Document 0gMpykjQE7xJBNpKBoQym1XJm
CG^32
CODE Rf-428-D PKG ____
( DATE > EST. WT.
_______ A2H4CL (LOT NUMBER)
^ LBS.
PREPARATION NOTES:
PROCESSES. ( 5RT-428-D (EO
(> () () () TYPED BY: JLC STANDARD HRS. ___________
APPROVED BY EWK 12/11/8i
l
TIME
EQUIP i
MENT I
-------------- j.
Ufl/u IJ-JOl
5tsss:ss!ss`s!sas:!!:r2 =
NAME: UATCHUNG RED B
} USE i LBS
NOTE: DO NOT START IF PRESS WILL NOT BE AVAILABLE WITHIN 3 HRS AFTER MAKING. MAKING SIJPV TO REVIEW WITH P.R. SUPV & RECORD: PRESS WILL BE READYM_____/PR SUP
START MAKING M/MAKG SUPV
NOTE: RUN 15' WATER INTO V-904. PUMP WATER FROM V-904 THRU DISTRIBUTOR. IF WATER DOES NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH FULL FORCE, NOTIFY SUPERVISOR
I N--CODE I
PREP 1
RECORD: j L__BATCHES SINCE SPARKLER LAST CLEANED. AFTER 4 BATCHES, CLEAN, DRESS SAWrCFR i, PRE COAT WITH 15* DICALITE
FILTER AID OBTAIN' FOR S11 -CHL0R0-4-AMINQT0LUENE--5-
ONIC ACID
AIN FOR S40 3-HYDR0XY-2-NAPHTH0IC ACID
INSTALL DV 4, CV RECORDER 4, CONTROLLER CHART I Nr*OuiTE. : NOTIFY PRESS ROOM BEFORE ROPING OFF **Af?A UNDER V 922 4YT CLOSE OVERFLOW OUTLET VALVE FOR DISTRIBUTOR
LINE AT REAR OF VAT.
777-A 740-C
S2-C
RUN 14" < 140G) WATER INTO
t, HEAT TO
1*30-100 DEG F
IN 2-3 MIN DRESINATE X
^^L^TlR 5 MIN 4, RECORD: JjSLvSk.. (9.5-10.5)
9r\. sj. 20 MIN OR LONGER TO DISSOLVE FOR S53
130 I 530-A | 1 3:) iI
(722G) WATER INTO V--922
HUM HYDROXIDE IN V-926 & RUN IN
_____,&&*,<6_%
TURN ON AGITATOR 4. STEAM ! DUMP IN FROM S2
2-CHLORO
LOT
100%
_%
4-AMI NOTOLUENE
1 5-iUkrtNE
75^. JjJbAP
3i^srr_
~ I 7--D I 740--C
2. s st
11157
-a c t iv a t e d ~c a r 56n
CN DICALITE FILTER AID TO 212-214 DEG F WATCH FOAM 'I RECORD: BY_dfc? + > IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 50%
1 1 3-B 777-A I 10
m 5 1981
DUP050110413
I
EQUIP MEN!
I -PAGE 2 OF 3
/' CjOl CG 32 CODE RT-428-D (B)
USE LBS
N-CODE
ACCT
LBS
922 3
CONT
If''"
I STIR 30 MIN AT 212-214 DEG F THEN SHUT OFF
STEAM WATCH FOAM*
I RECORD: SPARKLER PRESSURE_____Q. ..PSI
4T+1CFIRCNUOLTATZEERO15
NOTIFY MIN OR
SUPERVISOR LONGER THRU
SPARKLER
I UNTIL SOL'N IS CLEAR. MAINTAIN AT 190-195 F
1 FOR S22. ECtfRD: START...
,
I TOTAL MI, CLARITY_,,__ei5lai-rrT'
I HT___ L&3______ DEG F, AND REC_/.__ DEG F.
Pi I SC 4
5 -r
902 6
--*rarz:a-----------------------------------------------JRE ^TadL-lUNITS IN V-92.S FOR S33
DROCHLORIC ACID
M......
7.
OLVE STRONTIUM NITRATE IN 30 GAL WATER
55 GAL DRUM AT 90-110 DEG F FOR S52
WEIGH SODIUM NITRITE IN PT FOR S36
M___ %______
RUN 1 (^L&fG) WATER INTO V-J
NQJgT USE CV IF MTY. IF CV IS NOT AVAILABLE.
USE V-904
VAt -^OI
WHEN SI7 COMPLETE, PUMP IN V-922 THRU
SPARKLER, MAINTAIN-' V-922 AT 190-195 DEG F
RECORD: START^i, TOTAL V\iwj2_____ !
iiiT-JArAtU&l&ia.fc-
_________________--.
3N 56 (1455G) WATER INTO V-902 DUMP IN CALCIUM HYDROXIDE & STIR TO SMOOTH
JRRY FOR S42
28-1) 63 246-B,E
725-A
550 542- D
557
63
399
550
922 ^T\ UHN S22 COMPLETE, STOP PUMP & INSERT V-922 7 UF(3o t PLUG RUN IN 10" <207G) WATER &HEAT TO 180-19 F
I GWifCTJLATE 15 MIN THRU SPARKLER.
1 PUMP V922 THRU SPARKLER INTO V904/CV 3
922 9
WfH 10
CV 11
PA I RUN IN 4 * (103G) WATER INTO V922 t, HEAT TO 190-195 F. CIRCULATE 15 MIN THRU SPARKLER
P V-922 THRU SPARKLER INTO WGm
JKT
MTY BLOW OUT SPARKLER INTO V Wr'M OUR IN IGEPAL CO-630 HHEAT TO 165-170 DEG. F
78,
I NOTE: IF N-740-C SOL'N <S21&22) WAS PUMPED
-Hd IRECTLY FROM SPARKLER TO CV OMIT S'S 31,32
3T jJrtfN IN 1* <95G) WATER INTO V-$g4__
33^1 PUMP V-904 AT 165-170 F THRU UNDERSURFACE
I DISTRIBUTOR INTO CV AFAP <12-15 MIN>.
JJ4AINTAIN 165-17 DEG F IN CV.
33<TRUNj:N N-28-D HYDROCHLORIC ACID FROM SI8
L**f>2-T5 MIN
15 MIN AT 165-170 DEG F
35n ACJ TO 43* <4080G) AT 32-38 DEG F
50X330
36-^TRUN IN N-725-A SODIUM NITRITE FROM S20 AFAP
i <5-10 MIN) & RINSE IN PT
979-D
73
57-A /J?jSod
DUP050110414
EQUIP I MENT
MAKING INSTRUCTIONS:BATCH UNIT
I USE
OF 4 CG 32 CODE RT-428-D <B>
LBS
AC-CT LBS
STIR 30 MIN AT 32-38 DEG F MAINTAINING
fOR, ,+KI RECORD: TI^START&*^.EW_.,
CR ,rfcH< + >, KI__,,X-_< + > NOTE: .
1> IF CR-, KI-, ADD 20$ "AS IS* INCREMENTS
HYDROCHLORIC ACID RCRD: CR______ < + >,
KI______ < + )
_ ASSUME 32%
2) IF CR+, KI-, ADD 20$ "AS /ISjElNCREMENTS
SQDIUgUHITRITE RCRD: CR_j-T( + >,
KI_X-..< + )
ASSUME 33%
DUMP IN STRONTIUM NITRATE
DUMP IN BARIUM SULFATE
DUMP IN FROM S3 & STIR 10 MIN
LOT --<-
3-HYDRQXY-2-NAPHTHDIC ACID
725-A *<24^;, E
65-A 82-C
I 19? i I 1-057
ADD. FOR MAINTAINING 32-38 DEG F THRU S 48 30X3301 57-A
DUMP AMMONIUM CHLORIDE INTO V-902 & STIR 2-3 MIN
261
261
WITH V-902 AGITATOR ON, IMMEDIATELY AFTER S42 COMPLETE, RUN V-902 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN 18-22 MIN * MAINTAIN
32-38 DEG F IN CV. RECORD: START_JL',$4J^ TOTAL MIN__QS_______
1
I .1 57-A
,DUglNG S43, WEIGH SODIUM HYDROXIDEJN PT _____ DILUTE TO MAXIMUM VOLUME (+/-10OG) FOR S48
3ASK
1 157
WHEN S43 COMPLETE, STIR 30 MIN
RCRD PH_5^_<5.0-6.0) TEMP_3JV__F (32-38 F)
RUN IN N-7-D FROM S45 THRU UNDRSURFACE LINE
6 RINSE IN PT
STIR 15 MIN & RECORD: PH_&y___ (9.0-9.8)
IF PH IS BELOW 9*G ADJ TO PH 9.-9.8
SODIUM HYDROXIDE
ASSUME 50%
RECORD: PH _/_,,, DIAZO,,rr^._ (- > , BASE,,3^_ <+ )
POUR IN N-246-B,E SOLUTION FROM SI9
STEAM EJECT IN V-921/931 SOL1N FROM S8
HEAT TO 180-182 DEG F IN 65-75 WIN AND
RECORD: HT_7A.,,DEG F & REC_J_0,, DEG F
STIR 30 MIN AT-180-^82 DEG F*
RECORD: START
FLOOD TO 180-190' (+/-18.0&0G)
STIR 5 MIN 4. RECORD:
___ <8.8-9.3)
IF PH BELOW 8.8, ADJ TO PH 8.8-9.3
RECORD PH:_________ SODIUM HYDROXIDE
ASSUME 50%
STOP AGITATOR
7-D 7-D
OPEN WATER VALVE AT OVERFLOW FOR DISTRBUTR AND BACK FLUSH THRU CHECK VALVE AND DISTRIBUTOR FOR 2 MINUTES. SHUT OFF WATER. OPEN OVERFLOW OUTLET VALVE FOR DISTRIBUTOR REAR OF VAT.
DUP05011041 5
COMTYP JOB NAME = 32RT428DMB PAGE 04
DATE PRINTED:12/22/81
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MENT 1
) PAGE 4 OF 4 CG 32 CODE RT-428-D CEO LBS i
LBS
1 ! WHEN INSTRUCTED BY PROCESSING AREA HALFWAY 1 | THRU PRESSING 1 I (1) DUMP IN I OCTANOL 1 | (2) STIR 5 MIN
1 | (3) ADVISE PROCESSING TO RESUME PRESSING [
i! i1 ii i
,, START 7.00/1^
FIN .
OPTR
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