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LHC 11 Procedure 2TK/K-30 Commissioning LHC II Scope Commission for putting back in service Hazards If 2K-20 is to remain under pressure the oil drains on 2K-30 must be blinded before 2K-30 will depressure.

HYDROCHLORINATION REACTIONS VAPOR PHASE REACTION OVER ACTIVATED ALUMINA * 98 % MeOH Conversion * 20% XS HC1 CH3OH + HC1 --> CH3CI + H20 220C (Hr = -11.0 kcaL/mol) SIDE REACTION * Dimethyl ether production CH3OH + CH3OH --> CH3OCH3 + h2o 220C (Hr = -5.9 kcal/mol) DME CONSUMPTION __ * Cellulose mixture (70% DME, 30% Ml) CH3OCH3 + HC1 --> CH3CI + CH3OH 220C (Hr = -2.2 kcal/mol) DO A CONFTDFNTIAL

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