Document 0L4y6X8YnY0XdbgG6wjd1Ja5n
CG 5
CODE RT-160-P
1982
DA )
( l ot
F'KG
PROCESSES
APPROVED 'BY
< )RT~i60~P (B) EWK 12-03-81
COHTYP JOB NAME: 40RT16GPMB
TYPED BY: JMH
EST* WT, 643* LBS*
------
TIME
>: PREPARATION NOTES: SUPVR NOTE: DO NOT USE 16-303 FOR NAPHTMANIL.S WHEN ( 'CAMPAIGNING DALAMARS YC-39-A, YC-40-A, YT-839-P, YT-840-P, YT-858-D, AND
YT-868-D,
SEMI-BLEEDING
EQUIP WENT
PREP i
i|
NAME: NAPHTHANIL RED LIGHT
U^PoBTAIN 4-NITRO-2-AMINOTOLUENE FOR S6
I 2 I OBTAIN 3-HYDR0XY-2-NAPTHY:LAMIDE FOR SI 8 1 3 ,1 CLEAN, DRESS, CLOSE 24" CLARIF PRESS | | 15 FRAMES
DV 2o [
RUN J.%' (486 G> WATER INTO V~,,
RUN IN HYDROCHLORIC ACID FROM V~3
J_i M_____ _________
DUMP IN FROM Si
LOT
' 4-NITR0-2-AMINOTOLUENE
..%
1 USE i LBS 1--- 1 1 I 1
i
| N-CODE ACC
j LBS
1
1 504-C
1 150-C 1
41 xtiifj fa Wr
ilQif:ly> --'-.
j].2Z.
28-D 504-C
'
126 210
MI SC 3
I ^TTWEIGH ON POSTAL SCALE 3-NITR0-4-AMINgANIS0LE L. t___ ! j LADD k STIR 15 MIN TO WET * LOT_XTi^J?t_
^V^D.KTO 3C3L-' (1020 G) AT 40-45 DEG F
13X330 1
IN SODIUM^ NlTfi^E IN
.. i
STIR 5 MIN k RECORd T Ci:^i:<+ ), KI,,2|El<^ i"
I
i NOTE: < i ) IF CR-, Kl- ADD 20* "AS IS''
i
i
I IfrtEMENTS HYDROCHLORIC ACID ASSUME 32% l________i
I R&mto: CR_____,.< + > KI.,,*___< + ) ' *
ii
! <2'$HF 'CR+, Kl- ADD 10*- "AS IS* INCREMENTS i
!
IMODIUM NITRITE
ASSUME 33% I________ 1
ECORD: CR_______ ( + ) Kl_______ ( + )
i
-H | STIR 10 MIN AT 40~45*F MAINTAINING +CR, +KI 1
1 1
! FOR SI3 RECORD: TIME
I1
SLURRY DICALITE FILTER Afl.) IN 40 GAL WATER 1
I IN DRUM k PRECOAT CLARIF PRESS
!
5| 1
,396-C i 57-A
725-A
1 --1
95
28-D
725-A --
777-A | i
t;
u
DV 4
I
WHEN S11 STIR COMPLETE DUMP IN ACTIVATED L-CARBQN
1 11
15 `
1 11
'113-B
1|
15
l-K^rDUHP IN DICALITE FILTER AID
i io j 777-A | 10
|6*r ! STIR 30 MIN AT 40-45 DEG F
ASSUME 33% i____ ..... i 725-A 1
I | MAINTAINING +I<B?F0/L,S23.
i.,, i 57-A i
| | RECORD: START_X-fiLl&I_^.--'f!._._ < + >
ii
i
I RUN 13* (177G) WATER INTO V-330 t SLURRY TRISULPHOIL SOAP D IN 25G WATER k i POUR IN I DUMP IN 3-HYDR0XY-2-NAPTHYLAMIDE FROM S2 k i STIR 30 MIN OR LONGER TO WET. , LOT i r ec o r d:
! US Pr/
i /. i ! 16 |
.3.2o....
i
1 39-A |
16
150-C i 370
N38125
COMTYP JOB NAME 40RT160PMB
PAGE 02
DATE PRINTED:MM/DD/YY
EQUIP MENT
~T'~
PAGE 2 OF 3 CG 40 CODE RT-160-P <B)
"USE""'! LBS |
ACC'i LBS
------------- ------------------------------------------------ --"--"-i-----------r
302 N 12" <1^44G) WATER' INTO V-302
II
6
POURBi-yGDIUM HYDROXIDE
ASSUME 50%
| 58 I 7-D
SIPfTDN IN ACETIC ACID 6 STIR 3 MIN- ,
i /^ j
a <5
M____ l____ _,____% !
RECORD PHj l ij C. (6 * 7-7,5) IF NECESSARY ADJ TO I
! 30-D i
I 6*7-7*5*
ACETIC ACID ASSUME 70%l,,^jJ_| 30-D
I RECORD PH____ " SODIUM HYDROXIDE ASSUME 50%|_______j 7-D
DV TURN ON V-_^T_6 AGITATOR 6 ADD ICE, THEN `| 2X330
? I SjiLLP OFF AGITATOR
i
2Mr~Fm'P- DV THRU CLARIF PRESS INTO DV USED IN i
I S 23* MAINTAINING TEMP AT 40-45*F. RECORD: !
I STARX-^r./r/.' 1 P.&rf TOTAL MIN.I
\Wfit: DO NOT USE V-303 - TOO SMALL
i
ZJ^TWHEN S23A CLARIF COMPLETE WASH DV <S4>
|
I LINES .PUMP 6 PRESS FOR 20 MIN OR TO A -CR I
I TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT j
WHICHEVER COMES FIRST, COLLECT WASHINGS IN I
23) RECORD:
-s=rrt-'OR+) |
WHEN S24 IS COMPLETE TEST DVGSgS* ASSUME 33%l_______
, REfcORD : KI_;.___C + > TEMP,,JraL < 40-45* F) l_
LS^T WEIGH SULFAMIC ACID IN RUBBER BUCKET AND " !
^SE IN AND STIR 5 MIN,
I 10
\ppf" RECORD: KI__-!~L,,. MUST BE - & IF NECESSARY !
I >^ADJ TO -KX-WITH SULFAMIC ACID.
\p i ADJ TO _oXf--' <1925 G) AT 40-45 DEG F
H X33
^ r--- - -
---
i^fyj^RUH 39" <3900, G) WATER INTO V-260
' i
i yf \ INSTALL ..TEMP CHART 6 SET AGITATOft AT 16 RPM i
5 7-A
725-A 5 7-A
395-D 395-D
10
330
I WHEN SIS STIR COMPLETE, POUR IN SODIUM
I
HYDROXIDE IN 3-4 MIN,
ASSUME 50% I 220
9 | HEAT TO 128-132 DEG F AFAR 6 STIR 5 MIN TO I
I DISSOLVE. STOP AGITATOR,
i
7-D 110
| IMMEDIATELY RUN V-330 AFAP INTO CV. NO
I I AGITATION IN CV. RECORD: START.&l Au
I | .
TOTAL MIN ____ fi_____
i POUR IN ACETIC ACID 6 STIR 3 MIN. ^
jj
|^j
y
^^
*/
RECORD :
{ 1 o 75-T77o 7' ' ASSUME 50%
30-D | ISO 7-D j______
IF NECESSARY ADJ TO PH-10.5-11.0
I
RECORD; PH_____ _
ASSUME 70%
30-D U_____
U&& RUN IN V-302 AFAP ' yy&f- DUMF IN BARIUM SULFATE
I 35 63-A !' 35
.138 | HEAT TO 78-82 DEG F AND RECORD:
T i HT
DEG F AND REC,,,,.^____ DEG F
WHEN S28 COMPLETE, COUPLE DV UNDERSURFACE
I IN 65-70'MIN. MAINTAIN CV AT 78-82 DEG F I RECORD: STARTTOTAL MIN __________
^KO STIR 5 MIN, DISCONNECT TRANSFER LINE AT CV
I
I J>T1
6 RECORD : DIAZO,.-r~ --. <+/-) BASE_4r__(MUST BE +) PH_______ <4.2-4.6)
IF NECESSARY STIR TO - DIAZQ RECORD:
START____________ TOTAL MIN_______
RECORD: DIAZO _________ MUST BE -
BASE ___ MUST BE + OLI <A n~A A\ "
i
DUP050 047472
COMTYP JOB NAME 40RT160PMB
PAGE 03
DATE PRINTED:HK/DD/YY
EQUIP 1 i '
USE I N-CQDE I ACCT
M.ENT | ' I PAGE 3 OF . 3 CG 40 CODE RT-160-P <B> ) LBS I
i LBS
MISC 11 1
-r----- 260 3
12 *4<4
t
| |
I I |
p
ADD 30G WATER'AT 130-140*F TO DRUM FROM HOT| WATER MIXER ,ADD BLANCOL N 6STIR FOR S43 |
POUR IN N-567-B SOLUTION FROM S42
HEAT TO 194-196 DEG F IN 55-60 MIN AND
RECORD:
____.DEG F AND EEC./__DEG F
WHEN S44 HEATING COMPLETE, RUN IN ALUMINUM
SULFATE SOLUTION THRU BADGER METER. NOTE:
RINSE IN LINE AFTER N-i15-D SDL'N RUN IN.
STIR 30 MIN AT 194-196 DEG F
FLOOD TO 80" (7928G) AND STOP AGITATOR
I
30 120
|
VAT | V-303f V-31 51V-317JV-3221V-323
S4 <486G>
20* 14' 14* I 14* ! 14"
S8 <10200}I 43* 30" 30" I 30" I 30"
567-B | , 30 115-D ' 1 60
START
FIN
OPTR"-
J&L-
V &T I %l s+sw
\-
1
i DUP050047473
DUP050047474
PRODUCT NAME
NAPBTHANIL RED LIGHT
CG 40 CODE RT-160-P PKG
LOT
SEMI'-BLEEDING
PROCESSES
APPROVED BY -
RT-UO-P < B> EWK 12/03/81
TYPED BY JMH MAKING NOTES___________ !______
I JQB NAM: 40RT160Ppi'
INSTRUCTIONS
PRESSING * -
VAT ' M0& J
i
I
I I PRESSLOAD
I
DATE
Ur-HM'
I
I
I | STARTED .
TIME
i
) ) I CAKES USED
RELEASED Wfty J '
I I I WATER ON
PRESS ,
12~ I]
I { I HRS* WASHED
NO*OF CiM'ESS 2 44 I
|
I i M MHOS
PRESS WMHO
AGITATION
I HRS'* WASHED
WASH TO 1250 M MHOS - 35-75* P WATER 1 M MHOS
TEST AFTER 2 HOURS
I HRS* WASHED
LOAD IN N-i775-A NEW BLUE DRUMS AT I M MHOS .
CAKE CONDITION
' RECORD 1ST] 2ND] 3RD!
47Hi
5TH
EXPLAIN LOSSES.
* DRYING = *.*** DO NOT DRY *#**
- GRINDING **#* DO.NOT GRIND ****
*
DUP050047475