Document 0ygyLd8dno68733mMxO4o1Gb
AR226-0516
Testsuestawce ACUTE TOXICITY TO FISH TEST SUBSTANCE
Identity:
Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC-116, FC-126, FC-168, FC-143, or as a major component of FX-1003. (Octanoic acid, pentadecafluoro-, ammoniumsalt, CAS # 3825-26-1)
Remarks: The 3M production lot number was 2327. The test sample is FX-1003. It's purity was not sufficiently characterized, though current information indicates it is a solution of <45% ammonium perfluorooctanoate; 50% water, <3% inert perfluorinated compound and 1 - 2% Cs and C7 perfluofo analogue `compounds.
wewoo: The following summary applies to the test sample as a mixture of the test substance inwater solution with incompletely characterized concentrations of impurities. Data `may not accurately relate toxicity of the test sample with that of the test substance. METHOD:
Method: OECD 203 Type: Static acute
GLP: Yes
Year completed: 1990
on Species: Pimephales promelas
Supplier: Aquatic Research Organisms, Hampton, New Hampshire
Analytical monitoring: Temperature, PH, conductivity, and dissolved
Exposure period: 96-hours
Statistical methods: Non-linear interpolation, `moving average, and/or probit analysis
Test fish age: Juvenile
Length and weight:
Pretreatment: None. Test conditions:
Average length = 3.8 cm
Average weight = 0.45 g (wet)
Dilution water: Hampton, New Hampshire well water Dilution water chemistry:
pH:
Conductivity:
Hardness:
74
1500 pmhos/cm
88 mg/L (as CaCOs)
C03836
Lighting: Cool-white fluorescent bulbs with an intensity of 35 uEs'm2. A
dtahirloyugphhooutotptehreiotdesotfin1g6pehroiuords. light and 8 hours dark was maintained oTresttwiccoenddaiitliyodnusrirnegmtahreksac:clTihmaetifiosnhpweerrioed,fefdooadcboemimnegrcwiiatlhhfeilsdh food once t1h4rdouagyhsopurtiotrhetoteusstepeinriaosds.ayFsi.sh were acclimated to test temperature for
Aeration was employed after 48 hours to maintain dissolvedoxygen
Scotnoccekntarnadtitoensstasboolvuetiaocncperpetpaabrlaetlieovne:ls.Test solutions were created by dCiorneccetriintdriavitdiuoanlswdeoigshitngadrdaitteio:nsO.nce Stability of the test clremical solutions: Not noted
Exposure vessels: 19.6L glass aquaria containing 15 liters test solution
aNtuamnbaeprproofxriempaltiecadteepst:htowfo 17 cm.
LNouamdbienrg orfatfei:s0h.p3e0rgr/eLplicate: 10
WNautmebrecrhoefmicsotnrcyendturraitnigontsh:e fsitveudpyl:us a blank control
Conductivity range: (0-96 hours)
1200 1300
-
1500 1600
pmhos/cm pmhos/cm
(control exposure) (1,000 mg/L exposure
PH range (0-96 hours):
77..48 --88..24 ((c1o,n0t0r0olmegx/pLosexuproesure)
Temperature range (0-96 hours):
21.0 = 22.0 C (control exposure
Dissol2v1e.d0o-x2y2g.e0nrCa(n1g,e00(00-m9g6/hLoeurxsp)o:sure)
6.1 -9.2 mg/L (control exposure
6.2 -9.1 mg/L (1,000 mg/L exposure)
RESULTS
Nominal concentrations: Bk control, 150, 250, 400, 600, and 1,000
mg/L
Elementvalue: 96-hour LC50 = >1,000 mg/L
Element value based on nominal concentrations
Remarks: Testing was conducted on the mixture of the test substance as
tdoestchratibmeidxtiunrtehaentdestnostutbhsetatnesctesruebmsatrankcsef.ield. The values reported apply
03887
CC0 OONNcCLL0 uUsSiIOo0 NnSs 000000000
T>1h,e0t0e0stmgs/aLm.ple 96-hour LCsq for fathead minnow was determined to be
Submitter: 3M Company, St. Paul, Minnesota, 55133
Environmental
Laboratory,
P.O.
Box
33331,
b0 DaAtTAAQQuU0 AALITTYY0000000
tReeslitaibnigl.ityH:owKeiviemri,scsharmapnlkeinpgur2i.tyTwesatsinngotmepreotpsertlhye
criteriafor quality characterized and
it
lacks artalytical confirmation of test substance concentrations.
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