Document 0LdkKGpDkeg0p80zEGX931zkk

AR226-03MI TOXICITY TO AQUATIC INVERTABRATES (E.G., DAPHNIDS) TEST SUBSTANCE______________________________ Identity: N-Ethylperfluorooctanesulfonamide; may also be referred to as U1464, EtFOSA, EtPOSA, F-6309, or FX-12. (1Octanesulfonamlde, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8 ,8heptadecafluoro-N-ethyl-, CAS # 4151-50-2) Remarks: Material is a white solid, Lot 505 (cc842-3, F6309, L-1089). Sample purity was not recorded. The following summary is abbreviated due to the fact that this study has been superceded by a more recent test. METHOD__________________________________________________ Method: Not provided Type: Acute static GLP: No YSepaecr iceosm: Dplaeptehdn:ia1m98a4gna R E S U L T S ____________ 48-hour EC 50 (immobilization): 3.2 (2.9-3.6) mg/L (Probit analysis) DATA QUALITY__________________________________________ Reliability: Klimisch ranking = 3. This study was tested in excess of solubility and actual concentrations were not measured. Results were based on nominal concentrations. Additionally, sample purity was not adequately characterized. R EFER EN C ES____________________________________________ This study was conducted by the 3M Company, Environmental Laboratory, 1984. O T H E R ____________________________________________ Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 Last changed: 5/18/00 006072 ENVIRONMENTAL LABORATORY ftSfCiCHEMICAL ENVIRONMENTAL EFFECTS EVALUATION TOXICITY TEST: SUMMARY REPORT Teat Species : ,, ' ~ 7 ) ^ p h n l ^ HA Teat Da t e i ^ / - - ^ - l .r . > Analyst(s ) a iB a M a a M N ta M a a ,a l (EXposure/Test Conditions) Exposure Type: Static_ y / < r 7 % u rr< r . Static Recirculatory_ Diluent: Static/Continuous Orbital Shaking Static Renewal Flow-Through Aerated Well Water (Initial D.O m g/1? pH P i, ? j , Temp. 9C( PF )) Water Hardness: PP^ Hardness ClassiCication: r iW fi^ T ) ________ Dissolved Oxygen % Saturation: Control(s) Lowest Experimental Dose Highest Experimental Dose pH Levels: v^U l 48-hr mo JOQ. im . 96-hr Extended Exposure 48-hr 96-hr Extended Exposure Control(s) Lowest Experimental Dose V.OiM^Lf Highest Experimental Dose Test Temperature C (F): -fixS ft.a_ &k 48-hr 96-hr Extended Exposure asc <to. *C(__ ) C ( ____) 006073 Photoperiod: Sixteen houra light with a 15-30 minute tranaition period. BEST COP ENVIRONMENTAL LABORATORY AQUATIC TOXICITY DATA SHEET DEFINITIVE (FULL-SCALE TEST) is ^ J Z ^ C L TYPE T B B n M f j j / t . MATERIAL TESTED. i x /-? TEST ORGANISM ^ ^ 4 / ? 7 > ? _ I'EST RUNS RUN 24 HOURS _ f LC50'S (95% CONFIDENCE LIMITS) * PROBIT ANALYSIS 48 HOURS 72 HOURS 96 HOURS L .8 -'J ;o ) REPLICATE COMBINED LC50'S ( z ,u -z . ) * MOVING AVERAGE ANGLE METHOD 'EST RUNS RUN 24 HOURS REPLICATE 48 HOURS ~3i 3 / k^ ^ ( z ti-s .e ) 3. 72 HOURS 96 HOURS ._nOMMEHTS COMMENTS t CQft&ZNBD i LCso's ( z -- I5>b) t 006074 BEST COPY AVAILABLE T ire T e s t t w p & tm -. environmental labortory AQUATTC TOXICITY DATA SJEET u M aterial T e s t e d K O fTi Teesstt OOrrgganainsims e d // / ; i,t--M rfo u rr.e //y ^ </ - / - , O e te V 'd / j /p/B atch No. ; y r^ ' d Age: First-Instar young (0.5-1.5irm) No. i&ganisms per treatment //? Test Chamber: 250ml glass beaker Test Solution Vol.: 200ml Test Solution Depth: 6cm. Time Stvrted, Date Started J)ate Comnleted( Dilution Wfter Cartfon-filter^d^weit^Mater (Temp. ?V, C, D.O. j?.yppm. pf.y'V Investiga^^ ^ ^ ^ ^ ^ S ^ W ^ g ^ ^ y LC^ (95% Confidence limits') (Full SignatS^f ^ X)A'A^K3/3 3,gJ *< In it. Tank Cone. No. JffiZJL-- I T C ontrol MiV/Afy -rfi "To' t ir .. 24 Hours Amount T otal D.O. Added No. Dead P JP* * ViVp 48 Hours r ours T o ta l D.O. T otal D.O. No.Dead PH ppm No.Dead pH ppm n 3 ,*> J A . __ L i 2_ . - ^ 0 - -Q . - __ tf. fir fi 96 H oirrs T o ta l D. No.Dead >H np ___L k ? , . . , S ^ SA iJA- < fL o - 5 ,0 . -_Sj2_ . /> -vJ5 " jo . (9 _ ffifi .. 2 J (<p!, t f r fi . J O . . . Mu *T~h tf.f* Test Tesq> C. ... ? x r . -------- In trim u 3 Date _____ Z J . :y jz / / / a d d 'd .) s ' . rr>.^>> "T E ffe cts o ther than M o rta lity EC50- k / . ____________ f'rfi/kfy Tank No. C o n tro l Symptoms o r Reactions 24-H r. 48 T o ta l H r. No. A72ff-eHcrt.e d 96-H r. Commcnts: O6075 best copy i ENVIRONMENTAL LABORTORY AQUATTC TOXICITY DATA SHEET TVre Tests /ffa p a < ,/7 r 'to O H ' Material Tested t ,TeT T TestE Organisi.^,/,,!, / ^ S o u r Or Refe* y f r A ateh No._ a.Age: First-Instnr young (0,5-1.5mm) No. &rgani^ms per treatment //* ) Test Chamber: 250ml glass beaker Test Solution Vol.: 200ml Test Solution Depth: 6cm. Time Started Date Started ////^ Date Completed Dilution Wfter ^Carl^^lt^pdaiifill water (Temni ^ C, D.0. ppm, pH/?/7" Investigato r 2) LCr,, (95% Confidence limits) (Full Signat?5rW| 5 ( & #i r S > y y Tank No. In it. "Total" ' ----------R 1 tours Cone. Amount Total D.O. J 5 8 Z 1 _ . Added No. Dead pH PP ----------3 m iours T -- 7TBour Total D.O. Total D.O. No,Dead pH ppm No.Dead pH ppm 96 Hou Total r D.' No.Dead Sh PP it nei X . Control / ? P,?s fl, fa J _ -- LQ, .__ Z a X L n (*1 __ L b ___ JSUZ... ...rt n $ ,2t _ 2 s S _ . - ^ . C ? .... v 9 . . . j - a = i U fi d L - M-n - f i . o ...pi. f.3 %u 5 L -A .JZ JtL . - i n / c . fi A fi, (fi Test Temp. C. . 1 d1.._ -------I n i t i a l s 8 Pate* W ..- _____ l 5 ^ :T 3 .y A A / 1 . E ffects other than Mortality Tank No. Control Symptoms or Reactions 7 EC. 24-Hr. Total No. Affected 48 Hr. 72-Hr. 96-Hr. Comments: 006076