Document 06pyGwLjE3G1ZjoLXoEj84o3R

mmmm mix r4Tg May 57* lgb5 t o t c o n c l u s io n n o . t ^u c . 63-596.... OFFICIAL PRODUCT "Idthoaol" Add RM fipitolno-m-Tolu^^ Acid I P PRODUCT CODE NO 44Sg00~400Q------------------ pm imp s PRODUCT ACTUAL. ah ea.... Wise. Inter. ............b u il d in g bame . , TITLE. Revision of "Xithosoi" Acid Add) Process PREPARED BYi. . 2SjL#gr_. noygfrToiunissulfonie rpvcczr pur pose o f t est : To bring the Chambers works Process up-to-dafe* in line with current operating procedure. r esul t s o f t est : procedure. Satisfactory material has been mad using the revised r e c o mme n d a t io n s : it is recommended that these changes be mad part of the standard operating procedure. DISTRIBUTION: W. P. Tams* Jackson lab, Jackson lab. Library- Do B. Kirk* 2nd, Eng, Blv. J, T. Linster, Adm. Bldg. (5) Ro To McBally, Basic Lab. J. F Laucius* Azo Lab. R. Pody, Adm. Bldg. T. J. R, Stephens* Wise. Inter. H. 1. Stryker* Adm. Bldg. h/PPROVED BY: AUTHORIZED BY SUPT. PRODUCTION AREA 4@4752.R-9 DATE. 2t "eCTfe MJLp.> suprypRocess OEPARTlMNT DATE DATE t o t mmmimrim n o . t a s - JlzSSL OFFICIAL PRODUCT NAME- "Llthosol" Acid HBA (4-Aalno-ra-TolUfeneauIfonlc Acid) PRODUCT COOS MQ- 448300-4-000 *pp* Mise. Inter. ___POUNDS PRODUCT PROHJSE&, BUILDING MW, PMA^Buiifelng 234 TITLE- Revision of "Llthosol" Acid Acid) Process sn-Tolu@msulonie O pr epar ed r v - I S Hbrnbuckle RESPONSIBLE FOR TEST -AND TEST CONCLUSION:. L. S. Horribuekle pur po se o f t est : To bring the Chambers Works Process up-to-date, in line with current operating procedure. s t a n d a r d INVOLVED: ' Chambers Works Process for the Manufacture of "Llthosol" Acid RBA (4-Amino-m-Toldemsulfonio Acid), approved October 22, 1953* d u r at io n o f t es t : changes have already been mad. TEST DETAILS: (INCLUDE SAFETY) Process__ Actual Materials 4-Aminotoluene-3-Sulfon!e Acid Crude 2,500 pounds 4-Aminotoluene-3~Sulfonie Acid Crude 2,500 to 2,600 pounds 100$ 50$ Soda Canstie Liquid, approximately 535 pounds 100$ 50$ Soda caustic Liquid, approximately 445 pounds 100$ Bareo, 150 pounds mt Bareo, 100 pounds net Super-Cel, 125 " " Super"Cel, none Heating 95e. for on hour 950. for half hour DISTRIBUTION: V. P. Tams, -Jackson Lab. Jackson Lab. Library D. B. Kirk, Xnd, Eng. Div. J. T. Linster, Ada. Bldg. 0) R. T. McNally, Basie Lab. 2/- AUTif JRI2ED BY Jar SUPERINT EH bENTf FROOUCTiOff AFi^A MU-J752-B-R-? J. F. Lauclus, Azo lab. H. Pody, Adas. Bldg. T. J. R. Stephens, Miae. Inter. B. I. Stryker, Adas, Bldg. DATS DATE 6\ DATE DATS DUP050467907 N33039.01