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MICROBIAL INHIBITION (DEHYDROGENASE TEST-SUBSTA ICE ACTIVITY TEST) Identity:A mixturecontainingperfluorooctanesulfonatweh,ich may alsobe referredtoas PFOS, FC-95, or as a component of FC-206 or L3243. (1-Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The 3M productionlotnumber was notnoted. The testsample isFC-206. Currentinformationindicatesitisa mixtureof0.67% PFOS, 17.5% diethyleneglycolbutylether,78.91% water,1.33% Sultonefoamer, 1% sodium octylsulfate0,.04% sodium laurylsulfate0,.5% polyoxyethylene monooctylphenyl ether,and 0.05% benzotriazole. The followingsummary applies toa mixture with incompletely characterizedconcentrations ofimpurities.Data may not accurately reflectinhibitionby the fluorochemical component of the testsample. METHOD: Method: Not noted. GLP: No Year completed: 1973-1974 Analyticalmonitoring: % Transmittance Statisticamlethods: Resultswere determinedby calculatioonfthe % transmittanceand comparison withthe blank. Test organism source: Not given Contact time: Not given. RESJLTS Nominal concentrations:Blankcontrol0,.01,0.1,0.5,1,5,and 10% concentrationduringthe studyconducted in2/74. Blank control0,.1,0.5,and 1.0% concentrationduringthe studiesconducted in3/73 and 3/74. Element values: Not given. Remarks: Testingwas conducted on the mixtureas describedinthe Test Substance Remarks field.The valuesreportedapplytothatmixtureand not the fluorochemicalproportionalone. CONCLUSIONS No conclusionsgiven. Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 D&TA QUALITY ReliabilitKyl:imischranking3. Study lacksdescriptioannd recordsofthe method followed.The inoculumisnotproperlycharacterized.The sample puritywas not properlycharacterizedand the studylacksanalytical confirmationofthe amount offluorochemicalproportioninthe solution. REFERENCES The studieswere conducted by the 3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request Numbers 2034, 2093, 1973-1974. OTHER Last changed: 6/28/00 FORM 10620-PWO cc:LAB REQUEST BOOK - 42-5W Water and Wastewater REQUEST FOR LABORATORY WORK TO: ENVIRONMENTAL ENGINEERING LABORATORY- File: Lab Request No. BUILDING 53-6N Requestor Name'Z@@ 6:@Q -@@JRequest@Pate'/-z-1-7 FD e sc ritp-nt1fi1iir;gnoprcw Prob...-.-Code# Sample Date: Date Needed: Hold Sample For -Days EstT.ime: Hrs. Lab Personnel Date Rec'd.Sample: //-ao Analyst: y B p Date Completed: Hrs.Spent: Sample Description Total Hardness,mg/i as CaC03 Calcium Hardness,mg/i asCaC03 "P" Alkalinitym,g/i asCaCO3 "M" Alkalinitym,g/i asCaC03 pH Sulfate,mg/i asS04 Nitratem,g/l asN03 Chloride,mg/i as Cl Silicam,g/i as Si02 Tluorid-em,g/i as F Ortho Phosphate, mg/i as P Total Phosphate,mg/i as P Total Chromium, mg/lasCr CO*4@y-of Hex. Chromium, mg/i as Cr TotalCyanide,mg/l as CN Ferrocyanide,mg/i as CN Iron,mg/i as Fe -Manganese,mg/l as Mn Surfactant,mg/l as LAS Phenol,mg/i BOD, mg/i COD, mg/i(Short,Long,Dilute) TotalSuspended Solids,mg/i VolatileSuspended Solids,mg/i Turbidity,mg/iSilica TotalSolids,mg/l Total VolatileSolids,mg/i Conductivity,mhos TotalBacteria,No./100 ml TotalColiform,No./loo mi FecalColiform,No./100 mi FecalStreptocoocus,No./100 mi Ammonia Nitrogen,mg/l asN KjedldahlNitrogen,mg/i as N Oiland Grease,mg/l a vLe-. 6.01 611 ofA5 &a s fla- 70 4.7 26 1 t7 12.'5 I 41.T 113.5 13 19 34 T.C 4 3. Comments: e-"A White - Environmental o Engrg. Lab Canary - Environmental Engrg. Lob Pi-nk Environmental Engrg. Lob Goldenrod - Requesters 3M Copy PIIODUCT ECOLOCICAL ASSE53mm REQLTST FOR LAIMTORY WMK @llF.@ rC,R Lc@.6 PA I AWUTORY (_AJ @tt; NAMF.: Rl:i)LIFr-ST)ATE I'ROLILCT NO.: COLE NO.: SATAP1.E DA rF D.\TF \LEDLO. PP.OB. 4n.: DATE RECEIVED SANPLE: 2L -Z 1 14ANALYST: DikTI COWLIETED. HOtItS SPENT: 15h. t ION: 0 F 1'. T3 BIOAS@AY I:j---.shwatFeirsP TiYr-in-er'i- sh !@L,:i-o g qr.7.smi LEA:-"ifib IL In' Parent Miterial cW-m7 boris VIE/& SOD-, ulti-sate 1.5c Sloassai Othe; @Leachate COD mg"g Ll ultimate TOC -9,11s"-a0_; a@, Other 7777 ri.)vrric File: P.-IgNeo. W,*(jRK SIP*.ZT 74 lirs !24 44 0.o 4 14 45 0"5 37,s -3q. C7 AkL. t4ow% ell v t-t@e;ct 71 F(.-Z(l LI@,B !;()R@ "31!1*'-T Ll,t:ie t'ag,N-c) 1"4 ,,U 2.43 77 74,2 t ':.4. 74. 4C- 71,c' 74 -71 -7 70 74, <Q v -C Rev iewed bv: