m \ DURING S-45 SIFT N-711-B FROM S-6 INTO V-390
WITH AGITATOR ON IN 1-2 MIN
i STIR 1-2 MIN TO MILKY SOLUTION
' WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B I
SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV I
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP I
UNTIL FOAM SUBSIDES* DUMP IN BLANC FIXE N
I
I 275
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON J
TOP OF PAGE 1
I
cor d; code R 20 MIN * 2
__ , l o t
I I
RECORD: PH___ 5.8-6*0)
I
I&-NECESSARY, ADJ TO PH 5,-8-6.0
ASSUME 50% I.
|
it RECORD: PH-__<K.'l ___
ASSUME 66% I. w~~~
LS5 | FLOOD TO 153* <7298 G) 6 STOP AGITATOR
|
I
ART J*
1
128-A 7-D
33-D
90 275
DUP050059715