Document 0gVx83rq34vDy7BL88Kvkd7Gb
'CG 01 CODE YE-698-D
L2HZB
( DATE )
( LOT )
5527* LBS. ( EST WT >
PROCESSES ( > YE-698-D (T)
APPRQ\ FWP 10/15/82*
COMTYP JOB NAME: 01YE698DMT
BLENDED BACK: CG 01, PQ 98,
(CODE)
(LOT)
(POUNDS)
EQUIP MENT
PREP 1
11
1I
1 V^\ 1 12| 1A
NAME: MOLYBDATE ORANGE OBTAIN SODIUM SULFATE FOR S-13
CALCULATE A SET ON BADGER METER FOR, -16 (NITRIC ACID WEAK)
I USE I LBS
i 1 n -c o d e j ,i.,,
I 84 1 108-A
J__21/IT 33-D
1 Yy\ OBTAIN SODIUM CHLORIDE FOR $-33
1 734
4-A
Ya OBTAIN.SODA ASH FOR S~37
1 146
3-A
Y/\ OBTAIN SODIUM SILICATE FOR S-39 1 Y/i OBTAIN SODA ASH FOR S-43
1 23? 1 350
32-D 3-A
1 Y | OBTAIN ANTIMONY TRIOXIDE FOR $-46
I 70
711 ~B
-1 !M2
351 1 fi'HWElGH SODIUM CHROMATE INTO V-351--
o \'
OPTR_____, MK '&2Jr3?S%
1 0-D
359 3
t1
11 j
t-
1 <*,SH ,H
1
OPTR
OPTR
__
MK
MK____,
_ -- t-.--
?!JLr. 1 1
T-_ X
423-d 1
1 ACCT 1 LBS
1 84 l>TF i 734 1 146 1 237 1 350 1 70
1 1885
1 303
358 I-h H^UN 10* (500 G) WATER INTO V-358
\JS} RUN V-359 INTO V-351 A PUMP IN V-351
*Z \ ADJ ?G 55* (2600 G)
SIFT IN N-108-A FROM S 1
STIR 5 MIN & RECORD: PH_S.fe_(9*'0-10.0)
} ADJ TO PH 9.8-9.9 A RECORD: PH__$_8~
| | (CAUSTIC SODA SOLUTION)
ASSUME 50%
|L
ASSUME 66%
LMTj KADD N-33-D FROM S 2 USING BADGER METER
>**7 1 ADJ TO 66* (3121 G) AT 67-69*F
LA RECORD : VOL_jkA* 6 __A? *f
| STIR 5 MIN & RECORD: PH_2.,07*4-7.6) 6
G/ML
(1.080-1 .083)
I NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
.LIST 6 ATTACH. TAKE 1 QT SAMPLE
7-D 33-D-
NOV 5 1982
RUN 20* (996 G) WATER INTO V- 2+ RECORD N-41-D STORAGE TANK t o Tu mFf r o m,
IRCLE ONE: 402 410 411 42 424 425 CHECK WITH CU SUPV:
^STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402-49*, 410=25*, 411=48*, 420=25', 424=25" 425=31 *
k STORA&e 't ANK MUST HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMPLETE ^ METER FOR 300 G A PUMP TO SV ..Ax**
:v' y
N40880
AOT EQUIP ME NT |
SV 5
CONT
23
24
COMTYP JOB NAME: 01YE69SDMT PAGE 02
DATE PRINTED:i0/15/02 USE i N -- IACCT
LBS i CODE i LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP,
CHECK PH & DENSITY, RECORD BELOW, IF NOT
IN RANGE, STOP PUMPING & SEE SUPV. * PH:______ (2,2-3.7)
* DENSITY: ___ __ G/ML (1.270-1.323)
IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
DENSITY
G/ML ON TRAPPED SAMPLE
FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21.
CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
*#* TABLE *#*#
G/ML 1.270 1 ,271 1 ,272
1 .273 1 ,274 1 .275
1 .276 1 .277 1 .278 1 .27? 1 .280 1 ,281
1 .282 1 .283 1 ,284
1 .285 1 .286 1 ,286 1 .287 1 .288 1.28? 1 .2?0
JETTING I G/ML SETTING 1 G/ML 's e t t in g 1
1678 i 1.291 1534 1 1 .31 2 1410
1670 1 1.292 1527 1 1.313 1404
1663 1 1.293 1 521 1 1.314 1399
1656 1 1.294 1515 1 1.315 1 394
1649 | 1.295 1509 1 1.316 1388
1641 1 1.296 1503 1 1,317 1383
1634 ! 1.297 1497 I 1.318 1378
1627 1 1.298 1 490 1 1,319 1372
1620 1 1.299 . 1484 1 1.320 1367
1614 1 1.300 1478 [ 1.321 1362
1 607 1600
1 1.301 I 1.302
1473 1 1.322 1467 T 1,323
1357 1 1351
1593 I 1.303 1461 - 1 1.324 1346
1586 1 1.304 1455 1 1.325 1341
1580 1 1.305 1449 1 1.326 1336 1
1573 1 1.306 1444 1 1,327 1331 1
1566 1 1.307 1438 1 1.328 1326 1
1566 I 1.307 1438 1 1.328 1 326 1
155? 1 1.308 1432 1 1.32? 1543 l
1553 1 1.309 1'427 1 1.330 1 537 1
1546 1 1.310 1421 1 1.331 1 532
1540 1 1.311 1415 1 1.332 1526
125 SET METER 6 PUMP _______G (RECORD FROM TABLE)
|
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY |
30 SECONDS
|
126 ADJ LEAD NITRATE TO 76* (3625 G) AT 67-69*F.
J
RECORD: __________ ;F
|
127 STIR 5 MIN & RECORD PH: ______ (2.2-3.7)
|
128 IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 667. \
6 RECORD PH:______
ASSUME 50%|
NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING|
12? RECORD: _______ G/ML (1.143-1,144) IF OUT OF SPEC!
FILL OUT CHECK LIST 6 ATTACH.
.
|
130 STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE.
|
41-D | 5110 57-A |__
I 33-D |_____
7-0'|
DUP050059670
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COHTyj^JDB iNAME
PAGE 02 saw^twr-
DATE PRINTED.: 11 /2>82 J USE I, N- IACCT.
'i'tr | LBS
AT iAPPRPX^#;!0:pi|WHIlS'tCONj[^JffiI^<G^FrO P4JMP: a*
CHECK
DENSITVJfRECORD] EOOWS "I F 'NOT
IN R
l^eUMpN'GT"^'" '
PH 1
DENSIJ-Y:
3P3HBg$g3E
?IF S-22:?OKf
.,,.. ____w,.JCORD^teg**?
DENSITY!
feG/Hli^NimAPf^D^AMPDE^^'V - ........
. 0M ,END:fCE^^lMu'HPMG^^^MF*^&--rv'- '
u s in g ENSiiitoo&si23^^f*E^ER Ge t t in g f o r
I I
I CODE |-LBS
_I
1 ***0 ;.4?H *
I'" 6Id*-
............. - -- v^v-r-...
I -V} I ' \9?v I ? :* "I I
.1 I t' .*.X . (. .
II
SECOND^PUHPJ*NG"IN rrABEE^El^OWl^NOTEs?TABLE ACCQUNTS;FORS30 G ALREADY^PUHPED IN S-21 *
a;: ;CIRCLE,^EHp^^:^TTING||fN^ABLE BELOW* .
I -I
... Md{**** TABLE
. ; r.'
J
;1 i, G/ML
\l'.2?0
,1*271
fcl .272
-1.273
4.274
'1 .275
I:f&f*M,
1 .276 1.277
I 1.278
|T 1.279
I 1.28
i.*p 1.281
1.282
1 .283
1.284
1.285
tSi.' 'I 1 .286 1.287
1.288
1.289
1.29
SETTING;.,,a^/LiSETOir"GySTM SETTING
-.4^6441 Hfe
^4504i>::;-T;.4.3l2 1382
1371.292^^87,-i. J 1*313 1376
1^30^. I 1 *293 -; 1491 ?. I "1 * 314
1423^- I *1,2294^4*485 | 1 .315 1367
:1i61.6--tss' | 1*295^,41479 I 1609^4 1 "'1.2296-trr.f4473''
1361 1356
160244 !-'4-i297^SM3
1351
. 1595
,, 1345
1588
-1j.299.v:?;'4455.*
,iwr;.- -
1582
30
"m 1335
1575!
*31
tei;.322;'-,. 133 .
1568
3302
*l'4li323^ .<1324
*303
*324" ;131.9
' "" .
---1315
*t3271549^S.&1*305;iij420M^t?a1.326
1310 1305
I
1535jyl'.307 ^y44lWr':-1`328 130
1528jiS#-1.308 : ' ;4441-'-1.329 1295
i522ffi&3 1.309
1-33 1290
1515| 1.310 ' 1393|1.331 1285
1510 I 1.311
1387 I 1.332 128
* *J .* l'x 1
rm?'
1254-SET METER 6 PUMP Z<Z_G <RECORD FROM TABLE)
| | FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
I | 3 SECONDS
|2>KABvl LEAD NITRATE TO 3625 G <76*-242/245 6 74.5*
I 41-D 1 5110
| | .247) AT 67-69*F
II
I IJIECORD: __AJ___*F & ICE CONSUMED (3304/BLOCK) 1330x1!I 57-A |X.T
|27| STIR 5 MlN 6 RECORD PH: __4iF (2.2-3.?)
I | ***# USE TITRIMETER TO ADJUST N-41-D PH ****
II
.I28TIF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66%
33-D l__2TZ
' 1 l 6 RECORD PH: _3li.
ASSUME 50%
7-D
J | NOTE: DILUTE N-7rD 10:1 WITH WATER BEFORE ADDING
128T^REC0RD: JxLtZ'jfz/ML (1.143-1.144) IF OUT OF SPEC
|| FILL OUT CHECK LIST & ATTACH. I3^STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE.
DUP050059671
LOT: Emir ' ME'NT I
COMTYP JOB NAME: 01YE698DMT PAGE 03
DA TE PRINTED: 1 0/J 5/82 USE N- ACCT LBS CODE LBS
SV CONT
3^r OBTAIN 1 QT SAMPLES OF S-18 6 S-30 SOLUTIONS
"I & TITRATE TWICE
! NOTIFY SUPV IF ML N-IO-D IS NOT IN RANGE
I 7*1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
I MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL
I EQUIPMENT & REPEAT TITRATIONS). DO NOT
I PROCEED IF N-IO-D TITRATION IS OUT OF RANGE
] ADJUST V-358 FOR A TITRATION PH OFTO-. 28
I FROM. FINAL IN-LINE TITRAilON.-RECORD LOWEST
i ph jk/-% h ml N-io-D
/fr-a OS'
33-D 7-D
SV 6
390 7
S-31 TITRATION OK , STRIKE V-358 THRU
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN ^
//>
I RECORD: ST A RT.S_LL OZ2l TOTAL MIN__2j Q_____
I NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
i 6 BUBBLES APPEAR IN SIGHT GLASSES
^rlMMEDIATELY DUMP IN N-4-A FROM S 3 6 SET TIMER
U FOR 15 MINUTES
DURING S 33, WASH IN V~358 ,,
3<5-Y'STIR 2 MIN 6 RECORD PH_J^itr2< 1 .8-2.5) PBXS,__4H(MUST BE + )
I STIR TOTAL OF 15 MIN FROM S-33 6
) , RECORD: TEMP22-"L_*F <67-73*F)
3^T.DUMP N-3-A FROM S-4
38^T STIR 3 MIN POUR IN N-32-D FROM S-5
STIR' 2 MIN
4>*1 RUN IN LIQUID ALUM USING BADGER METER
STIR 3 MIN 6 FLUSH ALUM LINE WITH WATER
4$r i DUMP IN N--3 FROM S-6
4$^T STIR 4 MIN FOR S-48
r"JLr-'--------- ---------------- ---------------------- ----------------------------------
4-rTRUN IN HYDROCHLORIC ACID USING WEIGHT 6 LOW,
I CONTROL PANEL
*
MK ______ , A$JklL%
MK______ ,_________%
ib i DURING S-44 SIFT N-711-B FROM S-7 INTO V-39
WITH AGITATOR ON IN 1-2 MIN
/n i STIR 1-2 MIN TO MILKY SOLUTION
734 11S-D 367
28-0 28-D
105
SV 4.r't WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B 8 ' | SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
| WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
.I UNTIL FOAM SUBSIDES.
4*9 I niIMP TN Rl AWf* FIXE N
i^O I WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
! I TOP' OF PAGE 1 > ,
| | RECORD: CODE
LOT_________,________
t5- STIR 20 MIN ^
152 ,.+ RECORD : PH_
< 5.8-6.0 )
IF NECESSARY, ADJ TO PH 5.8-6.0
ASSUME 50%
i
& RECORD: PH-______~r_
ASSUME 66%
FLOOD TO 153* (7298 G) 6 STOP AGITATOR
330'
128-A 330
7-D 33-D
STARTS
>BTR Mtr'-t ?/
DUP050059672