Document 0qwkeRrjgBGJrDkbpzyQ00qpO
THE LABOBATOKT IS 1945
THE LABORATORY IN 1945
In 1945, the element of time seemed to be the one most Important factor in laboratory formulation. As one raw material crisis followed another, substitute formulas had to be developed rapidly in order to keep production moving. Every job was done against time and every day brought a new reformulation deadline. The jobs were done, the deadlines were met and our factories kept producing -- at least to the extent permitted by raw material restrictions.
Early in the war, when restrictions were still a novelty, one chemist remarked that paint could always be made from rosin and linseed oil -- no matter what happened. The year 1945 proved this prediction to be wrong for even rosin and linseed oil became formulating luxuries denied or restricted except for military use. By midyear, the raw material cupboard was bare. Each substitute had been examined, put into use and then discarded as It went on allocation. The European war ended just in time to prevent a complete breakdown in civilian paint quality.
Bad raw material news started January 1, 1945, with an oil quota reduction from 60% to 50%. On January 31, 1945, a 30-day Inventory restriction was imposed on the purchase of linseed oil thus forcing us to discontinue certain special oils purchased in small quan tities. In Maroh, the oil quota was reduced again, this time to 40%. During the first quarter of 1945, a considerable amount of laboratory work was devoted to the replacement of reportable linseed oil with China wood oil. As a result, "61" Floor Yarn!ah, "61" Floor & Porch Enamel, "61" Spar Varnish and seVeral other listed items were materially improved but only at the expense of profit. The cost Increase resulting from these changes averaged thirteen oents per gallon. In July, castor oil was placed under allocation and China wood oil was restricted. The restrictions on castor and China wood oils ended with Y-J Day, and in October, the oil quota was raised to 75%.
The restrictions and complications affecting drying oils resulted in laboratory expenditures which amounted to $1040. Among the many relief measures which were investigated was the use of fish oil in house paint. Fish oil formulas were set up but were held in abeyance for a last stand in the event that/ oil conditions became worse. It never became necessary to adopt these formulas.
The restrictions on rosin and rosin derivatives had a more damaging effect on quality and profit than any wartime raw material restric tion. Rumors of rosin restrictions were widespread before Order M340 was issued on February 6, 1945* This order was merely the entering wedge and provided nothing more than a tool for honoring preferred orders. It was succeeded by WPB Order M387 on
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February 28, 1945, whioh limited the consumption of rosin (as such and in its derivatives) to 30# of the usage in the corresponding period in 1944. Since all other widely used varnish resins had already become unobtainable, the rosin order was a heartbreaking blow* It immediately became necessary to revamp most of our industrial and trade sales finishes to reduce rosin consumption.
Our first step toward meeting this situation was the wholesale use of Picoolyte, a rosin-free terpene resin. Fiooolyte oost us 20-1/2 cents per pound -- three times as much as rosin and twice as much as ester gum -- and cost Increases in the order of ten cents per gallon Immediately took place in our finished products. Hardly a month had passed before Picoolyte shortages developed and by the end of April, Picoolyte was so scarce that it had to be taken out of all products except "61" Enamel White Gloss and "61" Q. D. Enamel White. In July, Picoolyte went on allocation.
In the meantime, we had turned our attention to another rosin-free resin, Velsicol, a petroleum derivative. Under normal conditions, Yelsicol would have been (and now is) a drug on the market for it was exorbitantly priced at 18-1/2 cents per pound and it was almost pitch black In color. In spite of these drawbacks, we were eager to buy carload quantities and soon had it in the bulk of our trade sales items. The best evidence of the fallacious value set on Velsicol is that it dropped 25# in coat as soon as rosin again became available.
During 1945, we consumed 30 tons of Picoolyte and 55 tons of Velsicol in the manufacture of 200,000 gallons of enamels, primers and undercoatings which we would not otherwise have made. Ho sales difficulties arose from the use of these two rosin substitutes.
One place in which we had consumed large quantities of rosin in the past was in the production of driers for our own as well as subsidiary company use. In 1944, approximately 42 tons of rosin and 10r000 gallons of oil went into these driers. The merits of purchased driers vs. driers of our own manufacture had been debated over a period of years but debating ended when the rosin situation forced us to take aotion. The changeover to purchased tall oil driers will save us about $8500 during the 12-month period follow ing the move. When we adopt naphthenate driers, which are again available and which are superior to tall oil driers, the annual saving will shrink to about $7000. A part of these savings repre sents the freight charges on driers heretofore made at Buffalo and shipped to the subsidiaries. Under the present plan, the subsidi aries are making their own driers from locally purchased drier concentrates. The Buffalo faotory has lost about 45,000 gallons of production as a result of this move, but the company as a whole has benefitted. The feeling of security fostered by 45,000 gallons of production may have been an expensive form of insurance.
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g
Bos in restrictions as a whole cost the ooapany #5410 in laboratory work. What they cost in profits due to the use of more expensive resins is a matter of guess, but it is probable that another #5000 was spent in this way.
In addition to oil and rosin problems, 1945 ushered In WPB Order M384 on lead chemicals which limited our use of lead carbonate to about one-third of our prior usage. This order was a major blow to subsidiary company production but it had no effect on Buffalo production. Little laboratory work was involved, other than the development of a new house paint white (No. 5 Exterior White) which was produced until Ootober when lead restrictions ended.
In the industrial field, one other raw material led to considerable reformulating work in 1945 and that was alkyd resin. In February, the phthalio anhydride content was reduoed by government order in all types of alkyd finishes including even military coatings. This required some very rapid formula juggling in order to produce contracted materials on time and with the reduoed volume of alkyd that was allocated each month. Out of this situation came a multi tude of non-phthalic alkyd coatings, some of which won a permanent place in industrial finishes. Wc developed a not too successful non-phthalic alkyd from azelaic acid and used it in a limited way in wrinkle finishes. The limitations on phthalio anhydride served one useful purpose in that they proved conclusively that positive drying, durable production finishes could be made only with a fairly high phthalio anhydride oontent. Reformulating work involv ing alkyd finishes cost us $2610 in 1945.
A multitude of minor raw material problems demanded a great deal of laboratory time in 1945. The raw materials involved were iron oxide, magnesium silicate (Asbestine), dlatomaoeous earth (Cellte), chrome pigments, organio colors and titanium dioxide.
In the aggregate, about #10,000 was spent in 1945 by the laboratory in raw material work, the sole purpose of which was ter keep pro duction moving. Moat of this work was technically unprof itable for it added little permanently useful knowledge. The conditions necessitating this work were short-liv8d. In all, 339 formula changes (exclusive of changes due to driers) were made in the 187 items listed in Temporary Price Schedule No. 119-T. In 1944, 306 changes were made in the then active 204 item price list.
General Research
The most outstanding single laboratory development in 1945 was a process for making alkyd rssins direotly from oils. Heretofore, we have made alkyds from the fatty adds of oils, since vegetable oils (except tung oil) have not readily combined with glycerine and
phthalio anhydride. A technique whereby alkyds can be made directly
from oil by a method known as alcoholysis was successfully worked out and put into use in 1945. Future savings of at least #10,000 per year should result from the prooees and will reach a peak after our new alkyd equipment is In operation.
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Trade Sales Developments
Formulas for virtually all of the proposed postwar finishes have now been established. These include the new Vitrallte Enamels and Undercoating, Sffeeto, Lyt-all Flowing Flat and Stippling Eggshell, Verdure Trim & Shutter Finish, House Paint, and "6l" Floor & Porch Enamel. The major effort is now being devoted to the transporta tion line.
Approximately $11,500 was spent on postwar development work in 1945.
Industrial Finishes
About half of the work done for the Industrial Sales Department in 1945 was confined to the following fields:
Industry, Type finish or Work
Total num ber problems
Dollar valt laboratory
Government Specifications (mostly aircraft)
Cloth and Textile Coatings
Wrinkle Finishes Army and Navy Inspection
Testing Electrical Fixtures and
Equipment Metal Decorating Collapsible Tube Coatings Casket Finishes
Paper Coatings
85 67 133
95
33 62 33 19
8
$ 5074 2975 2002
1293
1220 1132
975 , 523
410
Totals
540 $ 15,614
In past years, work on zinc chromate primer demanded a considerable part of the laboratory's time. Our troubles in this field were as numerous in 1945 as in preceding years, but the end of the war abruptly ended the demand for primer as well as for laboratory work
Only $832 was spent on zinc chromate primer work in 1945 whereas $8651 had been spent in the previous three years. Production like wise dropped. 29,500 gallons were produced in 1945 in comparison with a production of 47*150 gallons in 1944. During the entire war period, our company made 191*650 gallons of zinc chromate primer.
A very considerable amount of time and money was spent on other
aircraft specification items, most of which involved lacquer or synthetic enamel coatings. On one specification Job (A9-L 29* Lacquer Cellulose Nitrate) nineteen different colors were developed
and submitted for test. Insofar as can be determined, little, if any, business resulted from most of this work.
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One unusual aircraft coating developed in 1945 was a finish for the inside of aircraft engines (goods K920). This coating had to withstand the exceedingly high operating temperatures Inside engines as well as salt water, hot oil, etc.
In the cloth and textile field, a large amount of work continued to come into the laboratory even though Ur. Avallone's association with the company ended early In 1945. Probably the most interesting new development in 1945 was a solventless coating capable of appli cation at greater film thickness than any previously available solution type coating. Samples submitted to cloth ooaters have been very favorably received but no business has so far resulted.
The very fast baking postwar wrinkle finishes developed in 1944 are now being regularly supplied to several accounts. A novelty type wrinkle was oreated in 1945 under the name Blpplesoent finish. Blpplescent Finishes are clear wrinkles containing traces of color. When applied on polished metal, effects simulating gold, copper, brass and silver are obtained. In 1945* 40,290 gallons of all types of wrinkle finishes were produced. This gallonage represents a considerable shrinkage from the previous year's production of 60,000 gallons.
In the electrical field, several new products met with considerable success. A baking aluminum finish for flourescent' lighting fixtures (K7443) resulted in sales of 5500 gallons during the last six months of 1945. Two gray baking enamels (K7467 and K7474) were adopted by Western Electric Co. in 1945 and led to orders totaling 7500 gallons. A wide variety of finishes were developed for the liarkel Electric Co. ranging from a parchment finish for paper lamp shades to a plastic sealing compound for oases containing radar equipment. Much time and effort was spent on fungus resistant coatings for electrical equipment used in the tropics but the sudden termination of war ended interest in these coatings.
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In the metal decorating field, we have been engaged in improving the sanitary lacquers used on the Interior of caps and cans in order to make them more resistant to chemical agents and to forming. Better adhering sizes for tin and terns plate are being developed. Expanded use of vinyls and alkyds is being Investigated.
Delivery of a roller coating machine which was ordered in 1944 for testing metal decorating finishes has been delayed for a multitude of reasons but is being promised monthly. The punch press and knurling and threading equipment also ordered in 1944 have been recently Installed and the press is now in use. The knurling equipment lacks a special die which has not yet been received.
Three unusual tube coatings were developed in 1945. One was a quick bake enamel (GU17) curing la one minute at 350F. Conventional enamels require from 30 minutes to one hour at 150 - 180F to bake. A lacquer (79-555) was also produced. Both of these developments were aimed at faster production which means lower production costs for the tube manufacturer. The third development was an extremely
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resistant white tube ooating (028681). Tube manufacturers state that this is the most alkali resistant ooating they have ever examined and that it will eliminate the need for a final ooating of clear lacquer which has heretofore been used to obtain maximum, resistance.
A washing machine enamel (1296) was developed In 1945 and has met the production tests of one manufacturer.
New faster baking enamels were developed for Talon fasteners in place of prewar enamels which required a two-hour bake.
4300 gallons of a black primer (0215) was sold to Royal Typewriter in November and December 1945 for use on typewriter bases. This
product was similar to an enamel developed for aireraft engine
baffles and is one wartime development that has been utilized for peacetime purposes. The primer bakes in one minute at 400]?.
A new and unique white enamel containing silicone resin has been developed for household electric heaters. This enamel (1292) will withstand indefinite exposure to temperatures of 250- 400F without discoloration. All previously available finishes have yellowed.
In the wood furniture field, modifications of our proposed postwar "38" Trim Tarnish have been received with great Interest. One
account, Sikes Chair, has just placed an Initial order for 300 gallons.
The Carborundum Co. again became active late in 1945 and ordered approximately 44000 gallons of adhesives. Laboratory work has been
resumed on "repaint" and industrial sandpapers. The most important problem is a non-curling paper for mechanical sanding machines that
will be adopted by the automobile industry. A really sensational new
sandpaper adhesive (U4965) has been approved by the Carborundum Co. but the use of this adhesive is being delayed until suitable ovens
can be installed. This adhesive bakes in 4-8 minutes,at 250F whereas
frevlous adhesives required 8-12 hours at 170F. Manufacturer's tests ndicate that paper made from this adhesive has three times the sand ing efficiency of previous papers coupled with indefinite "cut" retention.
Personnel
Labor turnover increased slightly in 1945 end resulted in the third
highest separation rate in seventeen years. Data on separations
follow:
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1945 1944 1943
Resigned Transferred to other departments or
to subsidiaries Discharged Laid off Drafted or enlisted
Total separations
Average number employees Separation rate
6-- `
17
3 3
-
23
51 45*
15
3 1 1 20
4 42*
7
2
-
12 47 26*
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Over 80% of the labor turnover occurred after 7-1 Day and a third of the 80$ took place In the month following V-J Day. Half of all 1945 separations were related In some way to the end of the war. Pour women resigned to join husbands returning from the army or at some army post, four others found educational opportunity not pre viously available and a small number left their jobs following the removal of job controls.
The laboratory lost the services of its oldest (in service) employee Mr. Johnston, in 1945* Mr. Johnston had been associated with the laboratory organization for 28 years. Another veteran employee, Mr. A. Wolf, was transferred to the Dibble Color Co.
For the first time since war began, it has been possible to select employees rather than accept the only applicant that might offer himself or herself. The laboratory organization has been expanded slightly due to the return of four veterans, all of whom were former employees. Two other veterans are expected back shortly. Unskilled chemists are still difficult to obtain and will continue to be scarce for another four years. The laboratory is now stronger better coordinated and composed of higher caliber employees than it has been since weir began. The average age of the laboratory staff has dropped considerably since 1941* In April of that year, only two employees were under 21 years of age; today 15 employees are under 21.
In analyzing laboratory labor turnover, one fact deserves special emphasis. Over a period of years, the two or three laboratory employees who are transferred every year to some other department of the company now constitute a good sized group of men. In the last ten years, 25 employees have been trained for other depart ments and many now occupy positions of considerable responsibility in our sales offices, subsidiary companies and factory. In most oases, the best employees have been transferred and not employees of lesser abilities. While the laboratory affords a fine place for men to obtain basic training, the gradual elimination of older and well trained men is a weakening process. The problem created within the laboratory can be solved only by overstaffing.
In Addition to training men for our own company, the laboratory has also trained large numbers of men for competitors and raw material suppliers. In seventeen years, 25 laboratory employees have left our employ to go with other firms in the industry.
In 1945, the laboratory underwent a major reorganization. From 1924,when the laboratory was set up under Mr. Fuller's supervision, until September 1945* formulating activities had been departmental ized along product lines, i.e. paint, varnish, lacquer, etc. This arrangement was quite satisfactory when we made only varnish and enamel but with each succeeding year, new product types, such as Yinylltes and ureas have come on the scene to complicate the set-up. For quite some time it has been evident that a subdivision of formulating work by problem types -- i.e. industrial, architectural, etc. -- would provide greater efficiency and less overlapping of work.
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When Mr. Johnston was transferred to the General Sales Department, an opportunity was presented to consider a reallignment of personnel and departments. The resulting reorganization represents a long
step toward the ultimate goal. The names of the old and new laboratory departments are Indicated below:
Department Names Before Change
Present Department Hamas
Oil Base Enamel (originally Pigment Products)
Paint Lacquer Synthetic Enamel
Varnish General Besearch Analytical and Raw Materials
Physical and Weather Testing
Architectural Enamel and Paint Industrial Enamel and Lacquer Varnish and Wax
General Research Testing
In addition to the advantages already mentioned, the new set-up represents a consolidation of departments. Five departments now take the place of eight, thus minimizing overhead. Larger
laboratory groups also offer greater operating flexibility when peak loads develop. Overspeoiallzation in the former set-up frequently blinded the groups to the possibilities of other types of coatings. This has been minimized in the new set-up.
Complaints
The complaint record during 1945 continued the trend which started in 1940. Data are as follows:
Year
Total Complaints Reviewed
Per Cent Justified
Complaint Index*
1945 1944 1942
1940
87 37 98 36
119 34 248 22 *No. of complaints per million gallons
manufactured goods
35 30 52
134
While the total number of complaints dropped below the 1945 level, the per cent of justified complaints contihued to rise. Both figures are probably related to the wartime economic situation which has eliminated the superficial complainer.
The four commonest criticisms in 1945, as in previous years, were drying, consistency, color and gloss. Complaints on drying showed
an increase, but less than a fifth of these complaints were Justified
Color complaints increased numerically as well as in the percentage
which were Justified. In 1945, slightly more than half of the color complaints were justified. In previous years, about 40% of the
color complaints were justified. Wartime manufacturing conditions probably explain the Increase in both the drying and color complaints
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Expense
The overall cost of all laboratory operation was $150,109 In 1945. This compares with $141,782 in 1944. Of the $8,327 increase, $7,745 or 9Jp represents added labor costa. For the first time since the laboratory was organized, operating costs exceeded the
1929 figure of $142,728.
The following table provides a comparison between 1945 and 1944 laboratory costs in terms of production and sales.
Cost of Laboratory
Per Gallon of Production
(.B.umffa'jlro--a-nd--Ftr.rEor.ie)
Research and Form ulating
Manufacturing Serv
Toti
3.6 cents 2.5
6.1
2.6 cents 1.8
4.4
Per Sales Dollar
WkTO--------------
1.2 cents 0.9 cents 0.8 0.6 2.0 1.5
While 1945 operating costs exceeded 1944 costs on both a per gallon and per sales dollar basis, the operating costs in 1945 compared favorably with 1940 figures (6.2 cents per gallon and 2.8 cents per sales dollar). Operating costs in 1944 represented an all time low for the seventeen year period that data have been accumulated.
It should be remembered that manufacturing services (product control, raw material testing, small batch manufacture for the factory, factory problems and complaint investigations) account for U0p of all money expended in laboratory work. This pprtion of the laboratory's operating expense is primarily related to production and has nothing to do with research or sales developments.
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Of the $89,000 spent on development in 1945, about $30,000 was devoted to general research and the remaining $59,000 was spent on specific sales problems (laboratory requisitions). In 1944, $33,000 and $50,000 were spent, respectively on general research and specific sales problems.
In discussing 1945 laboratory operating costs, the following figures provide an interesting picture:
Production Cost of Re at Buffalo search and and Ft. Erie Development
Cost of Re search and
Development per gal, produced
Industrial Finishes
Architectural Finishes (excluding paint)
Paint
945,040 gels. $ 55,200
1,528,863 -_______
20,800 13.000
5.8 cents 1.4 _____
2,473,903 " tak$ 89,000, tot. 3.6 cents, avg.
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From these figures, it will be noted that the development of industrial finishes costs about four times as much per gallon pro duced as did trade sales finishes. This is quite understandable for industrial products are custom made for one specific account whereas trade sales developments are applicable to a large number of customers. Over 80$ of the cost of industrial development work is paid by the Industrial Sales Dept, in the form of laboratory charges ($44*842 in 1945) but less than half of trade sales developmental costs are paid by the Interested sales depart
ments (combined laboratory charges $9*859 in 1945). What this means is that the Industrial Sales Department pays most of the
technical expense involved in its operations, whereas the trade
sales divisions pay for no major developments but only for the
smaller specific problems arising in individual offices. In
other words. our research activities largely benefit the trade sales divisions of the company.
Interesting comparisons can be made with 1929* if certain liberties are taken with the 1929 figures. The juggling of these early
figures is necessary because of changes in laboratory and factory accounting practices since 1929* Assuming that the reworked figures are correct, 385,000 gallons of industrial goods were produced at Buffalo and Ft. Erie in 1929 with a laboratory expend
iture of $46,000. In other words, each gallon of industrial
production cost 12.1 cents per gallon. This i3 over double the 1945 figure. In the trade sales field, 2,160,000 gallons of paint
were produced in 1929 with a laboratory expenditure of $26,000 or
at a ooat of 1.2 cents per gallon. This figure does not differ
appreciably from the 1945 figure. There has apparently been a tremendous increase in laboratory efficiency in the industrial field since 1929, probably as a result of increased familiarity with its problems. We are now selling about three times the
volume of industrial goods that we did in 1929*with only 15# more
laboratory effort. The amount of money spent in 1945 on trade sales developments, excluding paint* was 20$ less than it was in
1929.
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Statistical Summary of Laboratory Work
Mew products developed Sales problems submitted to laboratory New research problems assigned Research problems completed Raw material shipments tested Batches tested by control laboratories Servioe calls made by Lab. employees
1945
1944
1,594
1,321
1,965
1,898
96 114
93 121
2,106
2,142
15,140
16,209
112 <
97
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