Document 0yJ6LwymRyrL0LQwr44DNbbk

PLAINTIFF'S EXHIBIT USG-436 Operating Division PBDXHJCT PBOCEDOBE Approvedi SPECIAL BULLETIN COttFmgftTiAL DO MOT RZPHODUCf Oil COPY BEAUT MIXED JOIST COMPOUND JE-533A - DALLAS No. 61-2-24-2-D Date 8-29-66 Page 2 Caneela Dated NEW FORMULA Mica JC Carey 7BF9 aaheatoe Methocel 6$BB - 4000 epe Excallo clay Pic Pleat JP 100 aeah Posselanlo Filler (box Co.) i eanm ne pentahorate PH 674 plaatlolsed eaulalon Carbltol <W.7. 0.6 Y valne aa req'd - approx.- 4.25JC 0.9* 2.556 to sake 100* IT lhe. car 2000 Ihe R.7. batch 230 to 280 lhe. nozaal range ahont 85 lbs. 18 lba. 50 lba. to aake 2000 lba. I.T. . 40.C* l.OJe 6.0* I.T. 800 lba. 20 lbs. *200 lba. 20 lba. *Baaed an 60^ eolide eanlaian. IT a diluted eaulalon le used the eaulalon weight aaa't he iaereaaed proportionately. BAV MITSUI* T, SPBffTWTrATIOSS All are current paint plant raw naterlala exoept the posaolaaie filler which la being sent to the Dallae Plant ty Hr. P. C. Appleyard'a direction. It aoat he eereened through a 100 aeeh screen before uee to rewore "grit". End M-i971r Mr. 9/6$ (Printed in U.3.A,) -3o O o J* '"V) 3PL3IXL imSIZN Operating Division ^ 'N'J PRODUCT PROCSDUi,E/} <^y) Approved: . zn ss*; r.~s:v^vzz oa cop? P.ZADT HXI.J JCILT UCtfCUND-ALL PURPOSE (JS-cC4-A> ^ uT.T.^S Ho. 61-2-42-2.* Djits rt-?? -67 ?*g* 2 ^________ Cancels Dated 2W FORMULA Mica 7HF9 Asbestos Ercello Clay Huber CUF Clay Methocel Pozzolanic Filler (Ground at Ft. Worth WHO plant) Micro!11 #2 G.P. 952-3 milo flour PH 4386 emulsion PMA 30 HAW MATERIALS JE-6C4-A . 0.8 Fornula V 5.03s H.y. 2.5 2.5 .8 t '' 40.0 To Make ICO? H.V. 1.5 4.5JS N.V. 1.2 lbs. per 230 gal. batch All raw materials are standard at Dallas except ths Ft. Worth grind pozzolanic filler. L H-U971rC Hev. 9/65 (Printed in U.S.A.) ~^wH O o 3 O a j) o Operating Division PRODUCT PROCEDURE^ Approved: SPECIAL BULLETIN HEIDI ITII7.D JOINT COMPOUND ALL PURPOSE (JE-604-A) DALLAS No. 61-2-2A-2-F Date 8-30-6-7 Pate 1 Cancels rage 1 Dated 8-22-67 . C This Bulletin expires 3*1-66. _____ ______ '' * Dallas is authorized to sake 1 batch (230 gallons) of JS-6Q4-A Raady Mixed Compound using pozsolanlc filler from the Ft. Worth (Western Mica) plant. Ship only for field triala as directed by #961 or #151. IDENTIFICATION AMD PACKAGING In standard 5 gal. 3M Cartons (or cans if so directed by AB Knud son). Add ?F after date-batch code. FINISHED PRODUCT SPECIFICATIONS Color Natural White Viscosity At nornal 525 BB, unless trials to be run with March Bros. (Houston). In this case adjust BB to 'March consistency' i.e. 460 BB. Other Properties Per Bulletin 61-2-24-2. -0- ^ y // /f t 7D 3 -- /" (o 0P009 1500 M-8971 1/63 (Printed in U.S.A.) Operating Division PRODUCT PROCEDURE/-) Approved; cs>5 ^t SPECIAL EULLSTIN O ^V ow -> j' 1:JJj -L._1Vv> 1f?3 N oJ " SJ 3 J A w-J 3 L: 20 nC7 22?n03CC" 00 GCPV 35LADX HILO JOINT cajPOUUD-ALL PURPOSE (JE-604-A) DALLAS No. 61-2-2 '-2-P pate 8-30-67 ' Pn-e 2___________ Cancels 61--2--42--2--? Dated 8-22-67 FORMULA Mica 7EF9 Aabestoa Uccello Clay Buber CUF Clay Methbcel Pozzolanlc Filler (Ground at Ft. Worth W2C plant) Mierofil #2 G.P. 952-3 olio flour PM 4386 emulsion PMA 30 SffJttXSSiAa?. J2-604-A 0.8 Foraala V 5.0$ N.V. 2.5 2.5 .8 *j 71 40.0 To Make 100? N.V. 1.5 4.5? N.V. 1.2 lbs. par 230 gal. batch All raw materials are standard at Dallas except the Ft. Worth grind poxsolanlc filler. 1C6T bOOdU Ii-fi971rC Rev. 9/65 (Prlntea in U.S.A.) End <o No. 61-2-24-AA Date 11-19-69 Page 2 Cancels Page 2 Dated 4-16-69 1SA3T-Mn23 JOINT CCMTCT3ND - all PURPOSE (J3-684?) * 7EIISHSD PHDDUCT SPECIFICATIONS A. Viscosity c c _ - Regular Merck Actra Mechanical Tools - 525 to 57533 600 * 30 33 - 425 to 47533 - Per Bulletin 61-2-24-2 700 30 33 - Per Bulletin 61-2-24-2 400 25 33 All viscosities run using VC-3 Bmbendsr, pin paddle, 7$ SB! 250 cb. gn. torque head. S. Bond - 4 Minima. Tested as par Bulletin 61-2-24-2. Z, Color - White or pignanted. To nateh standards. i 0. Application & .Dry - To natch plant standards. Ho grit or lunps In 1 Appearance 1 i application. No cracking on band test panel. Testing as per Bulletin 61-2-24-2. 1 i. Weight Par Gallon - 12.5 to 12.8 lbs. per gal. for regular viscosity natoriftl* i -o - . b t G l faOOdU M-6971 (Back) * TnH i f*m l.mn M44 + 4 -- r> Operating Division PRODUCT FRCCSDURS Approved: . SPICIAL B0U2TQI C0N?90ft?3&L DO DOT RCFOODVeS OS SOPY RSADT-MI4SD JOINT COMPOUND ALL FUHF0S2 (JE-684A) No 61--2--24--AA Date 11-19-69 Pa*e 3 Cancels Fags 3 Dated 4-16-69 PCRMULA Mica JC PC7RP9 Asbestos Methocel 65 HG C Plo-Ploat* Hsaseo 267 IH43S6 (u/o FHA-30) Tamol 850 IMA-30 Water % Non-Volatile V As req'd for vise. 4.5 to 5.52 normal 0.7 to 1001 N. V. 2.02 2.52 Founds-2000 Lbs. N. V. 280 to 300 approx. 90 to 11C approx. 14 1500 approx. 40 83.3 3 to 4 as rsq'd 1 160 to 162 gal. approx, for regular Ylscosity i l I Gypsum to use Stanelite, Per IMS 6-24-2 for Pigmented Read? Mix, and ,f*9NCS, per IMS 6-24-9, for White Reedy Mix. ! RAW MaTZRIALS Per Bulletin 61-2-24-2 plus: Taacl 350 Haaaco 267 IMS 6-177-9 A. S. Staley Mfg, Co., Dacatur, 111. MANUFACTURING P30C23URS General procedures as per Bulletin 61-2-42-2. Note: 1. eld Taool 850 to water and amulaion and mix before adding dry ingredients. 2. If PMA-30 is normally added to the emulsion in bulh, extra ' HU-30 will be necessary since the amount of emulsion has been reduced. This extra preservative should be added to the water/emulsion premix. i 310 :<-971rC Rev. 9/65 (Printed in U.S.A.) C Indicates Change A Indicates sjlt Operating Division pfcduct procedure Approved: JSG READY MIXED JCIET CO'TCUHD - ALL PURPOSE No. Date Page 61-2-2u_i 1-5-70 i Cancels Page 1 Dated L-I6-69 DESCRIPTI~?I A resin-emulsion base, ready-mixed Joint compound, with & package life of one year. MA;n;?ACTtrpi?;H plant Chamblee product A. USO Ready Mixed Joint Cortnound - All Pumose. Rerular Consistency 600-650 Erabender. B. Ares Consistency A USC Beady Mixed Joint Compound - All Purpose at an Anes Tool Consistency of 1*25-1*75 Brabender units, at 77 F, by diluting with extra water. C. Heavy Consistency On special order only. Brabender range to be 700-750. Cans to be marked "Heavy". 0. "EXTRA HEAVY" on special order only, 500-650 Bli. Cans to be marked "Extra Heavy". E. Special Ames Consistency Brabender to be on the hirh side of the Ames range. Cans vill not be marked special for customers who use this for hand application. IDEHTIFICATIOf.' AID PACKAGIKC A. 1 Callon Can C Per Pi'S fe-15-2. Master carton per PMC 8-10-31*. Label as directed by 11*7-2. B. 1* Gallon Carton Per-PMS e-10-29-2. Liner ner PMT 0-5-1*. C. 5 Gallon Pail Per PrS 0-29-3. D. 100* Pastern Two gallon cans per P*F 0-15-12 of compound packed with a 100' roll of PERF-A-TAPE on top of each can. .Master carton per P**E 0-10-1C. Label os directed by 11*7-2. Two (2) Wb-31* folders to be included in each master carton. 0P009 13V M-5791 I/63 (Printed in U.S.A.) C Indicates Change Operating Division PRODUCT PROCTERS Approved: SPECIAL BDLLBZZS CONF3D2N?!AL eo not axmoooet on copy READI-MIXED ALL PURPOSE JOZBT COM- POOBD-CP sons GATE No. Data 1-30-70 iUL 2 Caneala Dated BEV P0RH3LA (JE-6847) * Bon-Volatile Pounds-2000 Lbs. H.V. Mica JC UCC 210 Standard grade Asbestos Methocel 65 MW-325 Banaco 267 PM4386 (v/o PMA-30) Taaol 850 PMA-30 Water V As required for vise. 3* normal 0.8* . *TO 100* X.V. 20 2.5* 280 to 300 approx. 60 approx. 16 1900 aprox. 40 83.3 3 1 160 to 162 gal. approx, for regular viscosity. RAW MATERIALS Per Bulletin 61-2-24-4 plus< Tsmol 850 Banaco 267 PMS 6-177-9 A.E. Staley Mfg. Co. Decatur, HI. MABOyACTOHXBG PROCEDURE General procedure as par Bulletin 61-2-24-4. BOSE: 1. Add Ousel 850 to water and ewlslon and nix before adding dry Ingredients. 2. If PMA-30 is normally added to the emulsion in bulk extra PMA-30 will be necesaary since the amount of emulsion has been reduced. Ibis extra preservative should be added to the vater/enulslon premix. bH l l OOdli 1-69714 Rev. 9/65 (Printed in U.fl-A.) END Operating Division PRODUCT PROCEDURE Approved: SPECIAL BULLETIN READY-MIXED JOINT COMPOUNDALL PURPOSE (JE-68LF) 1st .Extension No. Date Page Cancels Dated 61-2-2U-AA 3-3-70 1 Page 1 11-19-69 C This bulletin expires 3-1-71. DESCRIPTION C Gypsum to manufacture Ready-Mixed Joint Compound . All Purpose and ship on all orders unless otherwise specified or authorized by Chicago #9T1-E. MANUFACTURING PUNT C Gypsum IDENTIFICATION AND PACKAGING C Packaging per Bulletin 61-2-2**. Letter "K" to follow code on all production. bOOdO M-8971. Rev. 1/63 (Printed in U.S.A.) C Indicates Change ^ T--.4 4 -- --+ ---- 4 Afi No. 61-2-2U-AA Date Page 3-3-70 2 Cancels Page 2 Dated 11-19-69 READY-MIXED JOINT COMPOUND - ALL PURPOSE (JE-68iF) *=>' FINISHED PRODUCT SPECIFICATIONS c A. Viscosity - Regular Extra Mechanical Tools 600 30 BB TOO 30 BB U00 25 BB All viscosities run using VC-3 Brabender, pin paddle* 6 7$ RPM 250 cm. gm. torque head. B. Bond - b minimum. Tested as per Bulletin 61-2-2U-2. C. Color - White or pigmented. To match standards. D Application l> Dry- To match plant standards. Mo grit or lumps in Appearance application. Mo cracking on bond test panel. Testing as per Bulletin 6l-2-2k-2. . Weight Per Gallon 12.5 to 12.8 lbs. per gal. for regular viscosity material. -0- 1P009 1055 M-8971 (Back) C Indicates Change Operating Division PRODUCT PSCCSDURS ^ Approved: - SPECIAL BOLUTXV CONFIDENTIAL DO DOT RCPROOUOt OR OOFT READT-MIXdD JOINT COMPOUND . ALL PURF052 (J3-684A) No. 61-2-24-AA Date 3-3-70 Paee 3 Cancels Page 3 D*^____ 11-19-69 FC.TMULA Mica JC J-C7.1P9 Asbestos Kathocel 65 HG C Carbonate Filler* Haaaeo 267 IMA386 (u/o FKA-30) Taaol 850 PMA-30 Water 1 Non-Volatile V Aa req'd for riae. 4.5 to 5.53 normal 0.7 to 1003 N. V. 2.03 2.53 Pounda-2000 Lba. K. T. 280 to 300 approx. 90 to 110 approx. 14 1500 approx. 40 83.3 3 to 4 aa req'd 1 160 to 162 gal. approx, for regular viscosity | * Gypsum to uae Stonellte, Per FMS 6-24-2 for Pigmented Ready Nix, and //9NCS, per IMS 6-24-9, for 'White Ready Mix. RAW MATERIALS Per Bulletin 61-2-24-2 plus: Taaol 850 C Haaaeo 267 HIS 6-177-9 PMS 6-12U-11 MANUFACTURING PRCCSDURS General procedures as per Bulletin 61-2-42-2. Note: 1. Add Taaol 850 to water and eoulsion and mix before adding dry ingredients. - 2. Zf PMA-30 ia normally added to the eoulsion in bulk, extra IMA-30 will be neoeaaary ainee the aaount of eonilalon haa been reduced. Thia extra preservative should be added to the water/eaulaion prnix. arc Iq p o c q 0 *** M-8971-0 Rev. 9/65 (Printed in U.S.A.) C Indicates Chanre l.- *" / SPECIAL BULLETIN Operating Division PRODUCT PROCEDURE ^BPro^ad: READY-MIXED JOINT COMPOUNDALL PURPOSE (JE-68UF) No. 61-2-24-AA Date 4-20-70 Page 1 Cancels Page 1 Dated 3-3-70 ' This bulletin expires 3-1-71. DESCRIPTION Gypsub to Manufacture Ready-Mixed Joint Co^ound - All Purpose end ship on til orders unless otherwise specified or authorised hy Chicago #971-E. MANUFACTURING PUNT C Gypsua Dd Midway IDENTIFICATION AND PACKAGING C Packaging per Bulletin 61-2-2U. 0P009 1091 M-8971 Rev. 1/63 (Printed in U.S.A.) C Indicates Change SPECIAL S3U2TH CONFIDENTIALOperating Diviaion Mo e Data --O--O A A 4-20-70 C PRODUCT FBOCZDUBS DO DOT RCPRODUCC 00 DOPY BEADT-MIZED J01HT COHFOUND - Fan 3 Caneela Page 3 Approved: ALL PURPOSE (JS-684A) Dated 3-3-70" ' FORMULA Mice JC c _ FC7RF9 iibwtoi c Mathocel 65 HB Carbonate Filler* Bamoo 267 BI4386 (w/o HU-30) Taaol 850 FMA-30 Water - 4.0* ____ ~0.8i . *to 100* I. . 20 2.531 Pounria-2000 Lba. K. T. 280 to 300 approx, - 80 ^loo 40 83.3 3 to 4 aa req'd 1 160 to 162 pal. approx, for regular vieooeity * Gypeun to nae Stonallte, Far FKS 6-24-2 for Plgnantail Bandy Mix, and #9HCS, par IMS 6-24-9, for White Bandy Kix. wmrnws Far Bollatln 61-2-24-2 plant 1 850 ,co 267 .MS 6-177-9_ FMS 6-124-~ll` MIHUPACTURIHG PB0CBPRB General proeedurea aa par Ball atIn 61-2-42-2. Bote: 1. Add Taaol 850 to water and emlaian and nix before dry lngredianta. If R1U30 la normlly added to the Million In bulk, extra FMA-30 will be neoeaaary ainea the aaount of mlalcn baa bean reduced. Thia extra preaerrative ahould be added to the water/aauleion praaix. OP009 1053 EHD c H-6971rC Bor. 9/65 (Printed In U.S.A.) C Indleataa Change Orielpally laiugd 3-3-70 SPECIAL BULLETIN Operating Division NO. 61-2-2U-DD READY-MIXED JOINT COMPOUND-ALL PURPOSE Date 5-11-70 c PRODUCT PROCEDURE . Approved: (JE-T74D) CHAMBLEE AND DALLAS Page Cancels Page 1 Dated 3-3-70 This bulletin expires 3-1-71. DESCRIPTION - Dallas to manufacture and ship Ready Mixed Joint Conpound - All Purpose JE-774D on all orders into both the Central and Southern Divisions unless otherwise specified or authorized by Chicago #971-E or Atlanta #961. Chanblee to aanufacture and ship JE-774D for field trials and initial shlpnents as directed by Atlanta #981. MANUFACTURING PLANTS - Dallas and Chanblee. IDENTIFICATION AND PACKAGING - Packaging for Dallas per 61-2-24-2-1 and Chanblee per 61-2-24-1. Letter "K" to follow code on all production. FINISHED PRODUCT SPECIFICATIONS - Dallas Chanblee A. Viscosity Extra Heavy Heavy Regular Marek Anes 700 to 750 BB 575 to 625 BB. 450 to 500 BB 400 to 450 SB 800 to 850 BB 700 to 750 BB 600 to 650 BB 425 to 475 BB All viscosities run using VC-3 Brabender, pin paddle. % 75 rpn with 250 en torque head. B. Bond - 4 mininun at 75F - 50? IH. C. Color (Chanblee) White unless ordered pignented. (Dallas) Unpignented only. D. pH - 8.9 to 9.2. - 0- 3P009 1017 ooo e M-8971 Rev. 1/63 (Printed in U.S.A.) c Indicates Change Operating Division PRODUCT PROCEDURE Approved: SPECIAL BDLLETU CONFIDENTIAL No. Date DO DOT RCPRO0UCS OR COPY Pace 6i-- 5-11-70 2 READY-MIXED JOINT COMPOUND-ALL PURPOSE Cancels Page 2 (JE-771D) - CHAMBLEE AND DALLAS Dated 3-3-70 FORMULA * NonVolatile Pounds 2000 lbs. H.V. Mica JC Asbestos JMRF02 Methocel 65HG #9NCS Carbonate Filler Hanaco 267 Huber Clay Nopco PD-1 PML386 (w/o PMA-30) CMP Acetate Iroyaan 17b RAW MATERIALS Formula y as reg'd for vise. .7 to 100* lt.V. 2.0 2.5 .3 2.5 - 280 to 300 approx. 60 to 70 approx. lb lb50 approx. bO 50 6 83.3 approx. 1- .1 Per Bulletin 61-2-21* except: Hanaco 267 Per PMS 6-121-11 HmjrkcrJt^?%$Eb\m*T *** 6*100-1^ General procedure as 61-2-21*. UOTE: 1. Add defoaaer and the tvo preservatives to water and enulslon and before adding drjr ingredients. t i O l bOOdO END M-897L-C Rev. 9/65 (Printed in U.S.A.) C Indicates Change A Indicates Addition D Indicates Deletion .X No. 61-2-24-AA Date Page 5-15-70 2 Cancels Page 2 Dated 3-3-70 READY-MIXED JOINT COMPOUND - ALL PURPOSE (JE-684F) FINISHED PRODUCT SPECIFICATIONS C A. Viscosity C Regular Extra Mechanical Tools Gypsum 630 30 BB 700 30 BB ^30 39 BB All viscosities run using VC-3 Brabender, pin paddle, T5 RPM 250 cm. ga. torque bead. B. Bond - k ainiaua. Tested as per Bulletin 61-2-2V-2. C. Color - White or plgaented. To aateh standards. 0. Application k Dry- To aateh plant standards. Ho grit or luops in Appearance application. No cracking on bond test panel. Testing as per Bulletin 61-2-24-2. E. Weight Per Gallon 12.5 to 12.8 lbs. per gal. for regular viscosity material. -0- 4* l 600dL 1 l I X-8971 (Back) C Indicates Change Operating Division PRODUCT FR0CZDUR2 Approved: ...... SPECIAL BULLETIN so ot otcmtooucc o copy READY-MIXED JOINT COMPOUND ALL FUSFCSE (JS-684A) No. 61--2--24--AA Date ' 5-15-7C Paee 3 Cancels _ Page 3 Dated 4-20-70 FORMULA Mica JC FC7RJ9 Asbestos Mathocel 65 BG Carbonate Filler* Hanaco 267 FX4386 (w/o FMA-30) Taaol 850 PKA-30 Water % Non-Volatile V 4.0> 0.8* to 1003 N. V. 2.03 2.53 Poanda-2000 Lbs. IT. V. 280 to 300 apprac. 00 16 1500 apprac. 40 83.3 3 to 4 aa raq'd 1 160 to 162 gal. approx, for regular viaeoaity } * Gypaua to uae Stoaellte, Par FMS 6-24-2 for Pigmented Heady Mix, and y9NCS, C per FMS 6-24-9, for White Heady Mix. MLdwey to uae felacy #3. RAW MATERIALS Per Bulletin 61-2-24-2 plua: Taaol 850 Baaaeo 267 PMS 6-177-9 pmS 6-124-11 MANUFACTURING PROCEDURE C General procedures as per Bulletin 61-2-24. Note: 1. Add Taaol 350 to water and eaulaion and aix before adding dry ingredients. 2. If FMA-30 is normally added to the anulaion in bulk, extra FMA-30 will be necessary since the aaount of esulsion has been reduced. This extra preservative should be added to the water/emulsion preaix. 2JD 1 OGGI GOOdU X-C9TL-C Rev. 9/65 (Printed la U.S.A.) C Indicates Change Operating Division product i accsaiaa Approved: SPECIAL BULLETIN COMFiSSNTiAL 80 MOT XCPRODUCC Oft COPY ALn.JY-MI.C42 JOINT CCKrCUNJ ALL FUHFCS3 (JS-684P) No. 61-2-24-AA Date 5-25-70 Pege 3 Cancels Fare 1 Deted 5-15-70 i j TO.'CTO,.'. Mica JC PC7RP9 Asbestos Mathoeel 65 HG Carbonate Filler* Haaaeo 267 FM4386 (v/o FMa-30) Taaol 850 FMA-30 Water 1 Non-Volatile V 4. Out 0-8* to 100,? N. V. 2.01 2.5,* ---- Pounds-2000 Lbs. II. V, 280 to 300 approx. 80 16 1500 approx. 40 83.3 3 to 4 as req'd 1 160 to 162 ftl. appro: regular viscosity Gypsum to use Stonellte, Per FKS 6-24-2 for Pigaented Heady Mix, aod ./9NCS, per IMS 6-24-9, for White Heady Mix. Midway to use Quincy #3. RAW MATERIALS Fer Bulletin 61-2-24-2 plus: Taaol 850 Haaaeo 267 PMS 6-177-9 pms 6-124-n manufacturing iaccam General procedures as per Bulletin 61-2-24. Note: 1. Add Taaol 350 to water and eaulsion and six before adding dT7 ingredients. 2. If FMA-30 is noraally added to the emulsion in bulk, extra * xKA-30 will be necessary since the amount of emulsion has been reduced. This extra preservative should be added to the water/eaulsion preoix. JID OPO09 1047 M-897L-C H*v. 9/65 (Printed in U.S.A.) C Indicates Change Operating Division PRODUCT PROCEDURE . Approved: special Bourrn CONFIDENTIAL DO DOT DSFDOOUOC 01 DOFY READY-MIXED all purpose joist com- pouhd-cf sours GATE No. 61-2-24-4-B Date Paae 5-2E-70 2 Cancels Page 2 Dated l-?n_70 PORMJLA (JE-684?) * Bon-Volatile Pouada-2000 ILa. H.V. Mica JC 7 UCC 210 Standard grade Asbestos As required for Mrthocel 65 vise. 3* normal 0.8i MW-325 Buaco 267 . *To 100* B.V. 20 FM4366 (v/o PMA-30) 2.5* Tool 890 c 'Troysan CMP acetate (liquid) A Troysan IT1* Water RAW MATERIALS 280 to 300 approx. 60 approx. - 16 1500 aprox. 40 83-3 3 1 2 l6n to 162 gal. approx, for regular viscosity. Per Bulletin 61-2-24-4 plus; Taaol 850 Bamaco 267 IMS 6-177-9 A.E. Staley Mfg. Co., Decatur, 111. MABU7ACTURIBG PROCEDURE General procedure as per Bulletin 61-2-24-4. BOTE: 1 Add Taaol 850 to water and eutlsion and mix before adding dry ingredients. .2 If PMA-30 is normally added to the emulsion in bulk extra PMA-30 will be necessary since the amount of emulsion has been reduced. This extra preservative should be added to the vater/emulalon premix. tL L I bOOdG EHD I-A97L-C Rev. 9/65 (Printed in U.S.A.) C. TfllMpatM HlBMpd Cperating DivisionPRODUCT PROCEDURE Approved s CONFIDENTIAL N* P oi-2-2**-.4 q DO NOT REPRODUCE OR COPY USG READY MIXED JOINT COMPOUKD Cancels Page 3 Dated 10-22-66 ________ALL PURPOSE: - SOUTH r.ATT_________ FORMULAS A. Formula JE-30bC - Special White and Regular (Tinted) Fillers ? Hon-Volatile (For 250 Gal.) Lbs. (Batch Aggrox.) Mica JC Formula V Astraeal M Sericite 10.0 Asbestos UC210 2.5 (approx.) #b00 Whiting or Marble White 325 To Make 9b? Methocel 65HG 0.8 275 (Approx.) 200 50 To Make 1880 Lbs. 16 Paste Mix 5 Non-Volatile Lbs. (for 250 gal. batch appr.) Fillers VA-301P Troysan CMP acetate (liquid) Troysan 17b Water B. Formula JE-201 9b.0 6.0 - i860 218 1 2 lbs. lbO gallons (approx.) Filler Mix S Non-Volatile Lbs. (For 9b5# Filler Charae) Mica JC MTO-50 Asbestos Floats Huber Clay Methocel HG Ferrite Yellow* *00 Whiting or Marble White 325 Formula V 150 approx. 30.0 300 As Reo'd. io.o 35 approx. 100 0.8 8 To match aanila color of SHEETROCK Face Paper. To make 9b. 5? To make up 9b5 lbs. * Plant to Manufacture unpigmented form when reauested by Sales Dept. Paste Mix 5 Ron-Volatile Lbs. (for approx. 130 <ral.) Fillers VA-301P Troysan CMP acetate (liquid) Troysan 17b Water 9b.5 5.5 - 9b 5 96 b ox. 8 ox. 71 gal. approx. 0PC09 172? rewwrym (Priniad in p.sxj------------------------------------------------------------------------------------ C Indicates Change A Indicates Addition No. Date Page Cancels Dated 61-2-24-4 5-2E-70 Page 1.30-66 CONFIDENTIAL DO NOT REPRODUCE OR COPY tz use READY-MIXED J0I1.T COttPOUIlD ALL PURPOSE - SOUTH GATE HAW MATERIALS VA-301P Hethocel HG P80F Mica Ser-X Asbeatos #400 Whiting or Marble White 325 Stonelite Nuodex PMA-16 D Huber CWF Clay M350 and ffTO-50 Sericite A Dolomite Astracal M Sericite A Troysan CMP Acetate (Liquid) A Troysan 174 Per BIS Bulletin Per Bulletin Per PMS Bulletin 6-104-55 6-25-6 6-143-1 6-146-2 6-14-5 6-24-1 6-24-2 6-100-2 6-36-5 6-146-2 58-2-2 6-146-2 6-100-5 6-100-14 C ( OP009 1711 r=W5>i-S (BadcT 0 Indicates Deletion A Indicates Addition t Operating Division PRODUCT 2ROCEDQRE . Approved: SPECIAL BOLLETDI CONFIDENTIAL DO DOT RKPRODUCI OR COPT READI-KlXKD JOUn? COMPOUND ALL PURPOSE (JB-684?) No. 61-2-24-AA Date Paee 6-8-70 3 Cancels Fags 3 _ Dated 1- TOHMOLA Mloe JC , PC7HT9 Astestos J ' k Mstboeel 65 BB Oerbonete Tiller* Beaeeo 267 n*386 (*/o PKA-30) TUnol 890 C CMP Acetate A Troysan 174 Water. 6 Hon-Volatile ' V * As rag'd for vise. 4.5 to 5.55 0.7 to 2005 X. 7. 2.06 2.56 Pouada-2000 Lbs. 1. T. 280 to 300 approx. 90 to 1X0 approx. - - .T 14. -v '' ' 1500 approx. v ,* . 40 83.3 ' 3 to 4 as rag'd .1 1 1 X60 to 162 gal. approx, for regular viscosity , :i.' *.*} 1* ,S ... y 7*/- :T- * Qypeua to use Stonalite, par PMB 6-24-2 for Pigaented Beady Mix, and #9BCS, par FK3 6-24-9, for White Beady Mix. RAW MA3ERIALS . : .v Per Bulletin 61-2-24-2 plus: .JfrA;. . ;r .* laaol 890 Bsaeoo 267 A CMP Aeatate A 17* IMS 6-177-9 IMS 6-124-11 FNS 6-100-5 PMB 6-100-14 MABURAC1URH0 TBOCBIOHE: General procedures as per Bulletin 61-2-42-2. C otet 1. Add Taeol 890 and the two preservatives to the water and eeulsien and nix before adding dry ingredients. D *1 ^. $V ^___ H-Oy7^ Rev. 9/65 (Printed in U.S.A. ) C Tndlaatee Qianae - ^-- ... .^v A indicates Additlan^D indicates Deletion ^^3, ooo Operating DiriBion PRODUCT WOCEDURE Approved: special mum CONFIDENTIAL 00 HOT RCRflOOVCC OR COPY RSADT-MDOSD JOIST CCMPCCHD-ALL HJRPOSE (JE-774D) - CEAKBLEZ AHD DAIiAS No. 61-2-24-DD Date 6-15-70 Paw 2___________ Cue*la Pag* 2 Dated 5-11-70 FORMULA t 8" Volatile Pouada 8000 lba. S.V. Klee JC Aabeetoa JMRVQfi Mrtbocal 65HD #9BCS Carbonate PUler Bueeo 867 Baber Clay Bopeo n>-l PM386 (v/o PHA-30) CMP Acetate Troyean 174 Formula V aa rag'd for nac. .8 to 100* B.V. 2.0 2.5 .15 2.5 880 to 300 approx. 80 to 90 approx. 16 14J0 approx. 40 50 3 83.3 approx. 1 1 RAV HABRIALS Par Bulletin 61-2-24 except: Baaaco 267 Bopco JD-1 CMP Acetate Troyeaa 174 Per IMS 6-124-11 Bopco Chemical Co. Per PMB 6-100-5 Per PMB 6-100-14 MAHOPACTORIBO PROCEDORE General procedure aa 61-2-24. NOTE: 1. Add Bopco PD-1 and tba two preaarratlras to wttr tad emulaion tad adjc before adding dry lagredleata. M-fl97J^C Rev. 9/65 (Printed In U.S.A.) C ladleatea Change oo'0 > o JO C* / *J Operating Division PRODUCT PROCEDURE . Approved: SPECIAL SCLIZm CONFIDENTIAL DO MOT MCFROOUOK OR CORY READY-MIXED JOUIT COMPOUND AIL PURPOSE (JB-684?) No. 61-2-24-AA Date Pare 6-18-70 3 Cane*la ____ Dated 6-6-70 | POHMOLA < Boo-Volatile Pounda-aOQO Lba. H. y. Mica JC PC7RP9 Albertos V 4.0* . 280 to 300 approx. 80 Metbocel 65 BB Carbonate Pillar* Baeeco 867 PM4386 (y/o IMA-30) Tfeaol 850 CMP Aeatata fcoyesn 174 Uttar 0.8 . *to 100* K. V. 20 2.5* 16 1500 approx, to 83.3 3 to k aa req'd 1 1 160 to 162 pal. approx, for regular viscosity Qjrpaun to uae Stonelite, per P*6 6-24-2 for Pi^ented Ready Mix, and #9RCS. par PW 6-24-9, for White Ready HU* Mldmy to uae ftilncy #3. RAW MATERIALS Per Bulletin 61-2-24-2 plus; Waal 850 Baaaeo 267 CMP Acetate Woysan 174 PMS 6-177-9 PMS 6-124-11 PMS 6-100-5 PMS 6-100-14 mabop-acturuk; procedure General proeeduree aa per Bulletin 61-2-24. Bote: 1. Add TUaOl 850 and the two preservative! to the water and eaulalon and nix before adding dry Ingredients. 01 bOOdO END M-0971-C Rev. 9/65 (Printed in U.S.A.) C Indicates Change Operating Division PRODUCT PROCEDURE Approved: special bulletin CONFIDENTIAL JAffiiLK fJE-77kD) - CHAMBLEE AMD DALLAS Nol 61-2-2WDD Date 11-9-70 Page 2 Cancels Page 2 Dated 6-15-70 FORMULA Mies JC -Asbestos JMRF02 Methocel 6$EG #9NCS Carbonate Filler Bamaco 267 Buber Clay Defoamer* PM-4386 (v/o PMA-30) CMP Acetate Troysan 174 RAW MATERIALS Per Bulletin 61-2-24 except; % BonVolatile Formula V as req'd for vise. .8 to IDO* N. V. 2.0 2.5 .15 2.5 m Pounds 2000 lbs. N. V. 280 to 300 approx. 80 to 90 approx. 16 1430 approx. 40 50 3 83.3 approx. 1 1 Bamaco 267 Sopeo PD-1 CMP Acetate Troysan 174 TSfflol 850 Per FC 6-124-11 Bopeo Chemical Co. Per PMS 6-100-5 Per PMS 6-100-14 Per ms 6-177-9 MAHUFACTORIWG PROCEDURE C General procedure as 61-2-24 except add CMP Acetate and Trojrsan 174 separately instead of mixing the two preservatives together- When mixed together in con centrated font and allowed to stand, some of the mercury is precipitated from solution. C NOTE: 1. Add Ropco PD-1 or *Tamol 850 and the two preservatives to the water and emulsion and mix before adding dry Ingredients. A 2. Dallas to add *Tanol 850, Chamblee to add *Nopco PD-1. 3P009 1015 END 0-4971-C i/68 (Printed in U.S.A.) 7 Indicator Change Irdic?tir Acdl'jicn / ut i.ginxj.y issued Operating division PRODUCT PROCEDURE Approved: iu ar&'.jJUi auiuicmxi CONFIDENTIAL (JE-774D) - CHAMBLEE AND DALLAS No. 61-2-Db-ao Date U-6-72 tan. 1 Cancels Page 1 Deted 2-18-71 This bulletin expiree 3-1-73. DESCRIPTION - Delias to manufacture and ship Reedy Mixed Joint Conpound All Purpose JE-774D on ell orders into both the Centre! end Southern Divisions unless otherwise specified or authorized by Chicago #971-2 or Atlanta #981. Chenblee to aaaufecture end ship JE-774D for field trials and initial shipments as directed by Atlanta #981. MANUFACTURING PLANTS - Dallas and Chenblee IDENTIFICATION AND PACKAGING - Packaging for Dallas per 61-2-24-2-1 and Chaablee per 61-2-24-1. Letter "K" to follow code on all production. FINISHED PRODUCT SPECIFICATIONS - Dallas Chaablee A. Viscosity Extra Heavy Heavy Regular Merck Asms 700 to 750 BB 575 to 625 BB U50 to 500 BB 400 to 1*50 BB 800 to 850 BB 700 to 750 BB 600 to 650 BB 425 to 475 BB All viscosities run using VC-3 Brabendar, pin paddle, 9 75 rpa with 250 ca torque head. B. Bond - 4 nrinlwun at 75F - 502 RH. C. Color (Chaablee) White unless ordered pignented. (Dallas) Uspignented only. D. pH - 8.9 to 9.2 i V 9 1 bOOdU (C) 1972 iisTTgp states G77SUM. UNAUTHORIZED USS OR REPRODUCTION PROHIBITED. 0-5791-C 1/68 (Printed in U.S.A.J T C Indicates Change r~~ No. Date -" 61-2-21*-AA 6-20-72 Cancels Reinstatement Dated CONFIDENTIAL READI-MIXED JOINT COMPOUND ALL PURPOSE - (JE-6BUF) FINISHED PRODUCT SPECIFICATIONS A. Viscosity - Regular Extra Mechanical Tools 630 30 BB TOO 30 BB *30 30 BB All viscosities run using VC-3 Brabender, pin paddle, 75 HPM 250 cm. ga. torque bead. B. Bond - U minimus. Tested as per Bulletin 6l-2-2l*-2. C. Color - White or pigmented. To match standards. - Midway to only produce implemented. Pigmented any be specially ordered with 5 days lead time to produce and with approval of the Division Product Manager; these orders Bust he in batch increments of 500 gallons. D. Application A Dry Appearance - To aatcb plant standards. Bo grit or lusps in application. Bo cracking on bond test panel. Testing as per Bulletin 6l-2-2k-2. E. Weight Per Gallon - 12.5 to 12.8 lbs. per gal. for regular viscosity aaterlal. k i d 600dti (C) 1972 UNITED STATES GIPSON. UNAUTHORIZED USE OR REPRODUCTION PROHIBITED. 0-5791-C (flack)T Operating Division PRODUCT PROCEDURE Approved: CONFIDENTIAL No. 61-2-2--AA Date 6-20-72 | i READY-MIXED J0IHT COMPOUND ALL PURPOSE - (JE-68bF) Cancels Reinstateaer.t Dated FORMULA 5 Han-Volatile Pounds-2000 Lbs. I. V. Mica JC PC7RF9 Asbestos Methocel 65 HG Carbonate Filler* Haaaco 267 PMb386 (v/o PMA-30) Taaol 850 CMP Acetate Troysan 17b Water V 3.05 0.8 to 1005 0. V. 2.05 2.55 -- 280 to 300 approx. 60 16 1500 approx. bo 83.3 3 to b as req'd. 1 1 160 to 162 gal. approx, regular viscosity Carbonate Filler to be Stonelite for pigmented product end for "one" in natural color. White to be 905 #9HCS and 105 Stonelite Filler. i i I l i RAW MATERIALS PMb386 Taanl 850 Haaaco 267 CMP Acetate Troyaan 17b Methyl Celluloae Aabeatoa Floata Carbonate Filler PKS 6-10b-55 PMS 6-177-9 PMS 6-12b.ll PMS 6-100-5 PMS 6-100-lb PMS 6-25-6 PMS 6-lb-5 PMS 6-2b-2 (Stonelite). 6-2b-9 (#9NCS) MANUFACTURING PROCEDURE I I General proeedurea aa per Bulletin 6l-2-2b. Rote: 1. Add Taaol 850 and the tvo preservatives to the vater, then eaulsion and i adz before adding dry ingredients. Add dry ingredients and necessary ! vater to keep at fairly heavy consistency. Mix at heavy consistency for 10 adnutes then adjust with vater to proper viscosity. a o end o o <3 O (C) 1972 UPfTED STATES GYPSUM. UHAUTHORIZO USE OR REPRODUCTION PROHIBITED. "0-5791-C 1/68 (Printed in U.S.AJT  t Operating Division PRODUCT PROCEDURE Approved: CONFIDENTIAL No. 61-2-2A-AA Date 9-28-72 READI-MIXED JOIST COMPOUND ALIPPURP06E - (JE-68AF) Cancels Page 3 Dated 6-20-72 FORMULA % loo-Volatile Pounds-2000 lbs. I. V. ffi.ee JC PC7RF9 Asbestos Methocel 65 HC Carbonate Filler* Haaaco 267 PMA386 (v/o PMA-30) Taaol 850 Cosaa 158 Voter V 3.05 0.8 to 1005 I. V. 2.05 2.55 280 to 300 approx. 60 16 1500 approx. Ao 83.3 3 to A as req'd. 2 160 to 162 gal. approx, regular viscosity for Carbonate Filler to be Stooellte for pignsnted produet and for "ones" in natural color. White to be 905 #9SCS and 105 8teoelite Filler. RAV MATERIALS FMA386 Taaol 850- Eaaaeo 267 Methyl Cellulose Asbestos Floats Carbonate Filler PIC 6-10A-55 FMS 6-177-9 PI6 6-12A.ll PMB 6-25-6 FMS 6-1A-5 Pie 6-2A-2 (Stonelite), 6-2A-9 (#9RCS) KAIUFACTURXBG PROCEDURE General procedures as per Bulletin 61-2-2A. ote: 1. Add Taaol 850 and the tvo preservatives to the voter, then eoulaion and aix before adding dry ingredients. Add dry Ingredients and necessary voter to keep at fairly heavy consistency. Mix at heavy consistency for 10 nlnutes then adjust vith voter to proper viscosity. DTD IP 009 1036 (C) 1972 UXXTED STATES GYPSUM. URA0TH0RI2H) USE OR REPR0DUCTI0H PROHIBITED. 0-5791-C 1/68 (Printed in U.S.A.Jfe * Indicates AdditionD Indicates Deletion o o o o n o o no .^finally Issued 3-3-70 SPECIAL BULLETIN 3rd Extension Operating Division PRODUCT PROCEDURE CONFIDENTIAL No. 6l-2-2*-DD Date 3-1-73 Pao 1 READY-MIXED JOINT COMPOUND-ALL PURPOSE Canoels Paco 1 (JE-77UD) - DALLAS Datad l*-6-72 This bulletin expiree 9-1*73. DESCRIPTION - Dallas to manufacture and ship Ready Mixed Joint Compound - All Purpose JE-77fcD on all orders into both the Central and Southern Dirialana unless othervise specified or authorised by Chicago #971-E or Atlanta #961. MANUFACTURING PLANT - Dallas IDENTIFICATION AND PACKAGING - Packaging per 6l-2-2b-2-l. Letter "K" to follow code on all production. FINISHED PRODUCT SPECIFICATIONS - Dallas A. Viscosity - Extra Heavy Heavy 700 to 750 BB Regular 575 to 625 BB March 1*50 to 500 BB Ames 1*00 to 1*50 BB All viscosities run using VC-3 Brebender, pin paddle, 75 rpm with 250 cm torque head. B. Bond - 1* minima at 75F - 505 RH. C. Color - Unpigmented only. D. pH - 8.9 to 9.2 oo J o o o 1973 UNITED STATE8 GYPSUM. UHAOTHORIZED USE OR REPRODUCTION PROHIBITED 0-5791-C Rev. 1/73 (Printed In U.8.A. )T C Indicates Change D Indicates Deletion o 1 Operatlaf Dirlslon PRODUCT PROCEDURE CONFIDENTIAL No. 6l--2--2L--0D Date 3-1-73 Page 2 READY-MIXED JOINT COMPOUND-ALL PURPOSE Cancels Page 2 (JE-mD) - DALLAS Dated 1-2L-73 FORMULA 5 NonVolatile Pounds 2000 lbs. N.V. Mica JC Asbeatoa JMRF02 Methocel 65HG #9NCS Carbonate Filler (Bote 1) Bamaco 267 Buber Clay Defoamer* PM-A3Q6 (w/o PMA-30) Troyaan EX 36k Formula V as req'd. for vise. .8 to 1005 N. V. 2.0 2.5 .15 2.5 280 to 300 approx. 80 to 90 approx. 16 Ib30 Aoproz. bO 50 3 83.3 approx. 2 BOTE 1: Dallaa to use Microfil fit. PAW MATERIALS Per Bulletin 61-2-21* except: D Bamaco 267 C Troyaan EX 361* Tanol 830 Microfil #U Per PMS 6-12U-U Troy Chemical Co. Per PMS 6-177-9 Per PMS 6-2U-10 MABUFACTURIBC PROCEDURE C General procedure as 61-2-21*. c BOTE: 1. Add Taaol 850 and the two preservatives to the water and emulsion and mix before adding dry ingredients. c END UL01 600dL 1973 UNITED STATES STMUi. UBAlfrsnuraEn USX OF REPRODUCTION PROHIBITED. 0-5T91-C Rev. 1/T3 (Printed la U.S.A. )T C Indicate* Change D Indicate* Deletion Operating Division PRODUCT PROCEDURE CONFIDENTIAL READY-MIXED JOINT COMPOUND-ALL PURPOSE (JE-77**D) - DALLAS No. 61-2-24-2-2 Date 3-14-73 Page 2 Cancels NEW Dated PORMUI^ f HonVolatile Pounds 2000 lba. N.V. Mica JC Asbestos JMRF02 Hethocel 65HG Mierofll #** Carbonate Filler Hamaco 267 Huber Clay Tamol 650 PM-A386 (v/o PMA-30) Troys an EX 36** Formula V as req'd. for vise. .6 to 1005 N.V. 2.0 2.5 .15 2.5 260 to 300 approx. 80 to 90 approx. 16 1*30 approx. 40 50 3 83.3 approx. 2 RAV MATERIALS Per Bulletin 61-2-2** except: Hamaco 267 Troysan EX 36** Tamol 850 Microfil #** Per PMS 6-124-11 Troy Chemical Co. Per PMS 6-177-9 Per PMS 6-2**-10 MANUFACTURING PROCEDURE General procedure as 61-2-2**. NOTE: 1. Add Taaol 650 and the tvo preservatives to the water and emulsion and mix before adding dry ingredients. C C ENG *1 9 1 bOOdli 19T3 UNITED STATES SXPSUM. UEADTHOJUZED USE OR HEPHOOUCTIOS PROHIBITED. 0-5791-C Rev. 1/73 {Printed laU.S.A.h' Operating Division PRODUCT PROCEDURE DESCRIPTION CONFIDENTIAL READY-MIXED JOIST COMPOUND-ALL PURPOSE JS-1128C - DALLAS Ho. 61-2-2*--2-2 Date 7-31-73 ? 1 Cancels Page 1 Dated 3-1A-73 An ulsinn based product containing tvo-thlrds the noival anount of nice in conjunction vltb DZV Minerallte to alleviate current nice shortage. HANPFACTURIJO PLANT Dallas IDENTIFICATION AND PACKAGING Par Bulletin 61--2--2A--2--1. FINISHED PRODUCT SPECIPICATIOHS Viscosity - 600 * 30 Brabender units vlth pin paddle at 77F. Color - Natural unless pignsntsd specified. Bond-to-Tape - 5 nlnlnta at 77F. - 50? RH. Weight par gallon - 12.8 to 13.0 lbs. par gallon. RAW MATERIAL NO. FORMULA ? N.V. LBS. PER 250 CAL. 617*7 61762 617*1 66*61 61*66 65272 66660 66685 RAW MATERIALS P-60F DXW Minerallte TRF02 Asbestos Methocel 65BG Microfill #* FM-A386 (60?) CMP Acetate Troysan 17* 2/3 fotsula V 15.0? . ?3.5 to *.0? 08 To nake 9*.5? 5.5 approx. 200 300 70 to 80 16 To sake 1,890 lbs. 183 1 1 81762 DXW Minerallte Per PIC 6-l*6-2 Other rav naterials per Bulletin 6l-2-2*-2-l. 66660 ' CMP Aeetste Per Pie 6-100-5 END 0PP09 I6 n 1973 UNITS) STATES GYPSUM. UEAPTH0R22SD USE OR igPRODUCTICN PROEXBITZD. 0-5791-C Rav. 1/73 (Printed In U.S.A. )T G2SBML REVISION