STL Burlington Colchester, Vermont Extended Data Package SDG: 117522 Case Narrative Chain of C ustody........................................................................................................

MA&6 _ 126g TSCA NCIC Notification Form for CB!

AR J U 6 - iS'IJf- TSCA NCIC Notification Form for CBI Documents RECEIVED Docket Number: ______ f l R Document Control Number: ( Document Date: _____________ Document Type: ^ q c \ f ~ ____________________ M o TJ TJ ro --I x=r O c~> co CO XT Th e d o c u m e n t r e f e r e n c e d a b o v e is c la im e d a s c o n fid e n tia l b u s in e s s in fo r m a tio n (CBI) u n d e r S e c t io n 14 o f the To xic S u bs tan c es C o n tro l A c t (TSCA).

3 GLP10-01-02 Interim Report 21: Analysis for PFOS, PFHS and PFBS in Decatur, AL Soils Collected from Well Location 610 in August, 2011 Study Title 3M Environmental Laboratory Analytical Protocol GLP10-01-01: Analysis of Perfluorooctane Sulfonate (PFOS), Perfluorohexane Sulfonate (PFHS) and Perfluorobutane Sulfonate (PFBS) in Groundwater, Soil and Sediment for the 3M Decatur Phase 3 Site-Related Monitoring Program Data Requirement Data Requirement EPA TSCA Good Laboratory Practice Standards 40 CFR Part 792 Study Director Jaisimha Kesari P.E., DEE Weston Solutions, Inc. 1400 Weston Way West Chester, PA 19380 Phone: 610-701-3761 Principal Analytical Investigator Cleston C.

Laboratory Report Analytical Report of Data for PFOSA Pharmacokinetic Study in Rats (Sera and Liver) Laboratory Report No.

BACK TO MAIN SUMMARY OF ANALYTICAL RESULTS: MULTI-CITY FOOD STUDY The Multi-City Study was originally designed by Battelle Memorial Institute (Columbus, OH), to obtain preliminary data about the presence of fluorochemicals in foods and in drinking water to understand the potential sources of human exposure.

BACK TO MAIN Study Title Characterization Study of PFOS, Primary Standard - Test Control Reference #TCR-00017-046 P h a s e : S o l u b il it y o f PFOS in W a t e r Data Requirement 40 CFR 160.105(b) Author Mark E.

Northwest Bioanalytical -ARA S L 6 - I A I O Study No.

AKAS6- 267 FlUO RIIW ED SDREAC1ANTS AND REPELLENTS RovSiseocdonadndEEdxitpioannded Erik Kissa W ilmiCngotnosnu, lDtaenltaware MARCEL OEKKER Marcel Dekker, In c.

Analytical Report Fluorochemical Characterization of Aqueous Samples Decatur Outfall 001 FC Monitoring (E03-0848) Exygen Research Laboratory Report No.

3M Environmental Laboratory IU26-002S M ethod E xtraction of Potassium Perfluorooctanesulfonate or other FLUOROCHEMICAL COMPOUNDS FROM URINE FOR ANALYSIS USING H P L C - Electrospray/M ass Spectrometry/M ass Spectrometry Method Number: ETS-8-96.0 Adoption Date: Author: Lisa Clemen, Glenn Langenburg Revision Date: /\/ j\ Approved By: Laboratory Manager v s f i f i n ------ Group Leader n l fr cluvu!

3M Environmental Laboratory AlWo e-os-ftyo M ethod Determination of Perfluorooctane sulfonate (PFOS), Perfluorooctane SULFONYLAMIDE (PFOSA), AND PERFLUOROOCTANOATE (POAA) IN W ATER BY LlQUIDSolid Extraction and High-Performance Liquid Chromatography/Tandem Mass Spectrometry (HPLC/MS/MS) Method Number: ETS-8-154.0 Adoption Date: Author: Kristen J.

BACK TO MAIN AR226-1030A012 Study Title Solubility Study of Perfluorooctanesulfonate (PFOS), SD-018 and Perfluorooctanesulfonamide (FOSA), SE-027 in Male/Female Human Urine Data Requirement 40 CFR 160.105(b) Author Mark E.

fik Z 2 . 6 - 0 S 7 o BIODEGRADATION (BOD/COD) TEST SUBSTANCE_______________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-780B. (1Octanesulfonic acid) (CAS # 2795-39-3).

\ IN WATER (3/15/84) and (6/4/84) o '1 CO LOCATION .