3M Environmental Laboratory Study BACK TO MAIN Analytical Report: FACT GEN-050 LIMS E01-0096 Analytical Laboratory Report Title Determination of PFOS, PFOSA, and PFOA Levels in Surface W ater Samples from Port St.

BACK TO MAIN BIOCONCENTRATION (n-OCTANOL/WATER PARTITION COEFFICIENT) TEST SUBSTANCE_________________________________________ Identity: N-methylperfluorooctane sulfonamidoethanol; may also be referred to as N-MeFOSE Alcohol, FC-790, FM-3925 or T-5874. (1-Octanesulfonamide, N-methyl1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-N-(2hydroxyethyl)-, CAS # 24448-09-7) Remarks: Material is a cream-colored solid of uncharacterized purity Batch 2334.

BACK TO MAIN SOIL ADSORPTION (METHOD DEVELOPMENT) TEST SUBSTANCE__________________ Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, PFO, FC-116, FC-126, FC-169, or FC-143.

BACK TO MAIN ENVIRONMENTAL LABORATORY AOUATIC TOXICITY DATA SHEET EXPLORATORY (RANGE-FINDING TEST) LR f s/t lr Z Type T e st A U ^ S ^ S s O S - a t e r i a l T ested Test O rganism ^ S o u rc Xf' X' OM HX OC/3) ____ D a tc R o c ' d ` Avg.

ARU6-0OO6 g ) FUNDAMENTAL AND AFFUED TOXICOLOGY 4. 972-976 (1984) Cholestyramine-Enhanced Fecal Elimination of C arbon-14 in Rats after Administration of Ammonium [14C]Perfluorooctanoate or Potassium [14C]Perfluorooctanesulfonate Ja m es D .

MICROBIOS MICROTOX TOXICITY TEST TEST SUBSTANCE______________________ _____________________ Identity: Perfluorooctanesulfonate; may also be referred to as PFO S or FC-95 or as part of the mixed product FM-3820 (see Remarks). (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The test sample is FM-3820, a mixture of the test substance in diethylene glycol butyl ether and water (approximately 24-28% test substance in diethylene glycol butyl ether and water).

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ARa k -.0678 MULTI-CITY STUDY FIELD REPORT FOR CLEVELAND TENNESSEE AND DECATUR ALABAMA - BATTELLE DUXBURY ACTIVITIES for Project Number N100672-01 submitted to July 9,1999 Prepared by Scott C.

AH 8.2.6 - 072j> ACUTE TOXICITY TO AQUATIC INVERTEBRATES (EASTERN OYSTER) TEST SUBSTANCE____________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3).

AA S & G -08/ TOXICITY TO AQUATIC PLANTS TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-206CE. (1Octanesulfonic acid) (CAS # 2795-39-3).

AR 2 6 _ 021 ACUTE TOXICITY TO FISH (BLUEGILL) TEST SUBSTANCE_______________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-600. (1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks: The 3M production lot number was not noted.

6 -- D&S5 ACTIVATED SLUDGE RESPIRATION INHIBITION TEST TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-603EF. (1Octanesulfonic acid) (CAS # 2795-39-3).

-f\&A6 - 1063 Guide tolde SafeHandling of Fluoropolymer Dispersions r * -.: - :) c di ro ro ro Prepared by the FLUOROPOLYMER MANUFACTURERS GROUP O cto b e r 2001 BZ-101 The Society o f th e Plastics Industry, Inc.

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